#------------------------------------------------------------------------------
#$Date: 2023-04-20 14:53:48 +0300 (Thu, 20 Apr 2023) $
#$Revision: 282777 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/54/78/1547846.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1547846
loop_
_publ_author_name
'Shen, Hui'
'Kubo, Kazuyuki'
'Kume, Shoko'
'Zhang, Limin'
'Mizuta, Tsutomu'
_publ_section_title
;
 Novel chloride-centered Ag ₁₈ clusters featuring a
 cuboctahedral Ag ₁₂ skeleton
;
_journal_issue                   46
_journal_name_full               'Dalton Transactions'
_journal_page_first              16199
_journal_page_last               16204
_journal_paper_doi               10.1039/C7DT03195E
_journal_volume                  46
_journal_year                    2017
_chemical_formula_sum            'C238 H196 Ag18 Cl F18 P6 Sb3'
_chemical_formula_weight         5926.12
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   difmap
_audit_update_record
;
2017-10-01 deposited with the CCDC.
2017-10-31 downloaded from the CCDC.
;
_cell_angle_alpha                117.4530(10)
_cell_angle_beta                 116.6710(10)
_cell_angle_gamma                92.003(2)
_cell_formula_units_Z            1
_cell_length_a                   18.465(2)
_cell_length_b                   19.820(2)
_cell_length_c                   20.121(3)
_cell_measurement_reflns_used    20715
_cell_measurement_temperature    173.(2)
_cell_measurement_theta_max      27.4004
_cell_measurement_theta_min      2.2394
_cell_volume                     5561.0(12)
_computing_cell_refinement       'SAINT V8.34A (Bruker AXS Inc., 2013)'
_computing_data_collection       'APEX2(Bruker AXS)'
_computing_data_reduction        'SAINT V8.34A (Bruker AXS Inc., 2013)'
_computing_molecular_graphics    'XSHELL V6.3.1(Bruker AXS)'
_computing_publication_material  'Generate Report (Bruker AXS)'
_computing_structure_refinement  'SHELXL-2014/6 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXL-2014/6 (Sheldrick, 2014)'
_diffrn_ambient_temperature      173.(2)
_diffrn_detector_area_resol_mean 8.3333
_diffrn_measured_fraction_theta_full 0.949
_diffrn_measured_fraction_theta_max 0.928
_diffrn_measurement_device_type  'Bruker D8 goniometer'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  'multilayered conforcal mirror'
_diffrn_radiation_type           MoKa
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0189
_diffrn_reflns_av_unetI/netI     0.0538
_diffrn_reflns_Laue_measured_fraction_full 0.949
_diffrn_reflns_Laue_measured_fraction_max 0.928
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            30384
_diffrn_reflns_point_group_measured_fraction_full 0.949
_diffrn_reflns_point_group_measured_fraction_max 0.928
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         27.408
_diffrn_reflns_theta_min         1.98
_diffrn_source                   'rotating-anode X-ray tube'
_diffrn_source_type              'Bruker Turbo X-ray Source'
_exptl_absorpt_coefficient_mu    2.022
_exptl_absorpt_correction_T_max  0.82
_exptl_absorpt_correction_T_min  0.65
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS V2014/4 (Bruker AXS Inc.)'
_exptl_crystal_colour            'clear pale orange'
_exptl_crystal_density_diffrn    1.770
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2892
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.210
_exptl_crystal_size_min          0.100
_refine_diff_density_max         1.751
_refine_diff_density_min         -1.015
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.020
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1280
_refine_ls_number_reflns         23488
_refine_ls_number_restraints     137
_refine_ls_restrained_S_all      1.022
_refine_ls_R_factor_all          0.0999
_refine_ls_R_factor_gt           0.0524
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0557P)²+33.5071P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1210
_refine_ls_wR_factor_ref         0.1549
_reflns_number_gt                14676
_reflns_number_total             23488
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c7dt03195e2.cif
_cod_data_source_block           Ag18(CCPh)14(PTol3)6Cl
_cod_database_code               1547846
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag Ag1 0.56525(4) 0.36043(4) 0.48259(4) 0.04641(15) Uani d . . . 1.0 . .
Ag Ag2 0.44032(4) 0.36109(4) 0.31966(4) 0.04525(15) Uani d . . . 1.0 . .
Ag Ag3 0.61796(4) 0.45650(4) 0.42646(4) 0.04534(15) Uani d . . . 1.0 . .
Ag Ag4 0.35278(4) 0.49264(4) 0.31464(4) 0.04711(15) Uani d . . . 1.0 . .
Ag Ag5 0.55980(4) 0.61473(4) 0.44275(4) 0.04408(14) Uani d . . . 1.0 . .
Ag Ag6 0.70164(4) 0.61852(4) 0.61364(4) 0.04406(14) Uani d . . . 1.0 . .
Ag Ag7 0.19385(3) 0.47136(4) 0.31803(4) 0.04481(15) Uani d . . . 1.0 . .
Ag Ag8 0.46389(4) 0.51957(3) 0.24908(4) 0.04226(14) Uani d . . . 1.0 . .
Ag Ag9 0.67282(3) 0.77180(3) 0.62273(4) 0.04340(14) Uani d . . . 1.0 . .
Cl Cl1 0.5 0.5 0.5 0.0393(5) Uani d . P S 1.0 . .
P P1 0.05185(12) 0.38949(12) 0.19621(13) 0.0411(4) Uani d . . . 1.0 . .
P P2 0.41336(12) 0.58908(12) 0.17426(13) 0.0415(4) Uani d . . . 1.0 . .
P P3 0.79612(12) 0.86280(12) 0.66296(13) 0.0424(5) Uani d . . . 1.0 . .
C C1 0.5609(5) 0.3247(4) 0.3557(5) 0.0424(17) Uani d . . . 1.0 . .
C C2 0.5731(5) 0.2680(5) 0.3068(5) 0.0442(18) Uani d . . . 1.0 . .
C C3 0.5833(5) 0.1995(5) 0.2450(5) 0.0474(19) Uani d . . . 1.0 . .
C C4 0.5558(6) 0.1242(6) 0.2257(7) 0.068(3) Uani d . . . 1.0 . .
H H4 0.5307 0.1162 0.2547 0.081 Uiso calc U . R 1.0 . .
C C5 0.5641(8) 0.0593(6) 0.1641(9) 0.091(4) Uani d . . . 1.0 . .
H H5 0.5447 0.0072 0.1507 0.109 Uiso calc U . R 1.0 . .
C C6 0.6010(8) 0.0714(8) 0.1223(9) 0.098(4) Uani d . . . 1.0 . .
H H6 0.6063 0.027 0.0799 0.117 Uiso calc U . R 1.0 . .
C C7 0.6302(7) 0.1474(8) 0.1415(8) 0.090(4) Uani d . . . 1.0 . .
H H7 0.6557 0.1554 0.1128 0.108 Uiso calc U . R 1.0 . .
C C8 0.6216(6) 0.2108(6) 0.2028(7) 0.067(3) Uani d . . . 1.0 . .
H H8 0.6419 0.2631 0.2169 0.08 Uiso calc U . R 1.0 . .
C C9 0.3788(5) 0.4073(5) 0.2246(6) 0.0428(17) Uani d . . . 1.0 . .
C C10 0.3773(4) 0.3580(5) 0.1596(6) 0.0456(19) Uani d . . . 1.0 . .
C C11 0.3765(5) 0.2985(5) 0.0819(6) 0.052(2) Uani d . . . 1.0 . .
C C12 0.3265(6) 0.2929(6) 0.0020(7) 0.066(3) Uani d . . . 1.0 . .
H H12 0.2933 0.328 -0.0015 0.079 Uiso calc U . R 1.0 . .
C C13 0.3252(8) 0.2351(8) -0.0735(8) 0.088(4) Uani d . . . 1.0 . .
H H13 0.2904 0.2301 -0.1285 0.106 Uiso calc U . R 1.0 . .
C C14 0.3761(9) 0.1852(7) -0.0663(9) 0.088(4) Uani d . . . 1.0 . .
H H14 0.3768 0.1469 -0.1165 0.105 Uiso calc U . R 1.0 . .
C C15 0.4243(7) 0.1910(6) 0.0112(8) 0.080(3) Uani d . . . 1.0 . .
H H15 0.4582 0.1564 0.0149 0.096 Uiso calc U . R 1.0 . .
C C16 0.4248(6) 0.2467(6) 0.0856(7) 0.063(2) Uani d . . . 1.0 . .
H H16 0.4585 0.2495 0.1395 0.076 Uiso calc U . R 1.0 . .
C C17 0.3049(5) 0.5776(5) 0.3767(5) 0.0457(19) Uani d . . . 1.0 . .
C C18 0.2729(5) 0.6301(5) 0.3995(6) 0.051(2) Uani d . . . 1.0 . .
C C19 0.2296(6) 0.6882(5) 0.4218(7) 0.056(3) Uani d . P G 0.708(9) A 1
C C20 0.1938(7) 0.7197(7) 0.3698(7) 0.079(5) Uani d . P G 0.708(9) A 1
H H20 0.1951 0.7007 0.3176 0.095 Uiso calc U P R 0.708(9) A 1
C C21 0.1562(7) 0.7789(8) 0.3940(10) 0.107(7) Uani d . P G 0.708(9) A 1
H H21 0.1317 0.8004 0.3584 0.128 Uiso calc U P R 0.708(9) A 1
C C22 0.1543(8) 0.8066(7) 0.4703(11) 0.107(6) Uani d . P G 0.708(9) A 1
H H22 0.1286 0.8471 0.4869 0.128 Uiso calc U P R 0.708(9) A 1
C C23 0.1900(9) 0.7752(8) 0.5224(8) 0.111(6) Uani d . P G 0.708(9) A 1
H H23 0.1887 0.7941 0.5745 0.133 Uiso calc U P R 0.708(9) A 1
C C24 0.2277(7) 0.7160(7) 0.4981(7) 0.090(5) Uani d . P G 0.708(9) A 1
H H24 0.2521 0.6945 0.5337 0.108 Uiso calc U P R 0.708(9) A 1
C C19B 0.2502(13) 0.7037(13) 0.4313(17) 0.056(3) Uani d . P G 0.292(9) A 2
C C20B 0.1682(12) 0.6975(14) 0.3736(18) 0.079(5) Uani d . P G 0.292(9) A 2
H H20B 0.136 0.6516 0.3156 0.095 Uiso calc U P R 0.292(9) A 2
C C21B 0.1334(12) 0.7584(19) 0.401(3) 0.107(7) Uani d . P G 0.292(9) A 2
H H21B 0.0773 0.7542 0.3612 0.128 Uiso calc U P R 0.292(9) A 2
C C22B 0.181(2) 0.8256(17) 0.485(3) 0.107(6) Uani d . P G 0.292(9) A 2
H H22B 0.1567 0.8673 0.5039 0.128 Uiso calc U P R 0.292(9) A 2
C C23B 0.262(2) 0.8318(15) 0.5431(16) 0.111(6) Uani d . P G 0.292(9) A 2
H H23B 0.2947 0.8778 0.6011 0.133 Uiso calc U P R 0.292(9) A 2
C C24B 0.2973(13) 0.7709(16) 0.5161(14) 0.090(5) Uani d . P G 0.292(9) A 2
H H24B 0.3534 0.7752 0.5555 0.108 Uiso calc U P R 0.292(9) A 2
C C25 0.5948(5) 0.5347(5) 0.3614(5) 0.0416(17) Uani d . . . 1.0 . .
