#------------------------------------------------------------------------------
#$Date: 2016-01-09 12:15:27 +0200 (Sat, 09 Jan 2016) $
#$Revision: 173731 $
#$URL: svn://www.crystallography.net/cod/cif/1/52/00/1520078.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1520078
loop_
_publ_author_name
'Avdeeva, Varvara V.'
'Buzin, Mikhail I.'
'Malinina, Elena A.'
'Kuznetsov, Nikolay T.'
'Vologzhanina, Anna V.'
_publ_section_title
;
 Reversible single-crystal-to-single-crystal photoisomerization of a
 silver(i) macropolyhedral borane
;
_journal_issue                   46
_journal_name_full               CrystEngComm
_journal_page_first              8870
_journal_paper_doi               10.1039/C5CE00859J
_journal_volume                  17
_journal_year                    2015
_chemical_formula_moiety         '2(C54 H45 Ag P3), B20 H18'
_chemical_formula_sum            'C108 H108 Ag2 B20 P6'
_chemical_formula_weight         2023.70
_chemical_name_systematic
;
 ?
;
_chemical_properties_physical    Light-sensitive
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_audit_creation_date             2015-03-12
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2015-03-12 deposited with the CCDC.
2015-05-28 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 131.733(2)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   12.9900(8)
_cell_length_b                   25.1550(14)
_cell_length_c                   21.7332(14)
_cell_measurement_reflns_used    5661
_cell_measurement_temperature    353
_cell_measurement_theta_max      26.06
_cell_measurement_theta_min      2.25
_cell_volume                     5299.6(6)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'olex2.solve (Bourhis et al., 2015)'
_diffrn_ambient_temperature      353
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0459
_diffrn_reflns_av_unetI/netI     0.0437
_diffrn_reflns_laue_measured_fraction_full 0.997
_diffrn_reflns_laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       37
_diffrn_reflns_limit_k_min       -37
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            80819
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         32.375
_diffrn_reflns_theta_min         1.923
_exptl_absorpt_coefficient_mu    0.507
_exptl_absorpt_correction_T_max  0.1591
_exptl_absorpt_correction_T_min  0.1074
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2012/1 (Bruker,2012) was used for absorption correction.
wR2(int) was 0.0957 before and 0.0455 after correction.
The Ratio of minimum to maximum transmission is 0.6750.
The λ/2 correction factor is 0.0015.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.268
_exptl_crystal_description       prism
_exptl_crystal_F_000             2080
_exptl_crystal_recrystallization_method
'solid state reaction by heating of the iso-isomer'
_exptl_crystal_size_max          0.52
_exptl_crystal_size_mid          0.38
_exptl_crystal_size_min          0.29
_refine_diff_density_max         0.640
_refine_diff_density_min         -0.320
_refine_diff_density_rms         0.057
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.011
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     608
_refine_ls_number_reflns         18906
_refine_ls_number_restraints     18
_refine_ls_restrained_S_all      1.036
_refine_ls_R_factor_all          0.1045
_refine_ls_R_factor_gt           0.0503
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0600P)²+1.5140P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1123
_refine_ls_wR_factor_ref         0.1385
_reflns_Friedel_coverage         0.000
_reflns_number_gt                10904
_reflns_number_total             18906
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5ce00859j2.cif
_cod_data_source_block           1ht
_cod_depositor_comments
'Adding full bibliography for 1520076--1520078.cif.'
_cod_database_code               1520078
_shelxl_version_number           2014-3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All B(H,H) groups, All C(H) groups
2. Restrained distances
 B7-B3A
 1.7 with sigma of 0.02
 B4-B3A
 1.7 with sigma of 0.02
 B10-B3A
 1.7 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
B3A \\sim B3: within 1.7A with sigma of 0.04 and sigma for terminal atoms of
0.08
B6 \\sim B6A: within 1.7A with sigma of 0.04 and sigma for terminal atoms of
0.08
B1 \\sim B1A: within 1.7A with sigma of 0.04 and sigma for terminal atoms of
0.08
B2A \\sim B2: within 1.7A with sigma of 0.04 and sigma for terminal atoms of
0.08
B10: within 1.7A with sigma of 0.04 and sigma for terminal atoms of 0.08
Uanis(C3) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.005
4. Others
 Fixed Sof: B1(0.75) H1(0.75) B2(0.75) B3(0.75) H3A(0.75) H5A(0.75) H5B(0.25)
 B6(0.75) H6A(0.75) H7A(0.75) H7B(0.25) H9A(0.75) H9B(0.25) H10B(0.25)
 H10A(0.75) B2A(0.25) H2A(0.25) B6A(0.25) H6AA(0.25) B3A(0.25) H3AA(0.25)
 B1A(0.25)
 Fixed Uiso: B2A(0.07)
5.a Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C11(H11),
 C12(H12), C14(H14), C15(H15), C16(H16), C17(H17), C18(H18), C20(H20), C21(H21),
  C22(H22), C23(H23), C24(H24), C26(H26), C27(H27), C28(H28), C29(H29),
 C30(H30), C32(H32), C33(H33), C34(H34), C35(H35), C36(H36), C38(H38), C39(H39),
  C40(H40), C41(H41), C42(H42), C44(H44), C45(H45), C46(H46), C47(H47),
 C48(H48), C50(H50), C51(H51), C52(H52), C53(H53), C54(H54)
5.b Boron cage BH refined with riding coordinates:
 B1(H1), B3(H3A), B4(H4A), B5(H5A), B5(H5B), B6(H6A), B7(H7A), B7(H7B),
 B8(H8A), B9(H9A), B9(H9B), B10(H10B), B10(H10A), B2A(H2A), B6A(H6AA), B3A(H3AA)
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.96991(2) 0.62725(2) 1.22092(2) 0.05027(7) Uani 1 1 d . . . . .
P1 P 0.98997(7) 0.56695(3) 1.13664(4) 0.05028(15) Uani 1 1 d . . . . .
P2 P 0.75391(6) 0.68248(2) 1.13850(4) 0.04538(14) Uani 1 1 d . . . . .
P3 P 1.19208(6) 0.66635(3) 1.34729(4) 0.04952(15) Uani 1 1 d . . . . .
C1 C 1.1455(3) 0.58211(11) 1.15457(17) 0.0552(6) Uani 1 1 d . . . . .
C2 C 1.2329(4) 0.54338(14) 1.1676(3) 0.0900(12) Uani 1 1 d . . . . .
H2 H 1.2105 0.5077 1.1640 0.108 Uiso 1 1 calc R . . . .
C3 C 1.3543(4) 0.55724(17) 1.1863(3) 0.1091(14) Uani 1 1 d . U . . .
H3 H 1.4139 0.5308 1.1963 0.131 Uiso 1 1 calc R . . . .
C4 C 1.3870(4) 0.60961(17) 1.1899(3) 0.1022(14) Uani 1 1 d . . . . .
H4 H 1.4682 0.6186 1.2019 0.123 Uiso 1 1 calc R . . . .
C5 C 1.3004(4) 0.64841(14) 1.1759(2) 0.0757(9) Uani 1 1 d . . . . .
H5 H 1.3219 0.6840 1.1778 0.091 Uiso 1 1 calc R . . . .
C6 C 1.1805(3) 0.63482(11) 1.15880(19) 0.0622(7) Uani 1 1 d . . . . .
H6 H 1.1224 0.6615 1.1500 0.075 Uiso 1 1 calc R . . . .
C7 C 0.8515(3) 0.57183(10) 1.02463(17) 0.0515(6) Uani 1 1 d . . . . .
C8 C 0.8731(3) 0.58757(12) 0.97314(18) 0.0628(7) Uani 1 1 d . . . . .
H8 H 0.9620 0.5949 0.9949 0.075 Uiso 1 1 calc R . . . .
C9 C 0.7622(4) 0.59256(14) 0.8887(2) 0.0761(8) Uani 1 1 d . . . . .
H9 H 0.7775 0.6031 0.8544 0.091 Uiso 1 1 calc R . . . .
C10 C 0.6316(4) 0.58215(14) 0.8562(2) 0.0773(9) Uani 1 1 d . . . . .
H10 H 0.5580 0.5858 0.7998 0.093 Uiso 1 1 calc R . . . .
C11 C 0.6083(3) 0.56637(13) 0.9063(2) 0.0759(9) Uani 1 1 d . . . . .
H11 H 0.5190 0.5590 0.8838 0.091 Uiso 1 1 calc R . . . .
C12 C 0.7172(3) 0.56139(12) 0.9903(2) 0.0634(7) Uani 1 1 d . . . . .
H12 H 0.7006 0.5510 1.0240 0.076 Uiso 1 1 calc R . . . .
C13 C 1.0017(3) 0.49623(11) 1.15739(19) 0.0572(6) Uani 1 1 d . . . . .
C14 C 0.9551(4) 0.45769(12) 1.0982(2) 0.0738(9) Uani 1 1 d . . . . .
H14 H 0.9149 0.4677 1.0451 0.089 Uiso 1 1 calc R . . . .
C15 C 0.9680(5) 0.40458(15) 1.1177(3) 0.0958(12) Uani 1 1 d . . . . .
H15 H 0.9366 0.3790 1.0776 0.115 Uiso 1 1 calc R . . . .
C16 C 1.0258(5) 0.38926(17) 1.1944(4) 0.1097(16) Uani 1 1 d . . . . .
H16 H 1.0332 0.3533 1.2068 0.132 Uiso 1 1 calc R . . . .
C17 C 1.0733(5) 0.42657(19) 1.2539(3) 0.1076(14) Uani 1 1 d . . . . .
H17 H 1.1139 0.4159 1.3068 0.129 Uiso 1 1 calc R . . . .
C18 C 1.0615(4) 0.48009(15) 1.2359(2) 0.0845(10) Uani 1 1 d . . . . .
H18 H 1.0937 0.5053 1.2765 0.101 Uiso 1 1 calc R . . . .
C19 C 0.5979(2) 0.64407(10) 1.06331(15) 0.0477(5) Uani 1 1 d . . . . .
C20 C 0.4986(3) 0.65638(11) 0.98114(17) 0.0601(7) Uani 1 1 d . . . . .
H20 H 0.5083 0.6869 0.9612 0.072 Uiso 1 1 calc R . . . .
C21 C 0.3843(3) 0.62417(13) 0.92727(19) 0.0698(8) Uani 1 1 d . . . . .
H21 H 0.3186 0.6329 0.8716 0.084 Uiso 1 1 calc R . . . .
C22 C 0.3682(3) 0.57989(15) 0.9557(2) 0.0810(10) Uani 1 1 d . . . . .
H22 H 0.2921 0.5579 0.9197 0.097 Uiso 1 1 calc R . . . .
C23 C 0.4649(4) 0.56766(17) 1.0381(3) 0.0993(13) Uani 1 1 d . . . . .
H23 H 0.4526 0.5379 1.0580 0.119 Uiso 1 1 calc R . . . .
C24 C 0.5800(3) 0.59901(14) 1.0916(2) 0.0766(9) Uani 1 1 d . . . . .
H24 H 0.6459 0.5898 1.1471 0.092 Uiso 1 1 calc R . . . .
C25 C 0.7108(2) 0.72212(10) 1.18887(16) 0.0510(6) Uani 1 1 d . . . . .
C26 C 0.5773(3) 0.73808(17) 1.1482(2) 0.0912(12) Uani 1 1 d . . . . .
H26 H 0.5060 0.7276 1.0939 0.109 Uiso 1 1 calc R . . . .
C27 C 0.5489(4) 0.76936(18) 1.1872(3) 0.1006(13) Uani 1 1 d . . . . .
H27 H 0.4585 0.7796 1.1593 0.121 Uiso 1 1 calc R . . . .
C28 C 0.6516(4) 0.78536(16) 1.2660(3) 0.0917(12) Uani 1 1 d . . . . .
