#------------------------------------------------------------------------------
#$Date: 2016-01-09 12:15:27 +0200 (Sat, 09 Jan 2016) $
#$Revision: 173731 $
#$URL: svn://www.crystallography.net/cod/cif/1/52/00/1520076.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1520076
loop_
_publ_author_name
'Avdeeva, Varvara V.'
'Buzin, Mikhail I.'
'Malinina, Elena A.'
'Kuznetsov, Nikolay T.'
'Vologzhanina, Anna V.'
_publ_section_title
;
 Reversible single-crystal-to-single-crystal photoisomerization of a
 silver(i) macropolyhedral borane
;
_journal_issue                   46
_journal_name_full               CrystEngComm
_journal_page_first              8870
_journal_paper_doi               10.1039/C5CE00859J
_journal_volume                  17
_journal_year                    2015
_chemical_formula_moiety         '2(C54 H45 Ag P3), B20 H18'
_chemical_formula_sum            'C108 H108 Ag2 B20 P6'
_chemical_formula_weight         2023.70
_chemical_name_systematic
;
 ? 
;
_chemical_properties_physical    Light-sensitive
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2015-01-26
_audit_creation_method
;
Olex2 1.2
(compiled 2014.09.19 svn.r3010 for OlexSys, GUI svn.r4874)
;
_audit_update_record
;
2015-03-12 deposited with the CCDC.
2015-05-28 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 131.7480(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   12.8280(6)
_cell_length_b                   25.0953(11)
_cell_length_c                   21.3666(9)
_cell_measurement_reflns_used    9847
_cell_measurement_temperature    120
_cell_measurement_theta_max      36.17
_cell_measurement_theta_min      2.27
_cell_volume                     5131.8(4)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      120
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.956
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0399
_diffrn_reflns_av_unetI/netI     0.0399
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       41
_diffrn_reflns_limit_k_min       -40
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            92500
_diffrn_reflns_theta_full        28.00
_diffrn_reflns_theta_max         36.28
_diffrn_reflns_theta_min         1.79
_diffrn_source                   'fine-focus sealed tube'
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.523
_exptl_absorpt_correction_T_max  0.1660
_exptl_absorpt_correction_T_min  0.1073
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2012/1 (Bruker,2012) was used for absorption correction.
wR2(int) was 0.0978 before and 0.0465 after correction.
The Ratio of minimum to maximum transmission is 0.6464.
The λ/2 correction factor is 0.0015.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.310
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2080
_exptl_crystal_size_max          0.52
_exptl_crystal_size_mid          0.38
_exptl_crystal_size_min          0.29
_refine_diff_density_max         0.934
_refine_diff_density_min         -0.644
_refine_diff_density_rms         0.082
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.032
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     617
_refine_ls_number_reflns         23755
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0587
_refine_ls_R_factor_gt           0.0384
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0400P)²+1.9610P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0842
_refine_ls_wR_factor_ref         0.0930
_reflns_number_gt                18384
_reflns_number_total             23755
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5ce00859j2.cif
_cod_data_source_block           1
_cod_depositor_comments
'Adding full bibliography for 1520076--1520078.cif.'
_cod_database_code               1520076
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Restrained distances
 B10-H10A
 1.1 with sigma of 0.02
3.a Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C11(H11),
 C12(H12), C14(H14), C15(H15), C16(H16), C17(H17), C18(H18), C20(H20), C21(H21),
  C22(H22), C23(H23), C24(H24), C26(H26), C27(H27), C28(H28), C29(H29),
 C30(H30), C32(H32), C33(H33), C34(H34), C35(H35), C36(H36), C38(H38), C39(H39),
  C40(H40), C41(H41), C42(H42), C44(H44), C45(H45), C46(H46), C47(H47),
 C48(H48), C50(H50), C51(H51), C52(H52), C53(H53), C54(H54)
3.b Boron cage BH refined with riding coordinates:
 B1(H1), B3(H3A), B4(H4A), B5(H5A), B6(H6A), B7(H7), B8(H8A), B9(H9A)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x, y+1/2, -z+1/2'
3 '-x, -y, -z'
4 'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags_posn
Ag1 Ag 0.466930(10) 0.371780(4) 0.218362(6) 0.01680(3) Uani 1 d .
P1 P 0.69144(3) 0.333644(14) 0.34618(2) 0.01687(6) Uani 1 d .
P2 P 0.25018(3) 0.316695(14) 0.13569(2) 0.01629(6) Uani 1 d .
P3 P 0.48800(4) 0.431181(14) 0.13338(2) 0.01745(6) Uani 1 d .
C1 C 0.67658(13) 0.30122(5) 0.41618(8) 0.0183(2) Uani 1 d .
C2 C 0.61988(16) 0.33159(6) 0.44226(10) 0.0240(3) Uani 1 d .
H2 H 0.5931 0.3675 0.4241 0.029 Uiso 1 calc R
C3 C 0.60256(17) 0.30973(7) 0.49438(11) 0.0285(3) Uani 1 d .
H3 H 0.5654 0.3308 0.5125 0.034 Uiso 1 calc R
C4 C 0.63961(16) 0.25709(7) 0.51999(10) 0.0271(3) Uani 1 d .
H4 H 0.6264 0.2419 0.5550 0.032 Uiso 1 calc R
C5 C 0.69619(16) 0.22656(6) 0.49444(9) 0.0245(3) Uani 1 d .
H5 H 0.7222 0.1906 0.5125 0.029 Uiso 1 calc R
C6 C 0.71494(14) 0.24833(6) 0.44263(9) 0.0207(2) Uani 1 d .
H6 H 0.7536 0.2274 0.4253 0.025 Uiso 1 calc R
C7 C 0.74170(14) 0.28108(5) 0.31186(8) 0.0186(2) Uani 1 d .
C8 C 0.63710(16) 0.24609(6) 0.24927(9) 0.0248(3) Uani 1 d .
H8 H 0.5450 0.2493 0.2285 0.030 Uiso 1 calc R
C9 C 0.66673(19) 0.20680(7) 0.21730(10) 0.0300(3) Uani 1 d .
H9 H 0.5956 0.1829 0.1757 0.036 Uiso 1 calc R
C10 C 0.8010(2) 0.20251(7) 0.24633(11) 0.0312(3) Uani 1 d .
H10 H 0.8212 0.1761 0.2238 0.037 Uiso 1 calc R
C11 C 0.90514(18) 0.23685(7) 0.30812(11) 0.0286(3) Uani 1 d .
H11 H 0.9968 0.2338 0.3281 0.034 Uiso 1 calc R
C12 C 0.87619(15) 0.27593(6) 0.34114(9) 0.0220(3) Uani 1 d .
H12 H 0.9484 0.2991 0.3837 0.026 Uiso 1 calc R
C13 C 0.84589(14) 0.37580(6) 0.41513(9) 0.0197(2) Uani 1 d .
C14 C 0.92556(16) 0.37860(7) 0.50156(10) 0.0272(3) Uani 1 d .
H14 H 0.9015 0.3573 0.5271 0.033 Uiso 1 calc R
C15 C 1.04050(18) 0.41264(8) 0.55038(11) 0.0340(4) Uani 1 d .
H15 H 1.0937 0.4148 0.6091 0.041 Uiso 1 calc R
C16 C 1.07783(18) 0.44323(7) 0.51423(12) 0.0333(4) Uani 1 d .
H16 H 1.1566 0.4662 0.5480 0.040 Uiso 1 calc R
C17 C 0.99996(18) 0.44031(7) 0.42843(12) 0.0314(3) Uani 1 d .
H17 H 1.0261 0.4610 0.4036 0.038 Uiso 1 calc R
C18 C 0.88390(16) 0.40721(6) 0.37884(10) 0.0266(3) Uani 1 d .
H18 H 0.8300 0.4059 0.3200 0.032 Uiso 1 calc R
C19 C 0.25578(13) 0.26788(5) 0.07455(9) 0.0182(2) Uani 1 d .