C C26 0.6245(5) 0.4990(5) 0.3166(5) 0.0463(19) Uani d . . . 1.0 . .
C C27 0.6599(5) 0.4536(5) 0.2642(6) 0.051(2) Uani d . . . 1.0 . .
C C28 0.6064(6) 0.3942(5) 0.1759(6) 0.058(2) Uani d . . . 1.0 . .
H H28 0.5466 0.3841 0.1495 0.07 Uiso calc U . R 1.0 . .
C C29 0.6386(7) 0.3500(6) 0.1264(7) 0.072(3) Uani d . . . 1.0 . .
H H29 0.6011 0.3101 0.066 0.087 Uiso calc U . R 1.0 . .
C C30 0.7234(8) 0.3631(7) 0.1632(8) 0.084(3) Uani d . . . 1.0 . .
H H30 0.7451 0.3313 0.1288 0.1 Uiso calc U . R 1.0 . .
C C31 0.7780(7) 0.4213(8) 0.2489(9) 0.102(4) Uani d . . . 1.0 . .
H H31 0.8376 0.4295 0.2745 0.123 Uiso calc U . R 1.0 . .
C C32 0.7467(7) 0.4687(7) 0.2990(7) 0.088(4) Uani d . . . 1.0 . .
H H32 0.7851 0.5119 0.3576 0.105 Uiso calc U . R 1.0 . .
C C33 0.5296(4) 0.7127(5) 0.5100(5) 0.0412(17) Uani d . . . 1.0 . .
C C34 0.5141(5) 0.7767(5) 0.5339(5) 0.052(2) Uani d . . . 1.0 . .
C C35 0.5064(15) 0.8516(15) 0.5458(18) 0.055(3) Uani d U P G 0.251(9) B 1
C C36 0.5055(12) 0.8861(16) 0.4991(14) 0.099(5) Uani d U P G 0.251(9) B 1
H H36 0.5106 0.8577 0.4492 0.119 Uiso calc U P R 0.251(9) B 1
C C37 0.4971(14) 0.9622(14) 0.5254(16) 0.142(9) Uani d U P G 0.251(9) B 1
H H37 0.4965 0.9857 0.4935 0.17 Uiso calc U P R 0.251(9) B 1
C C38 0.4896(18) 1.0038(12) 0.5985(17) 0.099(6) Uani d U P G 0.251(9) B 1
H H38 0.4839 1.0558 0.6165 0.119 Uiso calc U P R 0.251(9) B 1
C C39 0.491(2) 0.969(2) 0.6452(18) 0.091(5) Uani d U P G 0.251(9) B 1
H H39 0.4855 0.9977 0.6952 0.109 Uiso calc U P R 0.251(9) B 1
C C40 0.499(2) 0.893(2) 0.619(2) 0.082(4) Uani d U P G 0.251(9) B 1
H H40 0.4996 0.8696 0.6509 0.098 Uiso calc U P R 0.251(9) B 1
C C35B 0.4882(6) 0.8500(4) 0.5633(6) 0.055(3) Uani d U P G 0.749(9) B 2
C C36B 0.5349(6) 0.9150(6) 0.5746(8) 0.099(5) Uani d U P G 0.749(9) B 2
H H36B 0.58 0.9106 0.5636 0.119 Uiso calc U P R 0.749(9) B 2
C C37B 0.5156(7) 0.9865(5) 0.6020(9) 0.142(9) Uani d U P G 0.749(9) B 2
H H37B 0.5475 1.031 0.6098 0.17 Uiso calc U P R 0.749(9) B 2
C C38B 0.4496(7) 0.9930(5) 0.6181(8) 0.099(6) Uani d U P G 0.749(9) B 2
H H38B 0.4364 1.0419 0.6368 0.119 Uiso calc U P R 0.749(9) B 2
C C39B 0.4029(6) 0.9280(6) 0.6068(7) 0.091(5) Uani d U P G 0.749(9) B 2
H H39B 0.3578 0.9324 0.6178 0.109 Uiso calc U P R 0.749(9) B 2
C C40B 0.4222(6) 0.8565(5) 0.5794(7) 0.082(4) Uani d U P G 0.749(9) B 2
H H40B 0.3903 0.812 0.5717 0.098 Uiso calc U P R 0.749(9) B 2
C C41 0.7517(4) 0.5378(5) 0.5496(5) 0.0401(17) Uani d . . . 1.0 . .
C C42 0.7934(5) 0.4987(5) 0.5263(5) 0.0482(19) Uani d . . . 1.0 . .
C C43 0.8464(9) 0.4556(5) 0.4985(7) 0.046(3) Uani d . P G 0.730(10) C 1
C C44 0.8102(6) 0.3868(5) 0.4154(5) 0.065(3) Uani d . P G 0.730(10) C 1
H H44 0.7508 0.3699 0.3745 0.078 Uiso calc U P R 0.730(10) C 1
C C45 0.8609(7) 0.3427(5) 0.3921(6) 0.078(4) Uani d . P G 0.730(10) C 1
H H45 0.8362 0.2957 0.3353 0.093 Uiso calc U P R 0.730(10) C 1
C C46 0.9478(7) 0.3674(9) 0.4520(9) 0.084(5) Uani d . P G 0.730(10) C 1
H H46 0.9825 0.3373 0.4361 0.101 Uiso calc U P R 0.730(10) C 1
C C47 0.9840(6) 0.4362(10) 0.5351(8) 0.084(5) Uani d . P G 0.730(10) C 1
H H47 1.0434 0.453 0.576 0.101 Uiso calc U P R 0.730(10) C 1
C C48 0.9333(9) 0.4802(7) 0.5584(6) 0.068(5) Uani d . P G 0.730(10) C 1
H H48 0.9581 0.5272 0.6152 0.081 Uiso calc U P R 0.730(10) C 1
C C43B 0.846(3) 0.4448(16) 0.508(2) 0.046(3) Uani d . P G 0.270(10) C 2
C C44B 0.8094(16) 0.3624(16) 0.4553(17) 0.065(3) Uani d . P G 0.270(10) C 2
H H44B 0.7524 0.3392 0.4359 0.078 Uiso calc U P R 0.270(10) C 2
C C45B 0.857(2) 0.3138(16) 0.431(2) 0.078(4) Uani d . P G 0.270(10) C 2
H H45B 0.8318 0.2575 0.3949 0.093 Uiso calc U P R 0.270(10) C 2
C C46B 0.940(2) 0.348(3) 0.459(3) 0.084(5) Uani d . P G 0.270(10) C 2
H H46B 0.9722 0.3145 0.4428 0.101 Uiso calc U P R 0.270(10) C 2
C C47B 0.9762(19) 0.430(3) 0.512(3) 0.084(5) Uani d . P G 0.270(10) C 2
H H47B 1.0332 0.4534 0.5317 0.101 Uiso calc U P R 0.270(10) C 2
C C48B 0.929(3) 0.4788(18) 0.537(3) 0.068(5) Uani d . P G 0.270(10) C 2
H H48B 0.9538 0.5351 0.5727 0.081 Uiso calc U P R 0.270(10) C 2
C C49 0.6824(4) 0.7122(5) 0.7036(5) 0.0426(18) Uani d . . . 1.0 . .
C C50 0.6920(5) 0.7664(5) 0.7710(5) 0.0436(18) Uani d . . . 1.0 . .
C C51 0.7041(4) 0.8284(4) 0.8526(5) 0.0435(18) Uani d . . . 1.0 . .
C C52 0.6643(6) 0.8862(5) 0.8575(6) 0.059(2) Uani d . . . 1.0 . .
H H52 0.6289 0.887 0.8062 0.07 Uiso calc U . R 1.0 . .
C C53 0.6760(7) 0.9437(6) 0.9381(8) 0.076(3) Uani d . . . 1.0 . .
H H53 0.649 0.9842 0.9417 0.091 Uiso calc U . R 1.0 . .
C C54 0.7257(7) 0.9424(6) 1.0116(8) 0.075(3) Uani d . . . 1.0 . .
H H54 0.7315 0.9813 1.0655 0.09 Uiso calc U . R 1.0 . .
C C55 0.7677(6) 0.8864(6) 1.0098(6) 0.062(2) Uani d . . . 1.0 . .
H H55 0.8029 0.8868 1.0619 0.074 Uiso calc U . R 1.0 . .
C C56 0.7576(5) 0.8288(5) 0.9295(6) 0.052(2) Uani d . . . 1.0 . .
H H56 0.7868 0.7899 0.9269 0.062 Uiso calc U . R 1.0 . .
C C57 0.0445(5) 0.3228(5) 0.0924(5) 0.0418(17) Uani d . . . 1.0 . .
C C58 -0.0269(5) 0.2566(5) 0.0200(6) 0.053(2) Uani d . . . 1.0 . .
H H58 -0.0741 0.2433 0.024 0.063 Uiso calc U . R 1.0 . .
C C59 -0.0279(6) 0.2111(5) -0.0573(5) 0.053(2) Uani d . . . 1.0 . .
H H59 -0.077 0.1669 -0.1058 0.063 Uiso calc U . R 1.0 . .
C C60 0.0383(6) 0.2261(6) -0.0679(6) 0.058(2) Uani d . . . 1.0 . .
C C61 0.1080(6) 0.2914(6) 0.0040(6) 0.061(2) Uani d . . . 1.0 . .
H H61 0.1547 0.3043 -0.0009 0.073 Uiso calc U . R 1.0 . .
