#------------------------------------------------------------------------------
#$Date: 2019-11-17 13:26:47 +0200 (Sun, 17 Nov 2019) $
#$Revision: 230156 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/54/90/1549071.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1549071
loop_
_publ_author_name
'Lin, Yan-Ru'
'Kishore, Pilli V. V. N.'
'Liao, Jian-Hong'
'Kahlal, Samia'
'Liu, Yu-Chiao'
'Chiang, Ming-Hsi'
'Saillard, Jean-Yves'
'Liu, C. W.'
_publ_section_title
;
 Synthesis, structural characterization and transformation of an
 eight-electron superatomic alloy,
 [Au@Ag₁₉{S₂P(OPr)₂}₁₂].
;
_journal_issue                   15
_journal_name_full               Nanoscale
_journal_page_first              6855
_journal_page_last               6860
_journal_paper_doi               10.1039/c8nr00172c
_journal_volume                  10
_journal_year                    2018
_chemical_formula_sum            'C75 H175 Ag19 Au O24 P12 S24'
_chemical_formula_weight         4848.72
_chemical_properties_physical    Heat-sensitive
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_block_doi                 10.5517/ccdc.csd.cc1q5rk6
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2017-11-08 deposited with the CCDC.
2018-03-13 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 110.3727(6)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   29.6903(7)
_cell_length_b                   17.3784(4)
_cell_length_c                   30.3868(6)
_cell_measurement_reflns_used    9834
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      25.68
_cell_measurement_theta_min      2.16
_cell_volume                     14697.9(6)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0273
_diffrn_reflns_av_unetI/netI     0.0362
_diffrn_reflns_Laue_measured_fraction_full 0.986
_diffrn_reflns_Laue_measured_fraction_max 0.986
_diffrn_reflns_limit_h_max       35
_diffrn_reflns_limit_h_min       -35
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       35
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            58750
_diffrn_reflns_point_group_measured_fraction_full 0.986
_diffrn_reflns_point_group_measured_fraction_max 0.986
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.434
_exptl_absorpt_coefficient_mu    3.984
_exptl_absorpt_correction_T_max  0.7453
_exptl_absorpt_correction_T_min  0.5383
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.191
_exptl_crystal_description       plate
_exptl_crystal_F_000             9412
_exptl_crystal_size_max          0.19
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.711
_refine_diff_density_min         -1.634
_refine_diff_density_rms         0.194
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.033
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1432
_refine_ls_number_reflns         25525
_refine_ls_number_restraints     435
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.0574
_refine_ls_R_factor_gt           0.0426
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0386P)²+216.6700P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1012
_refine_ls_wR_factor_ref         0.1153
_reflns_Friedel_coverage         0.000
_reflns_number_gt                20994
_reflns_number_total             25525
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c8nr00172c2.cif
_cod_data_source_block           1
_cod_depositor_comments          'Adding full bibliography for 1549071.cif.'
_cod_database_code               1549071
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.23442(2) 0.63678(4) 0.23074(2) 0.02659(14) Uani 1 1 d . . . . .
Ag2 Ag 0.17925(2) 0.54050(4) 0.15249(2) 0.02870(15) Uani 1 1 d . . . . .
Ag3 Ag 0.15317(2) 0.55033(4) 0.23573(2) 0.02627(14) Uani 1 1 d . . . . .
Ag4 Ag 0.28675(2) 0.54459(4) 0.18462(2) 0.02904(15) Uani 1 1 d . . . . .
Ag5 Ag 0.23573(2) 0.40024(3) 0.15881(2) 0.02048(13) Uani 1 1 d . . . . .
Ag6 Ag 0.15227(2) 0.40126(4) 0.18889(2) 0.02672(14) Uani 1 1 d . . . . .
Ag7 Ag 0.19049(2) 0.41291(3) 0.28983(2) 0.01572(12) Uani 1 1 d . . . . .
Ag8 Ag 0.24032(2) 0.56021(3) 0.31632(2) 0.01493(11) Uani 1 1 d . . . . .
Ag9 Ag 0.32289(2) 0.55230(4) 0.28697(2) 0.02245(13) Uani 1 1 d . . . . .
Ag10 Ag 0.32441(2) 0.40635(4) 0.24079(2) 0.03006(15) Uani 1 1 d . . . . .
Ag11 Ag 0.24169(2) 0.31882(4) 0.24374(2) 0.02900(15) Uani 1 1 d . . . . .
Ag12 Ag 0.29673(2) 0.41350(4) 0.32338(2) 0.02912(15) Uani 1 1 d . . . . .
Ag13 Ag 0.13659(2) 0.40827(4) 0.08628(2) 0.03449(16) Uani 1 1 d . . . . .
Ag14 Ag 0.17694(3) 0.25279(4) 0.15348(3) 0.04101(18) Uani 1 1 d . . . . .
Ag15 Ag 0.33215(3) 0.69270(4) 0.23175(3) 0.03670(17) Uani 1 1 d . . . . .
Ag16 Ag 0.39699(3) 0.52920(4) 0.23992(3) 0.03807(17) Uani 1 1 d . . . . .
Ag17 Ag 0.14930(3) 0.52970(4) 0.33572(2) 0.03388(16) Uani 1 1 d . . . . .
Ag18 Ag 0.24684(3) 0.44413(4) 0.39093(3) 0.03623(16) Uani 1 1 d . . . . .
Ag19 Ag 0.24899(3) 0.27787(5) 0.34031(3) 0.0376(2) Uani 0.9159(16) 1 d . . P A
1
AgB9 Ag 0.1867(6) 0.6861(9) 0.2910(6) 0.0376(2) Uani 0.0452(14) 1 d . . P B 2
AgC9 Ag 0.2948(7) 0.2720(11) 0.1874(7) 0.0376(2) Uani 0.0388(14) 1 d . . P A 3
Au1 Au 0.23842(2) 0.47755(2) 0.23833(2) 0.02000(7) Uani 1 1 d . . . . .
C1 C 0.0702(5) 0.5350(8) -0.0353(4) 0.068(3) Uani 1 1 d D U . . .
H1A H 0.1031 0.5173 -0.0313 0.082 Uiso 1 1 calc R U . . .
H1B H 0.0621 0.5776 -0.0584 0.082 Uiso 1 1 calc R U . . .
C2 C 0.0358(5) 0.4703(7) -0.0542(5) 0.083(4) Uani 1 1 d D U . . .
H2A H 0.0046 0.4850 -0.0516 0.100 Uiso 1 1 calc R U . . .
H2B H 0.0306 0.4650 -0.0881 0.100 Uiso 1 1 calc R U . . .
C3 C 0.0493(5) 0.3932(8) -0.0320(6) 0.086(4) Uani 1 1 d D U . . .
H3A H 0.0801 0.3773 -0.0342 0.128 Uiso 1 1 calc R U . . .
H3B H 0.0245 0.3557 -0.0483 0.128 Uiso 1 1 calc R U . . .
H3C H 0.0522 0.3961 0.0010 0.128 Uiso 1 1 calc R U . . .
C4 C 0.1676(4) 0.7179(7) 0.0526(4) 0.054(3) Uani 1 1 d . U . . .
H4A H 0.1939 0.7120 0.0399 0.064 Uiso 1 1 calc R U . . .
H4B H 0.1797 0.7011 0.0858 0.064 Uiso 1 1 calc R U . . .
C5 C 0.1525(5) 0.8014(7) 0.0498(4) 0.062(3) Uani 1 1 d . U . . .
H5A H 0.1347 0.8149 0.0166 0.075 Uiso 1 1 calc R U . . .
H5B H 0.1305 0.8086 0.0676 0.075 Uiso 1 1 calc R U . . .
C6 C 0.1942(6) 0.8541(9) 0.0689(5) 0.083(4) Uani 1 1 d . U . . .
H6A H 0.2103 0.8440 0.1025 0.124 Uiso 1 1 calc R U . . .
H6B H 0.1830 0.9076 0.0645 0.124 Uiso 1 1 calc R U . . .
H6C H 0.2169 0.8455 0.0524 0.124 Uiso 1 1 calc R U . . .
C7 C 0.0598(3) 0.7510(6) 0.1985(3) 0.040(2) Uani 1 1 d . U . . .
H7A H 0.0851 0.7186 0.1936 0.048 Uiso 1 1 calc R U . . .
H7B H 0.0755 0.7970 0.2166 0.048 Uiso 1 1 calc R U . . .
C8 C 0.0253(4) 0.7749(7) 0.1528(4) 0.054(3) Uani 1 1 d . U . . .
H8A H -0.0012 0.8041 0.1577 0.064 Uiso 1 1 calc R U . . .
H8B H 0.0114 0.7287 0.1339 0.064 Uiso 1 1 calc R U . . .
C9 C 0.0491(5) 0.8246(8) 0.1261(5) 0.068(4) Uani 1 1 d . U . . .
H9A H 0.0618 0.8714 0.1442 0.102 Uiso 1 1 calc R U . . .
H9B H 0.0254 0.8387 0.0956 0.102 Uiso 1 1 calc R U . . .
H9C H 0.0754 0.7959 0.1213 0.102 Uiso 1 1 calc R U . . .
C10 C 0.0094(4) 0.6455(6) 0.3071(4) 0.043(2) Uani 1 1 d . U . . .
H10A H -0.0145 0.6859 0.2919 0.051 Uiso 1 1 calc R U . . .
H10B H 0.0385 0.6706 0.3290 0.051 Uiso 1 1 calc R U . . .
C11 C -0.0109(5) 0.5909(7) 0.3330(4) 0.057(3) Uani 1 1 d . U . . .
H11A H -0.0382 0.5630 0.3102 0.068 Uiso 1 1 calc R U . . .
