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#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/1/53/03/1530370.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1530370
loop_
_publ_author_name
'Matveeva, R.G.'
'Ilyukhin, V.V.'
'Belov, N.V.'
_publ_section_title
;
 The crystal structure of compound alkaline tetragermanate
;
_journal_name_full               'Doklady Akademii Nauk SSSR'
_journal_page_first              584
_journal_page_last               587
_journal_volume                  213
_journal_year                    1973
_chemical_formula_sum            'Ge4 Li Na O9'
_chemical_name_systematic        'Li Na (Ge4 O9)'
_space_group_IT_number           29
_symmetry_space_group_name_Hall  'P 2c -2ac'
_symmetry_space_group_name_H-M   'P c a 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   15.9
_cell_length_b                   4.683
_cell_length_c                   9.322
_cell_volume                     694.113
_citation_journal_id_ASTM        DANKAS
_cod_data_source_file            Matveeva_DANKAS_1973_759.cif
_cod_data_source_block           Ge4Li1Na1O9
_cod_original_cell_volume        694.1133
_cod_original_formula_sum        'Ge4 Li1 Na1 O9'
_cod_database_code               1530370
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,z+1/2
-x+1/2,y,z+1/2
x+1/2,-y,z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
Ge2 Ge+4 0.4048 0.0099 0.0881 1 0.0
Ge4 Ge+4 0.3449 0.4996 0.2915 1 0.0
O4 O-2 0.3361 0.2531 0.4548 1 0.0
O2 O-2 0.1417 0.1592 0.4269 1 0.0
O1 O-2 0.2587 0.7185 0.3872 1 0.0
O7 O-2 0.4291 0.2733 0.2 1 0.0
Ge1 Ge+4 0.0981 -0.0086 0.0057 1 0.0
O8 O-2 0.2611 0.2655 0.2131 1 0.0
Li1 Li+1 0.2661 0.4564 0.042 1 0.0
Ge3 Ge+4 0.2064 0.0019 0.2991 1 0.0
O6 O-2 0.4275 0.7189 0.3814 1 0.0
O5 O-2 0.1355 0.8518 0.1667 1 0.0
O3 O-2 0.0064 0.1665 0.0456 1 0.0
O9 O-2 0.3363 0.7148 0.1305 1 0.0
Na1 Na+1 0.0453 0.523 0.3168 1 0.0