C C62 0.1123(5) 0.3387(5) 0.0830(6) 0.051(2) Uani d . . . 1.0 . .
H H62 0.1619 0.3824 0.1312 0.061 Uiso calc U . R 1.0 . .
C C63 0.0342(8) 0.1763(6) -0.1534(7) 0.081(3) Uani d . . . 1.0 . .
H H63A 0.0471 0.1272 -0.1586 0.122 Uiso calc U . R 1.0 . .
H H63B 0.0758 0.2065 -0.1551 0.122 Uiso calc U . R 1.0 . .
H H63C -0.0231 0.1628 -0.2023 0.122 Uiso calc U . R 1.0 . .
C C64 -0.0036(5) 0.3266(4) 0.2129(5) 0.0436(18) Uani d . . . 1.0 . .
C C65 -0.0910(5) 0.2914(5) 0.1622(6) 0.056(2) Uani d . . . 1.0 . .
H H65 -0.125 0.3044 0.1204 0.067 Uiso calc U . R 1.0 . .
C C66 -0.1299(6) 0.2375(6) 0.1712(6) 0.060(2) Uani d . . . 1.0 . .
H H66 -0.1899 0.2132 0.135 0.072 Uiso calc U . R 1.0 . .
C C67 -0.0815(5) 0.2193(5) 0.2329(6) 0.055(2) Uani d . . . 1.0 . .
C C68 0.0054(5) 0.2561(5) 0.2849(6) 0.052(2) Uani d . . . 1.0 . .
H H68 0.0392 0.2451 0.3285 0.062 Uiso calc U . R 1.0 . .
C C69 0.0441(5) 0.3084(5) 0.2747(5) 0.0488(19) Uani d . . . 1.0 . .
H H69 0.1041 0.3322 0.3106 0.059 Uiso calc U . R 1.0 . .
C C70 -0.1230(6) 0.1561(6) 0.2395(7) 0.070(3) Uani d . . . 1.0 . .
H H70A -0.1166 0.1046 0.2056 0.106 Uiso calc U . R 1.0 . .
H H70B -0.1836 0.1512 0.216 0.106 Uiso calc U . R 1.0 . .
H H70C -0.0953 0.1722 0.3013 0.106 Uiso calc U . R 1.0 . .
C C71 -0.0119(5) 0.4541(5) 0.1764(5) 0.0439(18) Uani d . . . 1.0 . .
C C72 0.0101(6) 0.5303(5) 0.2479(6) 0.065(3) Uani d . . . 1.0 . .
H H72 0.0546 0.5454 0.3049 0.078 Uiso calc U . R 1.0 . .
C C73 -0.0319(6) 0.5843(6) 0.2370(7) 0.072(3) Uani d . . . 1.0 . .
H H73 -0.0158 0.6357 0.2869 0.086 Uiso calc U . R 1.0 . .
C C74 -0.0965(5) 0.5651(5) 0.1554(6) 0.052(2) Uani d . . . 1.0 . .
C C75 -0.1173(6) 0.4908(6) 0.0857(6) 0.066(3) Uani d . . . 1.0 . .
H H75 -0.1616 0.476 0.0287 0.079 Uiso calc U . R 1.0 . .
C C76 -0.0756(6) 0.4357(6) 0.0955(6) 0.062(2) Uani d . . . 1.0 . .
H H76 -0.0916 0.3846 0.0452 0.075 Uiso calc U . R 1.0 . .
C C77 -0.1386(6) 0.6265(6) 0.1444(7) 0.071(3) Uani d . . . 1.0 . .
H H77A -0.1513 0.6205 0.0888 0.106 Uiso calc U . R 1.0 . .
H H77B -0.1001 0.6802 0.1934 0.106 Uiso calc U . R 1.0 . .
H H77C -0.1915 0.6185 0.144 0.106 Uiso calc U . R 1.0 . .
C C78 0.3912(5) 0.5318(5) 0.0626(5) 0.0448(18) Uani d . . . 1.0 . .
C C79 0.4254(5) 0.4701(5) 0.0385(6) 0.051(2) Uani d . . . 1.0 . .
H H79 0.4615 0.4593 0.0815 0.062 Uiso calc U . R 1.0 . .
C C80 0.4086(6) 0.4237(6) -0.0463(6) 0.059(2) Uani d . . . 1.0 . .
H H80 0.4333 0.3819 -0.0604 0.07 Uiso calc U . R 1.0 . .
C C81 0.3566(5) 0.4374(5) -0.1109(5) 0.052(2) Uani d . . . 1.0 . .
C C82 0.3233(6) 0.5005(6) -0.0873(6) 0.060(2) Uani d . . . 1.0 . .
H H82 0.289 0.5121 -0.1302 0.072 Uiso calc U . R 1.0 . .
C C83 0.3389(5) 0.5466(5) -0.0031(5) 0.051(2) Uani d . . . 1.0 . .
H H83 0.3143 0.5886 0.0108 0.061 Uiso calc U . R 1.0 . .
C C84 0.3368(7) 0.3882(7) -0.2038(6) 0.075(3) Uani d . . . 1.0 . .
H H84A 0.3866 0.4031 -0.206 0.112 Uiso calc U . R 1.0 . .
H H84B 0.2884 0.3979 -0.242 0.112 Uiso calc U . R 1.0 . .
H H84C 0.3227 0.3314 -0.2241 0.112 Uiso calc U . R 1.0 . .
C C85 0.4898(5) 0.6842(5) 0.2270(5) 0.0467(18) Uani d . . . 1.0 . .
C C86 0.4981(5) 0.7155(5) 0.1810(6) 0.055(2) Uani d . . . 1.0 . .
H H86 0.4585 0.6898 0.1196 0.066 Uiso calc U . R 1.0 . .
C C87 0.5638(6) 0.7841(5) 0.2236(7) 0.064(3) Uani d . . . 1.0 . .
H H87 0.5674 0.8049 0.1908 0.077 Uiso calc U . R 1.0 . .
C C88 0.6238(7) 0.8228(6) 0.3122(7) 0.074(3) Uani d . . . 1.0 . .
C C89 0.6121(8) 0.7920(7) 0.3567(7) 0.092(4) Uani d U . . 1.0 . .
H H89 0.6513 0.818 0.4182 0.11 Uiso calc U . R 1.0 . .
C C90 0.5467(7) 0.7256(6) 0.3167(6) 0.074(3) Uani d . . . 1.0 . .
H H90 0.5404 0.708 0.3509 0.089 Uiso calc U . R 1.0 . .
C C91 0.6991(8) 0.8938(7) 0.3565(9) 0.108(5) Uani d . . . 1.0 . .
H H91A 0.6959 0.9054 0.3131 0.162 Uiso calc U . R 1.0 . .
H H91B 0.7521 0.8814 0.3816 0.162 Uiso calc U . R 1.0 . .
H H91C 0.698 0.9404 0.4035 0.162 Uiso calc U . R 1.0 . .
C C92 0.3130(5) 0.6057(5) 0.1609(5) 0.0442(18) Uani d . . . 1.0 . .
C C93 0.2899(5) 0.6708(5) 0.1562(5) 0.050(2) Uani d . . . 1.0 . .
H H93 0.3289 0.7103 0.1641 0.061 Uiso calc U . R 1.0 . .
C C94 0.2097(5) 0.6773(5) 0.1400(5) 0.052(2) Uani d . . . 1.0 . .
H H94 0.1939 0.7208 0.1356 0.063 Uiso calc U . R 1.0 . .
C C95 0.1520(5) 0.6207(6) 0.1302(6) 0.055(2) Uani d . . . 1.0 . .
C C96 0.1762(6) 0.5577(6) 0.1361(7) 0.065(3) Uani d . . . 1.0 . .
H H96 0.1378 0.5188 0.1298 0.078 Uiso calc U . R 1.0 . .
C C97 0.2557(5) 0.5497(5) 0.1511(6) 0.054(2) Uani d . . . 1.0 . .
H H97 0.2708 0.5057 0.1547 0.065 Uiso calc U . R 1.0 . .
C C98 0.0641(6) 0.6279(7) 0.1119(8) 0.081(3) Uani d . . . 1.0 . .
H H98A 0.0334 0.6271 0.057 0.121 Uiso calc U . R 1.0 . .
H H98B 0.0699 0.6782 0.1605 0.121 Uiso calc U . R 1.0 . .
H H98C 0.0323 0.5831 0.1063 0.121 Uiso calc U . R 1.0 . .
C C99 0.8326(5) 0.8167(5) 0.5869(5) 0.0454(18) Uani d . . . 1.0 . .
C C100 0.7888(5) 0.7408(5) 0.5168(6) 0.057(2) Uani d . . . 1.0 . .
H H100 0.7409 0.7122 0.5099 0.069 Uiso calc U . R 1.0 . .
C C101 0.8120(6) 0.7033(6) 0.4539(7) 0.071(3) Uani d . . . 1.0 . .
H H101 0.7791 0.6508 0.4042 0.085 Uiso calc U . R 1.0 . .
C C102 0.8826(6) 0.7431(6) 0.4649(6) 0.067(3) Uani d . . . 1.0 . .
C C103 0.9297(6) 0.8190(6) 0.5383(7) 0.071(3) Uani d . . . 1.0 . .
H H103 0.9796 0.8464 0.5472 0.085 Uiso calc U . R 1.0 . .
C C104 0.9058(6) 0.8557(6) 0.5985(6) 0.071(3) Uani d . . . 1.0 . .
H H104 0.9392 0.9079 0.6485 0.085 Uiso calc U . R 1.0 . .
C C105 0.9100(8) 0.7059(8) 0.3974(7) 0.093(4) Uani d . . . 1.0 . .
H H10A 0.8792 0.6487 0.3572 0.14 Uiso calc U . R 1.0 . .
H H10B 0.9713 0.7136 0.4281 0.14 Uiso calc U . R 1.0 . .
H H10C 0.8969 0.7318 0.3638 0.14 Uiso calc U . R 1.0 . .
C C106 0.7788(5) 0.9534(5) 0.6643(5) 0.051(2) Uani d . . . 1.0 . .
C C107 0.7775(8) 0.9680(6) 0.6026(7) 0.084(4) Uani d . . . 1.0 . .
H H107 0.7944 0.9353 0.5635 0.101 Uiso calc U . R 1.0 . .
C C108 0.7506(9) 1.0320(7) 0.5998(8) 0.095(4) Uani d U . . 1.0 . .