H28 H 0.6316 0.8054 1.2929 0.110 Uiso 1 1 calc R . . . .
C29 C 0.7833(4) 0.7721(2) 1.3053(2) 0.1072(15) Uani 1 1 d . . . . .
H29 H 0.8546 0.7852 1.3579 0.129 Uiso 1 1 calc R . . . .
C30 C 0.8132(3) 0.73908(16) 1.26794(19) 0.0820(10) Uani 1 1 d . . . . .
H30 H 0.9037 0.7284 1.2970 0.098 Uiso 1 1 calc R . . . .
C31 C 0.7607(2) 0.73087(10) 1.07860(16) 0.0493(5) Uani 1 1 d . . . . .
C32 C 0.7433(3) 0.78500(12) 1.0795(2) 0.0700(8) Uani 1 1 d . . . . .
H32 H 0.7203 0.7984 1.1089 0.084 Uiso 1 1 calc R . . . .
C33 C 0.7598(4) 0.81943(14) 1.0371(3) 0.0880(11) Uani 1 1 d . . . . .
H33 H 0.7483 0.8558 1.0384 0.106 Uiso 1 1 calc R . . . .
C34 C 0.7927(4) 0.80070(16) 0.9933(2) 0.0878(11) Uani 1 1 d . . . . .
H34 H 0.8037 0.8241 0.9649 0.105 Uiso 1 1 calc R . . . .
C35 C 0.8096(4) 0.74714(17) 0.9915(3) 0.0890(11) Uani 1 1 d . . . . .
H35 H 0.8315 0.7341 0.9614 0.107 Uiso 1 1 calc R . . . .
C36 C 0.7943(4) 0.71247(12) 1.0340(2) 0.0708(8) Uani 1 1 d . . . . .
H36 H 0.8067 0.6762 1.0327 0.085 Uiso 1 1 calc R . . . .
C37 C 1.3450(3) 0.62435(11) 1.41481(17) 0.0579(6) Uani 1 1 d . . . . .
C38 C 1.3814(4) 0.59325(14) 1.3795(2) 0.0801(9) Uani 1 1 d . . . . .
H38 H 1.3278 0.5939 1.3227 0.096 Uiso 1 1 calc R . . . .
C39 C 1.4975(4) 0.56108(16) 1.4283(3) 0.0973(12) Uani 1 1 d . . . . .
H39 H 1.5228 0.5410 1.4042 0.117 Uiso 1 1 calc R . . . .
C40 C 1.5743(4) 0.55878(17) 1.5109(3) 0.1024(14) Uani 1 1 d . . . . .
H40 H 1.6512 0.5367 1.5431 0.123 Uiso 1 1 calc R . . . .
C41 C 1.5397(4) 0.58837(19) 1.5465(3) 0.1037(13) Uani 1 1 d . . . . .
H41 H 1.5925 0.5862 1.6031 0.124 Uiso 1 1 calc R . . . .
C42 C 1.4256(4) 0.62224(15) 1.4994(2) 0.0807(9) Uani 1 1 d . . . . .
H42 H 1.4039 0.6432 1.5247 0.097 Uiso 1 1 calc R . . . .
C43 C 1.1798(2) 0.69923(10) 1.41724(15) 0.0519(6) Uani 1 1 d . . . . .
C44 C 1.1260(3) 0.66991(13) 1.4440(2) 0.0718(8) Uani 1 1 d . . . . .
H44 H 1.0976 0.6351 1.4260 0.086 Uiso 1 1 calc R . . . .
C45 C 1.1140(4) 0.69164(17) 1.4971(2) 0.0887(10) Uani 1 1 d . . . . .
H45 H 1.0812 0.6711 1.5165 0.106 Uiso 1 1 calc R . . . .
C46 C 1.1503(4) 0.74362(16) 1.5212(2) 0.0846(10) Uani 1 1 d . . . . .
H46 H 1.1388 0.7588 1.5553 0.102 Uiso 1 1 calc R . . . .
C47 C 1.2036(3) 0.77319(13) 1.4950(2) 0.0757(9) Uani 1 1 d . . . . .
H47 H 1.2297 0.8083 1.5123 0.091 Uiso 1 1 calc R . . . .
C48 C 1.2189(3) 0.75133(11) 1.44304(18) 0.0617(7) Uani 1 1 d . . . . .
H48 H 1.2553 0.7716 1.4256 0.074 Uiso 1 1 calc R . . . .
C49 C 1.2416(3) 0.71901(11) 1.31366(16) 0.0535(6) Uani 1 1 d . . . . .
C50 C 1.1395(3) 0.75315(13) 1.25187(19) 0.0723(8) Uani 1 1 d . . . . .
H50 H 1.0497 0.7492 1.2304 0.087 Uiso 1 1 calc R . . . .
C51 C 1.1689(4) 0.79284(15) 1.2218(2) 0.0903(11) Uani 1 1 d . . . . .
H51 H 1.0997 0.8159 1.1813 0.108 Uiso 1 1 calc R . . . .
C52 C 1.2999(5) 0.79831(16) 1.2515(3) 0.0935(12) Uani 1 1 d . . . . .
H52 H 1.3194 0.8246 1.2305 0.112 Uiso 1 1 calc R . . . .
C53 C 1.4023(4) 0.76502(16) 1.3122(2) 0.0852(10) Uani 1 1 d . . . . .
H53 H 1.4915 0.7691 1.3326 0.102 Uiso 1 1 calc R . . . .
C54 C 1.3742(3) 0.72545(13) 1.34334(19) 0.0655(7) Uani 1 1 d . . . . .
H54 H 1.4445 0.7030 1.3844 0.079 Uiso 1 1 calc R . . . .
B1 B 0.8772(5) 0.45992(17) 1.4406(3) 0.0611(11) Uani 0.75 1 d . U P A 1
H1 H 0.8471 0.4300 1.4629 0.073 Uiso 0.75 1 calc R . P A 1
B2 B 0.9739(4) 0.5110(2) 1.4547(3) 0.0484(9) Uiso 0.75 1 d . U P A 1
B3 B 0.9573(5) 0.4482(2) 1.4007(3) 0.0643(11) Uiso 0.75 1 d . U P A 1
H3A H 1.0216 0.4125 1.4204 0.077 Uiso 0.75 1 calc R . P A 1
B4 B 0.7805(4) 0.45726(17) 1.3382(2) 0.0756(10) Uani 1 1 d D . . . .
H4A H 0.7031 0.4253 1.3086 0.091 Uiso 1 1 calc R . . A 1
B5 B 0.7823(3) 0.51815(14) 1.3828(2) 0.0618(8) Uani 1 1 d . . . . .
H5A H 0.7119 0.5356 1.3889 0.074 Uiso 0.75 1 calc R . P A 1
H5B H 0.7023 0.5192 1.3868 0.074 Uiso 0.25 1 calc R . P A 2
B6 B 1.0079(5) 0.5086(2) 1.3859(3) 0.0603(10) Uiso 0.75 1 d . U P A 1
H6A H 1.1141 0.5117 1.4106 0.072 Uiso 0.75 1 calc R . P A 1
B7 B 0.8537(5) 0.4726(2) 1.2951(2) 0.0856(12) Uani 1 1 d D . . . .
H7A H 0.8340 0.4487 1.2457 0.103 Uiso 0.75 1 calc R . P A 1
H7B H 0.8560 0.4447 1.2570 0.103 Uiso 0.25 1 calc R . P A 2
B8 B 0.7378(3) 0.51979(17) 1.2857(2) 0.0704(9) Uani 1 1 d . . . . .
H8A H 0.6325 0.5308 1.2299 0.085 Uiso 1 1 calc R . . . .
B9 B 0.8745(4) 0.56099(16) 1.3692(2) 0.0719(9) Uiso 1 1 d . . . . .
H9A H 0.8761 0.6040 1.3790 0.086 Uiso 0.75 1 calc R . P A 1
H9B H 0.8654 0.6046 1.3651 0.086 Uiso 0.25 1 calc R . P A 2
B10 B 0.8819(4) 0.53751(19) 1.3000(3) 0.0795(11) Uani 1 1 d D U . . .
H10B H 0.8763 0.5598 1.2544 0.095 Uiso 0.25 1 calc R . P A 2
H10A H 0.8939 0.5614 1.2627 0.095 Uiso 0.75 1 calc R . P A 1
B2A B 0.9440(16) 0.5567(6) 1.4588(10) 0.070 Uiso 0.25 1 d . U P A 2
H2A H 0.9571 0.5930 1.4917 0.084 Uiso 0.25 1 calc R . P A 2
B6A B 1.0193(18) 0.5390(7) 1.4124(10) 0.076(4) Uiso 0.25 1 d . U P A 2
H6AA H 1.1197 0.5541 1.4365 0.091 Uiso 0.25 1 calc R . P A 2
B3A B 0.9718(11) 0.4780(5) 1.3800(7) 0.061(3) Uiso 0.25 1 d D U P A 2
H3AA H 1.0588 0.4511 1.4055 0.073 Uiso 0.25 1 calc R . P A 2
B1A B 0.9620(17) 0.4906(7) 1.4494(10) 0.064(4) Uiso 0.25 1 d . U P A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P2 Ag1 P1 114.89(2) . .
P3 Ag1 P1 115.56(2) . .
P3 Ag1 P2 119.25(2) . .
C1 P1 Ag1 110.73(8) . .
C1 P1 C7 103.77(13) . .
C7 P1 Ag1 116.15(8) . .
C13 P1 Ag1 116.17(9) . .
C13 P1 C1 104.69(12) . .
C13 P1 C7 104.00(13) . .
C19 P2 Ag1 113.24(8) . .
C19 P2 C25 103.09(11) . .
C19 P2 C31 105.51(12) . .
C25 P2 Ag1 121.18(9) . .
C25 P2 C31 104.07(12) . .
C31 P2 Ag1 108.41(8) . .
C37 P3 Ag1 119.77(9) . .
C37 P3 C43 104.11(13) . .
C43 P3 Ag1 114.47(8) . .
C49 P3 Ag1 107.57(8) . .
C49 P3 C37 104.88(13) . .
C49 P3 C43 104.72(12) . .
C2 C1 P1 122.7(2) . .
C2 C1 C6 118.3(3) . .
C6 C1 P1 118.9(2) . .
C1 C2 H2 119.8 . .
C1 C2 C3 120.3(3) . .
C3 C2 H2 119.8 . .
C2 C3 H3 119.8 . .
C4 C3 C2 120.5(3) . .
C4 C3 H3 119.8 . .
C3 C4 H4 120.1 . .
C5 C4 C3 119.9(3) . .
C5 C4 H4 120.1 . .
C4 C5 H5 120.1 . .
C4 C5 C6 119.9(3) . .
C6 C5 H5 120.1 . .
C1 C6 H6 119.5 . .
C5 C6 C1 121.1(3) . .
C5 C6 H6 119.5 . .
C8 C7 P1 123.2(2) . .
C8 C7 C12 118.5(3) . .
C12 C7 P1 118.2(2) . .
C7 C8 H8 119.9 . .
C7 C8 C9 120.3(3) . .
C9 C8 H8 119.9 . .
C8 C9 H9 119.8 . .
C10 C9 C8 120.4(3) . .
C10 C9 H9 119.8 . .
C9 C10 H10 119.9 . .
C9 C10 C11 120.2(3) . .
C11 C10 H10 119.9 . .
C10 C11 H11 119.9 . .
C10 C11 C12 120.2(3) . .
C12 C11 H11 119.9 . .
C7 C12 H12 119.8 . .
C11 C12 C7 120.5(3) . .
C11 C12 H12 119.8 . .
C14 C13 P1 122.8(2) . .
C18 C13 P1 118.6(2) . .
C18 C13 C14 118.6(3) . .
C13 C14 H14 119.9 . .
C15 C14 C13 120.2(4) . .
