#------------------------------------------------------------------------------
#$Date: 2016-02-13 14:50:18 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176428 $
#$URL: svn://www.crystallography.net/cod/cif/1/53/03/1530397.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1530397
loop_
_publ_author_name
'Pan, F.'
'Gao, S.'
'Liu, H. Z.'
_publ_section_title
;
 A heterometallic nanosized tube {Fe[(CN)6]2[Co(LN3O2)]3}nand two of its
 lamellar polymorphous isomers
;
_journal_issue                   39
_journal_name_full               CrystEngComm
_journal_page_first              7490
_journal_paper_doi               10.1039/C5CE01185J
_journal_volume                  17
_journal_year                    2015
_chemical_formula_moiety         'C57 H63 Co3 Fe2 N21 O6, 2(C H4 O), 14(H2 O)'
_chemical_formula_sum            'C59 H99 Co3 Fe2 N21 O22'
_chemical_formula_weight         1743.08
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_block_doi                 10.5517/cc14fwn3
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-08-17 deposited with the CCDC.
2015-09-08 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 108.29(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   26.362(5)
_cell_length_b                   16.670(3)
_cell_length_c                   19.521(4)
_cell_measurement_reflns_used    91674
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      3.395
_cell_volume                     8145(3)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor, 1997)'
_computing_data_collection       'KappaCCD (Nonius B. V., 1998)'
_computing_data_reduction
'HKL Denzo (Otwinowski & Minor, 1997) & maXus (Mackay et al., 1998)'
_computing_molecular_graphics    'Bruker SHELXTL V5.1 (Sheldrick, 1998)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 0.76
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'NONIUS KaooaCCD'
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1437
_diffrn_reflns_av_sigmaI/netI    0.1536
_diffrn_reflns_limit_h_max       31
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            42786
_diffrn_reflns_theta_full        25.68
_diffrn_reflns_theta_max         25.68
_diffrn_reflns_theta_min         3.64
_exptl_absorpt_coefficient_mu    1.025
_exptl_absorpt_correction_T_max  0.8212
_exptl_absorpt_correction_T_min  0.6727
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            'dark brown'
_exptl_crystal_density_diffrn    1.421
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       brick
_exptl_crystal_F_000             3636
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.786
_refine_diff_density_min         -0.606
_refine_diff_density_rms         0.103
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.203
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     494
_refine_ls_number_reflns         7612
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.203
_refine_ls_R_factor_all          0.1507
_refine_ls_R_factor_gt           0.0638
_refine_ls_shift/su_max          0.027
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0627P)²+0.2500P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1595
_refine_ls_wR_factor_ref         0.1747
_reflns_number_gt                3835
_reflns_number_total             7612
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5ce01185j2.cif
_cod_data_source_block           last
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 1530397--1530399.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               1530397
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Fe1 Fe 0.14543(3) 0.51882(5) 0.14795(4) 0.0257(3) Uani 1 1 d .
Co1 Co 0.0000 0.58289(6) 0.2500 0.0266(3) Uani 1 2 d S
Co2 Co 0.24888(3) 0.78223(5) 0.21873(5) 0.0315(3) Uani 1 1 d .
C1 C 0.1066(3) 0.5514(3) 0.2143(3) 0.0261(15) Uani 1 1 d .
C2 C 0.1937(2) 0.6103(4) 0.1758(3) 0.0267(15) Uani 1 1 d .
C3 C 0.1954(3) 0.4440(4) 0.2127(3) 0.0269(15) Uani 1 1 d .
C4 C 0.1765(3) 0.4884(4) 0.0747(3) 0.0318(16) Uani 1 1 d .
C5 C 0.0977(3) 0.4280(4) 0.1247(3) 0.0309(16) Uani 1 1 d .
C6 C 0.0962(2) 0.5896(4) 0.0818(3) 0.0304(16) Uani 1 1 d .
C7 C 0.0000 0.8736(6) 0.2500 0.059(3) Uani 1 2 d S
H7 H 0.0000 0.9294 0.2500 0.070 Uiso 1 2 calc SR
C8 C 0.0199(3) 0.8319(4) 0.3149(4) 0.052(2) Uani 1 1 d .