H H108 0.7491 1.042 0.5574 0.114 Uiso calc U . R 1.0 . .
C C109 0.7255(10) 1.0824(7) 0.6567(8) 0.099(4) Uani d . . . 1.0 . .
C C110 0.7379(8) 1.0708(7) 0.7219(7) 0.086(3) Uani d . . . 1.0 . .
H H110 0.7304 1.1081 0.7675 0.103 Uiso calc U . R 1.0 . .
C C111 0.7610(6) 1.0060(5) 0.7235(6) 0.060(2) Uani d . . . 1.0 . .
H H111 0.7646 0.9977 0.7676 0.072 Uiso calc U . R 1.0 . .
C C112 0.6931(11) 1.1492(8) 0.6486(9) 0.132(6) Uani d U . . 1.0 . .
H H11A 0.7415 1.1955 0.6778 0.198 Uiso calc U . R 1.0 . .
H H11B 0.6595 1.1643 0.6765 0.198 Uiso calc U . R 1.0 . .
H H11C 0.6574 1.131 0.5863 0.198 Uiso calc U . R 1.0 . .
C C113 0.8874(4) 0.8974(4) 0.7708(5) 0.0421(17) Uani d . . . 1.0 . .
C C114 0.9562(5) 0.9651(5) 0.8168(6) 0.059(2) Uani d . . . 1.0 . .
H H114 0.9544 0.9979 0.7938 0.07 Uiso calc U . R 1.0 . .
C C115 1.0268(5) 0.9845(5) 0.8957(5) 0.055(2) Uani d . . . 1.0 . .
H H115 1.0726 1.0312 0.9264 0.066 Uiso calc U . R 1.0 . .
C C116 1.0331(5) 0.9381(5) 0.9313(5) 0.0483(19) Uani d . . . 1.0 . .
C C117 0.9636(5) 0.8731(5) 0.8880(5) 0.0481(19) Uani d . . . 1.0 . .
H H117 0.9649 0.8418 0.9125 0.058 Uiso calc U . R 1.0 . .
C C118 0.8919(5) 0.8533(5) 0.8091(5) 0.0452(18) Uani d . . . 1.0 . .
H H118 0.8448 0.8085 0.7806 0.054 Uiso calc U . R 1.0 . .
C C119 1.1126(5) 0.9586(6) 1.0149(6) 0.059(2) Uani d . . . 1.0 . .
H H11D 1.1479 0.9256 1.0007 0.089 Uiso calc U . R 1.0 . .
H H11E 1.0971 0.9485 1.0508 0.089 Uiso calc U . R 1.0 . .
H H11F 1.1445 1.0151 1.0477 0.089 Uiso calc U . R 1.0 . .
Sb Sb1 0.64724(5) 0.14490(4) 0.89871(5) 0.06577(18) Uani d . . . 1.0 . .
F F1 0.6114(4) 0.1514(4) 0.7987(3) 0.0679(18) Uani d . P G 0.808(8) D 1
F F2 0.5336(3) 0.1176(5) 0.8630(5) 0.124(4) Uani d U P G 0.808(8) D 1
F F3 0.6595(6) 0.2519(3) 0.9618(4) 0.113(4) Uani d . P G 0.808(8) D 1
F F4 0.7604(3) 0.1735(5) 0.9318(5) 0.114(4) Uani d U P G 0.808(8) D 1
F F5 0.6350(5) 0.0365(2) 0.8339(4) 0.123(4) Uani d U P G 0.808(8) D 1
F F6 0.6796(4) 0.1366(4) 0.9939(4) 0.093(2) Uani d . P G 0.808(8) D 1
F F1B 0.628(2) 0.1651(17) 0.8161(16) 0.0679(18) Uani d . P G 0.192(8) D 2
F F2B 0.5655(18) 0.191(2) 0.914(2) 0.124(4) Uani d U P G 0.192(8) D 2
F F3B 0.7300(19) 0.2535(12) 0.9858(18) 0.113(4) Uani d . P G 0.192(8) D 2
F F4B 0.7431(17) 0.114(2) 0.905(2) 0.114(4) Uani d . P G 0.192(8) D 2
F F5B 0.5774(18) 0.0491(13) 0.8332(19) 0.123(4) Uani d U P G 0.192(8) D 2
F F6B 0.6768(19) 0.1386(18) 1.0009(17) 0.093(2) Uani d . P G 0.192(8) D 2
Sb Sb2 0.0360(7) 0.0594(5) 0.6114(6) 0.084(2) Uani d U P G 0.254(12) E -1
F F7 0.0465(16) 0.0339(14) 0.6920(13) 0.151(8) Uiso d . P G 0.254(12) E -1
F F8 -0.0116(15) 0.1364(11) 0.6567(15) 0.151(8) Uiso d . P G 0.254(12) E -1
F F9 -0.0710(9) -0.0164(12) 0.5310(12) 0.151(8) Uiso d . P G 0.254(12) E -1
F F10 0.0798(15) -0.0190(11) 0.5633(16) 0.151(8) Uiso d . P G 0.254(12) E -1
F F11 0.1413(10) 0.1362(12) 0.6889(13) 0.151(8) Uiso d . P G 0.254(12) E -1
F F12 0.0230(18) 0.0872(13) 0.5309(12) 0.151(8) Uiso d . P G 0.254(12) E -1
Sb Sb2B 0.0595(14) 0.0606(9) 0.6185(11) 0.137(6) Uani d . P G 0.180(12) F -2
F F7B 0.062(3) -0.0424(12) 0.560(2) 0.174(13) Uiso d . P G 0.180(12) F -2
F F8B 0.015(2) 0.029(2) 0.670(2) 0.174(13) Uiso d . P G 0.180(12) F -2
F F9B -0.0496(18) 0.031(2) 0.5244(19) 0.174(13) Uiso d . P G 0.180(12) F -2
F F10B 0.100(3) 0.092(2) 0.565(2) 0.174(13) Uiso d . P G 0.180(12) F -2
F F11B 0.1672(15) 0.093(2) 0.7143(18) 0.174(13) Uiso d . P G 0.180(12) F -2
F F12B 0.054(3) 0.1633(13) 0.679(2) 0.174(13) Uiso d . P G 0.180(12) F -2
Sb Sb2C 0.0149(11) 0.0209(11) 0.5400(15) 0.106(7) Uani d U P G 0.066(4) G -3
F F7C 0.086(5) 0.019(5) 0.498(6) 0.15(2) Uiso d . P G 0.066(4) G -3
F F8C 0.086(5) -0.017(5) 0.605(5) 0.15(2) Uiso d . P G 0.066(4) G -3
F F9C -0.049(5) -0.083(2) 0.445(4) 0.15(2) Uiso d . P G 0.066(4) G -3
F F10C -0.058(5) 0.056(5) 0.473(5) 0.15(2) Uiso d . P G 0.066(4) G -3
F F11C 0.077(5) 0.124(2) 0.636(4) 0.15(2) Uiso d . P G 0.066(4) G -3
F F12C -0.055(5) 0.020(5) 0.584(6) 0.15(2) Uiso d . P G 0.066(4) G -3
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
C1 Ag1 C33 . 2_666 123.4(3)
C1 Ag1 C17 . 2_666 123.4(3)
C33 Ag1 C17 2_666 2_666 105.4(3)
C1 Ag1 Ag3 . . 48.61(18)
C33 Ag1 Ag3 2_666 . 156.43(18)
C17 Ag1 Ag3 2_666 . 94.79(18)
C1 Ag1 Ag2 . . 47.72(19)
C33 Ag1 Ag2 2_666 . 99.68(18)
C17 Ag1 Ag2 2_666 . 150.77(19)
Ag3 Ag1 Ag2 . . 57.90(2)
C1 Ag1 Ag5 . 2_666 139.70(19)
C33 Ag1 Ag5 2_666 2_666 39.7(2)
C17 Ag1 Ag5 2_666 2_666 95.9(2)
Ag3 Ag1 Ag5 . 2_666 127.41(3)
Ag2 Ag1 Ag5 . 2_666 93.85(2)
C1 Ag1 Ag4 . 2_666 142.99(19)
C33 Ag1 Ag4 2_666 2_666 92.82(19)
C17 Ag1 Ag4 2_666 2_666 39.7(2)
Ag3 Ag1 Ag4 . 2_666 95.20(3)
Ag2 Ag1 Ag4 . 2_666 125.44(3)
Ag5 Ag1 Ag4 2_666 2_666 64.30(2)
C1 Ag2 C9 . . 128.8(3)
C1 Ag2 C49 . 2_666 120.6(3)
C9 Ag2 C49 . 2_666 101.5(2)
C1 Ag2 C50 . 2_666 108.9(3)
C9 Ag2 C50 . 2_666 95.2(2)
C49 Ag2 C50 2_666 2_666 27.1(3)
C1 Ag2 Ag3 . . 49.31(18)
C9 Ag2 Ag3 . . 102.35(17)
C49 Ag2 Ag3 2_666 . 152.82(19)
C50 Ag2 Ag3 2_666 . 157.94(17)
C1 Ag2 Ag1 . . 47.8(2)
C9 Ag2 Ag1 . . 159.47(19)
C49 Ag2 Ag1 2_666 . 94.86(18)
C50 Ag2 Ag1 2_666 . 104.99(17)
Ag3 Ag2 Ag1 . . 59.23(2)
C1 Ag2 Ag4 . . 148.74(19)
C9 Ag2 Ag4 . . 42.0(2)
C49 Ag2 Ag4 2_666 . 89.24(19)
C50 Ag2 Ag4 2_666 . 102.08(18)
Ag3 Ag2 Ag4 . . 99.92(2)
Ag1 Ag2 Ag4 . . 127.05(3)
C1 Ag3 C41 . . 129.0(3)
C1 Ag3 C25 . . 126.4(3)
C41 Ag3 C25 . . 98.1(3)
C1 Ag3 Ag2 . . 50.34(19)
C41 Ag3 Ag2 . . 160.08(19)
C25 Ag3 Ag2 . . 94.23(17)
C1 Ag3 Ag1 . . 49.7(2)
C41 Ag3 Ag1 . . 100.88(18)
C25 Ag3 Ag1 . . 153.42(18)