C15 C14 H14 119.9 . .
C14 C15 H15 119.7 . .
C16 C15 C14 120.7(4) . .
C16 C15 H15 119.7 . .
C15 C16 H16 120.0 . .
C15 C16 C17 120.1(4) . .
C17 C16 H16 120.0 . .
C16 C17 H17 119.8 . .
C16 C17 C18 120.4(4) . .
C18 C17 H17 119.8 . .
C13 C18 H18 120.0 . .
C17 C18 C13 120.0(4) . .
C17 C18 H18 120.0 . .
C20 C19 P2 124.7(2) . .
C20 C19 C24 118.3(3) . .
C24 C19 P2 117.0(2) . .
C19 C20 H20 119.4 . .
C19 C20 C21 121.2(3) . .
C21 C20 H20 119.4 . .
C20 C21 H21 120.0 . .
C22 C21 C20 119.9(3) . .
C22 C21 H21 120.0 . .
C21 C22 H22 120.2 . .
C21 C22 C23 119.6(3) . .
C23 C22 H22 120.2 . .
C22 C23 H23 119.7 . .
C22 C23 C24 120.7(3) . .
C24 C23 H23 119.7 . .
C19 C24 H24 119.9 . .
C23 C24 C19 120.3(3) . .
C23 C24 H24 119.9 . .
C26 C25 P2 122.1(2) . .
C30 C25 P2 119.8(2) . .
C30 C25 C26 118.1(3) . .
C25 C26 H26 119.7 . .
C27 C26 C25 120.7(3) . .
C27 C26 H26 119.7 . .
C26 C27 H27 119.8 . .
C28 C27 C26 120.4(3) . .
C28 C27 H27 119.8 . .
C27 C28 H28 120.2 . .
C29 C28 C27 119.6(3) . .
C29 C28 H28 120.2 . .
C28 C29 H29 119.7 . .
C28 C29 C30 120.6(3) . .
C30 C29 H29 119.7 . .
C25 C30 C29 120.5(3) . .
C25 C30 H30 119.7 . .
C29 C30 H30 119.7 . .
C32 C31 P2 124.1(2) . .
C36 C31 P2 117.7(2) . .
C36 C31 C32 118.1(3) . .
C31 C32 H32 119.7 . .
C33 C32 C31 120.6(3) . .
C33 C32 H32 119.7 . .
C32 C33 H33 119.7 . .
C34 C33 C32 120.6(3) . .
C34 C33 H33 119.7 . .
C33 C34 H34 120.3 . .
C33 C34 C35 119.4(3) . .
C35 C34 H34 120.3 . .
C34 C35 H35 119.8 . .
C34 C35 C36 120.4(3) . .
C36 C35 H35 119.8 . .
C31 C36 H36 119.6 . .
C35 C36 C31 120.8(3) . .
C35 C36 H36 119.6 . .
C38 C37 P3 118.2(2) . .
C38 C37 C42 118.7(3) . .
C42 C37 P3 123.1(3) . .
C37 C38 H38 119.8 . .
C37 C38 C39 120.4(4) . .
C39 C38 H38 119.8 . .
C38 C39 H39 119.8 . .
C40 C39 C38 120.3(4) . .
C40 C39 H39 119.8 . .
C39 C40 H40 119.9 . .
C41 C40 C39 120.3(4) . .
C41 C40 H40 119.9 . .
C40 C41 H41 119.6 . .
C40 C41 C42 120.8(4) . .
C42 C41 H41 119.6 . .
C37 C42 C41 119.5(4) . .
C37 C42 H42 120.3 . .
C41 C42 H42 120.3 . .
C44 C43 P3 117.2(2) . .
C48 C43 P3 123.6(2) . .
C48 C43 C44 119.2(3) . .
C43 C44 H44 119.6 . .
C45 C44 C43 120.8(3) . .
C45 C44 H44 119.6 . .
C44 C45 H45 120.1 . .
C46 C45 C44 119.8(3) . .
C46 C45 H45 120.1 . .
C45 C46 H46 120.0 . .
C45 C46 C47 120.0(3) . .
C47 C46 H46 120.0 . .
C46 C47 H47 119.7 . .
C46 C47 C48 120.6(3) . .
C48 C47 H47 119.7 . .
C43 C48 C47 119.6(3) . .
C43 C48 H48 120.2 . .
C47 C48 H48 120.2 . .
C50 C49 P3 118.1(2) . .
C54 C49 P3 123.9(2) . .
C54 C49 C50 117.9(3) . .
C49 C50 H50 119.4 . .
C51 C50 C49 121.2(3) . .
C51 C50 H50 119.4 . .
C50 C51 H51 120.0 . .
C52 C51 C50 119.9(4) . .
C52 C51 H51 120.0 . .
C51 C52 H52 120.0 . .
C51 C52 C53 120.0(3) . .
C53 C52 H52 120.0 . .
C52 C53 H53 119.7 . .
C52 C53 C54 120.5(3) . .
C54 C53 H53 119.7 . .
C49 C54 H54 119.8 . .
C53 C54 C49 120.4(3) . .
C53 C54 H54 119.8 . .
B2 B1 H1 96.5 3_768 .
B2 B1 H1 152.6 . .
B2 B1 B2 56.2(3) . 3_768
B2 B1 B3 66.6(3) . .
B2 B1 B4 94.7(3) . .
B2 B1 B5 65.3(2) . .
B3 B1 H1 126.9 . .
B3 B1 B2 101.0(3) . 3_768
B3 B1 B5 98.5(3) . .
B4 B1 H1 112.7 . .
B4 B1 B2 150.8(3) . 3_768
B4 B1 B3 60.5(3) . .
B4 B1 B5 62.8(2) . .
B5 B1 H1 126.2 . .
B5 B1 B2 101.7(3) . 3_768
B1 B2 B1 123.8(3) . 3_768
B1 B2 B2 68.5(3) . 3_768
B1 B2 B3 59.0(3) . .
B1 B2 B5 60.1(2) . .
B1 B2 B6 112.7(4) . .
B1 B2 B9 113.3(3) . .
B2 B2 B1 55.3(3) 3_768 3_768
B2 B2 B3 103.9(4) 3_768 .
B2 B2 B5 106.5(4) 3_768 .
B2 B2 B6 144.7(4) 3_768 .
B2 B2 B9 148.4(4) 3_768 .
B3 B2 B1 132.1(3) . 3_768
B5 B2 B1 133.9(3) . 3_768
B5 B2 B3 91.3(3) . .
B5 B2 B9 56.7(2) . .
B6 B2 B1 112.8(3) . 3_768
B6 B2 B3 56.8(2) . .
B6 B2 B5 103.4(3) . .
B6 B2 B9 65.9(2) . .
B9 B2 B1 114.3(3) . 3_768
B9 B2 B3 103.1(3) . .
B1 B3 B2 54.4(2) . .
B1 B3 H3A 119.2 . .
B1 B3 B7 112.2(3) . .
B2 B3 H3A 134.1 . .
B4 B3 B1 57.2(2) . .
B4 B3 B2 85.5(3) . .
B4 B3 H3A 132.6 . .
B4 B3 B6 101.7(3) . .
B4 B3 B7 59.3(2) . .
B6 B3 B1 111.0(3) . .
B6 B3 B2 59.6(3) . .
B6 B3 H3A 119.6 . .
B6 B3 B7 62.3(3) . .
B7 B3 B2 100.6(3) . .
B7 B3 H3A 119.7 . .
B1 B4 B3 62.3(3) . .
B1 B4 H4A 113.0 . .
B1 B4 B5 61.5(2) . .
B1 B4 B7 120.2(3) . .
B1 B4 B8 116.7(3) . .
B3 B4 H4A 125.4 . .
B3 B4 B5 98.9(3) . .
B3 B4 B7 62.9(3) . .
B3 B4 B8 107.4(3) . .
B5 B4 H4A 127.9 . .
B5 B4 B3A 88.1(4) . .
B5 B4 B1A 56.4(5) . .
B7 B4 H4A 117.0 . .
B7 B4 B5 106.3(3) . .
B7 B4 B8 61.3(2) . .
B7 B4 B3A 42.6(3) . .
B7 B4 B1A 86.4(5) . .
B8 B4 H4A 119.4 . .
B8 B4 B5 59.1(2) . .
B8 B4 B3A 80.3(4) . .
B8 B4 B1A 91.0(5) . .
B3A B4 B1A 45.7(6) . .
B1 B5 B2 54.6(2) . .
B1 B5 B4 55.7(2) . .
B1 B5 H5A 118.9 . .
B2 B5 H5A 133.5 . .
B4 B5 B2 84.3(2) . .
B4 B5 H5A 133.7 . .
B4 B5 H5B 112.8 . .
B4 B5 B2A 121.5(5) . .
B4 B5 B1A 70.5(6) . .
B8 B5 B1 112.4(3) . .
B8 B5 B2 101.2(2) . .
B8 B5 B4 60.3(2) . .
B8 B5 H5A 119.7 . .
B8 B5 H5B 121.1 . .
B8 B5 B2A 108.9(5) . .
B8 B5 B1A 100.3(5) . .
B9 B5 B1 112.9(3) . .
B9 B5 B2 61.8(2) . .
B9 B5 B4 101.2(3) . .
B9 B5 H5A 119.0 . .
B9 B5 H5B 141.0 . .
B9 B5 B8 60.7(2) . .
B9 B5 B2A 48.9(5) . .
B9 B5 B1A 73.9(6) . .
B2A B5 H5B 119.0 . .
B2A B5 B1A 54.4(7) . .
B1A B5 H5B 134.6 . .
B2 B6 H6A 120.5 . .
B2 B6 B7 102.1(3) . .
B2 B6 B9 58.3(2) . .
B3 B6 B2 63.7(3) . .
B3 B6 H6A 118.1 . .
B3 B6 B7 60.5(3) . .
B3 B6 B9 102.5(3) . .
B7 B6 H6A 131.9 . .
B7 B6 B9 86.4(3) . .
B9 B6 H6A 133.7 . .
B10 B6 B2 108.6(3) . .
B10 B6 B3 112.5(4) . .
B10 B6 H6A 120.5 . .
B10 B6 B7 56.5(3) . .
B10 B6 B9 53.7(2) . .
B3 B7 B6 57.2(2) . .
B3 B7 H7A 122.7 . .
B4 B7 B3 57.8(2) . .
B4 B7 B6 97.0(3) . .
B4 B7 H7A 122.7 . .
B4 B7 H7B 123.6 . .
B4 B7 B8 60.3(2) . .
B6 B7 H7A 133.4 . .
B8 B7 B3 102.8(3) . .
B8 B7 B6 91.6(3) . .
B8 B7 H7A 127.5 . .
B8 B7 H7B 140.0 . .
B10 B7 B3 107.5(3) . .
B10 B7 B4 110.7(3) . .
B10 B7 B6 54.4(2) . .
B10 B7 H7A 119.9 . .
B10 B7 H7B 124.1 . .
B10 B7 B8 59.7(2) . .
B3A B7 B4 80.1(6) . .
B3A B7 H7B 119.6 . .
B3A B7 B8 100.3(6) . .
B3A B7 B10 79.6(6) . .
B4 B8 B7 58.4(2) . .
B4 B8 H8A 123.5 . .
B5 B8 B4 60.5(2) . .
B5 B8 B7 105.1(2) . .
B5 B8 H8A 119.7 . .
B5 B8 B9 59.6(2) . .
B7 B8 H8A 128.2 . .
B9 B8 B4 100.5(2) . .
B9 B8 B7 94.3(2) . .
B9 B8 H8A 129.4 . .
B10 B8 B4 105.6(3) . .
B10 B8 B5 109.4(3) . .
B10 B8 B7 55.6(2) . .
B10 B8 H8A 122.3 . .
B10 B8 B9 56.5(2) . .