C20 C 0.29035(16) 0.28593(6) 0.02853(10) 0.0243(3) Uani 1 d .
H20 H 0.3045 0.3229 0.0273 0.029 Uiso 1 calc R
C21 C 0.30437(18) 0.25052(7) -0.01537(11) 0.0295(3) Uani 1 d .
H21 H 0.3269 0.2634 -0.0469 0.035 Uiso 1 calc R
C22 C 0.28553(17) 0.19625(7) -0.01333(11) 0.0296(3) Uani 1 d .
H22 H 0.2957 0.1719 -0.0431 0.035 Uiso 1 calc R
C23 C 0.25190(18) 0.17793(6) 0.03239(11) 0.0294(3) Uani 1 d .
H23 H 0.2391 0.1408 0.0340 0.035 Uiso 1 calc R
C24 C 0.23658(16) 0.21322(6) 0.07606(10) 0.0237(3) Uani 1 d .
H24 H 0.2130 0.2001 0.1070 0.028 Uiso 1 calc R
C25 C 0.20638(14) 0.27664(5) 0.18649(8) 0.0178(2) Uani 1 d .
C26 C 0.31339(14) 0.25527(6) 0.26553(9) 0.0221(3) Uani 1 d .
H26 H 0.4078 0.2639 0.2942 0.027 Uiso 1 calc R
C27 C 0.28259(16) 0.22124(7) 0.30285(10) 0.0264(3) Uani 1 d .
H27 H 0.3561 0.2060 0.3561 0.032 Uiso 1 calc R
C28 C 0.14436(17) 0.20962(7) 0.26211(11) 0.0270(3) Uani 1 d .
H28 H 0.1234 0.1868 0.2880 0.032 Uiso 1 calc R
C29 C 0.03724(17) 0.23122(7) 0.18391(11) 0.0301(3) Uani 1 d .
H29 H -0.0572 0.2233 0.1561 0.036 Uiso 1 calc R
C30 C 0.06799(15) 0.26456(7) 0.14612(10) 0.0262(3) Uani 1 d .
H30 H -0.0058 0.2792 0.0924 0.031 Uiso 1 calc R
C31 C 0.09286(13) 0.35570(5) 0.05924(8) 0.0169(2) Uani 1 d .
C32 C -0.00655(14) 0.34331(6) -0.02562(9) 0.0214(3) Uani 1 d .
H32 H 0.0035 0.3120 -0.0461 0.026 Uiso 1 calc R
C33 C -0.12098(15) 0.37671(6) -0.08073(9) 0.0244(3) Uani 1 d .
H33 H -0.1885 0.3682 -0.1387 0.029 Uiso 1 calc R
C34 C -0.13654(16) 0.42235(7) -0.05112(10) 0.0275(3) Uani 1 d .
H34 H -0.2136 0.4455 -0.0889 0.033 Uiso 1 calc R
C35 C -0.03927(18) 0.43413(7) 0.03377(11) 0.0328(4) Uani 1 d .
H35 H -0.0512 0.4649 0.0544 0.039 Uiso 1 calc R
C36 C 0.07558(16) 0.40125(6) 0.08892(9) 0.0262(3) Uani 1 d .
H36 H 0.1425 0.4098 0.1469 0.031 Uiso 1 calc R
C37 C 0.34838(14) 0.42717(5) 0.01966(9) 0.0186(2) Uani 1 d .
C38 C 0.21103(15) 0.43717(6) -0.01560(10) 0.0222(3) Uani 1 d .
H38 H 0.1932 0.4467 0.0196 0.027 Uiso 1 calc R
C39 C 0.10115(15) 0.43325(6) -0.10161(10) 0.0245(3) Uani 1 d .
H39 H 0.0085 0.4406 -0.1252 0.029 Uiso 1 calc R
C40 C 0.12605(16) 0.41864(6) -0.15348(10) 0.0256(3) Uani 1 d .
H40 H 0.0505 0.4157 -0.2123 0.031 Uiso 1 calc R
C41 C 0.26154(16) 0.40840(6) -0.11898(10) 0.0246(3) Uani 1 d .
H41 H 0.2787 0.3984 -0.1543 0.030 Uiso 1 calc R
C42 C 0.37254(15) 0.41274(6) -0.03270(9) 0.0211(2) Uani 1 d .
H42 H 0.4651 0.4058 -0.0095 0.025 Uiso 1 calc R
C43 C 0.64577(14) 0.41606(5) 0.15181(9) 0.0192(2) Uani 1 d .
C44 C 0.68071(16) 0.36266(6) 0.15543(9) 0.0218(3) Uani 1 d .
H44 H 0.6202 0.3353 0.1456 0.026 Uiso 1 calc R
C45 C 0.80353(17) 0.34945(6) 0.17339(10) 0.0262(3) Uani 1 d .
H45 H 0.8259 0.3131 0.1751 0.031 Uiso 1 calc R
C46 C 0.89315(19) 0.38904(7) 0.18880(13) 0.0344(4) Uani 1 d .
H46 H 0.9775 0.3799 0.2016 0.041 Uiso 1 calc R
C47 C 0.8595(2) 0.44232(7) 0.18544(15) 0.0404(5) Uani 1 d .
H47 H 0.9211 0.4696 0.1962 0.048 Uiso 1 calc R
C48 C 0.73577(17) 0.45574(6) 0.16630(12) 0.0300(3) Uani 1 d .
H48 H 0.7124 0.4922 0.1631 0.036 Uiso 1 calc R
C49 C 0.50175(15) 0.50202(6) 0.15603(9) 0.0204(2) Uani 1 d .
C50 C 0.57096(18) 0.51721(7) 0.23824(11) 0.0288(3) Uani 1 d .
H50 H 0.6090 0.4908 0.2804 0.035 Uiso 1 calc R
C51 C 0.5844(2) 0.57082(8) 0.25865(13) 0.0369(4) Uani 1 d .
H51 H 0.6316 0.5810 0.3147 0.044 Uiso 1 calc R
C52 C 0.5292(2) 0.60939(7) 0.19743(14) 0.0380(4) Uani 1 d .
H52 H 0.5381 0.6460 0.2115 0.046 Uiso 1 calc R
C53 C 0.4613(2) 0.59466(7) 0.11619(13) 0.0349(4) Uani 1 d .
H53 H 0.4241 0.6213 0.0744 0.042 Uiso 1 calc R
C54 C 0.44691(17) 0.54099(6) 0.09466(11) 0.0260(3) Uani 1 d .
H54 H 0.4000 0.5311 0.0385 0.031 Uiso 1 calc R
B1 B 0.37843(18) 0.54198(7) 0.44054(11) 0.0245(3) Uani 1 d .
H1 H 0.3490 0.5728 0.4644 0.029 Uiso 1 calc R
B2 B 0.47376(16) 0.49015(7) 0.45373(10) 0.0210(3) Uani 1 d .
B3 B 0.27891(16) 0.48489(7) 0.37862(10) 0.0207(3) Uani 1 d .
H3A H 0.2034 0.4678 0.3831 0.025 Uiso 1 calc R
B4 B 0.27750(18) 0.54646(7) 0.33330(11) 0.0240(3) Uani 1 d .
H4A H 0.1977 0.5791 0.3014 0.029 Uiso 1 calc R
B5 B 0.46406(19) 0.55231(7) 0.40174(11) 0.0260(3) Uani 1 d .
H5A H 0.5336 0.5879 0.4242 0.031 Uiso 1 calc R
B6 B 0.37493(17) 0.44145(7) 0.36739(11) 0.0228(3) Uani 1 d .
H6A H 0.3766 0.3978 0.3787 0.027 Uiso 1 calc R
B7 B 0.23793(16) 0.48287(7) 0.28112(10) 0.0218(3) Uani 1 d .
H7 H 0.1295 0.4723 0.2224 0.026 Uiso 1 calc R
B8 B 0.36535(19) 0.52952(8) 0.29636(11) 0.0264(3) Uani 1 d .