Ag2 Ag3 Ag1 . . 62.87(2)
C1 Ag3 Ag6 . . 143.2(2)
C41 Ag3 Ag6 . . 40.8(2)
C25 Ag3 Ag6 . . 88.28(19)
Ag2 Ag3 Ag6 . . 124.62(3)
Ag1 Ag3 Ag6 . . 94.00(3)
C1 Ag3 Ag5 . . 139.88(19)
C41 Ag3 Ag5 . . 89.9(2)
C25 Ag3 Ag5 . . 38.9(2)
Ag2 Ag3 Ag5 . . 89.91(2)
Ag1 Ag3 Ag5 . . 122.48(3)
Ag6 Ag3 Ag5 . . 59.741(19)
C17 Ag4 C9 . . 165.7(3)
C17 Ag4 Ag7 . . 50.0(2)
C9 Ag4 Ag7 . . 126.14(19)
C17 Ag4 Ag8 . . 125.0(2)
C9 Ag4 Ag8 . . 51.56(19)
Ag7 Ag4 Ag8 . . 156.55(3)
C17 Ag4 Ag2 . . 144.5(2)
C9 Ag4 Ag2 . . 48.6(2)
Ag7 Ag4 Ag2 . . 113.28(2)
Ag8 Ag4 Ag2 . . 82.75(2)
C17 Ag4 Ag1 . 2_666 47.4(2)
C9 Ag4 Ag1 . 2_666 144.9(2)
Ag7 Ag4 Ag1 . 2_666 84.34(2)
Ag8 Ag4 Ag1 . 2_666 107.97(2)
Ag2 Ag4 Ag1 . 2_666 107.22(2)
C33 Ag5 C25 . . 164.0(3)
C33 Ag5 Ag8 . . 120.7(2)
C25 Ag5 Ag8 . . 52.1(2)
C33 Ag5 Ag9 . . 49.18(19)
C25 Ag5 Ag9 . . 128.9(2)
Ag8 Ag5 Ag9 . . 152.71(3)
C33 Ag5 Ag1 . 2_666 46.40(19)
C25 Ag5 Ag1 . 2_666 146.7(2)
Ag8 Ag5 Ag1 . 2_666 111.48(3)
Ag9 Ag5 Ag1 . 2_666 79.92(2)
C33 Ag5 Ag6 . . 96.0(2)
C25 Ag5 Ag6 . . 93.6(2)
Ag8 Ag5 Ag6 . . 142.95(3)
Ag9 Ag5 Ag6 . . 57.59(2)
Ag1 Ag5 Ag6 2_666 . 89.55(2)
C33 Ag5 Ag3 . . 148.6(2)
C25 Ag5 Ag3 . . 46.79(19)
Ag8 Ag5 Ag3 . . 84.84(2)
Ag9 Ag5 Ag3 . . 115.39(2)
Ag1 Ag5 Ag3 2_666 . 110.04(2)
Ag6 Ag5 Ag3 . . 58.842(18)
C41 Ag6 C49 . . 165.9(3)
C41 Ag6 Ag7 . 2_666 55.5(2)
C49 Ag6 Ag7 . 2_666 115.54(19)
C41 Ag6 Ag9 . . 131.0(2)
C49 Ag6 Ag9 . . 50.95(18)
Ag7 Ag6 Ag9 2_666 . 152.33(3)
C41 Ag6 Ag3 . . 46.63(18)
C49 Ag6 Ag3 . . 147.3(2)
Ag7 Ag6 Ag3 2_666 . 84.94(2)
Ag9 Ag6 Ag3 . . 119.33(2)
C41 Ag6 Ag5 . . 95.82(19)
C49 Ag6 Ag5 . . 95.8(2)
Ag7 Ag6 Ag5 2_666 . 146.30(3)
Ag9 Ag6 Ag5 . . 59.041(18)
Ag3 Ag6 Ag5 . . 61.42(2)
C17 Ag7 P1 . . 144.13(19)
C17 Ag7 C41 . 2_666 97.1(2)
P1 Ag7 C41 . 2_666 117.91(16)
C17 Ag7 Ag6 . 2_666 97.0(2)
P1 Ag7 Ag6 . 2_666 113.28(5)
C41 Ag7 Ag6 2_666 2_666 43.61(19)
C17 Ag7 Ag4 . . 44.1(2)
P1 Ag7 Ag4 . . 128.14(6)
C41 Ag7 Ag4 2_666 . 100.11(17)
Ag6 Ag7 Ag4 2_666 . 71.03(2)
C25 Ag8 C9 . . 98.9(2)
C25 Ag8 P2 . . 135.37(18)
C9 Ag8 P2 . . 125.73(18)
C25 Ag8 Ag5 . . 44.0(2)
C9 Ag8 Ag5 . . 98.9(2)
P2 Ag8 Ag5 . . 117.62(6)
C25 Ag8 Ag4 . . 98.50(19)
C9 Ag8 Ag4 . . 43.4(2)
P2 Ag8 Ag4 . . 112.27(6)
Ag5 Ag8 Ag4 . . 70.28(2)
C33 Ag9 C49 . . 101.7(3)
C33 Ag9 P3 . . 136.86(19)
C49 Ag9 P3 . . 121.34(18)
C33 Ag9 C34 . . 27.1(3)
C49 Ag9 C34 . . 112.4(2)
P3 Ag9 C34 . . 121.82(18)
C33 Ag9 Ag6 . . 95.2(2)
C49 Ag9 Ag6 . . 43.3(2)
P3 Ag9 Ag6 . . 113.58(6)
C34 Ag9 Ag6 . . 120.43(18)
C33 Ag9 Ag5 . . 41.8(2)
C49 Ag9 Ag5 . . 93.8(2)
P3 Ag9 Ag5 . . 125.20(6)
C34 Ag9 Ag5 . . 67.88(19)
Ag6 Ag9 Ag5 . . 63.37(2)
C57 P1 C64 . . 105.8(3)
C57 P1 C71 . . 105.4(3)
C64 P1 C71 . . 106.8(4)
C57 P1 Ag7 . . 114.7(2)
C64 P1 Ag7 . . 114.6(3)
C71 P1 Ag7 . . 108.9(3)
C92 P2 C78 . . 104.0(4)
C92 P2 C85 . . 108.5(4)
C78 P2 C85 . . 105.7(4)
C92 P2 Ag8 . . 113.3(2)
C78 P2 Ag8 . . 111.6(3)
C85 P2 Ag8 . . 113.1(3)
C113 P3 C99 . . 105.4(4)
C113 P3 C106 . . 105.1(4)
C99 P3 C106 . . 105.7(4)
C113 P3 Ag9 . . 114.0(2)
C99 P3 Ag9 . . 111.6(2)
C106 P3 Ag9 . . 114.3(3)
C2 C1 Ag3 . . 132.4(6)
C2 C1 Ag2 . . 126.7(6)
Ag3 C1 Ag2 . . 80.3(2)
C2 C1 Ag1 . . 132.7(6)
Ag3 C1 Ag1 . . 81.7(3)
Ag2 C1 Ag1 . . 84.5(3)
C1 C2 C3 . . 177.2(8)
C4 C3 C8 . . 119.1(9)
C4 C3 C2 . . 122.0(8)
C8 C3 C2 . . 118.8(8)
C3 C4 C5 . . 120.6(10)
C3 C4 H4 . . 119.7
C5 C4 H4 . . 119.7
C6 C5 C4 . . 119.4(11)
C6 C5 H5 . . 120.3
C4 C5 H5 . . 120.3
C5 C6 C7 . . 121.1(11)
C5 C6 H6 . . 119.5
C7 C6 H6 . . 119.5
C8 C7 C6 . . 118.6(11)
C8 C7 H7 . . 120.7
C6 C7 H7 . . 120.7
C7 C8 C3 . . 121.1(10)
C7 C8 H8 . . 119.4
C3 C8 H8 . . 119.4
C10 C9 Ag4 . . 165.7(7)
C10 C9 Ag2 . . 102.2(6)
Ag4 C9 Ag2 . . 89.4(3)
C10 C9 Ag8 . . 96.3(5)
Ag4 C9 Ag8 . . 85.1(3)
Ag2 C9 Ag8 . . 118.8(3)
C9 C10 C11 . . 179.3(9)
C16 C11 C12 . . 119.0(9)
C16 C11 C10 . . 121.1(8)
C12 C11 C10 . . 119.8(9)
C11 C12 C13 . . 120.0(10)
C11 C12 H12 . . 120.0
C13 C12 H12 . . 120.0
C14 C13 C12 . . 118.9(11)
C14 C13 H13 . . 120.5
C12 C13 H13 . . 120.5
C15 C14 C13 . . 120.7(11)
C15 C14 H14 . . 119.6
C13 C14 H14 . . 119.6
C14 C15 C16 . . 120.8(12)
C14 C15 H15 . . 119.6
C16 C15 H15 . . 119.6
C15 C16 C11 . . 120.5(10)
C15 C16 H16 . . 119.8
C11 C16 H16 . . 119.8
C18 C17 Ag4 . . 166.7(7)
C18 C17 Ag7 . . 97.6(6)
Ag4 C17 Ag7 . . 85.9(3)
C18 C17 Ag1 . 2_666 95.2(6)
Ag4 C17 Ag1 . 2_666 92.9(3)
Ag7 C17 Ag1 . 2_666 126.7(3)
C17 C18 C19 . . 176.2(9)
C17 C18 C19B . . 168.2(12)
C20 C19 C24 . . 120.0
C20 C19 C18 . . 120.0(9)
C24 C19 C18 . . 119.9(9)
C19 C20 C21 . . 120.0
C19 C20 H20 . . 120.0
C21 C20 H20 . . 120.0
C20 C21 C22 . . 120.0
C20 C21 H21 . . 120.0
C22 C21 H21 . . 120.0
C23 C22 C21 . . 120.0
C23 C22 H22 . . 120.0
C21 C22 H22 . . 120.0
C22 C23 C24 . . 120.0
C22 C23 H23 . . 120.0
C24 C23 H23 . . 120.0
C23 C24 C19 . . 120.0
C23 C24 H24 . . 120.0
C19 C24 H24 . . 120.0
C20B C19B C24B . . 120.0
C20B C19B C18 . . 113.8(17)
C24B C19B C18 . . 125.3(18)
C21B C20B C19B . . 120.0
C21B C20B H20B . . 120.0
C19B C20B H20B . . 120.0
C20B C21B C22B . . 120.0
C20B C21B H21B . . 120.0
C22B C21B H21B . . 120.0
C23B C22B C21B . . 120.0
C23B C22B H22B . . 120.0
C21B C22B H22B . . 120.0
C24B C23B C22B . . 120.0
C24B C23B H23B . . 120.0
C22B C23B H23B . . 120.0
C23B C24B C19B . . 120.0
C23B C24B H24B . . 120.0
C19B C24B H24B . . 120.0
C26 C25 Ag5 . . 168.6(6)
C26 C25 Ag8 . . 98.3(6)
Ag5 C25 Ag8 . . 83.9(3)
C26 C25 Ag3 . . 93.5(5)
Ag5 C25 Ag3 . . 94.3(3)
Ag8 C25 Ag3 . . 125.3(3)
C25 C26 C27 . . 177.3(8)
C32 C27 C28 . . 117.6(9)
C32 C27 C26 . . 122.1(9)
C28 C27 C26 . . 120.3(7)
C29 C28 C27 . . 121.0(9)
C29 C28 H28 . . 119.5