B2 B9 B6 55.8(2) . .
B2 B9 H9A 123.7 . .
B5 B9 B2 61.5(2) . .
B5 B9 B6 99.7(3) . .
B5 B9 B8 59.7(2) . .
B5 B9 H9A 119.4 . .
B5 B9 H9B 124.7 . .
B6 B9 H9A 135.1 . .
B8 B9 B2 100.4(3) . .
B8 B9 B6 87.6(3) . .
B8 B9 H9A 129.9 . .
B8 B9 H9B 120.8 . .
B10 B9 B2 103.9(3) . .
B10 B9 B5 112.5(3) . .
B10 B9 B6 51.2(2) . .
B10 B9 B8 60.0(2) . .
B10 B9 H9A 121.1 . .
B10 B9 H9B 110.3 . .
B2A B9 B5 68.5(6) . .
B2A B9 B8 127.0(7) . .
B2A B9 H9B 96.6 . .
B2A B9 B10 142.2(7) . .
B2A B9 B6A 75.5(9) . .
B6A B9 B5 111.5(7) . .
B6A B9 B8 113.2(7) . .
B6A B9 H9B 115.4 . .
B6A B9 B10 69.2(7) . .
B6 B10 B7 69.1(3) . .
B6 B10 B8 103.5(3) . .
B6 B10 B9 75.1(3) . .
B6 B10 H10A 124.4 . .
B7 B10 B8 64.6(3) . .
B7 B10 B9 105.3(3) . .
B7 B10 H10B 124.3 . .
B7 B10 H10A 128.5 . .
B7 B10 B6A 94.9(6) . .
B7 B10 B3A 44.8(4) . .
B8 B10 H10B 123.5 . .
B8 B10 H10A 132.1 . .
B8 B10 B6A 102.8(6) . .
B8 B10 B3A 84.2(4) . .
B9 B10 B8 63.5(2) . .
B9 B10 H10B 128.3 . .
B9 B10 H10A 126.1 . .
B9 B10 B6A 51.9(6) . .
B9 B10 B3A 80.3(4) . .
B6A B10 H10B 127.8 . .
B6A B10 B3A 50.4(6) . .
B3A B10 H10B 145.5 . .
B5 B2A H2A 127.2 . .
B5 B2A B6A 94.8(9) . .
B5 B2A B1A 99.2(9) . 3_768
B9 B2A B5 62.6(6) . .
B9 B2A H2A 118.7 . .
B9 B2A B6A 53.0(7) . .
B9 B2A B1A 85.9(10) . .
B9 B2A B1A 144.0(12) . 3_768
B6A B2A H2A 129.7 . .
B6A B2A B1A 102.4(10) . 3_768
B1A B2A B5 63.2(8) . .
B1A B2A H2A 155.4 . .
B1A B2A H2A 97.1 3_768 .
B1A B2A B6A 62.8(9) . .
B1A B2A B1A 58.3(10) . 3_768
B9 B6A B10 58.9(6) . .
B9 B6A B2A 51.5(7) . .
B9 B6A H6AA 138.2 . .
B9 B6A B3A 96.7(10) . .
B9 B6A B1A 79.7(9) . .
B10 B6A B2A 109.3(10) . .
B10 B6A H6AA 115.9 . .
B10 B6A B1A 104.3(10) . .
B2A B6A H6AA 122.8 . .
B2A B6A B1A 54.5(9) . .
B3A B6A B10 69.6(8) . .
B3A B6A B2A 105.9(11) . .
B3A B6A H6AA 121.3 . .
B3A B6A B1A 55.0(9) . .
B1A B6A H6AA 135.0 . .
B4 B3A H3AA 126.7 . .
B7 B3A B4 57.4(4) . .
B7 B3A B10 55.6(5) . .
B7 B3A B6A 115.1(10) . .
B7 B3A H3AA 117.0 . .
B7 B3A B1A 122.8(10) . .
B10 B3A B4 88.4(5) . .
B10 B3A H3AA 135.7 . .
B6A B3A B4 115.3(9) . .
B6A B3A B10 60.0(7) . .
B6A B3A H3AA 113.3 . .
B1A B3A B4 69.1(8) . .
B1A B3A B10 107.6(9) . .
B1A B3A B6A 69.9(10) . .
B1A B3A H3AA 110.0 . .
B5 B1A B4 53.1(5) . .
B5 B1A B2A 129.7(10) . 3_768
B2A B1A B4 112.5(10) . .
B2A B1A B4 113.3(10) 3_768 .
B2A B1A B5 62.3(8) . .
B2A B1A B2A 121.7(10) . 3_768
B2A B1A B6A 62.7(10) . .
B2A B1A B1A 66.5(12) . 3_768
B6A B1A B4 103.0(9) . .
B6A B1A B5 94.3(9) . .
B6A B1A B2A 134.1(11) . 3_768
B3A B1A B4 65.2(7) . .
B3A B1A B5 100.4(9) . .
B3A B1A B2A 117.1(12) . 3_768
B3A B1A B2A 113.6(12) . .
B3A B1A B6A 55.1(8) . .
B3A B1A B1A 151.5(16) . 3_768
B1A B1A B4 142.8(15) 3_768 .
B1A B1A B5 103.9(13) 3_768 .
B1A B1A B2A 55.2(10) 3_768 3_768
B1A B1A B6A 107.9(16) 3_768 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 P1 2.5219(6) .
Ag1 P2 2.5140(6) .
Ag1 P3 2.5073(6) .
P1 C1 1.825(3) .
P1 C7 1.829(3) .
P1 C13 1.817(3) .
P2 C19 1.817(3) .
P2 C25 1.822(2) .
P2 C31 1.827(3) .
P3 C37 1.826(3) .
P3 C43 1.828(3) .
P3 C49 1.825(3) .
C1 C2 1.375(4) .
C1 C6 1.385(4) .
C2 H2 0.9300 .
C2 C3 1.386(5) .
C3 H3 0.9300 .
C3 C4 1.370(6) .
C4 H4 0.9300 .
C4 C5 1.362(5) .
C5 H5 0.9300 .
C5 C6 1.382(4) .
C6 H6 0.9300 .
C7 C8 1.380(4) .
C7 C12 1.391(4) .
C8 H8 0.9300 .
C8 C9 1.392(4) .
C9 H9 0.9300 .
C9 C10 1.359(5) .
C10 H10 0.9300 .
C10 C11 1.369(5) .
C11 H11 0.9300 .
C11 C12 1.382(5) .
C12 H12 0.9300 .
C13 C14 1.387(4) .
C13 C18 1.383(5) .
C14 H14 0.9300 .
C14 C15 1.378(5) .
C15 H15 0.9300 .
C15 C16 1.351(7) .
C16 H16 0.9300 .
C16 C17 1.367(7) .
C17 H17 0.9300 .
C17 C18 1.382(5) .
C18 H18 0.9300 .
C19 C20 1.372(4) .
C19 C24 1.381(4) .
C20 H20 0.9300 .
C20 C21 1.385(4) .
C21 H21 0.9300 .
C21 C22 1.356(5) .
C22 H22 0.9300 .
C22 C23 1.373(5) .
C23 H23 0.9300 .
C23 C24 1.376(5) .
C24 H24 0.9300 .
C25 C26 1.382(4) .
C25 C30 1.364(4) .
C26 H26 0.9300 .
C26 C27 1.375(4) .
C27 H27 0.9300 .
C27 C28 1.354(5) .
C28 H28 0.9300 .
C28 C29 1.350(5) .
C29 H29 0.9300 .
C29 C30 1.385(5) .
C30 H30 0.9300 .
C31 C32 1.382(4) .
C31 C36 1.381(4) .
C32 H32 0.9300 .
C32 C33 1.381(5) .
C33 H33 0.9300 .
C33 C34 1.361(5) .
C34 H34 0.9300 .
C34 C35 1.370(5) .
C35 H35 0.9300 .
C35 C36 1.379(5) .
C36 H36 0.9300 .
C37 C38 1.382(4) .
C37 C42 1.384(4) .
C38 H38 0.9300 .
C38 C39 1.387(5) .
C39 H39 0.9300 .
C39 C40 1.355(6) .
C40 H40 0.9300 .
C40 C41 1.348(6) .
C41 H41 0.9300 .
C41 C42 1.397(5) .
C42 H42 0.9300 .
C43 C44 1.383(4) .
C43 C48 1.382(4) .
C44 H44 0.9300 .
C44 C45 1.376(5) .
C45 H45 0.9300 .
C45 C46 1.370(5) .
C46 H46 0.9300 .
C46 C47 1.371(5) .
C47 H47 0.9300 .
C47 C48 1.385(4) .
C48 H48 0.9300 .
C49 C50 1.389(4) .
C49 C54 1.389(4) .
C50 H50 0.9300 .
C50 C51 1.379(5) .
C51 H51 0.9300 .
C51 C52 1.366(6) .
C52 H52 0.9300 .
C52 C53 1.370(6) .
C53 H53 0.9300 .
C53 C54 1.382(5) .
C54 H54 0.9300 .
B1 H1 1.1000 .
B1 B2 1.896(6) 3_768
B1 B2 1.676(6) .
B1 B3 1.767(7) .
B1 B4 1.676(6) .
B1 B5 1.784(5) .
B2 B1 1.896(6) 3_768
B2 B2 1.692(8) 3_768
B2 B3 1.893(7) .
B2 B5 1.869(5) .
B2 B6 1.821(6) .
B2 B9 1.873(6) .
B3 H3A 1.1000 .
B3 B4 1.737(6) .
B3 B6 1.767(7) .
B3 B7 1.829(6) .
B4 H4A 1.1000 .
B4 B5 1.804(6) .
B4 B7 1.766(6) .
B4 B8 1.800(6) .
B4 B3A 2.065(12) .
B4 B1A 2.125(18) .
B5 H5A 1.1000 .
B5 H5B 1.1000 .
B5 B8 1.779(5) .
B5 B9 1.776(5) .
B5 B2A 1.861(16) .
B5 B1A 1.877(16) .
B6 H6A 1.1000 .
B6 B7 1.862(7) .
B6 B9 2.009(6) .
B6 B10 1.620(6) .
B7 H7A 1.1000 .
B7 H7B 1.1000 .
B7 B8 1.820(6) .
B7 B10 1.662(7) .
B7 B3A 1.418(11) .
B8 H8A 1.1000 .
B8 B9 1.798(6) .
B8 B10 1.739(5) .
B9 H9A 1.1000 .
B9 H9B 1.1000 .
B9 B10 1.676(6) .
B9 B2A 1.509(16) .
B9 B6A 1.540(18) .
B10 H10B 1.1000 .
B10 H10A 1.1000 .
B10 B6A 1.830(18) .
B10 B3A 1.981(12) .
B2A H2A 1.1000 .
B2A B6A 1.87(2) .
B2A B1A 1.71(2) .
B2A B1A 1.91(2) 3_768
B6A H6AA 1.1000 .
B6A B3A 1.63(2) .
B6A B1A 1.87(2) .
B3A H3AA 1.1000 .
B3A B1A 1.63(2) .
B1A B2A 1.91(2) 3_768
B1A B1A 1.77(3) 3_768
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Ag1 P1 C1 C2 134.9(3) . .
Ag1 P1 C1 C6 -42.2(3) . .
Ag1 P1 C7 C8 117.8(2) . .
Ag1 P1 C7 C12 -59.3(2) . .
Ag1 P1 C13 C14 151.4(2) . .
Ag1 P1 C13 C18 -29.5(3) . .
Ag1 P2 C19 C20 -127.9(2) . .
Ag1 P2 C19 C24 51.4(3) . .
Ag1 P2 C25 C26 -157.9(3) . .
Ag1 P2 C25 C30 25.3(3) . .
Ag1 P2 C31 C32 -126.9(2) . .
Ag1 P2 C31 C36 48.6(2) . .