H8A H 0.3548 0.5548 0.2492 0.032 Uiso 1 calc R
B9 B 0.51224(18) 0.49108(7) 0.38554(11) 0.0248(3) Uani 1 d .
H9A H 0.6216 0.4860 0.4116 0.030 Uiso 1 calc R
B10 B 0.37932(18) 0.46236(8) 0.29376(11) 0.0250(3) Uani 1 d D
H10A H 0.390(3) 0.4376(9) 0.2556(14) 0.052(7) Uiso 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P1 Ag1 P2 119.589(12) . .
P1 Ag1 P3 114.876(13) . .
P2 Ag1 P3 115.143(12) . .
C1 P1 Ag1 113.31(4) . .
C1 P1 C7 105.41(6) . .
C1 P1 C13 104.32(6) . .
C7 P1 Ag1 107.31(4) . .
C7 P1 C13 105.05(6) . .
C13 P1 Ag1 120.27(5) . .
C19 P2 Ag1 108.78(4) . .
C25 P2 Ag1 121.65(4) . .
C25 P2 C19 103.34(6) . .
C31 P2 Ag1 112.62(4) . .
C31 P2 C19 105.49(6) . .
C31 P2 C25 103.54(6) . .
C37 P3 Ag1 116.72(4) . .
C37 P3 C43 103.90(6) . .
C43 P3 Ag1 111.09(4) . .
C49 P3 Ag1 115.32(5) . .
C49 P3 C37 104.10(6) . .
C49 P3 C43 104.38(6) . .
C2 C1 P1 116.74(10) . .
C6 C1 P1 123.74(11) . .
C6 C1 C2 119.51(13) . .
C1 C2 H2 119.7 . .
C3 C2 C1 120.55(14) . .
C3 C2 H2 119.7 . .
C2 C3 H3 120.1 . .
C2 C3 C4 119.86(15) . .
C4 C3 H3 120.1 . .
C3 C4 H4 120.0 . .
C3 C4 C5 120.03(14) . .
C5 C4 H4 120.0 . .
C4 C5 H5 119.8 . .
C6 C5 C4 120.46(14) . .
C6 C5 H5 119.8 . .
C1 C6 H6 120.2 . .
C5 C6 C1 119.59(14) . .
C5 C6 H6 120.2 . .
C8 C7 P1 117.78(11) . .
C12 C7 P1 123.34(11) . .
C12 C7 C8 118.78(13) . .
C7 C8 H8 119.6 . .
C9 C8 C7 120.77(15) . .
C9 C8 H8 119.6 . .
C8 C9 H9 120.1 . .
C8 C9 C10 119.86(15) . .
C10 C9 H9 120.1 . .
C9 C10 H10 120.1 . .
C11 C10 C9 119.84(15) . .
C11 C10 H10 120.1 . .
C10 C11 H11 119.8 . .
C10 C11 C12 120.44(15) . .
C12 C11 H11 119.8 . .
C7 C12 H12 119.9 . .
C11 C12 C7 120.29(14) . .
C11 C12 H12 119.9 . .
C14 C13 P1 122.86(12) . .
C14 C13 C18 119.08(14) . .
C18 C13 P1 118.06(11) . .
C13 C14 H14 120.0 . .
C15 C14 C13 119.93(16) . .
C15 C14 H14 120.0 . .
C14 C15 H15 119.7 . .
C16 C15 C14 120.66(16) . .
C16 C15 H15 119.7 . .
C15 C16 H16 120.1 . .
C15 C16 C17 119.79(15) . .
C17 C16 H16 120.1 . .
C16 C17 H17 119.9 . .
C16 C17 C18 120.17(16) . .
C18 C17 H17 119.9 . .
C13 C18 H18 119.8 . .
C17 C18 C13 120.37(15) . .
C17 C18 H18 119.8 . .
C20 C19 P2 117.91(11) . .
C20 C19 C24 118.56(13) . .
C24 C19 P2 123.38(11) . .
C19 C20 H20 119.6 . .
C21 C20 C19 120.87(14) . .
C21 C20 H20 119.6 . .
C20 C21 H21 119.9 . .
C20 C21 C22 120.20(15) . .
C22 C21 H21 119.9 . .
C21 C22 H22 120.3 . .
C23 C22 C21 119.39(15) . .
C23 C22 H22 120.3 . .
C22 C23 H23 119.6 . .
C22 C23 C24 120.77(15) . .
C24 C23 H23 119.6 . .
C19 C24 H24 119.9 . .
C23 C24 C19 120.21(14) . .
C23 C24 H24 119.9 . .
C26 C25 P2 119.31(10) . .
C26 C25 C30 119.17(13) . .
C30 C25 P2 121.44(10) . .
C25 C26 H26 119.9 . .
C25 C26 C27 120.28(13) . .
C27 C26 H26 119.9 . .
C26 C27 H27 120.0 . .
C28 C27 C26 120.00(14) . .
C28 C27 H27 120.0 . .
C27 C28 H28 120.0 . .
C29 C28 C27 120.07(14) . .
C29 C28 H28 120.0 . .
C28 C29 H29 120.0 . .
C28 C29 C30 119.96(14) . .
C30 C29 H29 120.0 . .
C25 C30 H30 119.7 . .
C29 C30 C25 120.52(14) . .
C29 C30 H30 119.7 . .
C32 C31 P2 123.83(11) . .
C32 C31 C36 119.42(13) . .
C36 C31 P2 116.73(10) . .
C31 C32 H32 119.9 . .
C31 C32 C33 120.19(13) . .
C33 C32 H32 119.9 . .
C32 C33 H33 119.9 . .
C34 C33 C32 120.16(14) . .
C34 C33 H33 119.9 . .
C33 C34 H34 120.1 . .
C33 C34 C35 119.74(14) . .
C35 C34 H34 120.1 . .
C34 C35 H35 119.8 . .
C34 C35 C36 120.39(15) . .
C36 C35 H35 119.8 . .
C31 C36 H36 120.0 . .
C35 C36 C31 120.08(14) . .
C35 C36 H36 120.0 . .
C38 C37 P3 118.28(11) . .
C42 C37 P3 122.55(10) . .
C42 C37 C38 119.13(13) . .
C37 C38 H38 119.9 . .
C39 C38 C37 120.26(14) . .
C39 C38 H38 119.9 . .
C38 C39 H39 119.9 . .
C38 C39 C40 120.27(14) . .
C40 C39 H39 119.9 . .
C39 C40 H40 120.1 . .
C41 C40 C39 119.77(14) . .
C41 C40 H40 120.1 . .
C40 C41 H41 119.9 . .
C40 C41 C42 120.23(14) . .
C42 C41 H41 119.9 . .
C37 C42 C41 120.33(13) . .
C37 C42 H42 119.8 . .
C41 C42 H42 119.8 . .
C44 C43 P3 118.65(10) . .
C48 C43 P3 122.31(11) . .
C48 C43 C44 118.97(13) . .
C43 C44 H44 119.8 . .
C45 C44 C43 120.41(14) . .
C45 C44 H44 119.8 . .
C44 C45 H45 119.9 . .
C46 C45 C44 120.24(14) . .
C46 C45 H45 119.9 . .
C45 C46 H46 120.1 . .
C45 C46 C47 119.85(15) . .
C47 C46 H46 120.1 . .
C46 C47 H47 120.0 . .
C48 C47 C46 120.10(16) . .
C48 C47 H47 120.0 . .
C43 C48 H48 119.8 . .
C47 C48 C43 120.42(15) . .
C47 C48 H48 119.8 . .
C50 C49 P3 118.03(12) . .
C50 C49 C54 119.52(14) . .
C54 C49 P3 122.44(12) . .
C49 C50 H50 119.9 . .
C51 C50 C49 120.16(17) . .
C51 C50 H50 119.9 . .
C50 C51 H51 119.9 . .
C52 C51 C50 120.14(18) . .
C52 C51 H51 119.9 . .
C51 C52 H52 120.0 . .