C27 C28 H28 . . 119.5
C30 C29 C28 . . 120.2(10)
C30 C29 H29 . . 119.9
C28 C29 H29 . . 119.9
C29 C30 C31 . . 120.7(11)
C29 C30 H30 . . 119.6
C31 C30 H30 . . 119.6
C30 C31 C32 . . 119.8(10)
C30 C31 H31 . . 120.1
C32 C31 H31 . . 120.1
C27 C32 C31 . . 120.5(11)
C27 C32 H32 . . 119.8
C31 C32 H32 . . 119.8
C34 C33 Ag5 . . 160.8(7)
C34 C33 Ag1 . 2_666 101.5(6)
Ag5 C33 Ag1 . 2_666 93.9(3)
C34 C33 Ag9 . . 93.0(5)
Ag5 C33 Ag9 . . 89.0(3)
Ag1 C33 Ag9 2_666 . 120.2(3)
C33 C34 C35 . . 162.2(16)
C33 C34 C35B . . 173.8(9)
C33 C34 Ag9 . . 59.9(5)
C35 C34 Ag9 . . 116.5(11)
C35B C34 Ag9 . . 123.4(6)
C36 C35 C40 . . 120.0
C36 C35 C34 . . 132.(2)
C40 C35 C34 . . 108.(2)
C35 C36 C37 . . 120.0
C35 C36 H36 . . 120.0
C37 C36 H36 . . 120.0
C36 C37 C38 . . 120.0
C36 C37 H37 . . 120.0
C38 C37 H37 . . 120.0
C39 C38 C37 . . 120.0
C39 C38 H38 . . 120.0
C37 C38 H38 . . 120.0
C38 C39 C40 . . 120.0
C38 C39 H39 . . 120.0
C40 C39 H39 . . 120.0
C39 C40 C35 . . 120.0
C39 C40 H40 . . 120.0
C35 C40 H40 . . 120.0
C36B C35B C40B . . 120.0
C36B C35B C34 . . 115.5(7)
C40B C35B C34 . . 124.5(7)
C37B C36B C35B . . 120.0
C37B C36B H36B . . 120.0
C35B C36B H36B . . 120.0
C36B C37B C38B . . 120.0
C36B C37B H37B . . 120.0
C38B C37B H37B . . 120.0
C39B C38B C37B . . 120.0
C39B C38B H38B . . 120.0
C37B C38B H38B . . 120.0
C38B C39B C40B . . 120.0
C38B C39B H39B . . 120.0
C40B C39B H39B . . 120.0
C39B C40B C35B . . 120.0
C39B C40B H40B . . 120.0
C35B C40B H40B . . 120.0
C42 C41 Ag6 . . 168.8(6)
C42 C41 Ag3 . . 98.5(6)
Ag6 C41 Ag3 . . 92.6(3)
C42 C41 Ag7 . 2_666 91.8(5)
Ag6 C41 Ag7 . 2_666 80.9(3)
Ag3 C41 Ag7 . 2_666 120.2(3)
C41 C42 C43 . . 176.5(9)
C41 C42 C43B . . 169.3(17)
C44 C43 C48 . . 120.0
C44 C43 C42 . . 120.6(9)
C48 C43 C42 . . 119.2(9)
C45 C44 C43 . . 120.0
C45 C44 H44 . . 120.0
C43 C44 H44 . . 120.0
C44 C45 C46 . . 120.0
C44 C45 H45 . . 120.0
C46 C45 H45 . . 120.0
C47 C46 C45 . . 120.0
C47 C46 H46 . . 120.0
C45 C46 H46 . . 120.0
C46 C47 C48 . . 120.0
C46 C47 H47 . . 120.0
C48 C47 H47 . . 120.0
C47 C48 C43 . . 120.0
C47 C48 H48 . . 120.0
C43 C48 H48 . . 120.0
C44B C43B C48B . . 120.0
C44B C43B C42 . . 121.(3)
C48B C43B C42 . . 119.(3)
C43B C44B C45B . . 120.0
C43B C44B H44B . . 120.0
C45B C44B H44B . . 120.0
C46B C45B C44B . . 120.0
C46B C45B H45B . . 120.0
C44B C45B H45B . . 120.0
C47B C46B C45B . . 120.0
C47B C46B H46B . . 120.0
C45B C46B H46B . . 120.0
C46B C47B C48B . . 120.0
C46B C47B H47B . . 120.0
C48B C47B H47B . . 120.0
C47B C48B C43B . . 120.0
C47B C48B H48B . . 120.0
C43B C48B H48B . . 120.0
C50 C49 Ag6 . . 162.5(7)
C50 C49 Ag9 . . 103.5(6)
Ag6 C49 Ag9 . . 85.7(3)
C50 C49 Ag2 . 2_666 88.9(5)
Ag6 C49 Ag2 . 2_666 98.9(3)
Ag9 C49 Ag2 . 2_666 122.2(3)
C49 C50 C51 . . 177.4(8)
C49 C50 Ag2 . 2_666 64.0(5)
C51 C50 Ag2 . 2_666 114.9(5)
C52 C51 C56 . . 119.6(8)
C52 C51 C50 . . 121.9(8)
C56 C51 C50 . . 118.5(7)
C51 C52 C53 . . 119.7(9)
C51 C52 H52 . . 120.2
C53 C52 H52 . . 120.2
C54 C53 C52 . . 120.5(10)
C54 C53 H53 . . 119.8
C52 C53 H53 . . 119.8
C53 C54 C55 . . 121.7(10)
C53 C54 H54 . . 119.1
C55 C54 H54 . . 119.1
C54 C55 C56 . . 118.5(10)
C54 C55 H55 . . 120.7
C56 C55 H55 . . 120.7
C55 C56 C51 . . 120.0(9)
C55 C56 H56 . . 120.0
C51 C56 H56 . . 120.0
C62 C57 C58 . . 117.7(8)
C62 C57 P1 . . 118.7(6)
C58 C57 P1 . . 123.6(6)
C59 C58 C57 . . 119.4(8)
C59 C58 H58 . . 120.3
C57 C58 H58 . . 120.3
C60 C59 C58 . . 123.7(8)
C60 C59 H59 . . 118.2
C58 C59 H59 . . 118.2
C59 C60 C61 . . 116.2(8)
C59 C60 C63 . . 122.2(9)
C61 C60 C63 . . 121.6(9)
C60 C61 C62 . . 122.3(8)
C60 C61 H61 . . 118.8
C62 C61 H61 . . 118.8
C61 C62 C57 . . 120.7(8)
C61 C62 H62 . . 119.7
C57 C62 H62 . . 119.7
C60 C63 H63A . . 109.5
C60 C63 H63B . . 109.5
H63A C63 H63B . . 109.5
C60 C63 H63C . . 109.5
H63A C63 H63C . . 109.5
H63B C63 H63C . . 109.5
C69 C64 C65 . . 118.3(7)
C69 C64 P1 . . 118.5(6)
C65 C64 P1 . . 123.0(6)
C64 C65 C66 . . 121.2(8)
C64 C65 H65 . . 119.4
C66 C65 H65 . . 119.4
C67 C66 C65 . . 120.0(8)
C67 C66 H66 . . 120.0
C65 C66 H66 . . 120.0
C68 C67 C66 . . 118.5(8)
C68 C67 C70 . . 121.0(9)
C66 C67 C70 . . 120.4(8)
C69 C68 C67 . . 121.4(8)
C69 C68 H68 . . 119.3
C67 C68 H68 . . 119.3
C68 C69 C64 . . 120.5(8)
C68 C69 H69 . . 119.7
C64 C69 H69 . . 119.7
C67 C70 H70A . . 109.5
C67 C70 H70B . . 109.5
H70A C70 H70B . . 109.5
C67 C70 H70C . . 109.5
H70A C70 H70C . . 109.5
H70B C70 H70C . . 109.5
C76 C71 C72 . . 117.1(8)
C76 C71 P1 . . 124.8(7)
C72 C71 P1 . . 117.8(6)
C73 C72 C71 . . 121.1(8)
C73 C72 H72 . . 119.4
C71 C72 H72 . . 119.4
C74 C73 C72 . . 121.4(9)
C74 C73 H73 . . 119.3
C72 C73 H73 . . 119.3
C75 C74 C73 . . 117.4(8)
C75 C74 C77 . . 122.1(8)
C73 C74 C77 . . 120.5(9)
C74 C75 C76 . . 122.0(8)
C74 C75 H75 . . 119.0
C76 C75 H75 . . 119.0
C71 C76 C75 . . 121.0(8)
C71 C76 H76 . . 119.5
C75 C76 H76 . . 119.5
C74 C77 H77A . . 109.5
C74 C77 H77B . . 109.5
H77A C77 H77B . . 109.5
C74 C77 H77C . . 109.5
H77A C77 H77C . . 109.5
H77B C77 H77C . . 109.5
C79 C78 C83 . . 117.1(8)
C79 C78 P2 . . 119.9(6)
C83 C78 P2 . . 122.9(7)
C78 C79 C80 . . 121.9(8)
C78 C79 H79 . . 119.0
C80 C79 H79 . . 119.0
C81 C80 C79 . . 121.0(9)
C81 C80 H80 . . 119.5
C79 C80 H80 . . 119.5
C80 C81 C82 . . 117.8(8)
C80 C81 C84 . . 122.6(9)
C82 C81 C84 . . 119.6(8)
C83 C82 C81 . . 121.5(8)
C83 C82 H82 . . 119.2
C81 C82 H82 . . 119.2
C82 C83 C78 . . 120.5(8)
C82 C83 H83 . . 119.7
C78 C83 H83 . . 119.7
C81 C84 H84A . . 109.5
C81 C84 H84B . . 109.5
H84A C84 H84B . . 109.5
C81 C84 H84C . . 109.5
H84A C84 H84C . . 109.5
H84B C84 H84C . . 109.5
C90 C85 C86 . . 117.5(8)