H11B H -0.0234 0.6204 0.3541 0.068 Uiso 1 1 calc R U . . .
C12 C 0.0253(6) 0.5334(8) 0.3616(5) 0.076(4) Uani 1 1 d . U . . .
H12A H 0.0351 0.4999 0.3405 0.113 Uiso 1 1 calc R U . . .
H12B H 0.0110 0.5022 0.3801 0.113 Uiso 1 1 calc R U . . .
H12C H 0.0535 0.5605 0.3826 0.113 Uiso 1 1 calc R U . . .
C13 C 0.1870(6) 0.8453(11) 0.2821(7) 0.109(6) Uani 1 1 d . U . . .
H13A H 0.1546 0.8336 0.2597 0.131 Uiso 1 1 calc R U . . .
H13B H 0.2011 0.7971 0.2985 0.131 Uiso 1 1 calc R U . . .
C14 C 0.1835(8) 0.9008(12) 0.3156(6) 0.117(6) Uani 1 1 d . U . . .
H14A H 0.1579 0.8886 0.3284 0.141 Uiso 1 1 calc R U . . .
H14B H 0.1800 0.9541 0.3035 0.141 Uiso 1 1 calc R U . . .
C15 C 0.2386(8) 0.8817(13) 0.3532(8) 0.139(7) Uani 1 1 d . U . . .
H15A H 0.2387 0.8311 0.3675 0.208 Uiso 1 1 calc R U . . .
H15B H 0.2480 0.9211 0.3778 0.208 Uiso 1 1 calc R U . . .
H15C H 0.2614 0.8816 0.3364 0.208 Uiso 1 1 calc R U . . .
C16 C 0.2993(4) 0.9241(7) 0.2223(5) 0.061(3) Uani 1 1 d . U . . .
H16A H 0.3281 0.8956 0.2420 0.073 Uiso 1 1 calc R U . . .
H16B H 0.2906 0.9625 0.2420 0.073 Uiso 1 1 calc R U . . .
C17 C 0.3086(6) 0.9640(11) 0.1801(7) 0.105(6) Uani 1 1 d . U . . .
H17A H 0.3185 0.9254 0.1612 0.127 Uiso 1 1 calc R U . . .
H17B H 0.2791 0.9898 0.1596 0.127 Uiso 1 1 calc R U . . .
C18 C 0.3484(7) 1.0227(13) 0.2005(8) 0.141(8) Uani 1 1 d . U . . .
H18A H 0.3379 1.0614 0.2183 0.211 Uiso 1 1 calc R U . . .
H18B H 0.3558 1.0479 0.1749 0.211 Uiso 1 1 calc R U . . .
H18C H 0.3772 0.9966 0.2213 0.211 Uiso 1 1 calc R U . . .
C19 C 0.4002(5) 0.7519(8) 0.1375(5) 0.073(4) Uani 1 1 d . U . . .
H19A H 0.4110 0.7547 0.1103 0.088 Uiso 1 1 calc R U . . .
H19B H 0.3677 0.7751 0.1282 0.088 Uiso 1 1 calc R U . . .
C20 C 0.4330(6) 0.7951(9) 0.1763(5) 0.094(5) Uani 1 1 d . U . . .
H20A H 0.4648 0.7696 0.1869 0.112 Uiso 1 1 calc R U . . .
H20B H 0.4209 0.7950 0.2028 0.112 Uiso 1 1 calc R U . . .
C21 C 0.4388(5) 0.8785(8) 0.1626(5) 0.083(4) Uani 1 1 d . U . . .
H21A H 0.4500 0.8789 0.1359 0.125 Uiso 1 1 calc R U . . .
H21B H 0.4622 0.9050 0.1893 0.125 Uiso 1 1 calc R U . . .
H21C H 0.4078 0.9050 0.1539 0.125 Uiso 1 1 calc R U . . .
C22 C 0.2961(4) 0.5918(9) 0.0438(4) 0.068(4) Uani 1 1 d D U . . .
H22A H 0.2675 0.6059 0.0516 0.082 Uiso 1 1 calc R U . . .
H22B H 0.3005 0.5354 0.0471 0.082 Uiso 1 1 calc R U . . .
C23 C 0.2891(6) 0.6152(14) -0.0054(4) 0.124(7) Uani 1 1 d D U . . .
H23A H 0.2743 0.6670 -0.0103 0.149 Uiso 1 1 calc R U . . .
H23B H 0.2652 0.5796 -0.0265 0.149 Uiso 1 1 calc R U . . .
C24 C 0.3312(6) 0.6180(17) -0.0215(6) 0.163(11) Uani 1 1 d D U . . .
H24A H 0.3556 0.6527 -0.0012 0.245 Uiso 1 1 calc R U . . .
H24B H 0.3208 0.6368 -0.0540 0.245 Uiso 1 1 calc R U . . .
H24C H 0.3448 0.5662 -0.0200 0.245 Uiso 1 1 calc R U . . .
C25 C 0.2255(5) 0.3491(9) -0.0147(5) 0.102(5) Uani 1 1 d D U . . .
H25A H 0.2393 0.3073 -0.0282 0.123 Uiso 1 1 calc R U . . .
H25B H 0.2521 0.3749 0.0102 0.123 Uiso 1 1 calc R U . . .
C26 C 0.1998(6) 0.4060(12) -0.0523(7) 0.121(7) Uani 1 1 d D U . . .
H26A H 0.1951 0.4560 -0.0390 0.145 Uiso 1 1 calc R U . . .
H26B H 0.1685 0.3861 -0.0733 0.145 Uiso 1 1 calc R U . . .
C27 C 0.2358(6) 0.4118(12) -0.0772(7) 0.113(6) Uani 1 1 d D U . . .
H27A H 0.2514 0.3618 -0.0762 0.169 Uiso 1 1 calc R U . . .
H27B H 0.2601 0.4506 -0.0616 0.169 Uiso 1 1 calc R U . . .
H27C H 0.2192 0.4269 -0.1100 0.169 Uiso 1 1 calc R U . . .
C28 C 0.2426(9) 0.1419(9) 0.0762(6) 0.145(8) Uani 1 1 d D U . . .
H28A H 0.2163 0.1271 0.0875 0.174 Uiso 1 1 calc R U . . .
H28B H 0.2703 0.1585 0.1037 0.174 Uiso 1 1 calc R U . . .
C29 C 0.2569(6) 0.0731(8) 0.0541(7) 0.107(6) Uani 1 1 d D U . . .
H29A H 0.2650 0.0292 0.0763 0.129 Uiso 1 1 calc R U . . .
H29B H 0.2303 0.0575 0.0254 0.129 Uiso 1 1 calc R U . . .
C30 C 0.2999(7) 0.0967(10) 0.0423(10) 0.153(10) Uani 1 1 d D U . . .
H30A H 0.2919 0.1417 0.0216 0.229 Uiso 1 1 calc R U . . .
H30B H 0.3096 0.0541 0.0263 0.229 Uiso 1 1 calc R U . . .
H30C H 0.3265 0.1096 0.0712 0.229 Uiso 1 1 calc R U . . .
C31 C -0.0026(4) 0.2744(7) 0.0485(3) 0.045(2) Uani 1 1 d . U . . .
H31A H 0.0027 0.3271 0.0389 0.054 Uiso 1 1 calc R U . . .
H31B H -0.0333 0.2739 0.0545 0.054 Uiso 1 1 calc R U . . .
C32 C -0.0052(4) 0.2190(7) 0.0102(4) 0.053(3) Uani 1 1 d . U . . .
H32A H 0.0254 0.2209 0.0041 0.064 Uiso 1 1 calc R U . . .
H32B H -0.0312 0.2353 -0.0188 0.064 Uiso 1 1 calc R U . . .
C33 C -0.0145(5) 0.1372(8) 0.0215(5) 0.072(4) Uani 1 1 d . U . . .
H33A H 0.0132 0.1182 0.0476 0.109 Uiso 1 1 calc R U . . .
H33B H -0.0194 0.1047 -0.0062 0.109 Uiso 1 1 calc R U . . .
H33C H -0.0432 0.1356 0.0303 0.109 Uiso 1 1 calc R U . . .
C34 C 0.0126(4) 0.3547(6) 0.1927(4) 0.044(2) Uani 1 1 d . U . . .
H34A H 0.0291 0.4041 0.1927 0.052 Uiso 1 1 calc R U . . .
H34B H 0.0321 0.3251 0.2207 0.052 Uiso 1 1 calc R U . . .
C35 C -0.0356(4) 0.3697(6) 0.1952(4) 0.045(2) Uani 1 1 d . U . . .
H35A H -0.0518 0.3203 0.1962 0.054 Uiso 1 1 calc R U . . .
H35B H -0.0555 0.3981 0.1668 0.054 Uiso 1 1 calc R U . . .
C36 C -0.0313(4) 0.4166(6) 0.2386(4) 0.050(3) Uani 1 1 d . U . . .
H36A H -0.0105 0.3895 0.2666 0.076 Uiso 1 1 calc R U . . .
H36B H -0.0632 0.4234 0.2408 0.076 Uiso 1 1 calc R U . . .
H36C H -0.0175 0.4670 0.2364 0.076 Uiso 1 1 calc R U . . .
C37 C 0.1232(7) 0.3330(12) 0.4452(5) 0.128(6) Uani 1 1 d D U . . .
H37A H 0.1568 0.3466 0.4639 0.153 Uiso 1 1 calc R U . . .
H37B H 0.1192 0.2770 0.4484 0.153 Uiso 1 1 calc R U . . .
C38 C 0.0898(5) 0.3759(9) 0.4637(5) 0.088(4) Uani 1 1 d D U . . .