Ag1 P3 C37 C38 49.7(3) . .
Ag1 P3 C37 C42 -130.3(2) . .
Ag1 P3 C43 C44 54.2(2) . .
Ag1 P3 C43 C48 -124.7(2) . .
Ag1 P3 C49 C50 42.4(2) . .
Ag1 P3 C49 C54 -134.4(2) . .
P1 C1 C2 C3 -175.8(4) . .
P1 C1 C6 C5 177.1(3) . .
P1 C7 C8 C9 -177.3(2) . .
P1 C7 C12 C11 177.7(2) . .
P1 C13 C14 C15 179.3(3) . .
P1 C13 C18 C17 -179.3(3) . .
P2 C19 C20 C21 178.2(2) . .
P2 C19 C24 C23 -179.4(3) . .
P2 C25 C26 C27 -178.0(3) . .
P2 C25 C30 C29 175.8(3) . .
P2 C31 C32 C33 175.3(3) . .
P2 C31 C36 C35 -176.0(3) . .
P3 C37 C38 C39 179.3(3) . .
P3 C37 C42 C41 179.0(3) . .
P3 C43 C44 C45 179.7(3) . .
P3 C43 C48 C47 178.8(2) . .
P3 C49 C50 C51 -178.1(3) . .
P3 C49 C54 C53 177.2(2) . .
C1 P1 C7 C8 -4.0(3) . .
C1 P1 C7 C12 178.9(2) . .
C1 P1 C13 C14 -86.1(3) . .
C1 P1 C13 C18 92.9(3) . .
C1 C2 C3 C4 -1.6(8) . .
C2 C1 C6 C5 -0.2(5) . .
C2 C3 C4 C5 0.6(8) . .
C3 C4 C5 C6 0.6(7) . .
C4 C5 C6 C1 -0.8(5) . .
C6 C1 C2 C3 1.3(6) . .
C7 P1 C1 C2 -99.8(3) . .
C7 P1 C1 C6 83.1(2) . .
C7 P1 C13 C14 22.5(3) . .
C7 P1 C13 C18 -158.5(2) . .
C7 C8 C9 C10 0.2(5) . .
C8 C7 C12 C11 0.4(4) . .
C8 C9 C10 C11 -0.4(5) . .
C9 C10 C11 C12 0.6(5) . .
C10 C11 C12 C7 -0.6(5) . .
C12 C7 C8 C9 -0.2(4) . .
C13 P1 C1 C2 9.0(3) . .
C13 P1 C1 C6 -168.1(2) . .
C13 P1 C7 C8 -113.3(2) . .
C13 P1 C7 C12 69.6(2) . .
C13 C14 C15 C16 0.1(6) . .
C14 C13 C18 C17 -0.2(5) . .
C14 C15 C16 C17 -0.6(7) . .
C15 C16 C17 C18 0.6(7) . .
C16 C17 C18 C13 -0.2(6) . .
C18 C13 C14 C15 0.3(5) . .
C19 P2 C25 C26 -30.0(3) . .
C19 P2 C25 C30 153.2(3) . .
C19 P2 C31 C32 111.5(3) . .
C19 P2 C31 C36 -73.0(2) . .
C19 C20 C21 C22 0.8(5) . .
C20 C19 C24 C23 -0.1(5) . .
C20 C21 C22 C23 0.7(6) . .
C21 C22 C23 C24 -1.9(7) . .
C22 C23 C24 C19 1.6(7) . .
C24 C19 C20 C21 -1.1(5) . .
C25 P2 C19 C20 99.4(3) . .
C25 P2 C19 C24 -81.3(3) . .
C25 P2 C31 C32 3.3(3) . .
C25 P2 C31 C36 178.8(2) . .
C25 C26 C27 C28 0.5(7) . .
C26 C25 C30 C29 -1.1(6) . .
C26 C27 C28 C29 2.5(7) . .
C27 C28 C29 C30 -4.8(8) . .
C28 C29 C30 C25 4.1(7) . .
C30 C25 C26 C27 -1.1(6) . .
C31 P2 C19 C20 -9.4(3) . .
C31 P2 C19 C24 169.8(2) . .
C31 P2 C25 C26 80.0(3) . .
C31 P2 C25 C30 -96.8(3) . .
C31 C32 C33 C34 0.3(6) . .
C32 C31 C36 C35 -0.2(5) . .
C32 C33 C34 C35 0.0(6) . .
C33 C34 C35 C36 -0.4(6) . .
C34 C35 C36 C31 0.5(6) . .
C36 C31 C32 C33 -0.2(5) . .
C37 P3 C43 C44 -78.4(2) . .
C37 P3 C43 C48 102.7(2) . .
C37 P3 C49 C50 170.9(2) . .
C37 P3 C49 C54 -5.8(3) . .
C37 C38 C39 C40 1.7(6) . .
C38 C37 C42 C41 -0.9(5) . .
C38 C39 C40 C41 -1.0(7) . .
C39 C40 C41 C42 -0.7(7) . .
C40 C41 C42 C37 1.7(6) . .
C42 C37 C38 C39 -0.7(5) . .
C43 P3 C37 C38 179.1(2) . .
C43 P3 C37 C42 -0.8(3) . .
C43 P3 C49 C50 -79.8(2) . .
C43 P3 C49 C54 103.5(2) . .
C43 C44 C45 C46 2.7(6) . .
C44 C43 C48 C47 0.0(4) . .
C44 C45 C46 C47 -2.6(6) . .
C45 C46 C47 C48 1.2(6) . .
C46 C47 C48 C43 0.1(5) . .
C48 C43 C44 C45 -1.4(5) . .
C49 P3 C37 C38 -71.1(3) . .
C49 P3 C37 C42 109.0(3) . .
C49 P3 C43 C44 171.8(2) . .
C49 P3 C43 C48 -7.1(3) . .
C49 C50 C51 C52 1.5(6) . .
C50 C49 C54 C53 0.5(4) . .
C50 C51 C52 C53 -1.2(6) . .
C51 C52 C53 C54 0.6(6) . .
C52 C53 C54 C49 -0.2(5) . .
C54 C49 C50 C51 -1.1(5) . .
B1 B2 B3 B1 109.4(4) 3_768 .
B1 B2 B3 B4 52.2(3) . .
B1 B2 B3 B4 161.7(4) 3_768 .
B1 B2 B3 B6 158.7(3) . .
B1 B2 B3 B6 -91.9(4) 3_768 .
B1 B2 B3 B7 109.8(3) . .
B1 B2 B3 B7 -140.8(4) 3_768 .
B1 B2 B5 B1 -109.8(4) 3_768 .
B1 B2 B5 B4 -161.2(4) 3_768 .
B1 B2 B5 B4 -51.4(3) . .
B1 B2 B5 B8 140.6(4) 3_768 .
B1 B2 B5 B8 -109.6(3) . .
B1 B2 B5 B9 -157.4(3) . .
B1 B2 B5 B9 92.8(4) 3_768 .
B1 B2 B5 B2A 144.1(8) . .
B1 B2 B5 B2A 34.3(8) 3_768 .
B1 B2 B5 B1A -21.2(19) . .
B1 B2 B5 B1A -131(2) 3_768 .
B1 B2 B6 B3 -19.7(3) . .
B1 B2 B6 B3 126.4(4) 3_768 .
B1 B2 B6 B7 28.3(4) . .
B1 B2 B6 B7 174.5(3) 3_768 .
B1 B2 B6 B9 106.4(3) . .
B1 B2 B6 B9 -107.5(4) 3_768 .
B1 B2 B6 B10 86.8(4) . .
B1 B2 B6 B10 -127.1(4) 3_768 .
B1 B2 B9 B5 -127.9(3) 3_768 .
B1 B2 B9 B5 21.3(3) . .
B1 B2 B9 B6 105.3(4) 3_768 .
B1 B2 B9 B6 -105.5(4) . .
B1 B2 B9 B8 -174.8(3) 3_768 .
B1 B2 B9 B8 -25.6(4) . .
B1 B2 B9 B10 123.8(3) 3_768 .
B1 B2 B9 B10 -87.0(4) . .
B1 B2 B9 B2A -38.7(9) 3_768 .
B1 B2 B9 B2A 110.5(10) . .
B1 B2 B9 B6A -136.9(9) . .
B1 B2 B9 B6A 73.9(9) 3_768 .
B1 B3 B4 B5 51.2(2) . .
B1 B3 B4 B7 155.1(3) . .
B1 B3 B4 B8 111.5(3) . .
B1 B3 B4 B3A 119.3(9) . .
B1 B3 B4 B1A 39.3(7) . .
B1 B3 B6 B2 18.4(3) . .
B1 B3 B6 B7 -104.9(4) . .
B1 B3 B6 B9 -26.3(4) . .
B1 B3 B6 B10 -82.0(4) . .
B1 B3 B7 B4 -22.5(3) . .
B1 B3 B7 B6 102.9(4) . .
B1 B3 B7 B8 19.4(4) . .
B1 B3 B7 B10 81.3(4) . .
B1 B3 B7 B3A 108.2(11) . .
B1 B4 B5 B2 50.4(2) . .
B1 B4 B5 B8 156.8(3) . .
B1 B4 B5 B9 110.1(3) . .
B1 B4 B5 B2A 61.7(6) . .
B1 B4 B5 B1A 41.9(6) . .
B1 B4 B7 B3 25.6(4) . .
B1 B4 B7 B6 -18.1(5) . .
B1 B4 B7 B8 -105.9(4) . .
B1 B4 B7 B10 -72.6(4) . .
B1 B4 B7 B3A 2.2(7) . .
B1 B4 B8 B5 -22.8(3) . .
B1 B4 B8 B7 111.6(4) . .
B1 B4 B8 B9 22.9(4) . .
B1 B4 B8 B10 80.9(4) . .
B1 B5 B8 B4 20.6(3) . .
B1 B5 B8 B7 -18.4(3) . .
B1 B5 B8 B9 -104.5(3) . .
B1 B5 B8 B10 -76.8(4) . .
B1 B5 B9 B2 -19.9(3) . .
B1 B5 B9 B6 22.3(3) . .
B1 B5 B9 B8 103.7(3) . .
B1 B5 B9 B10 74.2(4) . .
B1 B5 B9 B2A -64.9(7) . .
B1 B5 B9 B6A -1.3(8) . .
B1 B5 B2A B9 123.4(5) . .
B1 B5 B2A B6A 79.7(7) . .
B1 B5 B2A B1A 23.6(7) . .
B1 B5 B2A B1A -23.7(8) . 3_768
B1 B5 B1A B4 59.4(6) . .
B1 B5 B1A B2A -31.7(10) . 3_768
B1 B5 B1A B2A -141.4(11) . .
B1 B5 B1A B6A 162.6(13) . .
B1 B5 B1A B3A 107.3(13) . .
B1 B5 B1A B1A -87.8(14) . 3_768
B2 B1 B2 B1 0.001(1) 3_768 3_768
B2 B1 B2 B3 122.6(4) 3_768 .
B2 B1 B2 B5 -125.3(4) 3_768 .
B2 B1 B2 B6 141.8(5) 3_768 .
B2 B1 B2 B9 -145.8(5) 3_768 .
B2 B1 B3 B2 -45.5(3) 3_768 .
B2 B1 B3 B4 -155.7(3) 3_768 .
B2 B1 B3 B4 -110.3(3) . .
B2 B1 B3 B6 -19.6(3) . .
B2 B1 B3 B6 -65.1(4) 3_768 .
B2 B1 B3 B7 -132.7(3) 3_768 .
B2 B1 B3 B7 -87.2(3) . .
B2 B1 B4 B3 55.7(7) 3_768 .
B2 B1 B4 B3 59.8(3) . .
B2 B1 B4 B5 -63.1(7) 3_768 .
B2 B1 B4 B5 -59.1(3) . .