C53 C52 C51 119.99(16) . .
C53 C52 H52 120.0 . .
C52 C53 H53 119.7 . .
C52 C53 C54 120.58(17) . .
C54 C53 H53 119.7 . .
C49 C54 C53 119.61(16) . .
C49 C54 H54 120.2 . .
C53 C54 H54 120.2 . .
B2 B1 H1 152.6 . .
B2 B1 H1 97.1 3_666 .
B2 B1 B2 55.56(10) . 3_666
B2 B1 B3 65.36(10) . .
B2 B1 B4 95.28(12) . .
B2 B1 B5 65.42(10) . .
B3 B1 H1 126.8 . .
B3 B1 B2 101.23(11) . 3_666
B4 B1 H1 112.1 . .
B4 B1 B2 150.82(13) . 3_666
B4 B1 B3 62.28(10) . .
B4 B1 B5 61.54(10) . .
B5 B1 H1 127.6 . .
B5 B1 B2 100.24(11) . 3_666
B5 B1 B3 97.48(12) . .
B1 B2 B1 124.44(10) . 3_666
B1 B2 B2 69.27(12) . 3_666
B1 B2 B3 60.12(9) . .
B1 B2 B5 60.02(10) . .
B1 B2 B6 114.09(12) . .
B1 B2 B9 114.28(13) . .
B2 B2 B1 55.17(10) 3_666 3_666
B2 B2 B3 106.82(14) 3_666 .
B2 B2 B5 105.61(15) 3_666 .
B2 B2 B6 147.33(17) 3_666 .
B2 B2 B9 145.62(17) 3_666 .
B3 B2 B1 133.82(12) . 3_666
B3 B2 B5 91.54(10) . .
B5 B2 B1 132.52(12) . 3_666
B6 B2 B1 112.58(11) . 3_666
B6 B2 B3 57.19(8) . .
B6 B2 B5 103.26(11) . .
B9 B2 B1 111.52(11) . 3_666
B9 B2 B3 103.50(11) . .
B9 B2 B5 57.39(10) . .
B9 B2 B6 65.17(10) . .
B1 B3 B2 54.51(9) . .
B1 B3 H3A 118.5 . .
B1 B3 B4 57.36(9) . .
B2 B3 H3A 133.7 . .
B4 B3 B2 86.02(10) . .
B4 B3 H3A 132.0 . .
B6 B3 B1 112.01(12) . .
B6 B3 B2 60.57(9) . .
B6 B3 H3A 119.5 . .
B6 B3 B4 102.21(12) . .
B6 B3 B7 60.98(9) . .
B7 B3 B1 113.52(12) . .
B7 B3 B2 101.01(11) . .
B7 B3 H3A 119.4 . .
B7 B3 B4 60.63(9) . .
B1 B4 B3 60.36(10) . .
B1 B4 H4A 115.4 . .
B1 B4 B5 60.68(10) . .
B1 B4 B7 114.42(12) . .
B1 B4 B8 115.44(13) . .
B3 B4 H4A 128.8 . .
B5 B4 B3 95.77(11) . .
B5 B4 H4A 128.2 . .
B5 B4 B7 104.36(12) . .
B5 B4 B8 59.60(10) . .
B7 B4 B3 58.61(9) . .
B7 B4 H4A 120.1 . .
B8 B4 B3 104.19(12) . .
B8 B4 H4A 119.4 . .
B8 B4 B7 61.64(10) . .
B1 B5 B2 54.55(9) . .
B1 B5 B4 57.78(10) . .
B1 B5 H5A 118.6 . .
B1 B5 B8 113.58(12) . .
B2 B5 H5A 133.8 . .
B4 B5 B2 86.62(11) . .
B4 B5 H5A 131.5 . .
B8 B5 B2 101.08(12) . .
B8 B5 B4 60.44(10) . .
B8 B5 H5A 119.3 . .
B9 B5 B1 111.57(12) . .
B9 B5 B2 59.97(9) . .
B9 B5 B4 102.64(12) . .
B9 B5 H5A 119.6 . .
B9 B5 B8 61.60(10) . .
B2 B6 H6A 122.1 . .
B2 B6 B9 56.98(9) . .
B3 B6 B2 62.23(9) . .
B3 B6 H6A 119.1 . .
B3 B6 B7 59.54(9) . .
B3 B6 B9 101.22(11) . .
B7 B6 B2 101.17(11) . .
B7 B6 H6A 130.6 . .
B7 B6 B9 88.40(11) . .
B9 B6 H6A 133.6 . .
B10 B6 B2 107.36(12) . .
B10 B6 B3 112.96(13) . .
B10 B6 H6A 119.8 . .
B10 B6 B7 58.99(10) . .
B10 B6 B9 53.84(9) . .
B3 B7 B4 60.76(9) . .
B3 B7 B6 59.48(9) . .
B3 B7 H7 119.8 . .
B3 B7 B8 103.77(11) . .
B4 B7 H7 121.8 . .
B4 B7 B8 58.93(10) . .
B6 B7 B4 101.26(11) . .
B6 B7 H7 130.3 . .
B6 B7 B8 92.25(11) . .
B8 B7 H7 129.7 . .
B10 B7 B3 111.43(11) . .
B10 B7 B4 109.35(12) . .
B10 B7 B6 57.35(10) . .
B10 B7 H7 119.8 . .
B10 B7 B8 56.56(10) . .
B4 B8 B7 59.44(9) . .
B4 B8 H8A 121.5 . .
B4 B8 B9 100.32(12) . .
B5 B8 B4 59.96(10) . .
B5 B8 B7 103.01(12) . .
B5 B8 H8A 120.7 . .
B5 B8 B9 58.78(10) . .
B7 B8 H8A 129.5 . .
B9 B8 B7 91.50(11) . .
B9 B8 H8A 131.4 . .
B10 B8 B4 110.97(13) . .
B10 B8 B5 110.87(13) . .
B10 B8 B7 57.87(10) . .
B10 B8 H8A 119.0 . .
B10 B8 B9 56.77(10) . .
B2 B9 B6 57.85(9) . .
B2 B9 B8 101.56(11) . .
B2 B9 H9A 121.1 . .
B5 B9 B2 62.64(10) . .
B5 B9 B6 101.75(11) . .
B5 B9 B8 59.62(10) . .
B5 B9 H9A 119.0 . .
B6 B9 H9A 133.2 . .
B8 B9 B6 87.85(10) . .
B8 B9 H9A 131.3 . .
B10 B9 B2 108.84(12) . .
B10 B9 B5 112.63(13) . .
B10 B9 B6 54.56(10) . .
B10 B9 B8 57.85(10) . .
B10 B9 H9A 119.6 . .
B6 B10 B7 63.65(10) . .
B6 B10 B8 101.97(12) . .
B6 B10 H10A 127.5(13) . .
B7 B10 H10A 133.2(13) . .
B8 B10 B7 65.58(11) . .
B8 B10 H10A 130.6(13) . .
B9 B10 B6 71.60(11) . .
B9 B10 B7 101.48(12) . .
B9 B10 B8 65.38(11) . .
B9 B10 H10A 125.3(13) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 P1 2.4889(4) .
Ag1 P2 2.4943(4) .
Ag1 P3 2.4993(4) .
P1 C1 1.8208(14) .
P1 C7 1.8230(14) .
P1 C13 1.8243(14) .
P2 C19 1.8269(14) .
P2 C25 1.8211(14) .
P2 C31 1.8192(14) .
P3 C37 1.8238(14) .
P3 C43 1.8257(14) .
P3 C49 1.8200(14) .
C1 C2 1.400(2) .
C1 C6 1.3973(19) .
C2 H2 0.9500 .
C2 C3 1.386(2) .
C3 H3 0.9500 .
C3 C4 1.387(2) .
C4 H4 0.9500 .
C4 C5 1.393(2) .
C5 H5 0.9500 .
C5 C6 1.392(2) .
C6 H6 0.9500 .