H38A H 0.0846 0.3450 0.4889 0.105 Uiso 1 1 calc R U . . .
H38B H 0.0583 0.3815 0.4382 0.105 Uiso 1 1 calc R U . . .
C39 C 0.1076(8) 0.4546(11) 0.4829(8) 0.145(8) Uani 1 1 d D U . . .
H39A H 0.1404 0.4504 0.5057 0.218 Uiso 1 1 calc R U . . .
H39B H 0.0865 0.4762 0.4983 0.218 Uiso 1 1 calc R U . . .
H39C H 0.1077 0.4884 0.4571 0.218 Uiso 1 1 calc R U . . .
C40 C 0.0892(5) 0.2085(7) 0.3111(5) 0.075(4) Uani 1 1 d D U . . .
H40A H 0.0893 0.2306 0.2811 0.089 Uiso 1 1 calc R U . . .
H40B H 0.0591 0.2238 0.3158 0.089 Uiso 1 1 calc R U . . .
C41 C 0.0938(7) 0.1213(7) 0.3108(6) 0.106(5) Uani 1 1 d D U . . .
H41A H 0.0730 0.0998 0.2803 0.127 Uiso 1 1 calc R U . . .
H41B H 0.1275 0.1061 0.3164 0.127 Uiso 1 1 calc R U . . .
C42 C 0.0781(6) 0.0931(11) 0.3497(6) 0.107(6) Uani 1 1 d D U . . .
H42A H 0.0893 0.1288 0.3763 0.161 Uiso 1 1 calc R U . . .
H42B H 0.0917 0.0419 0.3598 0.161 Uiso 1 1 calc R U . . .
H42C H 0.0429 0.0900 0.3386 0.161 Uiso 1 1 calc R U . . .
C43 C 0.1596(4) 0.7160(6) 0.4295(4) 0.046(2) Uani 1 1 d . U . . .
H43A H 0.1752 0.7195 0.4640 0.055 Uiso 1 1 calc R U . . .
H43B H 0.1385 0.6701 0.4221 0.055 Uiso 1 1 calc R U . . .
C44 C 0.1308(4) 0.7865(7) 0.4110(5) 0.059(3) Uani 1 1 d . U . . .
H44A H 0.1031 0.7872 0.4219 0.071 Uiso 1 1 calc R U . . .
H44B H 0.1180 0.7838 0.3763 0.071 Uiso 1 1 calc R U . . .
C45 C 0.1580(5) 0.8600(7) 0.4253(4) 0.061(3) Uani 1 1 d . U . . .
H45A H 0.1689 0.8652 0.4596 0.091 Uiso 1 1 calc R U . . .
H45B H 0.1371 0.9035 0.4107 0.091 Uiso 1 1 calc R U . . .
H45C H 0.1859 0.8597 0.4151 0.091 Uiso 1 1 calc R U . . .
C46 C 0.2955(4) 0.6074(9) 0.5040(5) 0.080(4) Uani 1 1 d D U . . .
H46A H 0.3008 0.5650 0.4846 0.095 Uiso 1 1 calc R U . . .
H46B H 0.2802 0.5853 0.5254 0.095 Uiso 1 1 calc R U . . .
C47 C 0.3429(5) 0.6414(13) 0.5326(6) 0.129(7) Uani 1 1 d D U . . .
H47A H 0.3621 0.6024 0.5550 0.154 Uiso 1 1 calc R U . . .
H47B H 0.3376 0.6853 0.5509 0.154 Uiso 1 1 calc R U . . .
C48 C 0.3705(6) 0.6687(14) 0.5022(6) 0.131(8) Uani 1 1 d D U . . .
H48A H 0.3854 0.6244 0.4926 0.197 Uiso 1 1 calc R U . . .
H48B H 0.3956 0.7047 0.5201 0.197 Uiso 1 1 calc R U . . .
H48C H 0.3486 0.6945 0.4743 0.197 Uiso 1 1 calc R U . . .
C49 C 0.4034(5) 0.7650(8) 0.3894(4) 0.070(4) Uani 1 1 d D U . . .
H49A H 0.3749 0.7334 0.3869 0.084 Uiso 1 1 calc R U . . .
H49B H 0.3931 0.8195 0.3850 0.084 Uiso 1 1 calc R U . . .
C50 C 0.4405(5) 0.7550(15) 0.4377(5) 0.140(8) Uani 1 1 d D U . . .
H50A H 0.4273 0.7782 0.4603 0.168 Uiso 1 1 calc R U . . .
H50B H 0.4437 0.6991 0.4444 0.168 Uiso 1 1 calc R U . . .
C51 C 0.4903(6) 0.7866(12) 0.4485(6) 0.114(6) Uani 1 1 d D U . . .
H51A H 0.5060 0.7600 0.4293 0.171 Uiso 1 1 calc R U . . .
H51B H 0.5089 0.7786 0.4818 0.171 Uiso 1 1 calc R U . . .
H51C H 0.4884 0.8417 0.4414 0.171 Uiso 1 1 calc R U . . .
C52 C 0.5088(4) 0.5785(8) 0.3596(5) 0.075(4) Uani 1 1 d D U . . .
H52A H 0.5060 0.5728 0.3263 0.090 Uiso 1 1 calc R U . . .
H52B H 0.4940 0.5329 0.3687 0.090 Uiso 1 1 calc R U . . .
C53 C 0.5612(4) 0.5843(10) 0.3904(5) 0.095(5) Uani 1 1 d D U . . .
H53A H 0.5797 0.5421 0.3829 0.113 Uiso 1 1 calc R U . . .
H53B H 0.5747 0.6339 0.3848 0.113 Uiso 1 1 calc R U . . .
C54 C 0.5648(7) 0.5788(12) 0.4410(5) 0.125(6) Uani 1 1 d D U . . .
H54A H 0.5986 0.5825 0.4614 0.187 Uiso 1 1 calc R U . . .
H54B H 0.5466 0.6209 0.4483 0.187 Uiso 1 1 calc R U . . .
H54C H 0.5516 0.5294 0.4463 0.187 Uiso 1 1 calc R U . . .
C55 C 0.4740(4) 0.3258(7) 0.1877(4) 0.054(3) Uani 1 1 d . U . . .
H55A H 0.4432 0.3097 0.1638 0.065 Uiso 1 1 calc R U . . .
H55B H 0.4938 0.2793 0.1995 0.065 Uiso 1 1 calc R U . . .
C56 C 0.4995(5) 0.3796(8) 0.1669(5) 0.070(3) Uani 1 1 d . U . . .
H56A H 0.4801 0.4270 0.1570 0.083 Uiso 1 1 calc R U . . .
H56B H 0.5025 0.3557 0.1385 0.083 Uiso 1 1 calc R U . . .
C57 C 0.5487(5) 0.4009(9) 0.2000(6) 0.087(4) Uani 1 1 d . U . . .
H57A H 0.5457 0.4310 0.2261 0.130 Uiso 1 1 calc R U . . .
H57B H 0.5653 0.4316 0.1832 0.130 Uiso 1 1 calc R U . . .
H57C H 0.5671 0.3540 0.2122 0.130 Uiso 1 1 calc R U . . .
C58 C 0.4176(5) 0.2015(7) 0.2828(6) 0.075(4) Uani 1 1 d . U . . .
H58A H 0.3897 0.1861 0.2551 0.090 Uiso 1 1 calc R U . . .
H58B H 0.4058 0.2214 0.3074 0.090 Uiso 1 1 calc R U . . .
C59 C 0.4522(8) 0.1335(10) 0.3014(9) 0.130(7) Uani 1 1 d . U . . .
H59A H 0.4779 0.1505 0.3305 0.156 Uiso 1 1 calc R U . . .
H59B H 0.4343 0.0918 0.3103 0.156 Uiso 1 1 calc R U . . .
C60 C 0.4750(8) 0.1011(10) 0.2706(9) 0.137(8) Uani 1 1 d . U . . .
H60A H 0.4505 0.0906 0.2399 0.206 Uiso 1 1 calc R U . . .
H60B H 0.4912 0.0531 0.2842 0.206 Uiso 1 1 calc R U . . .
H60C H 0.4985 0.1377 0.2670 0.206 Uiso 1 1 calc R U . . .
C61 C 0.1662(4) 0.0473(7) 0.1993(5) 0.064(3) Uani 1 1 d . U . . .
H61A H 0.1498 0.0973 0.1977 0.076 Uiso 1 1 calc R U . . .
H61B H 0.1496 0.0083 0.2119 0.076 Uiso 1 1 calc R U . . .
C62 C 0.1646(6) 0.0239(12) 0.1507(6) 0.104(6) Uani 1 1 d . U . . .
H62A H 0.1849 0.0594 0.1403 0.124 Uiso 1 1 calc R U . . .
H62B H 0.1779 -0.0286 0.1521 0.124 Uiso 1 1 calc R U . . .
C63 C 0.1151(6) 0.0254(12) 0.1164(6) 0.107(6) Uani 1 1 d . U . . .
H63A H 0.0954 -0.0121 0.1256 0.161 Uiso 1 1 calc R U . . .
H63B H 0.1157 0.0122 0.0852 0.161 Uiso 1 1 calc R U . . .
H63C H 0.1016 0.0770 0.1155 0.161 Uiso 1 1 calc R U . . .
C64 C 0.2954(4) 0.0629(9) 0.3264(5) 0.080(4) Uani 1 1 d D U . . .
H64A H 0.2766 0.0146 0.3183 0.097 Uiso 1 1 calc R U . . .
H64B H 0.2836 0.0934 0.3477 0.097 Uiso 1 1 calc R U . . .