H8 H 0.0332 0.8590 0.3585 0.063 Uiso 1 1 calc R
C9 C 0.0191(2) 0.7487(4) 0.3124(4) 0.0330(16) Uani 1 1 d .
C10 C 0.0379(3) 0.6966(4) 0.3760(4) 0.0380(18) Uani 1 1 d .
C11 C 0.0603(3) 0.7322(4) 0.4496(4) 0.066(2) Uani 1 1 d .
H11A H 0.0709 0.6901 0.4847 0.099 Uiso 1 1 calc R
H11B H 0.0336 0.7648 0.4599 0.099 Uiso 1 1 calc R
H11C H 0.0908 0.7647 0.4514 0.099 Uiso 1 1 calc R
C12 C 0.0478(3) 0.5618(4) 0.4192(3) 0.0458(19) Uani 1 1 d .
H12A H 0.0184 0.5522 0.4381 0.055 Uiso 1 1 calc R
H12B H 0.0786 0.5794 0.4584 0.055 Uiso 1 1 calc R
C13 C 0.0612(3) 0.4846(4) 0.3848(3) 0.0441(18) Uani 1 1 d .
H13A H 0.0947 0.4906 0.3746 0.053 Uiso 1 1 calc R
H13B H 0.0641 0.4393 0.4170 0.053 Uiso 1 1 calc R
C14 C 0.0235(3) 0.4013(4) 0.2836(3) 0.0427(18) Uani 1 1 d .
H14A H 0.0228 0.3547 0.3130 0.051 Uiso 1 1 calc R
H14B H 0.0567 0.4011 0.2719 0.051 Uiso 1 1 calc R
C15 C 0.1820(4) 0.8924(5) 0.0010(4) 0.104(4) Uani 1 1 d .
H15A H 0.1463 0.9039 0.0011 0.156 Uiso 1 1 calc R
H15B H 0.1805 0.8609 -0.0408 0.156 Uiso 1 1 calc R
H15C H 0.2005 0.9417 -0.0002 0.156 Uiso 1 1 calc R
C16 C 0.2109(4) 0.8467(4) 0.0675(4) 0.059(2) Uani 1 1 d .
C17 C 0.2684(4) 0.8230(4) 0.0787(4) 0.050(2) Uani 1 1 d .
C18 C 0.2967(5) 0.8335(5) 0.0298(5) 0.073(3) Uani 1 1 d .
H18 H 0.2806 0.8573 -0.0148 0.088 Uiso 1 1 calc R
C19 C 0.3473(5) 0.8087(6) 0.0488(6) 0.086(4) Uani 1 1 d .
H19 H 0.3666 0.8159 0.0166 0.104 Uiso 1 1 calc R
C20 C 0.3722(3) 0.7726(5) 0.1147(5) 0.066(3) Uani 1 1 d .
H20 H 0.4071 0.7538 0.1265 0.079 Uiso 1 1 calc R
C21 C 0.3426(3) 0.7655(4) 0.1633(4) 0.0424(19) Uani 1 1 d .
C22 C 0.3623(3) 0.7337(4) 0.2374(4) 0.0425(19) Uani 1 1 d .
C23 C 0.4186(3) 0.7029(4) 0.2647(4) 0.070(3) Uani 1 1 d .
H23A H 0.4259 0.6841 0.3134 0.105 Uiso 1 1 calc R
H23B H 0.4429 0.7453 0.2636 0.105 Uiso 1 1 calc R
H23C H 0.4229 0.6595 0.2347 0.105 Uiso 1 1 calc R
C24 C 0.3425(3) 0.7092(4) 0.3463(4) 0.0465(19) Uani 1 1 d .
H24A H 0.3798 0.7199 0.3717 0.056 Uiso 1 1 calc R
H24B H 0.3364 0.6520 0.3479 0.056 Uiso 1 1 calc R
C25 C 0.3081(3) 0.7535(4) 0.3808(4) 0.056(2) Uani 1 1 d .