C7 C8 1.404(2) .
C7 C12 1.3954(19) .
C8 H8 0.9500 .
C8 C9 1.389(2) .
C9 H9 0.9500 .
C9 C10 1.393(3) .
C10 H10 0.9500 .
C10 C11 1.386(3) .
C11 H11 0.9500 .
C11 C12 1.395(2) .
C12 H12 0.9500 .
C13 C14 1.395(2) .
C13 C18 1.401(2) .
C14 H14 0.9500 .
C14 C15 1.394(2) .
C15 H15 0.9500 .
C15 C16 1.381(3) .
C16 H16 0.9500 .
C16 C17 1.388(3) .
C17 H17 0.9500 .
C17 C18 1.389(2) .
C18 H18 0.9500 .
C19 C20 1.396(2) .
C19 C24 1.3977(19) .
C20 H20 0.9500 .
C20 C21 1.388(2) .
C21 H21 0.9500 .
C21 C22 1.389(2) .
C22 H22 0.9500 .
C22 C23 1.383(2) .
C23 H23 0.9500 .
C23 C24 1.392(2) .
C24 H24 0.9500 .
C25 C26 1.3917(19) .
C25 C30 1.3957(19) .
C26 H26 0.9500 .
C26 C27 1.393(2) .
C27 H27 0.9500 .
C27 C28 1.390(2) .
C28 H28 0.9500 .
C28 C29 1.384(2) .
C29 H29 0.9500 .
C29 C30 1.390(2) .
C30 H30 0.9500 .
C31 C32 1.3897(19) .
C31 C36 1.395(2) .
C32 H32 0.9500 .
C32 C33 1.394(2) .
C33 H33 0.9500 .
C33 C34 1.386(2) .
C34 H34 0.9500 .
C34 C35 1.386(2) .
C35 H35 0.9500 .
C35 C36 1.389(2) .
C36 H36 0.9500 .
C37 C38 1.4025(19) .
C37 C42 1.393(2) .
C38 H38 0.9500 .
C38 C39 1.387(2) .
C39 H39 0.9500 .
C39 C40 1.392(2) .
C40 H40 0.9500 .
C40 C41 1.387(2) .
C41 H41 0.9500 .
C41 C42 1.394(2) .
C42 H42 0.9500 .
C43 C44 1.399(2) .
C43 C48 1.394(2) .
C44 H44 0.9500 .
C44 C45 1.391(2) .
C45 H45 0.9500 .
C45 C46 1.383(2) .
C46 H46 0.9500 .
C46 C47 1.392(3) .
C47 H47 0.9500 .
C47 C48 1.391(2) .
C48 H48 0.9500 .
C49 C50 1.394(2) .
C49 C54 1.394(2) .
C50 H50 0.9500 .
C50 C51 1.389(2) .
C51 H51 0.9500 .
C51 C52 1.384(3) .
C52 H52 0.9500 .
C52 C53 1.377(3) .
C53 H53 0.9500 .
C53 C54 1.395(2) .
C54 H54 0.9500 .
B1 H1 1.1200 .
B1 B2 1.676(2) .
B1 B2 1.909(2) 3_666
B1 B3 1.784(2) .
B1 B4 1.729(2) .
B1 B5 1.782(3) .
B2 B1 1.909(2) 3_666
B2 B2 1.683(3) 3_666
B2 B3 1.870(2) .
B2 B5 1.871(2) .
B2 B6 1.841(2) .
B2 B9 1.823(2) .
B3 H3A 1.1200 .
B3 B4 1.817(2) .
B3 B6 1.777(2) .
B3 B7 1.778(2) .
B4 H4A 1.1200 .
B4 B5 1.796(2) .
B4 B7 1.815(2) .
B4 B8 1.805(3) .
B5 H5A 1.1200 .
B5 B8 1.790(3) .
B5 B9 1.774(3) .
B6 H6A 1.1200 .
B6 B7 1.803(2) .
B6 B9 1.974(2) .
B6 B10 1.695(3) .
B7 H7 1.1200 .
B7 B8 1.855(3) .
B7 B10 1.725(2) .
B8 H8A 1.1200 .
B8 B9 1.825(3) .
B8 B10 1.700(3) .
B9 H9A 1.1200 .
B9 B10 1.679(2) .
B10 H10A 1.101(16) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Ag1 P1 C1 C2 -54.28(12) . .
Ag1 P1 C1 C6 124.07(11) . .
Ag1 P1 C7 C8 -43.06(12) . .
Ag1 P1 C7 C12 133.20(11) . .
Ag1 P1 C13 C14 128.55(12) . .
Ag1 P1 C13 C18 -50.40(13) . .
Ag1 P2 C19 C20 -48.09(12) . .
Ag1 P2 C19 C24 127.46(11) . .
Ag1 P2 C25 C26 -30.99(13) . .
Ag1 P2 C25 C30 152.40(11) . .
Ag1 P2 C31 C32 126.45(11) . .
Ag1 P2 C31 C36 -51.82(13) . .
Ag1 P3 C37 C38 57.65(12) . .
Ag1 P3 C37 C42 -119.97(11) . .
Ag1 P3 C43 C44 43.04(13) . .
Ag1 P3 C43 C48 -133.87(13) . .
Ag1 P3 C49 C50 33.25(13) . .
Ag1 P3 C49 C54 -147.26(11) . .
P1 Ag1 P2 C19 -75.94(5) . .
P1 Ag1 P2 C25 43.78(6) . .
P1 Ag1 P2 C31 167.48(5) . .
P1 Ag1 P3 C37 142.61(5) . .
P1 Ag1 P3 C43 23.77(5) . .
P1 Ag1 P3 C49 -94.72(5) . .
P1 C1 C2 C3 178.88(12) . .
P1 C1 C6 C5 -178.25(11) . .
P1 C7 C8 C9 176.82(12) . .
P1 C7 C12 C11 -175.79(12) . .
P1 C13 C14 C15 -178.45(13) . .
P1 C13 C18 C17 179.51(13) . .
P2 Ag1 P1 C1 -47.62(5) . .
P2 Ag1 P1 C7 68.31(5) . .
P2 Ag1 P1 C13 -171.90(5) . .
P2 Ag1 P3 C37 -2.36(5) . .
P2 Ag1 P3 C43 -121.20(5) . .
P2 Ag1 P3 C49 120.31(5) . .
P2 C19 C20 C21 176.26(12) . .
P2 C19 C24 C23 -175.51(12) . .
P2 C25 C26 C27 -175.14(12) . .
P2 C25 C30 C29 176.00(14) . .
P2 C31 C32 C33 -176.98(11) . .
P2 C31 C36 C35 177.60(14) . .
P3 Ag1 P1 C1 169.08(5) . .
P3 Ag1 P1 C7 -74.99(5) . .
P3 Ag1 P1 C13 44.80(6) . .
P3 Ag1 P2 C19 67.27(5) . .
P3 Ag1 P2 C25 -173.01(5) . .
P3 Ag1 P2 C31 -49.31(5) . .
P3 C37 C38 C39 -178.38(11) . .
P3 C37 C42 C41 177.69(11) . .
P3 C43 C44 C45 -176.87(12) . .
P3 C43 C48 C47 175.82(16) . .
P3 C49 C50 C51 179.87(13) . .
P3 C49 C54 C53 -179.81(12) . .
C1 P1 C7 C8 77.99(12) . .
C1 P1 C7 C12 -105.75(12) . .
C1 P1 C13 C14 0.10(14) . .
C1 P1 C13 C18 -178.85(12) . .
C1 C2 C3 C4 -1.0(2) . .
C2 C1 C6 C5 0.0(2) . .
C2 C3 C4 C5 1.0(2) . .
C3 C4 C5 C6 -0.5(2) . .
C4 C5 C6 C1 0.0(2) . .
C6 C1 C2 C3 0.5(2) . .
C7 P1 C1 C2 -171.33(11) . .
C7 P1 C1 C6 7.01(13) . .