C65 C 0.3485(5) 0.0454(12) 0.3496(6) 0.114(6) Uani 1 1 d D U . . .
H65A H 0.3599 0.0149 0.3280 0.137 Uiso 1 1 calc R U . . .
H65B H 0.3670 0.0941 0.3567 0.137 Uiso 1 1 calc R U . . .
C66 C 0.3569(9) 0.0009(18) 0.3943(8) 0.206(15) Uani 1 1 d D U . . .
H66A H 0.3290 0.0065 0.4041 0.310 Uiso 1 1 calc R U . . .
H66B H 0.3855 0.0209 0.4189 0.310 Uiso 1 1 calc R U . . .
H66C H 0.3616 -0.0536 0.3888 0.310 Uiso 1 1 calc R U . . .
C67 C 0.4431(4) 0.3808(9) 0.4202(4) 0.072(4) Uani 1 1 d . U . . .
H67A H 0.4298 0.3663 0.3866 0.086 Uiso 1 1 calc R U . . .
H67B H 0.4397 0.4372 0.4225 0.086 Uiso 1 1 calc R U . . .
C68 C 0.4931(5) 0.3602(11) 0.4391(6) 0.090(4) Uani 1 1 d . U . . .
H68A H 0.5052 0.3607 0.4739 0.108 Uiso 1 1 calc R U . . .
H68B H 0.5130 0.3949 0.4276 0.108 Uiso 1 1 calc R U . . .
C69 C 0.4921(8) 0.2707(13) 0.4182(9) 0.148(8) Uani 1 1 d . U . . .
H69A H 0.4738 0.2371 0.4316 0.222 Uiso 1 1 calc R U . . .
H69B H 0.5251 0.2514 0.4268 0.222 Uiso 1 1 calc R U . . .
H69C H 0.4770 0.2714 0.3839 0.222 Uiso 1 1 calc R U . . .
C70 C 0.3620(4) 0.2255(7) 0.4827(4) 0.061(3) Uani 1 1 d . U . . .
H70A H 0.3954 0.2166 0.4842 0.073 Uiso 1 1 calc R U . . .
H70B H 0.3409 0.1884 0.4601 0.073 Uiso 1 1 calc R U . . .
C71 C 0.3586(5) 0.2135(7) 0.5295(4) 0.059(3) Uani 1 1 d . U . . .
H71A H 0.3251 0.2231 0.5278 0.071 Uiso 1 1 calc R U . . .
H71B H 0.3796 0.2510 0.5518 0.071 Uiso 1 1 calc R U . . .
C72 C 0.3729(6) 0.1337(8) 0.5476(5) 0.082(4) Uani 1 1 d . U . . .
H72A H 0.3564 0.0963 0.5232 0.124 Uiso 1 1 calc R U . . .
H72B H 0.3640 0.1249 0.5754 0.124 Uiso 1 1 calc R U . . .
H72C H 0.4077 0.1277 0.5561 0.124 Uiso 1 1 calc R U . . .
C73 C 0.4798(8) 0.9902(13) 0.5084(8) 0.125(7) Uani 1 1 d . U . . .
H73A H 0.4604 1.0373 0.5064 0.150 Uiso 1 1 calc R U . . .
H73B H 0.4589 0.9520 0.4865 0.150 Uiso 1 1 calc R U . . .
C74 C 0.4933(9) 0.9592(17) 0.5567(9) 0.158(9) Uani 1 1 d . U . . .
H74A H 0.5144 0.9140 0.5594 0.189 Uiso 1 1 calc R U . . .
H74B H 0.5123 0.9987 0.5789 0.189 Uiso 1 1 calc R U . . .
C75 C 0.4530(8) 0.9359(16) 0.5712(9) 0.158(10) Uani 1 1 d . U . . .
H75A H 0.4287 0.9767 0.5633 0.238 Uiso 1 1 calc R U . . .
H75B H 0.4646 0.9271 0.6052 0.238 Uiso 1 1 calc R U . . .
H75C H 0.4387 0.8884 0.5549 0.238 Uiso 1 1 calc R U . . .
O1 O 0.0695(3) 0.5630(5) 0.0082(3) 0.062(2) Uani 1 1 d . U . . .
O2 O 0.1278(3) 0.6710(5) 0.0265(2) 0.0539(19) Uani 1 1 d . U . . .
O3 O 0.0357(2) 0.7077(4) 0.2251(2) 0.0332(14) Uani 1 1 d . U . . .
O4 O 0.0214(2) 0.6020(4) 0.2718(2) 0.0354(14) Uani 1 1 d . U . . .
O5 O 0.2173(3) 0.8751(4) 0.2565(3) 0.060(2) Uani 1 1 d . U . . .
O6 O 0.2599(3) 0.8722(4) 0.2010(3) 0.0517(19) Uani 1 1 d . U . . .
O7 O 0.3977(2) 0.6710(5) 0.1505(2) 0.0491(18) Uani 1 1 d . U . . .
O8 O 0.3384(3) 0.6307(5) 0.0756(2) 0.053(2) Uani 1 1 d . U . . .
O9 O 0.1927(4) 0.3186(6) 0.0043(3) 0.095(4) Uani 1 1 d D U . . .
O10 O 0.2273(5) 0.2040(6) 0.0449(4) 0.109(4) Uani 1 1 d D U . . .
O11 O 0.0372(2) 0.2527(4) 0.0916(2) 0.0357(15) Uani 1 1 d . U . . .
O12 O 0.0087(2) 0.3115(4) 0.1504(2) 0.0337(14) Uani 1 1 d . U . . .
O13 O 0.1137(4) 0.3514(8) 0.3982(4) 0.110(4) Uani 1 1 d D U . . .
O14 O 0.1296(4) 0.2340(6) 0.3489(4) 0.097(3) Uani 1 1 d . U . . .
O15 O 0.1957(2) 0.7093(3) 0.4077(2) 0.0318(14) Uani 1 1 d . U . . .
O16 O 0.2638(2) 0.6626(4) 0.4741(2) 0.0430(16) Uani 1 1 d . U . . .
O17 O 0.4214(3) 0.7426(4) 0.3521(2) 0.0462(17) Uani 1 1 d . U . . .
O18 O 0.4848(2) 0.6476(4) 0.3656(3) 0.0484(18) Uani 1 1 d . U . . .
O19 O 0.4650(2) 0.3643(4) 0.2260(2) 0.0426(16) Uani 1 1 d . U . . .
O20 O 0.4469(3) 0.2588(4) 0.2702(3) 0.0525(19) Uani 1 1 d . U . . .
O21 O 0.2157(3) 0.0536(4) 0.2295(3) 0.055(2) Uani 1 1 d . U . . .
O22 O 0.2907(3) 0.1055(5) 0.2851(3) 0.061(2) Uani 1 1 d . U . . .
O23 O 0.4167(2) 0.3416(4) 0.4459(2) 0.0480(18) Uani 1 1 d . U . . .
O24 O 0.3474(2) 0.3044(4) 0.4668(2) 0.0446(17) Uani 1 1 d . U . . .
P1 P 0.11709(9) 0.59486(17) 0.04916(8) 0.0397(6) Uani 1 1 d . . . . .
P2 P 0.05996(8) 0.63034(13) 0.25031(8) 0.0270(5) Uani 1 1 d . . . . .
P3 P 0.23957(10) 0.81671(15) 0.22992(11) 0.0425(6) Uani 1 1 d . . . . .
P4 P 0.34920(9) 0.62555(17) 0.13034(9) 0.0409(6) Uani 1 1 d . . . . .
P5 P 0.21041(11) 0.28451(18) 0.05475(9) 0.0501(7) Uani 1 1 d . . . . .
P6 P 0.05438(8) 0.30867(14) 0.13466(8) 0.0300(5) Uani 1 1 d . . . . .
P7 P 0.14150(11) 0.3211(2) 0.36487(10) 0.0552(8) Uani 1 1 d . . . . .
P8 P 0.23390(8) 0.64182(14) 0.42124(8) 0.0292(5) Uani 1 1 d . . . . .
P9 P 0.42905(9) 0.65806(15) 0.33793(9) 0.0357(6) Uani 1 1 d . . . . .
P10 P 0.42404(9) 0.33676(15) 0.24435(10) 0.0380(6) Uani 1 1 d . . . . .
P11 P 0.23975(9) 0.13317(14) 0.24990(10) 0.0401(6) Uani 1 1 d . . . . .
P12 P 0.35991(9) 0.34142(16) 0.42508(9) 0.0394(6) Uani 1 1 d . . . . .
S1 S 0.10086(8) 0.61406(14) 0.10554(8) 0.0342(5) Uani 1 1 d . . . . .
S2 S 0.17252(8) 0.52120(16) 0.05849(8) 0.0390(6) Uani 1 1 d . . . . .
S3 S 0.06318(8) 0.55254(14) 0.20418(8) 0.0317(5) Uani 1 1 d . . . . .
S4 S 0.12245(9) 0.65826(14) 0.30051(8) 0.0371(5) Uani 1 1 d . . . . .
S5 S 0.18976(10) 0.75255(16) 0.18431(10) 0.0471(6) Uani 1 1 d . . . . .
S6 S 0.29226(11) 0.75993(15) 0.28003(9) 0.0450(6) Uani 1 1 d . . . . .
S7 S 0.29540(9) 0.67949(16) 0.14401(9) 0.0422(6) Uani 1 1 d . . . . .
S8 S 0.36048(9) 0.51643(16) 0.15167(9) 0.0420(6) Uani 1 1 d . . . . .