H25A H 0.3105 0.7297 0.4270 0.067 Uiso 1 1 calc R
H25B H 0.3193 0.8091 0.3886 0.067 Uiso 1 1 calc R
C26 C 0.2167(4) 0.7860(5) 0.3606(4) 0.066(2) Uani 1 1 d .
H26A H 0.2254 0.8422 0.3708 0.079 Uiso 1 1 calc R
H26B H 0.2159 0.7598 0.4046 0.079 Uiso 1 1 calc R
C27 C 0.1640(4) 0.7770(5) 0.3021(5) 0.077(3) Uani 1 1 d .
H27A H 0.1551 0.7207 0.2926 0.092 Uiso 1 1 calc R
H27B H 0.1357 0.8027 0.3161 0.092 Uiso 1 1 calc R
C28 C 0.1268(3) 0.8049(5) 0.1757(5) 0.072(3) Uani 1 1 d .
H28A H 0.0943 0.8250 0.1829 0.087 Uiso 1 1 calc R
H28B H 0.1219 0.7484 0.1634 0.087 Uiso 1 1 calc R
C29 C 0.1385(3) 0.8499(5) 0.1172(5) 0.077(3) Uani 1 1 d .
H29A H 0.1356 0.9070 0.1244 0.093 Uiso 1 1 calc R
H29B H 0.1131 0.8354 0.0710 0.093 Uiso 1 1 calc R
C30 C 0.2321(3) 0.4452(5) 0.8767(4) 0.069(2) Uani 1 1 d .
N1 N 0.0775(2) 0.5718(3) 0.2431(3) 0.0302(13) Uani 1 1 d .
N2 N 0.2189(2) 0.6666(3) 0.1911(3) 0.0338(14) Uani 1 1 d .
N3 N 0.2240(2) 0.3971(3) 0.2440(3) 0.0348(14) Uani 1 1 d .
N4 N 0.1950(2) 0.4698(3) 0.0315(3) 0.0504(16) Uani 1 1 d .
N5 N 0.0722(2) 0.3707(3) 0.1151(3) 0.0449(15) Uani 1 1 d .
N6 N 0.0689(2) 0.6375(3) 0.0452(3) 0.0442(15) Uani 1 1 d .
N7 N 0.0000 0.7090(4) 0.2500 0.0292(18) Uani 1 2 d S
N8 N 0.03297(19) 0.6227(3) 0.3623(3) 0.0330(13) Uani 1 1 d .
N9 N 0.2914(2) 0.7897(3) 0.1438(3) 0.0364(14) Uani 1 1 d .
N10 N 0.1934(2) 0.8296(3) 0.1184(3) 0.0514(17) Uani 1 1 d .
N11 N 0.3291(2) 0.7358(3) 0.2717(3) 0.0339(13) Uani 1 1 d .
O1 O 0.01826(16) 0.4732(2) 0.3200(2) 0.0320(10) Uani 1 1 d .
O2 O 0.17041(19) 0.8154(3) 0.2389(3) 0.0520(13) Uani 1 1 d .
O3 O 0.25422(19) 0.7489(2) 0.3331(2) 0.0427(12) Uani 1 1 d .
O4 O 0.4703(2) 0.5617(3) 0.1763(3) 0.0786(17) Uani 1 1 d .
O5 O 0.0717(2) 0.0290(3) 0.0273(3) 0.0820(18) Uani 1 1 d .
O6 O 0.0728(6) 0.9905(9) 0.1698(7) 0.311(8) Uani 1 1 d .
O7 O 0.1443(2) 0.8999(3) 0.4648(3) 0.0749(17) Uani 1 1 d .
O8 O 0.1838(5) 0.9794(7) 0.7723(7) 0.032(5) Uani 0.306(9) 1 d PU
O9 O 0.1249(3) 0.0147(4) 0.8362(4) 0.063(3) Uani 0.694(9) 1 d P
O10 O 0.0150(2) 0.8938(3) 0.9499(3) 0.0674(16) Uani 1 1 d .
O11 O 0.01546(17) 0.7344(2) 0.9316(2) 0.0415(12) Uani 1 1 d .