C7 P1 C13 C14 -110.54(13) . .
C7 P1 C13 C18 70.51(13) . .
C7 C8 C9 C10 -1.2(2) . .
C8 C7 C12 C11 0.4(2) . .
C8 C9 C10 C11 1.2(3) . .
C9 C10 C11 C12 -0.4(2) . .
C10 C11 C12 C7 -0.4(2) . .
C12 C7 C8 C9 0.4(2) . .
C13 P1 C1 C2 78.29(12) . .
C13 P1 C1 C6 -103.37(12) . .
C13 P1 C7 C8 -172.15(11) . .
C13 P1 C7 C12 4.11(14) . .
C13 C14 C15 C16 -0.9(3) . .
C14 C13 C18 C17 0.5(2) . .
C14 C15 C16 C17 0.3(3) . .
C15 C16 C17 C18 0.7(3) . .
C16 C17 C18 C13 -1.1(3) . .
C18 C13 C14 C15 0.5(2) . .
C19 P2 C25 C26 91.34(12) . .
C19 P2 C25 C30 -85.27(13) . .
C19 P2 C31 C32 7.93(14) . .
C19 P2 C31 C36 -170.35(12) . .
C19 C20 C21 C22 -0.7(2) . .
C20 C19 C24 C23 0.0(2) . .
C20 C21 C22 C23 0.4(3) . .
C21 C22 C23 C24 0.1(3) . .
C22 C23 C24 C19 -0.3(2) . .
C24 C19 C20 C21 0.5(2) . .
C25 P2 C19 C20 -178.64(11) . .
C25 P2 C19 C24 -3.10(13) . .
C25 P2 C31 C32 -100.31(13) . .
C25 P2 C31 C36 81.42(13) . .
C25 C26 C27 C28 -1.7(2) . .
C26 C25 C30 C29 -0.6(2) . .
C26 C27 C28 C29 1.0(3) . .
C27 C28 C29 C30 0.0(3) . .
C28 C29 C30 C25 -0.2(3) . .
C30 C25 C26 C27 1.6(2) . .
C31 P2 C19 C20 72.97(12) . .
C31 P2 C19 C24 -111.48(12) . .
C31 P2 C25 C26 -158.82(12) . .
C31 P2 C25 C30 24.58(14) . .
C31 C32 C33 C34 -0.3(2) . .
C32 C31 C36 C35 -0.7(2) . .
C32 C33 C34 C35 -1.2(3) . .
C33 C34 C35 C36 1.7(3) . .
C34 C35 C36 C31 -0.7(3) . .
C36 C31 C32 C33 1.3(2) . .
C37 P3 C43 C44 -83.25(12) . .
C37 P3 C43 C48 99.84(14) . .
C37 P3 C49 C50 162.42(12) . .
C37 P3 C49 C54 -18.09(14) . .
C37 C38 C39 C40 0.9(2) . .
C38 C37 C42 C41 0.1(2) . .
C38 C39 C40 C41 -0.5(2) . .
C39 C40 C41 C42 -0.1(2) . .
C40 C41 C42 C37 0.3(2) . .
C42 C37 C38 C39 -0.7(2) . .
C43 P3 C37 C38 -179.70(11) . .
C43 P3 C37 C42 2.68(13) . .
C43 P3 C49 C50 -88.92(12) . .
C43 P3 C49 C54 90.58(13) . .
C43 C44 C45 C46 0.7(2) . .
C44 C43 C48 C47 -1.1(3) . .
C44 C45 C46 C47 -0.7(3) . .
C45 C46 C47 C48 -0.3(3) . .
C46 C47 C48 C43 1.1(3) . .
C48 C43 C44 C45 0.1(2) . .
C49 P3 C37 C38 -70.67(12) . .
C49 P3 C37 C42 111.71(12) . .
C49 P3 C43 C44 167.94(12) . .
C49 P3 C43 C48 -8.97(15) . .
C49 C50 C51 C52 0.0(3) . .
C50 C49 C54 C53 -0.3(2) . .
C50 C51 C52 C53 -0.3(3) . .
C51 C52 C53 C54 0.3(3) . .
C52 C53 C54 C49 0.0(2) . .
C54 C49 C50 C51 0.4(2) . .
B1 B2 B3 B1 110.65(16) 3_666 .
B1 B2 B3 B4 52.10(10) . .
B1 B2 B3 B4 162.74(15) 3_666 .
B1 B2 B3 B6 -90.84(17) 3_666 .
B1 B2 B3 B6 158.51(13) . .
B1 B2 B3 B7 -138.22(15) 3_666 .
B1 B2 B3 B7 111.13(13) . .
B1 B2 B5 B1 -110.91(16) 3_666 .
B1 B2 B5 B4 -52.16(10) . .
B1 B2 B5 B4 -163.06(15) 3_666 .
B1 B2 B5 B8 137.94(15) 3_666 .
B1 B2 B5 B8 -111.15(13) . .
B1 B2 B5 B9 90.24(16) 3_666 .
B1 B2 B5 B9 -158.85(13) . .
B1 B2 B6 B3 128.61(13) 3_666 .
B1 B2 B6 B3 -20.36(13) . .
B1 B2 B6 B7 26.17(16) . .
B1 B2 B6 B7 175.14(11) 3_666 .
B1 B2 B6 B9 -104.20(13) 3_666 .
B1 B2 B6 B9 106.83(14) . .
B1 B2 B6 B10 -124.09(13) 3_666 .
B1 B2 B6 B10 86.94(15) . .
B1 B2 B9 B5 -127.61(13) 3_666 .
B1 B2 B9 B5 20.05(12) . .
B1 B2 B9 B6 -106.54(13) . .
B1 B2 B9 B6 105.81(12) 3_666 .
B1 B2 B9 B8 -26.55(16) . .
B1 B2 B9 B8 -174.21(12) 3_666 .
B1 B2 B9 B10 126.06(13) 3_666 .
B1 B2 B9 B10 -86.28(16) . .
B1 B3 B4 B5 51.41(11) . .
B1 B3 B4 B7 154.73(12) . .
B1 B3 B4 B8 111.47(13) . .
B1 B3 B6 B2 18.77(12) . .
B1 B3 B6 B7 -105.54(13) . .
B1 B3 B6 B9 -24.16(15) . .
B1 B3 B6 B10 -79.46(15) . .
B1 B3 B7 B4 -23.09(11) . .
B1 B3 B7 B6 103.06(13) . .
B1 B3 B7 B8 18.66(15) . .
B1 B3 B7 B10 77.77(15) . .
B1 B4 B5 B2 49.50(10) . .
B1 B4 B5 B8 154.27(13) . .
B1 B4 B5 B9 107.70(13) . .
B1 B4 B7 B3 24.05(12) . .
B1 B4 B7 B6 -21.13(16) . .
B1 B4 B7 B8 -106.93(14) . .
B1 B4 B7 B10 -80.26(16) . .
B1 B4 B8 B5 -24.79(13) . .
B1 B4 B8 B7 105.27(14) . .
B1 B4 B8 B9 19.66(17) . .
B1 B4 B8 B10 77.87(17) . .
B1 B5 B8 B4 23.63(12) . .
B1 B5 B8 B7 -18.94(16) . .
B1 B5 B8 B9 -102.71(14) . .
B1 B5 B8 B10 -79.20(16) . .
B1 B5 B9 B2 -18.42(11) . .
B1 B5 B9 B6 25.55(15) . .
B1 B5 B9 B8 105.97(14) . .
B1 B5 B9 B10 81.85(16) . .
B2 B1 B2 B1 0.0 3_666 3_666
B2 B1 B2 B3 125.05(14) 3_666 .
B2 B1 B2 B5 -123.41(14) 3_666 .
B2 B1 B2 B6 144.76(19) 3_666 .
B2 B1 B2 B9 -142.88(18) 3_666 .
B2 B1 B3 B2 -43.50(12) 3_666 .
B2 B1 B3 B4 -154.32(13) 3_666 .
