Crystallography Open Database

Information card for entry 1543257

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Structure parameters

Chemical name	Bis[μ-2-(trimethylsilylamido)-6-(trimethylsilylamino)pyridine-κ^3^<i>N</i>^1^,<i>N</i>^2^:<i>N</i>^2^]bis[(diethyl ether-κ<i>O</i>)lithium(I)]
Formula	C30 H64 Li2 N6 O2 Si4
Calculated formula	C30 H64 Li2 N6 O2 Si4
Title of publication	Bis[μ-2-(trimethylsilylamido)-6-(trimethylsilylamino)pyridine-κ^3^<i>N</i>^1^,<i>N</i>^2^:<i>N</i>^2^]bis[(diethyl ether-κ<i>O</i>)lithium(I)]
Authors of publication	Rave, Justin A.; Garcia, Diego A.; Hillesheim, Patrick C.; Guillet, Gary L.
Journal of publication	IUCrData
Year of publication	2016
Journal volume	1
Journal issue	5
Pages of publication	x160707
a	9.87 ± 0.007 Å
b	10.624 ± 0.008 Å
c	11.319 ± 0.007 Å
α	74.34 ± 0.02°
β	81.35 ± 0.02°
γ	68.246 ± 0.019°
Cell volume	1059.8 ± 1.3 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1087
Residual factor for significantly intense reflections	0.0592
Weighted residual factors for significantly intense reflections	0.1249
Weighted residual factors for all reflections included in the refinement	0.1575
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
183649 (current)	2016-06-17	cif/ Updating files of 1543257 Original log message: Adding full bibliography for 1543257.cif.	1543257.cif 1543257.hkl
182574	2016-05-05	cif/ hkl/ Adding structures of 1543257 via cif-deposit CGI script.	1543257.cif 1543257.hkl