O12 O 0.25148(19) 0.4063(3) 0.9473(3) 0.0602(14) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C6 Fe1 C4 91.0(3) . .
C6 Fe1 C5 94.1(3) . .
C4 Fe1 C5 91.0(3) . .
C6 Fe1 C2 87.2(3) . .
C4 Fe1 C2 91.2(2) . .
C5 Fe1 C2 177.5(2) . .
C6 Fe1 C3 178.0(2) . .
C4 Fe1 C3 87.4(3) . .
C5 Fe1 C3 84.8(2) . .
C2 Fe1 C3 94.0(2) . .
C6 Fe1 C1 83.8(2) . .
C4 Fe1 C1 173.9(3) . .
C5 Fe1 C1 86.3(2) . .
C2 Fe1 C1 91.7(2) . .
C3 Fe1 C1 97.7(2) . .
N1 Co1 N1 169.8(3) . 2
N1 Co1 N7 95.08(13) . .
N1 Co1 N7 95.08(13) 2 .
N1 Co1 N8 90.12(19) . .
N1 Co1 N8 92.95(19) 2 .
N7 Co1 N8 72.39(14) . .
N1 Co1 N8 92.95(19) . 2
N1 Co1 N8 90.12(19) 2 2
N7 Co1 N8 72.39(14) . 2
N8 Co1 N8 144.8(3) . 2
N1 Co1 O1 85.18(17) . 2
N1 Co1 O1 86.55(17) 2 2
N7 Co1 O1 144.62(10) . 2
N8 Co1 O1 142.93(18) . 2
N8 Co1 O1 72.26(17) 2 2
N1 Co1 O1 86.55(17) . .
N1 Co1 O1 85.18(17) 2 .
N7 Co1 O1 144.62(10) . .
N8 Co1 O1 72.26(17) . .
N8 Co1 O1 142.93(18) 2 .
O1 Co1 O1 70.8(2) 2 .
N2 Co2 N3 173.9(2) . 4
N2 Co2 N9 96.69(19) . .
N3 Co2 N9 89.36(19) 4 .
N2 Co2 N11 91.59(19) . .
N3 Co2 N11 89.16(19) 4 .
N9 Co2 N11 72.7(2) . .
N2 Co2 N10 90.5(2) . .
N3 Co2 N10 92.3(2) 4 .
N9 Co2 N10 73.1(2) . .
N11 Co2 N10 145.7(2) . .
N2 Co2 O3 85.95(18) . .
N3 Co2 O3 88.47(18) 4 .
N9 Co2 O3 144.9(2) . .
N11 Co2 O3 72.21(19) . .
N10 Co2 O3 142.0(2) . .
N2 Co2 O2 88.72(18) . .
N3 Co2 O2 87.00(18) 4 .
N9 Co2 O2 144.1(2) . .
N11 Co2 O2 142.8(2) . .
N10 Co2 O2 71.4(2) . .
O3 Co2 O2 70.70(18) . .
N1 C1 Fe1 169.2(5) . .
N2 C2 Fe1 175.5(5) . .
N3 C3 Fe1 173.3(6) . .
N4 C4 Fe1 179.5(6) . .
N5 C5 Fe1 174.6(6) . .
N6 C6 Fe1 174.3(6) . .
C8 C7 C8 120.2(10) 2 .
C9 C8 C7 117.9(7) . .
N7 C9 C8 121.6(6) . .
N7 C9 C10 114.1(5) . .
C8 C9 C10 124.3(6) . .
N8 C10 C9 114.4(6) . .
N8 C10 C11 125.3(7) . .
C9 C10 C11 120.3(6) . .
N8 C12 C13 106.9(5) . .
O1 C13 C12 105.8(5) . .
O1 C14 C14 104.8(4) . 2
N10 C16 C15 126.2(9) . .
N10 C16 C17 115.3(7) . .
C15 C16 C17 118.3(9) . .
N9 C17 C18 121.3(8) . .
N9 C17 C16 112.2(7) . .
C18 C17 C16 126.5(9) . .
C19 C18 C17 118.4(9) . .
C18 C19 C20 122.1(9) . .
C19 C20 C21 117.5(9) . .