B2 B1 B4 B7 30.0(9) 3_768 .
B2 B1 B4 B7 34.0(5) . .
B2 B1 B4 B8 -36.8(4) . .
B2 B1 B4 B8 -40.8(9) 3_768 .
B2 B1 B4 B3A 31.5(8) 3_768 .
B2 B1 B4 B3A 35.6(4) . .
B2 B1 B4 B1A 7.9(9) 3_768 .
B2 B1 B4 B1A 11.9(8) . .
B2 B1 B5 B2 43.8(3) 3_768 .
B2 B1 B5 B4 109.8(3) . .
B2 B1 B5 B4 153.6(4) 3_768 .
B2 B1 B5 B8 88.0(3) . .
B2 B1 B5 B8 131.8(3) 3_768 .
B2 B1 B5 B9 21.6(3) . .
B2 B1 B5 B9 65.4(4) 3_768 .
B2 B1 B5 B2A 22.3(5) 3_768 .
B2 B1 B5 B2A -21.5(5) . .
B2 B1 B5 B1A 9.0(8) . .
B2 B1 B5 B1A 52.8(8) 3_768 .
B2 B2 B3 B1 53.9(4) 3_768 .
B2 B2 B3 B4 106.1(4) 3_768 .
B2 B2 B3 B6 -147.4(4) 3_768 .
B2 B2 B3 B7 163.7(4) 3_768 .
B2 B2 B5 B1 -52.4(4) 3_768 .
B2 B2 B5 B4 -103.7(4) 3_768 .
B2 B2 B5 B8 -162.0(4) 3_768 .
B2 B2 B5 B9 150.3(5) 3_768 .
B2 B2 B5 B2A 91.8(9) 3_768 .
B2 B2 B5 B1A -74(2) 3_768 .
B2 B2 B6 B3 64.7(8) 3_768 .
B2 B2 B6 B7 112.7(8) 3_768 .
B2 B2 B6 B9 -169.2(9) 3_768 .
B2 B2 B6 B10 171.2(8) 3_768 .
B2 B2 B9 B5 -65.1(9) 3_768 .
B2 B2 B9 B6 168.1(10) 3_768 .
B2 B2 B9 B8 -112.1(9) 3_768 .
B2 B2 B9 B10 -173.5(8) 3_768 .
B2 B2 B9 B2A 24.1(12) 3_768 .
B2 B2 B9 B6A 136.6(13) 3_768 .
B2 B3 B4 B1 -49.9(2) . .
B2 B3 B4 B5 1.3(3) . .
B2 B3 B4 B7 105.2(3) . .
B2 B3 B4 B8 61.6(3) . .
B2 B3 B4 B3A 69.4(9) . .
B2 B3 B4 B1A -10.6(7) . .
B2 B3 B6 B7 -123.3(3) . .
B2 B3 B6 B9 -44.8(3) . .
B2 B3 B6 B10 -100.4(4) . .
B2 B3 B7 B4 -78.2(3) . .
B2 B3 B7 B6 47.2(3) . .
B2 B3 B7 B8 -36.3(3) . .
B2 B3 B7 B10 25.6(4) . .
B2 B3 B7 B3A 52.5(11) . .
B2 B5 B8 B4 76.8(3) . .
B2 B5 B8 B7 37.7(3) . .
B2 B5 B8 B9 -48.4(3) . .
B2 B5 B8 B10 -20.7(4) . .
B2 B5 B9 B6 42.2(2) . .
B2 B5 B9 B8 123.6(3) . .
B2 B5 B9 B10 94.1(3) . .
B2 B5 B9 B2A -45.0(7) . .
B2 B5 B9 B6A 18.6(7) . .
B2 B5 B2A B9 94.8(8) . .
B2 B5 B2A B6A 51.2(8) . .
B2 B5 B2A B1A -52.2(7) . 3_768
B2 B5 B2A B1A -5.0(8) . .
B2 B5 B1A B4 -148(2) . .
B2 B5 B1A B2A 121(3) . 3_768
B2 B5 B1A B2A 11.2(17) . .
B2 B5 B1A B6A -44.8(17) . .
B2 B5 B1A B3A -100(2) . .
B2 B5 B1A B1A 64.8(19) . 3_768
B2 B6 B7 B3 -50.0(3) . .
B2 B6 B7 B4 -6.0(4) . .
B2 B6 B7 B8 54.3(3) . .
B2 B6 B7 B10 104.5(3) . .
B2 B6 B7 B3A -56.2(12) . .
B2 B6 B10 B7 -92.4(4) . .
B2 B6 B10 B8 -36.7(4) . .
B2 B6 B10 B9 20.7(3) . .
B2 B6 B10 B6A 55.7(12) . .
B2 B6 B10 B3A -78.1(10) . .
B2 B9 B10 B6 -19.6(3) . .
B2 B9 B10 B7 43.3(3) . .
B2 B9 B10 B8 94.1(3) . .
B2 B9 B10 B6A -40.9(7) . .
B2 B9 B10 B3A 5.8(4) . .
B2 B9 B2A B5 -70.9(7) . .
B2 B9 B2A B6A 49.7(9) . .
B2 B9 B2A B1A -9.0(7) . .
B2 B9 B2A B1A -4.9(13) . 3_768
B2 B9 B6A B10 127.4(7) . .
B2 B9 B6A B2A -38.9(8) . .
B2 B9 B6A B3A 66.1(8) . .
B2 B9 B6A B1A 13.6(6) . .
B3 B1 B2 B1 -122.6(4) . 3_768
B3 B1 B2 B2 -122.6(4) . 3_768
B3 B1 B2 B5 112.1(3) . .
B3 B1 B2 B6 19.2(3) . .
B3 B1 B2 B9 91.6(3) . .
B3 B1 B4 B5 -118.8(3) . .
B3 B1 B4 B7 -25.7(4) . .
B3 B1 B4 B8 -96.6(3) . .
B3 B1 B4 B3A -24.2(4) . .
B3 B1 B4 B1A -47.9(8) . .
B3 B1 B5 B2 -59.3(3) . .
B3 B1 B5 B4 50.5(3) . .
B3 B1 B5 B8 28.7(3) . .
B3 B1 B5 B9 -37.7(4) . .
B3 B1 B5 B2A -80.8(5) . .
B3 B1 B5 B1A -50.3(8) . .
B3 B2 B5 B1 52.6(3) . .
B3 B2 B5 B4 1.2(3) . .
B3 B2 B5 B8 -57.0(3) . .
B3 B2 B5 B9 -104.8(3) . .
B3 B2 B5 B2A -163.3(8) . .
B3 B2 B5 B1A 31.4(19) . .
B3 B2 B6 B7 48.0(3) . .
B3 B2 B6 B9 126.1(3) . .
B3 B2 B6 B10 106.5(4) . .
B3 B2 B9 B5 82.9(3) . .
B3 B2 B9 B6 -43.9(3) . .
B3 B2 B9 B8 35.9(3) . .
B3 B2 B9 B10 -25.5(3) . .
B3 B2 B9 B2A 172.1(10) . .
B3 B2 B9 B6A -75.4(9) . .
B3 B4 B5 B1 -51.7(3) . .
B3 B4 B5 B2 -1.3(3) . .
B3 B4 B5 B8 105.1(3) . .
B3 B4 B5 B9 58.4(3) . .
B3 B4 B5 B2A 10.0(6) . .
B3 B4 B5 B1A -9.8(6) . .
B3 B4 B7 B6 -43.7(3) . .
B3 B4 B7 B8 -131.5(3) . .
B3 B4 B7 B10 -98.2(3) . .
B3 B4 B7 B3A -23.4(6) . .
B3 B4 B8 B5 -90.0(3) . .
B3 B4 B8 B7 44.4(3) . .
B3 B4 B8 B9 -44.2(3) . .
B3 B4 B8 B10 13.7(4) . .
B3 B6 B7 B4 44.0(3) . .
B3 B6 B7 B8 104.3(3) . .
B3 B6 B7 B10 154.5(4) . .
B3 B6 B7 B3A -6.2(12) . .
B3 B6 B10 B7 -23.9(3) . .
B3 B6 B10 B8 31.8(4) . .
B3 B6 B10 B9 89.2(4) . .
B3 B6 B10 B6A 124.1(13) . .
B3 B6 B10 B3A -9.7(9) . .
B3 B7 B8 B4 -40.6(3) . .
B3 B7 B8 B5 -0.4(4) . .
B3 B7 B8 B9 59.2(3) . .
B3 B7 B8 B10 103.0(3) . .
B3 B7 B10 B6 22.3(3) . .
B3 B7 B10 B8 -94.9(3) . .
B3 B7 B10 B9 -44.7(4) . .
B3 B7 B10 B6A 7.0(6) . .
B3 B7 B10 B3A 13.7(5) . .
B3 B7 B3A B4 -40.7(9) . .
B3 B7 B3A B10 -154.0(10) . .
B3 B7 B3A B6A -145.7(17) . .
B3 B7 B3A B1A -64.3(12) . .
B4 B1 B2 B1 -177.6(4) . 3_768
B4 B1 B2 B2 -177.6(4) . 3_768
B4 B1 B2 B3 -55.0(3) . .
B4 B1 B2 B5 57.1(3) . .
B4 B1 B2 B6 -35.8(4) . .
B4 B1 B2 B9 36.6(4) . .
B4 B1 B3 B2 110.3(3) . .
B4 B1 B3 B6 90.7(4) . .
B4 B1 B3 B7 23.0(3) . .
B4 B1 B5 B2 -109.8(3) . .
B4 B1 B5 B8 -21.8(3) . .
B4 B1 B5 B9 -88.2(3) . .
B4 B1 B5 B2A -131.3(5) . .
B4 B1 B5 B1A -100.8(8) . .
B4 B3 B6 B2 77.5(3) . .
B4 B3 B6 B7 -45.8(3) . .
B4 B3 B6 B9 32.8(4) . .
B4 B3 B6 B10 -22.8(4) . .
B4 B3 B7 B6 125.3(3) . .
B4 B3 B7 B8 41.9(3) . .
B4 B3 B7 B10 103.8(3) . .
B4 B3 B7 B3A 130.7(11) . .
B4 B5 B8 B7 -39.1(3) . .
B4 B5 B8 B9 -125.2(3) . .
B4 B5 B8 B10 -97.4(3) . .
B4 B5 B9 B2 -77.2(3) . .
B4 B5 B9 B6 -35.0(3) . .
B4 B5 B9 B8 46.4(2) . .
B4 B5 B9 B10 16.8(3) . .
B4 B5 B9 B2A -122.2(7) . .
B4 B5 B9 B6A -58.7(8) . .
B4 B5 B2A B9 76.7(6) . .
B4 B5 B2A B6A 33.0(9) . .
B4 B5 B2A B1A -70.4(9) . 3_768
B4 B5 B2A B1A -23.1(9) . .
B4 B5 B1A B2A 159.2(8) . .
B4 B5 B1A B2A -91.2(14) . 3_768
B4 B5 B1A B6A 103.1(8) . .
B4 B5 B1A B3A 47.9(8) . .
B4 B5 B1A B1A -147.2(15) . 3_768
B4 B7 B8 B5 40.1(2) . .
B4 B7 B8 B9 99.7(3) . .
B4 B7 B8 B10 143.5(3) . .
B4 B7 B10 B6 83.7(3) . .
B4 B7 B10 B8 -33.5(3) . .
B4 B7 B10 B9 16.7(4) . .
B4 B7 B10 B6A 68.4(6) . .
B4 B7 B10 B3A 75.1(6) . .
B4 B7 B3A B10 -113.4(3) . .
B4 B7 B3A B6A -105.1(10) . .
B4 B7 B3A B1A -23.6(12) . .
B4 B8 B9 B2 1.7(3) . .
B4 B8 B9 B5 -46.4(2) . .
B4 B8 B9 B6 56.3(3) . .