S9 S 0.2627(2) 0.3275(4) 0.1036(2) 0.0432(13) Uani 0.5 1 d . U P A 1
S9B S 0.2617(2) 0.3673(4) 0.0912(2) 0.0432(13) Uani 0.5 1 d . . P A 2
S10 S 0.14816(10) 0.26977(17) 0.06628(10) 0.0517(7) Uani 1 1 d . U . . .
S11 S 0.06727(8) 0.41573(13) 0.11732(8) 0.0304(5) Uani 1 1 d . . . . .
S12 S 0.10833(8) 0.25831(15) 0.18551(9) 0.0384(6) Uani 1 1 d . . . . .
S13 S 0.11616(9) 0.39249(16) 0.30986(9) 0.0409(6) Uani 1 1 d . . . . .
S14 S 0.21217(10) 0.31475(16) 0.40164(10) 0.0469(6) Uani 1 1 d . . . . .
S15 S 0.20070(9) 0.54015(14) 0.42228(8) 0.0363(5) Uani 1 1 d . . . . .
S16 S 0.27419(9) 0.65145(15) 0.38191(9) 0.0386(6) Uani 1 1 d . . . . .
S17 S 0.39185(9) 0.58138(15) 0.35901(8) 0.0398(6) Uani 1 1 d . . . . .
S18 S 0.42017(9) 0.66431(15) 0.26881(8) 0.0376(5) Uani 1 1 d . . . . .
S19 S 0.36217(9) 0.31775(18) 0.19399(11) 0.0542(8) Uani 1 1 d . . . . .
S20 S 0.42212(9) 0.41490(16) 0.29260(9) 0.0411(6) Uani 1 1 d . . . . .
S21 S 0.25700(9) 0.19470(15) 0.20278(10) 0.0429(6) Uani 1 1 d . . . . .
S22 S 0.19940(9) 0.18485(16) 0.28161(10) 0.0439(6) Uani 1 1 d . . . . .
S23 S 0.33928(10) 0.27571(17) 0.36733(10) 0.0475(6) Uani 1 1 d . . . . .
S24 S 0.33719(9) 0.45044(16) 0.41702(9) 0.0437(6) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
S5 Ag1 Au1 146.31(7) .
S5 Ag1 AgB9 80.6(3) .
Au1 Ag1 AgB9 105.5(3) .
S5 Ag1 S6 78.37(9) .
Au1 Ag1 S6 135.28(6) .
AgB9 Ag1 S6 77.0(3) .
S5 Ag1 Ag8 136.31(7) .
Au1 Ag1 Ag8 58.364(18) .
AgB9 Ag1 Ag8 55.7(3) .
S6 Ag1 Ag8 92.11(6) .
S5 Ag1 Ag3 99.00(7) .
Au1 Ag1 Ag3 59.328(19) .
AgB9 Ag1 Ag3 60.4(3) .
S6 Ag1 Ag3 136.91(6) .
Ag8 Ag1 Ag3 60.04(2) .
S5 Ag1 Ag2 88.00(7) .
Au1 Ag1 Ag2 59.275(19) .
AgB9 Ag1 Ag2 116.2(3) .
S6 Ag1 Ag2 159.47(6) .
Ag8 Ag1 Ag2 108.29(3) .
Ag3 Ag1 Ag2 60.01(2) .
S5 Ag1 Ag4 115.49(7) .
Au1 Ag1 Ag4 58.423(19) .
AgB9 Ag1 Ag4 163.1(3) .
S6 Ag1 Ag4 110.16(6) .
Ag8 Ag1 Ag4 107.86(3) .
Ag3 Ag1 Ag4 109.55(3) .
Ag2 Ag1 Ag4 62.07(2) .
S5 Ag1 Ag9 153.23(7) .
Au1 Ag1 Ag9 57.084(18) .
AgB9 Ag1 Ag9 108.7(3) .
S6 Ag1 Ag9 79.47(6) .
Ag8 Ag1 Ag9 59.19(2) .
Ag3 Ag1 Ag9 107.43(3) .
Ag2 Ag1 Ag9 108.65(3) .
Ag4 Ag1 Ag9 59.47(2) .
S5 Ag1 Ag15 93.66(7) .
Au1 Ag1 Ag15 107.68(3) .
AgB9 Ag1 Ag15 126.1(3) .
S6 Ag1 Ag15 49.66(6) .
Ag8 Ag1 Ag15 112.37(3) .
Ag3 Ag1 Ag15 166.79(3) .
Ag2 Ag1 Ag15 117.10(3) .
Ag4 Ag1 Ag15 60.96(2) .
Ag9 Ag1 Ag15 60.32(2) .
S1 Ag2 Au1 148.30(6) .
S1 Ag2 S2 76.59(7) .
Au1 Ag2 S2 134.15(6) .
S1 Ag2 Ag6 107.89(6) .
Au1 Ag2 Ag6 59.028(19) .
S2 Ag2 Ag6 110.97(6) .
S1 Ag2 Ag3 89.42(5) .
Au1 Ag2 Ag3 58.883(18) .
S2 Ag2 Ag3 161.37(6) .
Ag6 Ag2 Ag3 61.37(2) .
S1 Ag2 Ag1 107.93(6) .
Au1 Ag2 Ag1 58.118(19) .
S2 Ag2 Ag1 136.12(6) .
Ag6 Ag2 Ag1 108.79(3) .
Ag3 Ag2 Ag1 59.79(2) .
S1 Ag2 Ag5 145.85(6) .
Au1 Ag2 Ag5 57.049(18) .
S2 Ag2 Ag5 78.69(6) .
Ag6 Ag2 Ag5 60.39(2) .
Ag3 Ag2 Ag5 108.24(3) .
Ag1 Ag2 Ag5 106.22(3) .
S1 Ag2 Ag4 144.58(6) .
Au1 Ag2 Ag4 57.032(18) .
S2 Ag2 Ag4 91.42(5) .
Ag6 Ag2 Ag4 107.53(3) .
Ag3 Ag2 Ag4 107.00(3) .
Ag1 Ag2 Ag4 59.07(2) .
Ag5 Ag2 Ag4 58.49(2) .
S1 Ag2 Ag13 85.48(6) .
Au1 Ag2 Ag13 107.65(3) .
S2 Ag2 Ag13 50.88(6) .
Ag6 Ag2 Ag13 60.70(2) .
Ag3 Ag2 Ag13 116.62(3) .
Ag1 Ag2 Ag13 165.59(3) .
Ag5 Ag2 Ag13 60.58(2) .
Ag4 Ag2 Ag13 112.73(3) .
S3 Ag3 Au1 148.12(6) .
S3 Ag3 AgB9 108.6(3) .
Au1 Ag3 AgB9 103.2(3) .
S3 Ag3 Ag8 147.84(6) .
Au1 Ag3 Ag8 57.911(17) .
AgB9 Ag3 Ag8 55.0(3) .
S3 Ag3 Ag1 140.39(6) .
Au1 Ag3 Ag1 58.301(18) .
AgB9 Ag3 Ag1 58.4(3) .
Ag8 Ag3 Ag1 59.66(2) .
S3 Ag3 Ag7 112.13(6) .
Au1 Ag3 Ag7 56.530(17) .
AgB9 Ag3 Ag7 111.1(3) .
Ag8 Ag3 Ag7 60.88(2) .
Ag1 Ag3 Ag7 107.30(3) .
S3 Ag3 Ag2 103.91(6) .
Au1 Ag3 Ag2 59.019(18) .
AgB9 Ag3 Ag2 114.6(3) .
Ag8 Ag3 Ag2 108.15(3) .
Ag1 Ag3 Ag2 60.20(2) .
Ag7 Ag3 Ag2 106.36(3) .
S3 Ag3 Ag6 89.97(6) .
Au1 Ag3 Ag6 58.305(18) .
AgB9 Ag3 Ag6 161.5(3) .
Ag8 Ag3 Ag6 108.46(3) .
Ag1 Ag3 Ag6 107.37(3) .
Ag7 Ag3 Ag6 59.12(2) .
Ag2 Ag3 Ag6 59.16(2) .
S3 Ag3 Ag17 88.76(6) .
Au1 Ag3 Ag17 105.13(2) .
AgB9 Ag3 Ag17 69.2(3) .
Ag8 Ag3 Ag17 60.20(2) .
Ag1 Ag3 Ag17 115.33(3) .
Ag7 Ag3 Ag17 59.02(2) .
Ag2 Ag3 Ag17 163.97(3) .
Ag6 Ag3 Ag17 111.95(3) .
S7 Ag4 S8 76.93(8) .
S7 Ag4 Au1 141.53(6) .
S8 Ag4 Au1 141.19(7) .
S7 Ag4 Ag5 138.77(6) .
S8 Ag4 Ag5 98.92(6) .
Au1 Ag4 Ag5 57.778(18) .
S7 Ag4 Ag1 83.91(6) .
S8 Ag4 Ag1 154.16(6) .
Au1 Ag4 Ag1 58.395(18) .
Ag5 Ag4 Ag1 106.92(3) .
S7 Ag4 Ag9 112.87(6) .
S8 Ag4 Ag9 110.63(6) .
Au1 Ag4 Ag9 57.755(18) .
Ag5 Ag4 Ag9 106.99(3) .
Ag1 Ag4 Ag9 61.40(2) .
S7 Ag4 Ag10 153.94(6) .
S8 Ag4 Ag10 82.85(6) .
Au1 Ag4 Ag10 58.987(19) .
Ag5 Ag4 Ag10 60.36(2) .
Ag1 Ag4 Ag10 109.28(3) .
Ag9 Ag4 Ag10 59.56(2) .
S7 Ag4 Ag2 97.56(6) .
S8 Ag4 Ag2 140.35(6) .
Au1 Ag4 Ag2 58.112(18) .
