#------------------------------------------------------------------------------
#$Date: 2016-12-04 14:50:07 +0200 (Sun, 04 Dec 2016) $
#$Revision: 188874 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/54/47/1544719.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1544719
loop_
_publ_author_name
'Yamamoto, N.'
'Oka, Y.'
'Tamada, O.'
_publ_section_title
;
 Single crystal growth and structure determination of Rb1.5Mn8O16
 hollandite
;
_journal_name_full               'Mineralogical Journal'
_journal_page_first              41
_journal_page_last               49
_journal_volume                  15
_journal_year                    1990
_chemical_formula_sum            'Mn8 O16 Rb1.5'
_chemical_name_common            Rb1.5Mn8O16
_chemical_name_mineral           'synthetic hollandite'
_space_group_IT_number           87
_space_group_name_H-M_alt        'I 4/m'
_symmetry_space_group_name_Hall  '-I 4'
_symmetry_space_group_name_H-M   'I 4/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   9.915(9)
_cell_length_b                   9.915(9)
_cell_length_c                   2.866(3)
_cell_volume                     281.7(5)
_cod_data_source_file            Rb1.5Mn8O16.cif
_cod_data_source_block           RbxMn8O16
_cod_original_formula_sum        'Rb1.5 Mn8 O16'
_cod_database_code               1544719
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
'-x, -y, z'
'x, y, -z'
'-y, x, z'
'y, -x, -z'
'y, -x, z'
'-y, x, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, -z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, y+1/2, -z+1/2'
'-y+1/2, x+1/2, z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'y+1/2, -x+1/2, z+1/2'
'-y+1/2, x+1/2, -z+1/2'
loop_
_atom_site_label
_atom_site_occupancy
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_B_iso_or_equiv
_atom_site_type_symbol
Rb1 0.3750 0.000000 0.000000 0.500000 Biso 1.438916 Rb
Rb2 0.1910 0.000000 0.000000 0.689(2) Biso 0.667027 Rb
Mn 1.0 0.34870(10) 0.16500(10) 0.000000 Biso 0.423480 Mn
O1 1.0 0.1570(7) 0.2057(7) 0.000000 Biso 0.712297 O
O2 1.0 0.5415(7) 0.1633(7) 0.000000 Biso 0.929006 O