C90 C85 P2 . . 119.2(6)
C86 C85 P2 . . 123.2(6)
C85 C86 C87 . . 120.7(8)
C85 C86 H86 . . 119.7
C87 C86 H86 . . 119.7
C88 C87 C86 . . 121.9(8)
C88 C87 H87 . . 119.0
C86 C87 H87 . . 119.0
C89 C88 C87 . . 116.0(9)
C89 C88 C91 . . 122.5(10)
C87 C88 C91 . . 121.4(10)
C90 C89 C88 . . 123.1(10)
C90 C89 H89 . . 118.4
C88 C89 H89 . . 118.4
C89 C90 C85 . . 120.6(9)
C89 C90 H90 . . 119.7
C85 C90 H90 . . 119.7
C88 C91 H91A . . 109.5
C88 C91 H91B . . 109.5
H91A C91 H91B . . 109.5
C88 C91 H91C . . 109.5
H91A C91 H91C . . 109.5
H91B C91 H91C . . 109.5
C97 C92 C93 . . 119.0(8)
C97 C92 P2 . . 118.2(6)
C93 C92 P2 . . 122.7(6)
C94 C93 C92 . . 119.9(8)
C94 C93 H93 . . 120.0
C92 C93 H93 . . 120.0
C93 C94 C95 . . 120.9(8)
C93 C94 H94 . . 119.5
C95 C94 H94 . . 119.5
C96 C95 C94 . . 118.4(8)
C96 C95 C98 . . 121.0(8)
C94 C95 C98 . . 120.7(8)
C95 C96 C97 . . 121.4(8)
C95 C96 H96 . . 119.3
C97 C96 H96 . . 119.3
C92 C97 C96 . . 120.4(8)
C92 C97 H97 . . 119.8
C96 C97 H97 . . 119.8
C95 C98 H98A . . 109.5
C95 C98 H98B . . 109.5
H98A C98 H98B . . 109.5
C95 C98 H98C . . 109.5
H98A C98 H98C . . 109.5
H98B C98 H98C . . 109.5
C100 C99 C104 . . 117.9(8)
C100 C99 P3 . . 119.4(6)
C104 C99 P3 . . 122.7(7)
C99 C100 C101 . . 121.9(8)
C99 C100 H100 . . 119.0
C101 C100 H100 . . 119.0
C102 C101 C100 . . 119.4(9)
C102 C101 H101 . . 120.3
C100 C101 H101 . . 120.3
C101 C102 C103 . . 118.9(9)
C101 C102 C105 . . 121.8(10)
C103 C102 C105 . . 119.3(9)
C104 C103 C102 . . 121.2(9)
C104 C103 H103 . . 119.4
C102 C103 H103 . . 119.4
C103 C104 C99 . . 120.5(9)
C103 C104 H104 . . 119.7
C99 C104 H104 . . 119.7
C102 C105 H10A . . 109.5
C102 C105 H10B . . 109.5
H10A C105 H10B . . 109.5
C102 C105 H10C . . 109.5
H10A C105 H10C . . 109.5
H10B C105 H10C . . 109.5
C111 C106 C107 . . 118.4(8)
C111 C106 P3 . . 119.4(6)
C107 C106 P3 . . 122.0(7)
C106 C107 C108 . . 118.1(11)
C106 C107 H107 . . 120.9
C108 C107 H107 . . 120.9
C107 C108 C109 . . 123.0(11)
C107 C108 H108 . . 118.5
C109 C108 H108 . . 118.5
C110 C109 C108 . . 115.8(11)
C110 C109 C112 . . 122.9(12)
C108 C109 C112 . . 121.2(11)
C109 C110 C111 . . 121.4(10)
C109 C110 H110 . . 119.3
C111 C110 H110 . . 119.3
C106 C111 C110 . . 122.5(9)
C106 C111 H111 . . 118.7
C110 C111 H111 . . 118.7
C109 C112 H11A . . 109.5
C109 C112 H11B . . 109.5
H11A C112 H11B . . 109.5
C109 C112 H11C . . 109.5
H11A C112 H11C . . 109.5
H11B C112 H11C . . 109.5
C118 C113 C114 . . 117.6(7)
C118 C113 P3 . . 119.2(5)
C114 C113 P3 . . 123.2(6)
C115 C114 C113 . . 120.1(8)
C115 C114 H114 . . 120.0
C113 C114 H114 . . 120.0
C116 C115 C114 . . 122.2(7)
C116 C115 H115 . . 118.9
C114 C115 H115 . . 118.9
C117 C116 C115 . . 117.7(7)
C117 C116 C119 . . 121.3(8)
C115 C116 C119 . . 120.9(7)
C116 C117 C118 . . 120.6(8)
C116 C117 H117 . . 119.7
C118 C117 H117 . . 119.7
C117 C118 C113 . . 121.6(7)
C117 C118 H118 . . 119.2
C113 C118 H118 . . 119.2
C116 C119 H11D . . 109.5
C116 C119 H11E . . 109.5
H11D C119 H11E . . 109.5
C116 C119 H11F . . 109.5
H11D C119 H11F . . 109.5
H11E C119 H11F . . 109.5
F5B Sb1 F1B . . 99.4(10)
F6 Sb1 F3 . . 92.4(2)
F6 Sb1 F2 . . 92.05(19)
F3 Sb1 F2 . . 91.48(18)
F6 Sb1 F4 . . 89.89(17)
F3 Sb1 F4 . . 87.95(17)
F2 Sb1 F4 . . 178.0(2)
F5B Sb1 F2B . . 92.6(9)
F1B Sb1 F2B . . 89.9(7)
F5B Sb1 F4B . . 96.0(9)
F1B Sb1 F4B . . 94.6(10)
F2B Sb1 F4B . . 169.4(12)
F6 Sb1 F5 . . 88.21(16)
F3 Sb1 F5 . . 179.4(3)
F2 Sb1 F5 . . 88.77(17)
F4 Sb1 F5 . . 91.78(18)
F6 Sb1 F1 . . 178.6(2)
F3 Sb1 F1 . . 88.50(15)
F2 Sb1 F1 . . 86.85(16)
F4 Sb1 F1 . . 91.21(19)
F5 Sb1 F1 . . 90.92(19)
F5B Sb1 F6B . . 88.4(8)
F1B Sb1 F6B . . 172.0(12)
F2B Sb1 F6B . . 88.0(9)
F4B Sb1 F6B . . 86.1(7)
F5B Sb1 F3B . . 173.1(12)
F1B Sb1 F3B . . 87.5(8)
F2B Sb1 F3B . . 86.9(8)
F4B Sb1 F3B . . 83.8(8)
F6B Sb1 F3B . . 84.7(8)
F7 Sb2 F10 . . 92.8
F7 Sb2 F11 . . 92.7
F10 Sb2 F11 . . 92.7
F7 Sb2 F9 . . 89.1
F10 Sb2 F9 . . 87.7
F11 Sb2 F9 . . 178.1
F7 Sb2 F8 . . 87.7
F10 Sb2 F8 . . 178.2
F11 Sb2 F8 . . 89.0
F9 Sb2 F8 . . 90.5
F7 Sb2 F12 . . 178.1
F10 Sb2 F12 . . 89.0
F11 Sb2 F12 . . 87.6
F9 Sb2 F12 . . 90.5
F8 Sb2 F12 . . 90.5
F7B Sb2B F10B . . 92.8
F7B Sb2B F11B . . 92.7
F10B Sb2B F11B . . 92.7
F7B Sb2B F9B . . 89.1
F10B Sb2B F9B . . 87.7
F11B Sb2B F9B . . 178.1
F7B Sb2B F8B . . 87.7
F10B Sb2B F8B . . 178.2
F11B Sb2B F8B . . 89.0
F9B Sb2B F8B . . 90.5
F7B Sb2B F12B . . 178.2
F10B Sb2B F12B . . 89.0
F11B Sb2B F12B . . 87.6
F9B Sb2B F12B . . 90.5
F8B Sb2B F12B . . 90.5
F7C Sb2C F10C . . 92.8
F7C Sb2C F11C . . 92.7
F10C Sb2C F11C . . 92.7
F7C Sb2C F9C . . 89.1
F10C Sb2C F9C . . 87.7
F11C Sb2C F9C . . 178.1
F7C Sb2C F8C . . 87.7
F10C Sb2C F8C . . 178.16(19)
F11C Sb2C F8C . . 89.0
F9C Sb2C F8C . . 90.5
F7C Sb2C F12C . . 178.1
F10C Sb2C F12C . . 89.0
F11C Sb2C F12C . . 87.6
F9C Sb2C F12C . . 90.53(6)
F8C Sb2C F12C . . 90.5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Ag1 C1 . 2.273(8)
Ag1 C33 2_666 2.334(7)
Ag1 C17 2_666 2.401(7)
Ag1 Ag3 . 2.9476(8)
Ag1 Ag2 . 3.0530(9)
Ag1 Ag5 2_666 3.2160(9)
Ag1 Ag4 2_666 3.2573(10)
Ag2 C1 . 2.269(8)
Ag2 C9 . 2.351(7)
Ag2 C49 2_666 2.379(7)
Ag2 C50 2_666 2.646(7)
Ag2 Ag3 . 2.9060(8)
Ag2 Ag4 . 3.1324(9)
Ag3 C1 . 2.235(7)
Ag3 C41 . 2.319(7)
Ag3 C25 . 2.391(7)
Ag3 Ag6 . 3.1876(9)
Ag3 Ag5 . 3.2710(9)
Ag4 C17 . 2.082(9)
Ag4 C9 . 2.095(9)
Ag4 Ag7 . 2.9856(9)
Ag4 Ag8 . 3.0390(9)
Ag4 Ag1 2_666 3.2573(10)
Ag5 C33 . 2.059(8)
Ag5 C25 . 2.059(8)
Ag5 Ag8 . 2.9450(9)
Ag5 Ag9 . 3.0867(9)
Ag5 Ag1 2_666 3.2160(9)
Ag5 Ag6 . 3.2175(9)
Ag6 C41 . 2.084(8)
Ag6 C49 . 2.092(9)
Ag6 Ag7 2_666 2.9842(9)
Ag6 Ag9 . 3.0389(9)
Ag7 C17 . 2.294(7)
Ag7 P1 . 2.4046(19)