B2 B1 B3 B4 -110.82(12) . .
B2 B1 B3 B6 -20.13(12) . .
B2 B1 B3 B6 -63.63(14) 3_666 .
B2 B1 B3 B7 -130.38(12) 3_666 .
B2 B1 B3 B7 -86.88(13) . .
B2 B1 B4 B3 58.57(10) . .
B2 B1 B4 B3 60.7(3) 3_666 .
B2 B1 B4 B5 -58.32(11) . .
B2 B1 B4 B5 -56.2(3) 3_666 .
B2 B1 B4 B7 37.1(3) 3_666 .
B2 B1 B4 B7 34.97(15) . .
B2 B1 B4 B8 -33.82(16) . .
B2 B1 B4 B8 -31.7(3) 3_666 .
B2 B1 B5 B2 44.40(12) 3_666 .
B2 B1 B5 B4 155.68(13) 3_666 .
B2 B1 B5 B4 111.29(12) . .
B2 B1 B5 B8 131.35(13) 3_666 .
B2 B1 B5 B8 86.95(14) . .
B2 B1 B5 B9 19.62(12) . .
B2 B1 B5 B9 64.02(14) 3_666 .
B2 B2 B3 B1 53.12(14) 3_666 .
B2 B2 B3 B4 105.21(16) 3_666 .
B2 B2 B3 B6 -148.37(18) 3_666 .
B2 B2 B3 B7 164.25(15) 3_666 .
B2 B2 B5 B1 -54.16(14) 3_666 .
B2 B2 B5 B4 -106.31(15) 3_666 .
B2 B2 B5 B8 -165.31(14) 3_666 .
B2 B2 B5 B9 146.99(16) 3_666 .
B2 B2 B6 B3 68.4(3) 3_666 .
B2 B2 B6 B7 115.0(3) 3_666 .
B2 B2 B6 B9 -164.4(3) 3_666 .
B2 B2 B6 B10 175.7(3) 3_666 .
B2 B2 B9 B5 -68.3(3) 3_666 .
B2 B2 B9 B6 165.1(3) 3_666 .
B2 B2 B9 B8 -114.9(3) 3_666 .
B2 B2 B9 B10 -174.7(3) 3_666 .
B2 B3 B4 B1 -49.73(10) . .
B2 B3 B4 B5 1.68(11) . .
B2 B3 B4 B7 105.00(10) . .
B2 B3 B4 B8 61.74(12) . .
B2 B3 B6 B7 -124.31(12) . .
B2 B3 B6 B9 -42.93(10) . .
B2 B3 B6 B10 -98.23(13) . .
B2 B3 B7 B4 -79.01(11) . .
B2 B3 B7 B6 47.13(10) . .
B2 B3 B7 B8 -37.27(13) . .
B2 B3 B7 B10 21.84(15) . .
B2 B5 B8 B4 79.62(12) . .
B2 B5 B8 B7 37.05(14) . .
B2 B5 B8 B9 -46.72(10) . .
B2 B5 B8 B10 -23.21(16) . .
B2 B5 B9 B6 43.98(10) . .
B2 B5 B9 B8 124.40(12) . .
B2 B5 B9 B10 100.27(14) . .
B2 B6 B7 B3 -48.16(10) . .
B2 B6 B7 B4 -2.23(13) . .
B2 B6 B7 B8 56.52(12) . .
B2 B6 B7 B10 103.66(12) . .
B2 B6 B9 B5 -46.75(11) . .
B2 B6 B9 B8 -105.10(12) . .
B2 B6 B9 B10 -156.29(14) . .
B2 B6 B10 B7 -92.81(12) . .
B2 B6 B10 B8 -38.02(14) . .
B2 B6 B10 B9 20.69(12) . .
B2 B9 B10 B6 -21.09(12) . .
B2 B9 B10 B7 35.90(16) . .
B2 B9 B10 B8 92.04(13) . .
B3 B1 B2 B1 -125.05(14) . 3_666
B3 B1 B2 B2 -125.05(14) . 3_666
B3 B1 B2 B5 111.55(11) . .
B3 B1 B2 B6 19.71(12) . .
B3 B1 B2 B9 92.07(13) . .
B3 B1 B4 B5 -116.89(12) . .
B3 B1 B4 B7 -23.59(12) . .
B3 B1 B4 B8 -92.39(14) . .
B3 B1 B5 B2 -58.51(10) . .
B3 B1 B5 B4 52.78(11) . .
B3 B1 B5 B8 28.44(15) . .
B3 B1 B5 B9 -38.88(14) . .
B3 B2 B5 B1 53.78(10) . .
B3 B2 B5 B4 1.63(11) . .
B3 B2 B5 B8 -57.37(12) . .
B3 B2 B5 B9 -105.07(11) . .
B3 B2 B6 B7 46.53(10) . .
B3 B2 B6 B9 127.19(12) . .
B3 B2 B6 B10 107.30(13) . .
B3 B2 B9 B5 83.07(11) . .
B3 B2 B9 B6 -43.52(10) . .
B3 B2 B9 B8 36.46(14) . .
B3 B2 B9 B10 -23.27(16) . .
B3 B4 B5 B1 -51.18(10) . .
B3 B4 B5 B2 -1.68(11) . .
B3 B4 B5 B8 103.08(12) . .
B3 B4 B5 B9 56.51(13) . .
B3 B4 B7 B6 -45.18(10) . .
B3 B4 B7 B8 -130.97(12) . .
B3 B4 B7 B10 -104.31(13) . .
B3 B4 B8 B5 -88.39(12) . .
B3 B4 B8 B7 41.67(10) . .
B3 B4 B8 B9 -43.95(14) . .
B3 B4 B8 B10 14.27(16) . .
B3 B6 B7 B4 45.93(11) . .
B3 B6 B7 B8 104.68(11) . .
B3 B6 B7 B10 151.82(13) . .
B3 B6 B9 B2 45.95(10) . .
B3 B6 B9 B5 -0.80(13) . .
B3 B6 B9 B8 -59.16(12) . .
B3 B6 B9 B10 -110.34(13) . .
B3 B6 B10 B7 -26.24(12) . .
B3 B6 B10 B8 28.55(16) . .
B3 B6 B10 B9 87.26(13) . .
B3 B7 B8 B4 -42.71(11) . .
B3 B7 B8 B5 0.14(14) . .
B3 B7 B8 B9 58.39(12) . .
B3 B7 B8 B10 106.80(13) . .
B3 B7 B10 B6 25.92(12) . .
B3 B7 B10 B8 -92.70(13) . .
B3 B7 B10 B9 -36.70(16) . .
B4 B1 B2 B1 178.76(15) . 3_666
B4 B1 B2 B2 178.76(15) . 3_666
B4 B1 B2 B3 -56.20(10) . .
B4 B1 B2 B5 55.35(11) . .
B4 B1 B2 B6 -36.49(15) . .
B4 B1 B2 B9 35.88(15) . .
B4 B1 B3 B2 110.82(12) . .
B4 B1 B3 B6 90.69(13) . .
B4 B1 B3 B7 23.94(12) . .
B4 B1 B5 B2 -111.29(12) . .
B4 B1 B5 B8 -24.34(13) . .
B4 B1 B5 B9 -91.66(13) . .
B4 B3 B6 B2 78.26(11) . .
B4 B3 B6 B7 -46.05(10) . .
B4 B3 B6 B9 35.33(13) . .
B4 B3 B6 B10 -19.97(15) . .
B4 B3 B7 B6 126.14(12) . .
B4 B3 B7 B8 41.74(11) . .
B4 B3 B7 B10 100.85(13) . .
B4 B5 B8 B7 -42.57(11) . .
B4 B5 B8 B9 -126.33(12) . .
B4 B5 B8 B10 -102.82(14) . .
B4 B5 B9 B2 -78.49(12) . .
B4 B5 B9 B6 -34.52(14) . .
B4 B5 B9 B8 45.90(11) . .
B4 B5 B9 B10 21.78(17) . .