B4 B8 B9 B10 101.9(3) . .
B4 B8 B9 B2A -33.1(9) . .
B4 B8 B9 B6A 55.8(8) . .
B4 B8 B10 B6 -27.0(4) . .
B4 B8 B10 B7 31.7(3) . .
B4 B8 B10 B9 -92.5(3) . .
B4 B8 B10 B6A -57.6(6) . .
B4 B8 B10 B3A -10.4(5) . .
B4 B3A B1A B5 -40.8(6) . .
B4 B3A B1A B2A 104.6(12) . 3_768
B4 B3A B1A B2A -105.0(11) . .
B4 B3A B1A B6A -128.8(9) . .
B4 B3A B1A B1A 171(4) . 3_768
B5 B1 B2 B1 125.3(4) . 3_768
B5 B1 B2 B2 125.3(4) . 3_768
B5 B1 B2 B3 -112.1(3) . .
B5 B1 B2 B6 -92.9(3) . .
B5 B1 B2 B9 -20.5(3) . .
B5 B1 B3 B2 58.3(2) . .
B5 B1 B3 B4 -51.9(3) . .
B5 B1 B3 B6 38.7(4) . .
B5 B1 B3 B7 -28.9(4) . .
B5 B1 B4 B3 118.8(3) . .
B5 B1 B4 B7 93.1(4) . .
B5 B1 B4 B8 22.3(3) . .
B5 B1 B4 B3A 94.6(4) . .
B5 B1 B4 B1A 71.0(8) . .
B5 B2 B3 B1 -53.5(2) . .
B5 B2 B3 B4 -1.2(3) . .
B5 B2 B3 B6 105.2(3) . .
B5 B2 B3 B7 56.4(3) . .
B5 B2 B6 B3 -82.6(3) . .
B5 B2 B6 B7 -34.6(4) . .
B5 B2 B6 B9 43.5(2) . .
B5 B2 B6 B10 23.9(4) . .
B5 B2 B9 B6 -126.8(3) . .
B5 B2 B9 B8 -46.9(2) . .
B5 B2 B9 B10 -108.3(3) . .
B5 B2 B9 B2A 89.2(9) . .
B5 B2 B9 B6A -158.2(9) . .
B5 B4 B7 B3 91.7(3) . .
B5 B4 B7 B6 48.0(3) . .
B5 B4 B7 B8 -39.7(2) . .
B5 B4 B7 B10 -6.5(4) . .
B5 B4 B7 B3A 68.3(6) . .
B5 B4 B8 B7 134.4(3) . .
B5 B4 B8 B9 45.8(2) . .
B5 B4 B8 B10 103.8(3) . .
B5 B8 B9 B2 48.1(2) . .
B5 B8 B9 B6 102.7(2) . .
B5 B8 B9 B10 148.2(3) . .
B5 B8 B9 B2A 13.3(8) . .
B5 B8 B9 B6A 102.2(7) . .
B5 B8 B10 B6 36.7(4) . .
B5 B8 B10 B7 95.4(3) . .
B5 B8 B10 B9 -28.8(3) . .
B5 B8 B10 B6A 6.1(7) . .
B5 B8 B10 B3A 53.3(5) . .
B5 B9 B10 B6 -84.3(3) . .
B5 B9 B10 B7 -21.3(4) . .
B5 B9 B10 B8 29.5(3) . .
B5 B9 B10 B6A -105.5(8) . .
B5 B9 B10 B3A -58.9(4) . .
B5 B9 B2A B6A 120.6(8) . .
B5 B9 B2A B1A 61.9(7) . .
B5 B9 B2A B1A 66.0(18) . 3_768
B5 B9 B6A B10 106.9(4) . .
B5 B9 B6A B2A -59.4(7) . .
B5 B9 B6A B3A 45.6(10) . .
B5 B9 B6A B1A -6.9(9) . .
B5 B2A B6A B9 50.1(6) . .
B5 B2A B6A B10 37.6(10) . .
B5 B2A B6A B3A -35.8(11) . .
B5 B2A B6A B1A -56.5(8) . .
B5 B2A B1A B4 17.9(7) . .
B5 B2A B1A B2A -121.6(12) . 3_768
B5 B2A B1A B6A 111.4(9) . .
B5 B2A B1A B3A 89.6(11) . .
B5 B2A B1A B1A -121.6(12) . 3_768
B6 B2 B3 B1 -158.7(3) . .
B6 B2 B3 B4 -106.5(3) . .
B6 B2 B3 B7 -48.9(3) . .
B6 B2 B5 B1 108.6(4) . .
B6 B2 B5 B4 57.3(3) . .
B6 B2 B5 B8 -0.9(4) . .
B6 B2 B5 B9 -48.7(3) . .
B6 B2 B5 B2A -107.2(8) . .
B6 B2 B5 B1A 87(2) . .
B6 B2 B9 B5 126.8(3) . .
B6 B2 B9 B8 79.8(3) . .
B6 B2 B9 B10 18.5(3) . .
B6 B2 B9 B2A -144.0(10) . .
B6 B2 B9 B6A -31.5(8) . .
B6 B3 B4 B1 -107.5(3) . .
B6 B3 B4 B5 -56.3(3) . .
B6 B3 B4 B7 47.6(3) . .
B6 B3 B4 B8 4.0(4) . .
B6 B3 B4 B3A 11.8(8) . .
B6 B3 B4 B1A -68.3(7) . .
B6 B3 B7 B4 -125.3(3) . .
B6 B3 B7 B8 -83.5(3) . .
B6 B3 B7 B10 -21.6(3) . .
B6 B3 B7 B3A 5.3(11) . .
B6 B7 B8 B4 -97.2(3) . .
B6 B7 B8 B5 -57.1(3) . .
B6 B7 B8 B9 2.5(3) . .
B6 B7 B8 B10 46.3(3) . .
B6 B7 B10 B8 -117.2(3) . .
B6 B7 B10 B9 -67.1(3) . .
B6 B7 B10 B6A -15.3(6) . .
B6 B7 B10 B3A -8.6(6) . .
B6 B7 B3A B4 129.3(12) . .
B6 B7 B3A B10 15.9(11) . .
B6 B7 B3A B6A 24.2(9) . .
B6 B7 B3A B1A 105.6(18) . .
B6 B9 B10 B7 62.9(3) . .
B6 B9 B10 B8 113.7(3) . .
B6 B9 B10 B6A -21.2(7) . .
B6 B9 B10 B3A 25.4(3) . .
B6 B9 B2A B5 -100.0(3) . .
B6 B9 B2A B6A 20.6(7) . .
B6 B9 B2A B1A -34.0(18) . 3_768
B6 B9 B2A B1A -38.1(8) . .
B6 B9 B6A B10 40.7(12) . .
B6 B9 B6A B2A -125.6(16) . .
B6 B9 B6A B3A -20.6(9) . .
B6 B9 B6A B1A -73.1(14) . .
B6 B10 B6A B9 -135.3(14) . .
B6 B10 B6A B2A -124.0(17) . .
B6 B10 B6A B3A -23.6(8) . .
B6 B10 B6A B1A -67.0(11) . .
B7 B3 B4 B1 -155.1(3) . .
B7 B3 B4 B5 -103.9(3) . .
B7 B3 B4 B8 -43.6(3) . .
B7 B3 B4 B3A -35.7(9) . .
B7 B3 B4 B1A -115.8(7) . .
B7 B3 B6 B2 123.3(3) . .
B7 B3 B6 B9 78.5(3) . .
B7 B3 B6 B10 22.9(3) . .
B7 B4 B5 B1 -116.0(3) . .
B7 B4 B5 B2 -65.6(3) . .
B7 B4 B5 B8 40.8(2) . .
B7 B4 B5 B9 -5.9(3) . .
B7 B4 B5 B2A -54.3(6) . .
B7 B4 B5 B1A -74.1(6) . .
B7 B4 B8 B5 -134.4(3) . .
B7 B4 B8 B9 -88.6(3) . .
B7 B4 B8 B10 -30.6(3) . .
B7 B6 B10 B8 55.7(3) . .
B7 B6 B10 B9 113.1(3) . .
B7 B6 B10 B6A 148.1(12) . .
B7 B6 B10 B3A 14.3(10) . .
B7 B8 B9 B2 -56.9(3) . .
B7 B8 B9 B5 -105.0(3) . .
B7 B8 B9 B6 -2.3(3) . .
B7 B8 B9 B10 43.2(3) . .
B7 B8 B9 B2A -91.7(8) . .
B7 B8 B9 B6A -2.8(7) . .
B7 B8 B10 B6 -58.7(3) . .
B7 B8 B10 B9 -124.2(3) . .
B7 B8 B10 B6A -89.3(6) . .
B7 B8 B10 B3A -42.1(4) . .
B7 B10 B6A B9 -105.6(5) . .
B7 B10 B6A B2A -94.3(9) . .
B7 B10 B6A B3A 6.1(7) . .
B7 B10 B6A B1A -37.3(9) . .
B7 B3A B1A B4 21.2(10) . .
B7 B3A B1A B5 -19.6(15) . .
B7 B3A B1A B2A 125.8(12) . 3_768
B7 B3A B1A B2A -83.8(15) . .
B7 B3A B1A B6A -107.6(13) . .
B7 B3A B1A B1A -168(3) . 3_768
B8 B4 B5 B1 -156.8(3) . .
B8 B4 B5 B2 -106.4(2) . .
B8 B4 B5 B9 -46.6(2) . .
B8 B4 B5 B2A -95.1(6) . .
B8 B4 B5 B1A -114.9(6) . .
B8 B4 B7 B3 131.5(3) . .
B8 B4 B7 B6 87.8(3) . .
B8 B4 B7 B10 33.3(3) . .
B8 B4 B7 B3A 108.1(6) . .
B8 B5 B9 B2 -123.6(3) . .
B8 B5 B9 B6 -81.4(3) . .
B8 B5 B9 B10 -29.6(3) . .
B8 B5 B9 B2A -168.6(7) . .
B8 B5 B9 B6A -105.1(8) . .
B8 B5 B2A B9 10.5(6) . .
B8 B5 B2A B6A -33.2(9) . .
B8 B5 B2A B1A -136.6(7) . 3_768
B8 B5 B2A B1A -89.3(7) . .
B8 B5 B1A B4 -53.2(3) . .
B8 B5 B1A B2A -144.4(13) . 3_768
B8 B5 B1A B2A 105.9(7) . .
B8 B5 B1A B6A 49.9(9) . .
B8 B5 B1A B3A -5.4(10) . .
B8 B5 B1A B1A 159.5(13) . 3_768
B8 B7 B10 B6 117.2(3) . .
B8 B7 B10 B9 50.1(3) . .
B8 B7 B10 B6A 101.9(6) . .
B8 B7 B10 B3A 108.6(6) . .
B8 B7 B3A B4 57.1(3) . .
B8 B7 B3A B10 -56.3(3) . .
B8 B7 B3A B6A -48.0(11) . .
B8 B7 B3A B1A 33.4(13) . .
B8 B9 B10 B6 -113.7(3) . .
B8 B9 B10 B7 -50.8(3) . .
B8 B9 B10 B6A -134.9(7) . .
B8 B9 B10 B3A -88.3(4) . .
B8 B9 B2A B5 -12.3(7) . .
B8 B9 B2A B6A 108.3(9) . .
B8 B9 B2A B1A 49.6(11) . .
B8 B9 B2A B1A 54(2) . 3_768
B8 B9 B6A B10 41.8(5) . .
B8 B9 B6A B2A -124.5(7) . .
B8 B9 B6A B3A -19.4(11) . .
B8 B9 B6A B1A -72.0(8) . .
B8 B10 B6A B9 -40.5(6) . .
B8 B10 B6A B2A -29.2(10) . .
B8 B10 B6A B3A 71.2(7) . .