Ag5 Ag4 Ag2 59.56(2) .
Ag1 Ag4 Ag2 58.86(2) .
Ag9 Ag4 Ag2 107.65(3) .
Ag10 Ag4 Ag2 108.50(3) .
S7 Ag4 Ag15 51.73(6) .
S8 Ag4 Ag15 92.51(6) .
Au1 Ag4 Ag15 108.36(2) .
Ag5 Ag4 Ag15 166.14(3) .
Ag1 Ag4 Ag15 61.83(2) .
Ag9 Ag4 Ag15 61.22(2) .
Ag10 Ag4 Ag15 113.87(3) .
Ag2 Ag4 Ag15 115.03(3) .
S7 Ag4 Ag16 94.10(6) .
S8 Ag4 Ag16 50.46(6) .
Au1 Ag4 Ag16 107.86(3) .
Ag5 Ag4 Ag16 115.01(3) .
Ag1 Ag4 Ag16 115.02(3) .
Ag9 Ag4 Ag16 60.23(2) .
Ag10 Ag4 Ag16 60.11(2) .
Ag2 Ag4 Ag16 165.96(3) .
Ag15 Ag4 Ag16 66.91(2) .
S9 Ag5 Au1 160.26(15) .
S9B Ag5 Au1 156.10(16) .
Au1 Ag5 AgC9 107.2(4) .
S9 Ag5 Ag11 115.20(16) .
S9B Ag5 Ag11 132.86(16) .
Au1 Ag5 Ag11 58.648(18) .
AgC9 Ag5 Ag11 59.6(4) .
S9 Ag5 Ag4 111.59(16) .
S9B Ag5 Ag4 98.02(16) .
Au1 Ag5 Ag4 58.962(18) .
AgC9 Ag5 Ag4 113.3(4) .
Ag11 Ag5 Ag4 108.56(3) .
S9 Ag5 Ag6 137.10(16) .
S9B Ag5 Ag6 142.71(15) .
Au1 Ag5 Ag6 59.303(17) .
AgC9 Ag5 Ag6 114.7(4) .
Ag11 Ag5 Ag6 61.30(2) .
Ag4 Ag5 Ag6 109.30(3) .
S9 Ag5 Ag2 134.58(16) .
S9B Ag5 Ag2 118.08(16) .
Au1 Ag5 Ag2 59.330(18) .
AgC9 Ag5 Ag2 166.5(4) .
Ag11 Ag5 Ag2 108.75(2) .
Ag4 Ag5 Ag2 61.95(2) .
Ag6 Ag5 Ag2 59.14(2) .
S9 Ag5 Ag10 100.94(15) .
S9B Ag5 Ag10 105.32(15) .
Au1 Ag5 Ag10 59.400(18) .
AgC9 Ag5 Ag10 58.7(4) .
Ag11 Ag5 Ag10 60.11(2) .
Ag4 Ag5 Ag10 60.49(2) .
Ag6 Ag5 Ag10 110.03(2) .
Ag2 Ag5 Ag10 110.51(3) .
S9 Ag5 Ag13 89.54(15) .
S9B Ag5 Ag13 84.91(15) .
Au1 Ag5 Ag13 110.15(2) .
AgC9 Ag5 Ag13 128.1(4) .
Ag11 Ag5 Ag13 114.65(3) .
Ag4 Ag5 Ag13 116.44(3) .
Ag6 Ag5 Ag13 60.57(2) .
Ag2 Ag5 Ag13 61.35(2) .
Ag10 Ag5 Ag13 169.48(3) .
S9 Ag5 Ag14 81.30(16) .
S9B Ag5 Ag14 95.59(16) .
Au1 Ag5 Ag14 107.27(2) .
AgC9 Ag5 Ag14 68.5(4) .
Ag11 Ag5 Ag14 59.77(2) .
Ag4 Ag5 Ag14 166.23(3) .
Ag6 Ag5 Ag14 59.60(2) .
Ag2 Ag5 Ag14 112.90(3) .
Ag10 Ag5 Ag14 113.64(3) .
Ag13 Ag5 Ag14 66.83(2) .
S11 Ag6 S12 76.13(7) .
S11 Ag6 Au1 143.73(5) .
S12 Ag6 Au1 140.09(5) .
S11 Ag6 Ag7 139.38(5) .
S12 Ag6 Ag7 96.17(6) .
Au1 Ag6 Ag7 56.615(17) .
S11 Ag6 Ag2 85.41(5) .
S12 Ag6 Ag2 156.96(6) .
Au1 Ag6 Ag2 59.112(19) .
Ag7 Ag6 Ag2 106.84(3) .
S11 Ag6 Ag5 113.80(5) .
S12 Ag6 Ag5 114.78(6) .
Au1 Ag6 Ag5 57.101(17) .
Ag7 Ag6 Ag5 105.69(2) .
Ag2 Ag6 Ag5 60.47(2) .
S11 Ag6 Ag3 98.93(5) .
S12 Ag6 Ag3 136.43(6) .
Au1 Ag6 Ag3 58.253(18) .
Ag7 Ag6 Ag3 59.42(2) .
Ag2 Ag6 Ag3 59.47(2) .
Ag5 Ag6 Ag3 106.84(3) .
S11 Ag6 Ag11 153.80(6) .
S12 Ag6 Ag11 84.62(5) .
Au1 Ag6 Ag11 57.103(18) .
Ag7 Ag6 Ag11 59.49(2) .
Ag2 Ag6 Ag11 107.85(3) .
Ag5 Ag6 Ag11 58.84(2) .
Ag3 Ag6 Ag11 107.27(3) .
S11 Ag6 Ag14 93.89(5) .
S12 Ag6 Ag14 52.21(6) .
Au1 Ag6 Ag14 108.00(3) .
Ag7 Ag6 Ag14 112.91(3) .
Ag2 Ag6 Ag14 116.81(3) .
Ag5 Ag6 Ag14 62.67(2) .
Ag3 Ag6 Ag14 166.14(3) .
Ag11 Ag6 Ag14 60.05(2) .
S11 Ag6 Ag13 52.84(5) .
S12 Ag6 Ag13 95.56(6) .
Au1 Ag6 Ag13 108.71(3) .
Ag7 Ag6 Ag13 165.25(3) .
Ag2 Ag6 Ag13 61.95(2) .
Ag5 Ag6 Ag13 61.03(2) .
Ag3 Ag6 Ag13 116.05(3) .
Ag11 Ag6 Ag13 112.92(3) .
Ag14 Ag6 Ag13 68.15(2) .
S13 Ag7 Au1 152.22(7) .
S13 Ag7 Ag6 101.21(6) .
Au1 Ag7 Ag6 60.277(18) .
S13 Ag7 Ag3 93.40(7) .
Au1 Ag7 Ag3 60.123(17) .
Ag6 Ag7 Ag3 61.47(2) .
S13 Ag7 Ag11 133.59(7) .
Au1 Ag7 Ag11 58.966(18) .
Ag6 Ag7 Ag11 61.68(2) .
Ag3 Ag7 Ag11 110.62(2) .
S13 Ag7 Ag8 117.39(6) .
Au1 Ag7 Ag8 58.478(16) .
Ag6 Ag7 Ag8 109.15(2) .
Ag3 Ag7 Ag8 59.39(2) .
Ag11 Ag7 Ag8 109.02(2) .
S13 Ag7 Ag17 55.94(6) .
Au1 Ag7 Ag17 112.07(2) .
Ag6 Ag7 Ag17 118.40(3) .
Ag3 Ag7 Ag17 64.01(2) .
Ag11 Ag7 Ag17 170.36(3) .
Ag8 Ag7 Ag17 61.47(2) .
S13 Ag7 Ag12 147.03(6) .
Au1 Ag7 Ag12 58.946(18) .
Ag6 Ag7 Ag12 110.14(2) .
Ag3 Ag7 Ag12 110.15(2) .
Ag11 Ag7 Ag12 59.57(2) .
Ag8 Ag7 Ag12 61.69(2) .
Ag17 Ag7 Ag12 113.67(3) .
S13 Ag7 Ag18 90.07(6) .
Au1 Ag7 Ag18 107.49(2) .
Ag6 Ag7 Ag18 167.76(3) .
Ag3 Ag7 Ag18 113.61(3) .
Ag11 Ag7 Ag18 113.45(3) .
Ag8 Ag7 Ag18 60.69(2) .
Ag17 Ag7 Ag18 64.32(2) .
Ag12 Ag7 Ag18 59.83(2) .
S13 Ag7 Ag19 99.59(7) .
Au1 Ag7 Ag19 107.06(2) .
Ag6 Ag7 Ag19 115.59(3) .
Ag3 Ag7 Ag19 167.00(3) .
Ag11 Ag7 Ag19 59.97(2) .
Ag8 Ag7 Ag19 113.32(3) .
Ag17 Ag7 Ag19 123.77(3) .
Ag12 Ag7 Ag19 57.93(2) .
Ag18 Ag7 Ag19 66.43(2) .
S16 Ag8 AgB9 74.9(4) .
S16 Ag8 Au1 155.43(6) .
AgB9 Ag8 Au1 110.5(4) .
S16 Ag8 Ag1 108.22(6) .
AgB9 Ag8 Ag1 61.0(4) .
Au1 Ag8 Ag1 59.077(17) .
S16 Ag8 Ag3 135.77(7) .
AgB9 Ag8 Ag3 62.2(4) .
Au1 Ag8 Ag3 59.651(17) .
Ag1 Ag8 Ag3 60.31(2) .
S16 Ag8 Ag9 97.40(6) .
AgB9 Ag8 Ag9 115.9(4) .
Au1 Ag8 Ag9 58.340(16) .