B4 B7 B8 B5 42.85(11) . .
B4 B7 B8 B9 101.10(12) . .
B4 B7 B8 B10 149.51(13) . .
B4 B7 B10 B6 91.19(13) . .
B4 B7 B10 B8 -27.43(12) . .
B4 B7 B10 B9 28.58(16) . .
B4 B8 B9 B2 3.28(14) . .
B4 B8 B9 B5 -45.14(11) . .
B4 B8 B9 B6 59.83(12) . .
B4 B8 B9 B10 108.40(13) . .
B4 B8 B10 B6 -25.63(16) . .
B4 B8 B10 B7 27.90(12) . .
B4 B8 B10 B9 -88.75(13) . .
B5 B1 B2 B1 123.41(14) . 3_666
B5 B1 B2 B2 123.41(14) . 3_666
B5 B1 B2 B3 -111.55(11) . .
B5 B1 B2 B6 -91.84(13) . .
B5 B1 B2 B9 -19.47(12) . .
B5 B1 B3 B2 58.55(10) . .
B5 B1 B3 B4 -52.26(11) . .
B5 B1 B3 B6 38.43(14) . .
B5 B1 B3 B7 -28.32(14) . .
B5 B1 B4 B3 116.89(12) . .
B5 B1 B4 B7 93.29(14) . .
B5 B1 B4 B8 24.50(13) . .
B5 B2 B3 B1 -53.71(11) . .
B5 B2 B3 B4 -1.61(11) . .
B5 B2 B3 B6 104.81(12) . .
B5 B2 B3 B7 57.43(12) . .
B5 B2 B6 B3 -83.17(11) . .
B5 B2 B6 B7 -36.64(13) . .
B5 B2 B6 B9 44.02(10) . .
B5 B2 B6 B10 24.13(14) . .
B5 B2 B9 B6 -126.59(11) . .
B5 B2 B9 B8 -46.60(11) . .
B5 B2 B9 B10 -106.33(14) . .
B5 B4 B7 B3 88.02(12) . .
B5 B4 B7 B6 42.84(14) . .
B5 B4 B7 B8 -42.96(11) . .
B5 B4 B7 B10 -16.29(16) . .
B5 B4 B8 B7 130.06(12) . .
B5 B4 B8 B9 44.44(11) . .
B5 B4 B8 B10 102.66(14) . .
B5 B8 B9 B2 48.42(11) . .
B5 B8 B9 B6 104.97(11) . .
B5 B8 B9 B10 153.54(14) . .
B5 B8 B10 B6 39.05(16) . .
B5 B8 B10 B7 92.58(13) . .
B5 B8 B10 B9 -24.07(13) . .
B5 B9 B10 B6 -88.52(13) . .
B5 B9 B10 B7 -31.52(17) . .
B5 B9 B10 B8 24.61(13) . .
B6 B2 B3 B1 -158.51(13) . .
B6 B2 B3 B4 -106.42(11) . .
B6 B2 B3 B7 -47.38(11) . .
B6 B2 B5 B1 110.38(12) . .
B6 B2 B5 B4 58.22(12) . .
B6 B2 B5 B8 -0.77(14) . .
B6 B2 B5 B9 -48.47(11) . .
B6 B2 B9 B5 126.59(11) . .
B6 B2 B9 B8 79.98(11) . .
B6 B2 B9 B10 20.26(12) . .
B6 B3 B4 B1 -108.47(12) . .
B6 B3 B4 B5 -57.06(13) . .
B6 B3 B4 B7 46.26(10) . .
B6 B3 B4 B8 3.00(14) . .
B6 B3 B7 B4 -126.14(12) . .
B6 B3 B7 B8 -84.40(12) . .
B6 B3 B7 B10 -25.29(12) . .
B6 B7 B8 B4 -101.80(11) . .
B6 B7 B8 B5 -58.96(13) . .
B6 B7 B8 B9 -0.70(11) . .
B6 B7 B8 B10 47.71(10) . .
B6 B7 B10 B8 -118.62(12) . .
B6 B7 B10 B9 -62.61(12) . .
B6 B9 B10 B7 56.99(11) . .
B6 B9 B10 B8 113.13(12) . .
B7 B3 B4 B1 -154.73(12) . .
B7 B3 B4 B5 -103.32(12) . .
B7 B3 B4 B8 -43.26(11) . .
B7 B3 B6 B2 124.31(12) . .
B7 B3 B6 B9 81.38(11) . .
B7 B3 B6 B10 26.08(12) . .
B7 B4 B5 B1 -110.22(13) . .
B7 B4 B5 B2 -60.72(12) . .
B7 B4 B5 B8 44.05(11) . .
B7 B4 B5 B9 -2.52(15) . .
B7 B4 B8 B5 -130.06(12) . .
B7 B4 B8 B9 -85.61(12) . .
B7 B4 B8 B10 -27.40(12) . .
B7 B6 B9 B2 104.44(11) . .
B7 B6 B9 B5 57.69(12) . .
B7 B6 B9 B8 -0.66(11) . .
B7 B6 B9 B10 -51.84(11) . .
B7 B6 B10 B8 54.79(11) . .
B7 B6 B10 B9 113.50(12) . .
B7 B8 B9 B2 -55.90(12) . .
B7 B8 B9 B5 -104.32(12) . .
B7 B8 B9 B6 0.64(10) . .
B7 B8 B9 B10 49.21(10) . .
B7 B8 B10 B6 -53.52(11) . .
B7 B8 B10 B9 -116.65(12) . .
B8 B4 B5 B1 -154.27(13) . .
B8 B4 B5 B2 -104.77(12) . .
B8 B4 B5 B9 -46.57(11) . .
B8 B4 B7 B3 130.97(12) . .
B8 B4 B7 B6 85.79(11) . .
B8 B4 B7 B10 26.66(12) . .
B8 B5 B9 B2 -124.40(12) . .
B8 B5 B9 B6 -80.42(11) . .
B8 B5 B9 B10 -24.13(13) . .
B8 B7 B10 B6 118.62(12) . .
B8 B7 B10 B9 56.01(12) . .
B8 B9 B10 B6 -113.13(12) . .
B8 B9 B10 B7 -56.14(12) . .
B9 B2 B3 B1 -110.48(13) . .
B9 B2 B3 B4 -58.38(12) . .
B9 B2 B3 B6 48.04(11) . .
B9 B2 B3 B7 0.66(14) . .
B9 B2 B5 B1 158.85(13) . .
B9 B2 B5 B4 106.70(12) . .
B9 B2 B5 B8 47.70(11) . .
B9 B2 B6 B3 -127.19(12) . .
B9 B2 B6 B7 -80.65(11) . .
B9 B2 B6 B10 -19.89(11) . .
B9 B5 B8 B4 126.33(12) . .
B9 B5 B8 B7 83.77(12) . .
B9 B5 B8 B10 23.51(12) . .
B9 B6 B7 B3 -104.02(11) . .
B9 B6 B7 B4 -58.09(12) . .
B9 B6 B7 B8 0.65(10) . .
B9 B6 B7 B10 47.79(10) . .
B9 B6 B10 B7 -113.50(12) . .
B9 B6 B10 B8 -58.71(11) . .
B9 B8 B10 B6 63.12(11) . .
B9 B8 B10 B7 116.65(12) . .
B10 B6 B7 B3 -151.82(13) . .
B10 B6 B7 B4 -105.88(13) . .
B10 B6 B7 B8 -47.14(11) . .
B10 B6 B9 B2 156.29(14) . .
B10 B6 B9 B5 109.54(13) . .
B10 B6 B9 B8 51.18(11) . .
B10 B7 B8 B4 -149.51(13) . .
B10 B7 B8 B5 -106.66(13) . .
B10 B7 B8 B9 -48.41(11) . .
B10 B8 B9 B2 -105.12(13) . .
B10 B8 B9 B5 -153.54(14) . .
B10 B8 B9 B6 -48.57(10) . .