Ag7 C41 2_666 2.490(7)
Ag7 Ag6 2_666 2.9841(9)
Ag8 C25 . 2.337(7)
Ag8 C9 . 2.389(7)
Ag8 P2 . 2.4035(19)
Ag9 C33 . 2.336(7)
Ag9 C49 . 2.367(7)
Ag9 P3 . 2.409(2)
Ag9 C34 . 2.697(8)
P1 C57 . 1.820(8)
P1 C64 . 1.823(8)
P1 C71 . 1.827(8)
P2 C92 . 1.814(8)
P2 C78 . 1.815(8)
P2 C85 . 1.817(8)
P3 C113 . 1.813(8)
P3 C99 . 1.819(9)
P3 C106 . 1.826(8)
C1 C2 . 1.216(10)
C2 C3 . 1.448(11)
C3 C4 . 1.368(12)
C3 C8 . 1.405(12)
C4 C5 . 1.389(14)
C4 H4 . 0.95
C5 C6 . 1.382(17)
C5 H5 . 0.95
C6 C7 . 1.389(17)
C6 H6 . 0.95
C7 C8 . 1.374(14)
C7 H7 . 0.95
C8 H8 . 0.95
C9 C10 . 1.205(11)
C10 C11 . 1.454(13)
C11 C16 . 1.390(13)
C11 C12 . 1.394(12)
C12 C13 . 1.409(15)
C12 H12 . 0.95
C13 C14 . 1.399(17)
C13 H13 . 0.95
C14 C15 . 1.349(16)
C14 H14 . 0.95
C15 C16 . 1.386(14)
C15 H15 . 0.95
C16 H16 . 0.95
C17 C18 . 1.220(12)
C17 Ag1 2_666 2.401(7)
C18 C19 . 1.441(13)
C18 C19B . 1.46(2)
C19 C20 . 1.39
C19 C24 . 1.39
C20 C21 . 1.39
C20 H20 . 0.95
C21 C22 . 1.39
C21 H21 . 0.95
C22 C23 . 1.39
C22 H22 . 0.95
C23 C24 . 1.39
C23 H23 . 0.95
C24 H24 . 0.95
C19B C20B . 1.39
C19B C24B . 1.39
C20B C21B . 1.39
C20B H20B . 0.95
C21B C22B . 1.39
C21B H21B . 0.95
C22B C23B . 1.39
C22B H22B . 0.95
C23B C24B . 1.39
C23B H23B . 0.95
C24B H24B . 0.95
C25 C26 . 1.224(11)
C26 C27 . 1.461(12)
C27 C32 . 1.383(12)
C27 C28 . 1.391(12)
C28 C29 . 1.369(13)
C28 H28 . 0.95
C29 C30 . 1.349(14)
C29 H29 . 0.95
C30 C31 . 1.358(16)
C30 H30 . 0.95
C31 C32 . 1.385(15)
C31 H31 . 0.95
C32 H32 . 0.95
C33 C34 . 1.229(11)
C33 Ag1 2_666 2.334(7)
C34 C35 . 1.41(2)
C34 C35B . 1.483(11)
C35 C36 . 1.39
C35 C40 . 1.39
C36 C37 . 1.39
C36 H36 . 0.95
C37 C38 . 1.39
C37 H37 . 0.95
C38 C39 . 1.39
C38 H38 . 0.95
C39 C40 . 1.39
C39 H39 . 0.95
C40 H40 . 0.95
C35B C36B . 1.39
C35B C40B . 1.39
C36B C37B . 1.39
C36B H36B . 0.95
C37B C38B . 1.39
C37B H37B . 0.95
C38B C39B . 1.39
C38B H38B . 0.95
C39B C40B . 1.39
C39B H39B . 0.95
C40B H40B . 0.95
C41 C42 . 1.203(11)
C41 Ag7 2_666 2.490(7)
C42 C43 . 1.453(14)
C42 C43B . 1.49(3)
C43 C44 . 1.39
C43 C48 . 1.39
C44 C45 . 1.39
C44 H44 . 0.95
C45 C46 . 1.39
C45 H45 . 0.95
C46 C47 . 1.39
C46 H46 . 0.95
C47 C48 . 1.39
C47 H47 . 0.95
C48 H48 . 0.95
C43B C44B . 1.39
C43B C48B . 1.39
C44B C45B . 1.39
C44B H44B . 0.95
C45B C46B . 1.39
C45B H45B . 0.95
C46B C47B . 1.39
C46B H46B . 0.95
C47B C48B . 1.39
C47B H47B . 0.95
C48B H48B . 0.95
C49 C50 . 1.205(11)
C49 Ag2 2_666 2.379(7)
C50 C51 . 1.431(12)
C50 Ag2 2_666 2.646(7)
C51 C52 . 1.372(11)
C51 C56 . 1.410(11)
C52 C53 . 1.392(14)
C52 H52 . 0.95
C53 C54 . 1.360(15)
C53 H53 . 0.95
C54 C55 . 1.373(15)
C54 H54 . 0.95
C55 C56 . 1.401(12)
C55 H55 . 0.95
C56 H56 . 0.95
C57 C62 . 1.394(11)
C57 C58 . 1.405(11)
C58 C59 . 1.383(12)
C58 H58 . 0.95
C59 C60 . 1.376(13)
C59 H59 . 0.95
C60 C61 . 1.383(13)
C60 C63 . 1.500(13)
C61 C62 . 1.386(12)
C61 H61 . 0.95
C62 H62 . 0.95
C63 H63A . 0.98
C63 H63B . 0.98
C63 H63C . 0.98
C64 C69 . 1.380(11)
C64 C65 . 1.385(10)
C65 C66 . 1.390(12)
C65 H65 . 0.95
C66 C67 . 1.383(13)
C66 H66 . 0.95
C67 C68 . 1.381(12)
C67 C70 . 1.534(12)
C68 C69 . 1.379(11)
C68 H68 . 0.95
C69 H69 . 0.95
C70 H70A . 0.98
C70 H70B . 0.98
C70 H70C . 0.98
C71 C76 . 1.368(11)
C71 C72 . 1.394(11)
C72 C73 . 1.384(13)
C72 H72 . 0.95
C73 C74 . 1.377(12)
C73 H73 . 0.95
C74 C75 . 1.362(12)
C74 C77 . 1.516(12)
C75 C76 . 1.395(12)
C75 H75 . 0.95
C76 H76 . 0.95
C77 H77A . 0.98
C77 H77B . 0.98
C77 H77C . 0.98
C78 C79 . 1.382(11)
C78 C83 . 1.412(10)
C79 C80 . 1.384(12)
C79 H79 . 0.95
C80 C81 . 1.380(12)
C80 H80 . 0.95
C81 C82 . 1.392(13)
C81 C84 . 1.504(12)
C82 C83 . 1.380(12)
C82 H82 . 0.95
C83 H83 . 0.95
C84 H84A . 0.98
C84 H84B . 0.98
C84 H84C . 0.98
C85 C90 . 1.380(12)
C85 C86 . 1.383(11)
C86 C87 . 1.389(12)
C86 H86 . 0.95
C87 C88 . 1.378(14)
C87 H87 . 0.95
C88 C89 . 1.374(14)
C88 C91 . 1.518(13)
C89 C90 . 1.370(13)
C89 H89 . 0.95
C90 H90 . 0.95
C91 H91A . 0.98
C91 H91B . 0.98
C91 H91C . 0.98
C92 C97 . 1.387(10)
C92 C93 . 1.403(11)
C93 C94 . 1.391(12)
C93 H93 . 0.95
C94 C95 . 1.398(12)
C94 H94 . 0.95
C95 C96 . 1.381(12)
C95 C98 . 1.522(12)
C96 C97 . 1.389(12)
C96 H96 . 0.95
C97 H97 . 0.95
C98 H98A . 0.98
C98 H98B . 0.98
C98 H98C . 0.98
C99 C100 . 1.357(11)
C99 C104 . 1.397(11)
C100 C101 . 1.408(13)
C100 H100 . 0.95
C101 C102 . 1.370(13)
C101 H101 . 0.95
C102 C103 . 1.382(14)
C102 C105 . 1.537(14)
C103 C104 . 1.372(13)
C103 H103 . 0.95
C104 H104 . 0.95
C105 H10A . 0.98
C105 H10B . 0.98
C105 H10C . 0.98
C106 C111 . 1.357(12)
C106 C107 . 1.389(12)
C107 C108 . 1.394(15)
C107 H107 . 0.95
C108 C109 . 1.406(17)
C108 H108 . 0.95
C109 C110 . 1.357(15)
C109 C112 . 1.518(16)
C110 C111 . 1.377(13)
C110 H110 . 0.95
C111 H111 . 0.95
C112 H11A . 0.98
C112 H11B . 0.98
C112 H11C . 0.98
C113 C118 . 1.390(10)
C113 C114 . 1.397(10)
C114 C115 . 1.383(11)
C114 H114 . 0.95
C115 C116 . 1.383(11)
C115 H115 . 0.95
C116 C117 . 1.383(11)
C116 C119 . 1.504(11)
C117 C118 . 1.389(10)
C117 H117 . 0.95
C118 H118 . 0.95
C119 H11D . 0.98
C119 H11E . 0.98
C119 H11F . 0.98
Sb1 F5B . 1.732(18)
Sb1 F1B . 1.773(18)
Sb1 F6 . 1.823(4)
Sb1 F3 . 1.841(4)
Sb1 F2 . 1.850(4)
Sb1 F4 . 1.857(4)
Sb1 F2B . 1.860(19)
Sb1 F4B . 1.863(19)
Sb1 F5 . 1.866(4)
Sb1 F1 . 1.884(4)
Sb1 F6B . 1.943(19)
Sb1 F3B . 1.981(19)
Sb2 F7 . 1.8463
Sb2 F10 . 1.8467
Sb2 F11 . 1.8472
Sb2 F9 . 1.8602
Sb2 F8 . 1.8606
Sb2 F12 . 1.8611
Sb2B F7B . 1.8463
Sb2B F10B . 1.8468
Sb2B F11B . 1.8473
Sb2B F9B . 1.8602
Sb2B F8B . 1.8606
Sb2B F12B . 1.8611
Sb2C F7C . 1.8463
Sb2C F10C . 1.8468
Sb2C F11C . 1.8472
Sb2C F9C . 1.8601
Sb2C F8C . 1.8606
Sb2C F12C . 1.8611