B8 B10 B6A B1A 27.8(10) . .
B9 B2 B3 B1 -109.5(3) . .
B9 B2 B3 B4 -57.3(3) . .
B9 B2 B3 B6 49.2(3) . .
B9 B2 B3 B7 0.3(4) . .
B9 B2 B5 B1 157.4(3) . .
B9 B2 B5 B4 106.0(3) . .
B9 B2 B5 B8 47.8(2) . .
B9 B2 B5 B2A -58.5(8) . .
B9 B2 B5 B1A 136(2) . .
B9 B2 B6 B3 -126.1(3) . .
B9 B2 B6 B7 -78.1(3) . .
B9 B2 B6 B10 -19.6(3) . .
B9 B5 B8 B4 125.2(3) . .
B9 B5 B8 B7 86.1(3) . .
B9 B5 B8 B10 27.8(3) . .
B9 B5 B2A B6A -43.6(6) . .
B9 B5 B2A B1A -147.0(11) . 3_768
B9 B5 B2A B1A -99.8(9) . .
B9 B5 B1A B4 -108.5(3) . .
B9 B5 B1A B2A 50.7(7) . .
B9 B5 B1A B2A 160.3(15) . 3_768
B9 B5 B1A B6A -5.4(7) . .
B9 B5 B1A B3A -60.6(9) . .
B9 B5 B1A B1A 104.3(14) . 3_768
B9 B6 B7 B3 -106.5(3) . .
B9 B6 B7 B4 -62.5(3) . .
B9 B6 B7 B8 -2.2(2) . .
B9 B6 B7 B10 47.9(2) . .
B9 B6 B7 B3A -112.7(13) . .
B9 B6 B10 B7 -113.1(3) . .
B9 B6 B10 B8 -57.4(3) . .
B9 B6 B10 B6A 34.9(12) . .
B9 B6 B10 B3A -98.9(10) . .
B9 B8 B10 B6 65.5(3) . .
B9 B8 B10 B7 124.2(3) . .
B9 B8 B10 B6A 34.8(6) . .
B9 B8 B10 B3A 82.0(4) . .
B9 B10 B6A B2A 11.3(7) . .
B9 B10 B6A B3A 111.7(9) . .
B9 B10 B6A B1A 68.3(9) . .
B9 B2A B6A B10 -12.4(7) . .
B9 B2A B6A B3A -85.9(11) . .
B9 B2A B6A B1A -106.6(10) . .
B9 B2A B1A B4 -43.3(10) . .
B9 B2A B1A B5 -61.3(6) . .
B9 B2A B1A B2A 177.2(12) . 3_768
B9 B2A B1A B6A 50.1(8) . .
B9 B2A B1A B3A 28.3(12) . .
B9 B2A B1A B1A 177.2(13) . 3_768
B9 B6A B3A B4 -18.7(12) . .
B9 B6A B3A B7 45.3(13) . .
B9 B6A B3A B10 53.2(6) . .
B9 B6A B3A B1A -72.4(10) . .
B9 B6A B1A B4 59.2(9) . .
B9 B6A B1A B5 6.1(8) . .
B9 B6A B1A B2A -158.6(15) . 3_768
B9 B6A B1A B2A -49.7(8) . .
B9 B6A B1A B3A 105.8(10) . .
B9 B6A B1A B1A -100.0(14) . 3_768
B10 B6 B7 B3 -154.5(4) . .
B10 B6 B7 B4 -110.4(3) . .
B10 B6 B7 B8 -50.2(3) . .
B10 B6 B7 B3A -160.6(13) . .
B10 B7 B8 B4 -143.5(3) . .
B10 B7 B8 B5 -103.4(3) . .
B10 B7 B8 B9 -43.8(2) . .
B10 B7 B3A B4 113.4(3) . .
B10 B7 B3A B6A 8.3(10) . .
B10 B7 B3A B1A 89.7(12) . .
B10 B8 B9 B2 -100.2(3) . .
B10 B8 B9 B5 -148.2(3) . .
B10 B8 B9 B6 -45.6(2) . .
B10 B8 B9 B2A -135.0(8) . .
B10 B8 B9 B6A -46.1(7) . .
B10 B9 B2A B5 -99.4(9) . .
B10 B9 B2A B6A 21.2(12) . .
B10 B9 B2A B1A -33(3) . 3_768
B10 B9 B2A B1A -37.5(14) . .
B10 B9 B6A B2A -166.3(8) . .
B10 B9 B6A B3A -61.3(8) . .
B10 B9 B6A B1A -113.8(8) . .
B10 B6A B3A B4 -72.0(7) . .
B10 B6A B3A B7 -7.9(9) . .
B10 B6A B3A B1A -125.6(9) . .
B10 B6A B1A B4 5.2(11) . .
B10 B6A B1A B5 -47.9(10) . .
B10 B6A B1A B2A 147.4(14) . 3_768
B10 B6A B1A B2A -103.7(11) . .
B10 B6A B1A B3A 51.8(9) . .
B10 B6A B1A B1A -154.0(13) . 3_768
B10 B3A B1A B4 81.2(6) . .
B10 B3A B1A B5 40.4(10) . .
B10 B3A B1A B2A -174.2(10) . 3_768
B10 B3A B1A B2A -23.8(14) . .
B10 B3A B1A B6A -47.6(8) . .
B10 B3A B1A B1A -108(4) . 3_768
B2A B5 B8 B4 116.1(6) . .
B2A B5 B8 B7 77.1(6) . .
B2A B5 B8 B9 -9.0(5) . .
B2A B5 B8 B10 18.7(6) . .
B2A B5 B9 B2 45.0(7) . .
B2A B5 B9 B6 87.2(7) . .
B2A B5 B9 B8 168.6(7) . .
B2A B5 B9 B10 139.1(7) . .
B2A B5 B9 B6A 63.6(10) . .
B2A B5 B1A B4 -159.2(8) . .
B2A B5 B1A B2A 109.7(15) . 3_768
B2A B5 B1A B6A -56.1(9) . .
B2A B5 B1A B3A -111.3(12) . .
B2A B5 B1A B1A 53.6(13) . 3_768
B2A B9 B10 B6 -0.8(11) . .
B2A B9 B10 B7 62.1(11) . .
B2A B9 B10 B8 112.9(11) . .
B2A B9 B10 B6A -22.0(12) . .
B2A B9 B10 B3A 24.6(11) . .
B2A B9 B6A B10 166.3(8) . .
B2A B9 B6A B3A 105.0(11) . .
B2A B9 B6A B1A 52.5(9) . .
B2A B6A B3A B4 33.1(12) . .
B2A B6A B3A B7 97.2(12) . .
B2A B6A B3A B10 105.1(10) . .
B2A B6A B3A B1A -20.6(10) . .
B2A B6A B1A B4 108.9(10) . .
B2A B6A B1A B5 55.8(8) . .
B2A B6A B1A B2A -108.9(17) . 3_768
B2A B6A B1A B3A 155.5(12) . .
B2A B6A B1A B1A -50.3(13) . 3_768
B6A B9 B10 B6 21.2(7) . .
B6A B9 B10 B7 84.1(7) . .
B6A B9 B10 B8 134.9(7) . .
B6A B9 B10 B3A 46.6(8) . .
B6A B9 B2A B5 -120.6(8) . .
B6A B9 B2A B1A -54.6(19) . 3_768
B6A B9 B2A B1A -58.7(10) . .
B6A B2A B1A B4 -93.5(10) . .
B6A B2A B1A B5 -111.4(9) . .
B6A B2A B1A B2A 127.0(13) . 3_768
B6A B2A B1A B3A -21.8(11) . .
B6A B2A B1A B1A 127.0(13) . 3_768
B6A B3A B1A B4 128.8(9) . .
B6A B3A B1A B5 87.9(10) . .
B6A B3A B1A B2A 23.7(12) . .
B6A B3A B1A B2A -126.6(13) . 3_768
B6A B3A B1A B1A -60(4) . 3_768
B3A B4 B5 B1 -77.0(4) . .
B3A B4 B5 B2 -26.6(4) . .
B3A B4 B5 B8 79.8(4) . .
B3A B4 B5 B9 33.1(4) . .
B3A B4 B5 B2A -15.3(7) . .
B3A B4 B5 B1A -35.1(6) . .
B3A B4 B7 B3 23.4(6) . .
B3A B4 B7 B6 -20.3(5) . .
B3A B4 B7 B8 -108.1(6) . .
B3A B4 B7 B10 -74.8(6) . .
B3A B4 B8 B5 -93.7(4) . .
B3A B4 B8 B7 40.7(4) . .
B3A B4 B8 B9 -47.9(4) . .
B3A B4 B8 B10 10.1(4) . .
B3A B7 B8 B4 -72.2(6) . .
B3A B7 B8 B5 -32.0(6) . .
B3A B7 B8 B9 27.6(6) . .
B3A B7 B8 B10 71.4(6) . .
B3A B7 B10 B6 8.6(6) . .
B3A B7 B10 B8 -108.6(6) . .
B3A B7 B10 B9 -58.5(6) . .
B3A B7 B10 B6A -6.7(8) . .
B3A B10 B6A B9 -111.7(9) . .
B3A B10 B6A B2A -100.4(12) . .
B3A B10 B6A B1A -43.4(8) . .
B3A B6A B1A B4 -46.6(8) . .
B3A B6A B1A B5 -99.7(9) . .
B3A B6A B1A B2A -155.5(12) . .
B3A B6A B1A B2A 95.6(17) . 3_768
B3A B6A B1A B1A 154.2(17) . 3_768
B1A B4 B5 B1 -41.9(6) . .
B1A B4 B5 B2 8.5(6) . .
B1A B4 B5 B8 114.9(6) . .
B1A B4 B5 B9 68.2(6) . .
B1A B4 B5 B2A 19.8(8) . .
B1A B4 B7 B3 38.4(5) . .
B1A B4 B7 B6 -5.3(5) . .
B1A B4 B7 B8 -93.1(5) . .
B1A B4 B7 B10 -59.8(5) . .
B1A B4 B7 B3A 15.0(7) . .
B1A B4 B8 B5 -49.1(5) . .
B1A B4 B8 B7 85.3(5) . .
B1A B4 B8 B9 -3.3(5) . .
B1A B4 B8 B10 54.7(5) . .
B1A B5 B8 B4 60.4(6) . .
B1A B5 B8 B7 21.3(6) . .
B1A B5 B8 B9 -64.8(6) . .
B1A B5 B8 B10 -37.1(7) . .
B1A B5 B9 B2 -11.6(6) . .
B1A B5 B9 B6 30.7(6) . .
B1A B5 B9 B8 112.1(6) . .
B1A B5 B9 B10 82.5(6) . .
B1A B5 B9 B2A -56.6(8) . .
B1A B5 B9 B6A 7.0(9) . .
B1A B5 B2A B9 99.8(9) . .
B1A B5 B2A B6A 56.2(9) . .
B1A B5 B2A B1A -47.2(11) . 3_768
B1A B2A B6A B9 150.7(12) 3_768 .
B1A B2A B6A B9 106.6(10) . .
B1A B2A B6A B10 94.2(11) . .
B1A B2A B6A B10 138.2(10) 3_768 .
B1A B2A B6A B3A 20.7(10) . .
B1A B2A B6A B3A 64.8(13) 3_768 .
B1A B2A B6A B1A 44.0(12) 3_768 .
B1A B2A B1A B4 139.5(15) 3_768 .
B1A B2A B1A B5 121.6(12) 3_768 .
B1A B2A B1A B2A 0.000(2) 3_768 3_768
B1A B2A B1A B6A -127.0(13) 3_768 .
B1A B2A B1A B3A -148.8(18) 3_768 .
B1A B6A B3A B4 53.7(9) . .
B1A B6A B3A B7 117.8(12) . .
B1A B6A B3A B10 125.6(9) . .
