#------------------------------------------------------------------------------
#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/1/53/56/1535691.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1535691
loop_
_publ_author_name
'Huppertz, H.'
_publ_section_title
;
 Multianvil high-pressure/high-temperatuer preparation, crystal structure,
 and properties of the new oxoborates Dy4 B6 O14 (O H)2 and Ho4 B6 O14 (O
 H)2
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              3700
_journal_page_last               3708
_journal_volume                  177
_journal_year                    2004
_chemical_formula_sum            'B6 H2 Ho4 O16'
_chemical_name_systematic        'Ho4 (B6 O14 (O H)2)'
_space_group_IT_number           60
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   12.9278
_cell_length_b                   4.362
_cell_length_c                   8.8713
_cell_volume                     500.262
_citation_journal_id_ASTM        JSSCBI
_cod_data_source_file            Huppertz_JSSCBI_2004_1529.cif
_cod_data_source_block           H2B6Ho4O16
_cod_original_formula_sum        'H2 B6 Ho4 O16'
_cod_database_code               1535691
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x+1/2,-y+1/2,z+1/2
x+1/2,-y+1/2,-z
-x,y,-z+1/2
-x,-y,-z
x-1/2,y-1/2,-z-1/2
-x-1/2,y-1/2,z
x,-y,z-1/2
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
O4 O-2 -0.0042 0.2434 0.1088 1 0.0
O3 O-2 -0.094 0.6381 0.2598 1 0.0
O1 O-2 0.3109 0.0358 0.4647 1 0.0
B1 B+3 0 0.4394 0.25 1 0.0
Ho1 Ho+3 0.140357 0.04323 0.53922 1 0.0
O2 O-2 0.2169 0.2077 0.2466 1 0.0
B2 B+3 0.3066 0.025 0.3035 1 0.0