N9 C21 C20 120.2(8) . .
N9 C21 C22 113.6(6) . .
C20 C21 C22 126.2(8) . .
N11 C22 C21 115.0(6) . .
N11 C22 C23 126.5(7) . .
C21 C22 C23 118.5(7) . .
N11 C24 C25 108.2(6) . .
O3 C25 C24 107.4(6) . .
O3 C26 C27 105.0(6) . .
O2 C27 C26 106.0(6) . .
O2 C28 C29 107.6(7) . .
C28 C29 N10 108.3(7) . .
C1 N1 Co1 151.7(5) . .
C2 N2 Co2 167.0(5) . .
C3 N3 Co2 157.3(5) . 4_545
C9 N7 C9 120.7(8) . 2
C9 N7 Co1 119.6(4) . .
C9 N7 Co1 119.6(4) 2 .
C10 N8 C12 122.1(6) . .
C10 N8 Co1 119.4(4) . .
C12 N8 Co1 118.5(4) . .
C17 N9 C21 120.4(7) . .
C17 N9 Co2 120.1(5) . .
C21 N9 Co2 119.4(5) . .
C16 N10 C29 122.6(7) . .
C16 N10 Co2 118.8(6) . .
C29 N10 Co2 118.1(6) . .
C22 N11 C24 122.3(6) . .
C22 N11 Co2 119.3(5) . .
C24 N11 Co2 118.4(4) . .
C13 O1 C14 112.5(4) . .
C13 O1 Co1 113.1(3) . .
C14 O1 Co1 114.7(3) . .
C28 O2 C27 114.2(7) . .
C28 O2 Co2 110.6(4) . .
C27 O2 Co2 113.2(4) . .
C26 O3 C25 113.5(6) . .
C26 O3 Co2 115.8(4) . .
C25 O3 Co2 111.7(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Fe1 C6 1.922(7) .
Fe1 C4 1.927(7) .
Fe1 C5 1.929(7) .
Fe1 C2 1.951(7) .
Fe1 C3 1.960(7) .
Fe1 C1 1.964(7) .
Co1 N1 2.096(5) .
Co1 N1 2.096(5) 2
Co1 N7 2.103(7) .
Co1 N8 2.191(5) .
Co1 N8 2.191(5) 2
Co1 O1 2.243(4) 2
Co1 O1 2.243(4) .
Co2 N2 2.090(5) .
Co2 N3 2.093(5) 4
Co2 N9 2.106(5) .
Co2 N11 2.184(5) .
Co2 N10 2.191(6) .
Co2 O3 2.262(4) .
Co2 O2 2.292(5) .
C1 N1 1.137(7) .
C2 N2 1.133(7) .
C3 N3 1.124(7) .
C4 N4 1.140(7) .
C5 N5 1.149(7) .
C6 N6 1.159(7) .
C7 C8 1.395(8) 2
C7 C8 1.395(8) .
C8 C9 1.387(9) .
C9 N7 1.337(7) .
C9 C10 1.469(9) .
C10 N8 1.259(7) .
C10 C11 1.494(8) .
C12 N8 1.465(7) .
C12 C13 1.542(8) .
C13 O1 1.421(7) .
C14 O1 1.423(7) .
C14 C14 1.494(12) 2
C15 C16 1.491(10) .
C16 N10 1.253(9) .
C16 C17 1.513(11) .
C17 N9 1.345(8) .
C17 C18 1.394(10) .
C18 C19 1.335(12) .
C19 C20 1.386(12) .
C20 C21 1.410(10) .
C21 N9 1.345(8) .
C21 C22 1.473(9) .
C22 N11 1.259(8) .
C22 C23 1.500(9) .
C24 N11 1.454(8) .
C24 C25 1.486(9) .
C25 O3 1.434(8) .
C26 O3 1.407(8) .
C26 C27 1.504(11) .
C27 O2 1.446(9) .
C28 O2 1.410(8) .
C28 C29 1.477(11) .
C29 N10 1.481(9) .
C30 O12 1.462(8) .
N3 Co2 2.093(5) 4_545
N7 C9 1.337(7) 2