Ag1 Ag8 Ag9 62.19(2) .
Ag3 Ag8 Ag9 110.01(2) .
S16 Ag8 Ag7 143.93(6) .
AgB9 Ag8 Ag7 116.5(3) .
Au1 Ag8 Ag7 56.648(16) .
Ag1 Ag8 Ag7 106.90(2) .
Ag3 Ag8 Ag7 59.72(2) .
Ag9 Ag8 Ag7 106.00(2) .
S16 Ag8 Ag18 85.44(6) .
AgB9 Ag8 Ag18 130.5(4) .
Au1 Ag8 Ag18 106.08(2) .
Ag1 Ag8 Ag18 165.15(3) .
Ag3 Ag8 Ag18 113.95(3) .
Ag9 Ag8 Ag18 111.34(3) .
Ag7 Ag8 Ag18 60.75(2) .
S16 Ag8 Ag17 95.51(6) .
AgB9 Ag8 Ag17 73.4(4) .
Au1 Ag8 Ag17 109.03(2) .
Ag1 Ag8 Ag17 118.92(3) .
Ag3 Ag8 Ag17 63.50(2) .
Ag9 Ag8 Ag17 165.76(3) .
Ag7 Ag8 Ag17 59.78(2) .
Ag18 Ag8 Ag17 63.75(2) .
S16 Ag8 Ag12 115.16(7) .
AgB9 Ag8 Ag12 168.0(4) .
Au1 Ag8 Ag12 57.663(17) .
Ag1 Ag8 Ag12 108.26(2) .
Ag3 Ag8 Ag12 108.78(2) .
Ag9 Ag8 Ag12 58.13(2) .
Ag7 Ag8 Ag12 59.682(19) .
Ag18 Ag8 Ag12 59.21(2) .
Ag17 Ag8 Ag12 110.59(3) .
S17 Ag9 Au1 152.89(6) .
S17 Ag9 Ag12 94.72(6) .
Au1 Ag9 Ag12 59.501(18) .
S17 Ag9 Ag8 104.31(6) .
Au1 Ag9 Ag8 58.393(16) .
Ag12 Ag9 Ag8 63.17(2) .
S17 Ag9 Ag10 117.28(7) .
Au1 Ag9 Ag10 59.568(18) .
Ag12 Ag9 Ag10 60.31(2) .
Ag8 Ag9 Ag10 110.37(3) .
S17 Ag9 Ag4 146.76(6) .
Au1 Ag9 Ag4 58.533(18) .
Ag12 Ag9 Ag4 108.88(3) .
Ag8 Ag9 Ag4 107.12(2) .
Ag10 Ag9 Ag4 60.47(2) .
S17 Ag9 Ag1 134.49(7) .
Au1 Ag9 Ag1 57.814(18) .
Ag12 Ag9 Ag1 109.43(3) .
Ag8 Ag9 Ag1 58.622(19) .
Ag10 Ag9 Ag1 108.20(3) .
Ag4 Ag9 Ag1 59.14(2) .
S17 Ag9 Ag15 96.83(6) .
Au1 Ag9 Ag15 108.91(2) .
Ag12 Ag9 Ag15 168.40(3) .
Ag8 Ag9 Ag15 112.53(3) .
Ag10 Ag9 Ag15 114.58(3) .
Ag4 Ag9 Ag15 61.12(2) .
Ag1 Ag9 Ag15 61.07(2) .
S17 Ag9 Ag16 86.07(6) .
Au1 Ag9 Ag16 111.01(2) .
Ag12 Ag9 Ag16 114.05(3) .
Ag8 Ag9 Ag16 169.30(3) .
Ag10 Ag9 Ag16 61.45(2) .
Ag4 Ag9 Ag16 63.29(2) .
Ag1 Ag9 Ag16 115.72(3) .
Ag15 Ag9 Ag16 68.00(2) .
S19 Ag10 S20 77.16(8) .
S19 Ag10 AgC9 45.5(4) .
S20 Ag10 AgC9 115.3(4) .
S19 Ag10 Au1 143.68(6) .
S20 Ag10 Au1 138.52(6) .
AgC9 Ag10 Au1 104.6(4) .
S19 Ag10 Ag12 143.52(8) .
S20 Ag10 Ag12 93.54(6) .
AgC9 Ag10 Ag12 114.2(4) .
Au1 Ag10 Ag12 58.459(19) .
S19 Ag10 Ag9 149.65(8) .
S20 Ag10 Ag9 82.45(6) .
AgC9 Ag10 Ag9 162.1(4) .
Au1 Ag10 Ag9 57.506(18) .
Ag12 Ag10 Ag9 59.24(2) .
S19 Ag10 Ag11 103.65(7) .
S20 Ag10 Ag11 137.21(6) .
AgC9 Ag10 Ag11 59.0(4) .
Au1 Ag10 Ag11 57.616(18) .
Ag12 Ag10 Ag11 60.06(2) .
Ag9 Ag10 Ag11 106.59(3) .
S19 Ag10 Ag5 86.82(6) .
S20 Ag10 Ag5 159.19(6) .
AgC9 Ag10 Ag5 58.0(4) .
Au1 Ag10 Ag5 56.971(17) .
Ag12 Ag10 Ag5 107.19(3) .
Ag9 Ag10 Ag5 106.37(3) .
Ag11 Ag10 Ag5 59.34(2) .
S19 Ag10 Ag4 108.44(8) .
S20 Ag10 Ag4 113.38(6) .
AgC9 Ag10 Ag4 111.5(4) .
Au1 Ag10 Ag4 57.725(18) .
Ag12 Ag10 Ag4 107.62(3) .
Ag9 Ag10 Ag4 59.97(2) .
Ag11 Ag10 Ag4 106.89(3) .
Ag5 Ag10 Ag4 59.15(2) .
S19 Ag10 Ag16 88.24(7) .
S20 Ag10 Ag16 50.55(6) .
AgC9 Ag10 Ag16 131.3(4) .
Au1 Ag10 Ag16 109.28(3) .
Ag12 Ag10 Ag16 113.10(3) .
Ag9 Ag10 Ag16 61.42(2) .
Ag11 Ag10 Ag16 166.79(3) .
Ag5 Ag10 Ag16 116.62(3) .
Ag4 Ag10 Ag16 63.11(2) .
S21 Ag11 Au1 143.67(7) .
S21 Ag11 AgC9 40.9(4) .
Au1 Ag11 AgC9 105.5(4) .
S21 Ag11 Ag5 86.88(7) .
Au1 Ag11 Ag5 57.918(18) .
AgC9 Ag11 Ag5 58.2(4) .
S21 Ag11 Ag7 154.63(6) .
Au1 Ag11 Ag7 56.836(17) .
AgC9 Ag11 Ag7 162.3(4) .
Ag5 Ag11 Ag7 105.96(3) .
S21 Ag11 Ag12 136.32(6) .
Au1 Ag11 Ag12 58.885(19) .
AgC9 Ag11 Ag12 113.4(4) .
Ag5 Ag11 Ag12 107.89(3) .
Ag7 Ag11 Ag12 61.15(2) .
S21 Ag11 Ag10 97.36(6) .
Au1 Ag11 Ag10 59.337(19) .
AgC9 Ag11 Ag10 58.5(4) .
Ag5 Ag11 Ag10 60.55(2) .
Ag7 Ag11 Ag10 108.00(3) .
Ag12 Ag11 Ag10 59.73(2) .
S21 Ag11 Ag19 108.08(7) .
Au1 Ag11 Ag19 106.77(3) .
Ag5 Ag11 Ag19 164.67(3) .
Ag7 Ag11 Ag19 61.70(2) .
Ag12 Ag11 Ag19 58.98(2) .
Ag10 Ag11 Ag19 112.64(3) .
S21 Ag11 Ag6 113.70(6) .
Au1 Ag11 Ag6 58.556(19) .
AgC9 Ag11 Ag6 112.3(4) .
Ag5 Ag11 Ag6 59.86(2) .
Ag7 Ag11 Ag6 58.83(2) .
Ag12 Ag11 Ag6 109.12(3) .
Ag10 Ag11 Ag6 109.23(3) .
Ag19 Ag11 Ag6 114.61(3) .
S21 Ag11 Ag14 53.53(6) .
Au1 Ag11 Ag14 109.39(3) .
AgC9 Ag11 Ag14 69.4(4) .
Ag5 Ag11 Ag14 63.10(2) .
Ag7 Ag11 Ag14 112.51(3) .
Ag12 Ag11 Ag14 168.20(3) .
Ag10 Ag11 Ag14 116.96(3) .
Ag19 Ag11 Ag14 128.53(3) .
Ag6 Ag11 Ag14 60.26(2) .
S24 Ag12 Au1 140.42(6) .
S24 Ag12 S23 75.27(8) .
Au1 Ag12 S23 143.96(6) .
S24 Ag12 Ag9 97.07(6) .
Au1 Ag12 Ag9 58.152(18) .
S23 Ag12 Ag9 139.45(6) .
S24 Ag12 Ag19 94.06(6) .
Au1 Ag12 Ag19 107.79(3) .
S23 Ag12 Ag19 52.32(6) .
Ag9 Ag12 Ag19 165.90(3) .
S24 Ag12 Ag10 138.68(6) .
Au1 Ag12 Ag10 59.196(19) .
S23 Ag12 Ag10 99.11(6) .
Ag9 Ag12 Ag10 60.45(2) .
Ag19 Ag12 Ag10 115.05(3) .
S24 Ag12 Ag11 155.20(6) .
Au1 Ag12 Ag11 57.894(19) .
S23 Ag12 Ag11 86.73(6) .
Ag9 Ag12 Ag11 107.66(3) .
Ag19 Ag12 Ag11 61.22(3) .
Ag10 Ag12 Ag11 60.21(2) .
S24 Ag12 Ag7 112.73(6) .
Au1 Ag12 Ag7 55.901(17) .
S23 Ag12 Ag7 114.12(6) .
Ag9 Ag12 Ag7 105.62(3) .
Ag19 Ag12 Ag7 61.82(2) .
Ag10 Ag12 Ag7 106.91(3) .
Ag11 Ag12 Ag7 59.28(2) .
S24 Ag12 Ag18 52.14(6) .
Au1 Ag12 Ag18 105.70(3) .
S23 Ag12 Ag18 94.24(6) .
Ag9 Ag12 Ag18 112.51(3) .
Ag19 Ag12 Ag18 68.22(3) .
Ag10 Ag12 Ag18 164.88(3) .
Ag11 Ag12 Ag18 113.91(3) .
Ag7 Ag12 Ag18 60.65(2) .
S24 Ag12 Ag8 84.72(6) .
Au1 Ag12 Ag8 56.455(17) .
S23 Ag12 Ag8 153.91(6) .
Ag9 Ag12 Ag8 58.70(2) .
Ag19 Ag12 Ag8 114.06(3) .
Ag10 Ag12 Ag8 106.98(3) .
Ag11 Ag12 Ag8 106.34(2) .
Ag7 Ag12 Ag8 58.632(19) .
Ag18 Ag12 Ag8 59.95(2) .
S2 Ag13 S10 123.47(10) .
S2 Ag13 S11 125.17(8) .
S10 Ag13 S11 109.35(9) .
S2 Ag13 Ag6 116.84(6) .
S10 Ag13 Ag6 103.09(7) .
S11 Ag13 Ag6 57.91(5) .
S2 Ag13 Ag5 82.00(6) .
S10 Ag13 Ag5 87.24(6) .
S11 Ag13 Ag5 116.24(6) .
Ag6 Ag13 Ag5 58.40(2) .
S2 Ag13 Ag2 60.17(6) .
S10 Ag13 Ag2 145.10(7) .
S11 Ag13 Ag2 85.43(6) .
Ag6 Ag13 Ag2 57.36(2) .
Ag5 Ag13 Ag2 58.07(2) .
S2 Ag13 Ag14 136.97(6) .
S10 Ag13 Ag14 47.95(7) .
S11 Ag13 Ag14 88.79(6) .
Ag6 Ag13 Ag14 55.82(2) .
Ag5 Ag13 Ag14 57.57(2) .
Ag2 Ag13 Ag14 103.26(3) .
S10 Ag14 S21 125.20(9) .
S10 Ag14 S12 112.12(9) .
S21 Ag14 S12 119.94(9) .
S10 Ag14 Ag11 143.41(8) .
S21 Ag14 Ag11 55.77(6) .
S12 Ag14 Ag11 88.82(6) .
S10 Ag14 Ag6 104.11(7) .
S21 Ag14 Ag6 115.37(7) .
S12 Ag14 Ag6 60.01(6) .
Ag11 Ag14 Ag6 59.69(2) .
S10 Ag14 Ag5 86.32(8) .
S21 Ag14 Ag5 84.40(6) .
S12 Ag14 Ag5 117.63(6) .
Ag11 Ag14 Ag5 57.13(2) .
Ag6 Ag14 Ag5 57.73(2) .
S10 Ag14 AgC9 104.6(3) .
S21 Ag14 AgC9 35.2(3) .
S12 Ag14 AgC9 141.1(3) .
Ag11 Ag14 AgC9 53.1(3) .
Ag6 Ag14 AgC9 99.6(3) .
Ag5 Ag14 AgC9 51.6(3) .
S10 Ag14 Ag13 48.78(7) .
S21 Ag14 Ag13 138.10(7) .
S12 Ag14 Ag13 92.22(6) .
Ag11 Ag14 Ag13 103.30(3) .
Ag6 Ag14 Ag13 56.02(2) .
Ag5 Ag14 Ag13 55.60(2) .
AgC9 Ag14 Ag13 103.0(3) .
S6 Ag15 S18 117.73(9) .
S6 Ag15 S7 123.42(9) .
S18 Ag15 S7 117.23(8) .
S6 Ag15 Ag4 117.12(7) .
S18 Ag15 Ag4 105.55(6) .
S7 Ag15 Ag4 57.53(7) .
S6 Ag15 Ag9 84.11(7) .
S18 Ag15 Ag9 82.76(6) .
S7 Ag15 Ag9 115.11(7) .
Ag4 Ag15 Ag9 57.66(2) .
S6 Ag15 Ag1 60.44(7) .
S18 Ag15 Ag1 141.32(6) .
S7 Ag15 Ag1 84.27(6) .
Ag4 Ag15 Ag1 57.21(2) .
Ag9 Ag15 Ag1 58.61(2) .
S20 Ag16 S18 122.29(9) .
S20 Ag16 S8 122.16(9) .
S18 Ag16 S8 114.58(9) .
S20 Ag16 Ag9 84.67(6) .
S18 Ag16 Ag9 82.39(6) .
S8 Ag16 Ag9 113.41(6) .
S20 Ag16 Ag10 59.35(6) .
S18 Ag16 Ag10 139.52(6) .
S8 Ag16 Ag10 84.49(6) .
Ag9 Ag16 Ag10 57.13(2) .
S20 Ag16 Ag4 115.84(7) .
S18 Ag16 Ag4 102.45(6) .
S8 Ag16 Ag4 57.00(6) .
Ag9 Ag16 Ag4 56.48(2) .
Ag10 Ag16 Ag4 56.78(2) .
S4 Ag17 S15 111.56(8) .
S4 Ag17 S13 131.66(9) .
S15 Ag17 S13 113.96(8) .
S4 Ag17 Ag7 122.49(6) .
S15 Ag17 Ag7 109.78(6) .
S13 Ag17 Ag7 53.27(6) .
S4 Ag17 Ag8 86.13(6) .
S15 Ag17 Ag8 86.19(6) .
S13 Ag17 Ag8 112.00(6) .
Ag7 Ag17 Ag8 58.748(19) .
S4 Ag17 Ag3 65.80(6) .
S15 Ag17 Ag3 142.22(6) .
S13 Ag17 Ag3 87.08(6) .
Ag7 Ag17 Ag3 56.97(2) .
Ag8 Ag17 Ag3 56.295(19) .
S4 Ag17 Ag18 138.34(6) .
S15 Ag17 Ag18 51.51(6) .
S13 Ag17 Ag18 84.80(6) .
Ag7 Ag17 Ag18 58.37(2) .
Ag8 Ag17 Ag18 57.87(2) .
Ag3 Ag17 Ag18 103.55(3) .
S24 Ag18 S14 115.62(9) .
S24 Ag18 S15 120.41(9) .
S14 Ag18 S15 103.74(9) .
S24 Ag18 Ag12 59.52(7) .
S14 Ag18 Ag12 104.59(7) .
S15 Ag18 Ag12 147.12(6) .
S24 Ag18 Ag8 89.43(6) .
S14 Ag18 Ag8 140.54(7) .
S15 Ag18 Ag8 86.58(6) .
Ag12 Ag18 Ag8 60.84(2) .
S24 Ag18 Ag7 118.96(7) .
S14 Ag18 Ag7 82.21(7) .
S15 Ag18 Ag7 108.77(6) .
Ag12 Ag18 Ag7 59.52(2) .
Ag8 Ag18 Ag7 58.56(2) .
S24 Ag18 Ag17 145.37(7) .
S14 Ag18 Ag17 98.44(7) .
S15 Ag18 Ag17 51.56(6) .
Ag12 Ag18 Ag17 107.60(3) .
Ag8 Ag18 Ag17 58.38(2) .
Ag7 Ag18 Ag17 57.31(2) .
S24 Ag18 Ag19 89.63(7) .
S14 Ag18 Ag19 49.93(7) .
S15 Ag18 Ag19 148.53(6) .
Ag12 Ag18 Ag19 54.73(2) .
Ag8 Ag18 Ag19 104.19(3) .
Ag7 Ag18 Ag19 56.95(2) .
Ag17 Ag18 Ag19 109.17(3) .
S22 Ag19 S23 121.61(9) .
S22 Ag19 S14 113.07(10) .
S23 Ag19 S14 116.39(10) .
S22 Ag19 Ag12 127.60(7) .
S23 Ag19 Ag12 62.42(7) .
S14 Ag19 Ag12 106.69(7) .
S22 Ag19 Ag11 67.80(7) .
S23 Ag19 Ag11 91.67(7) .
S14 Ag19 Ag11 139.83(7) .
Ag12 Ag19 Ag11 59.80(2) .
S22 Ag19 Ag7 92.81(7) .
S23 Ag19 Ag7 122.64(7) .
S14 Ag19 Ag7 81.84(7) .
Ag12 Ag19 Ag7 60.25(2) .
Ag11 Ag19 Ag7 58.33(2) .
S22 Ag19 Ag18 143.89(7) .
S23 Ag19 Ag18 93.01(7) .
S14 Ag19 Ag18 49.70(6) .
Ag12 Ag19 Ag18 57.05(2) .
Ag11 Ag19 Ag18 104.28(3) .
Ag7 Ag19 Ag18 56.62(2) .
S4 AgB9 Ag8 104.7(6) .
S4 AgB9 Ag1 135.5(7) .
Ag8 AgB9 Ag1 63.3(4) .
S4 AgB9 Ag3 75.0(5) .
Ag8 AgB9 Ag3 62.8(4) .
Ag1 AgB9 Ag3 61.2(3) .
S21 AgC9 S19 150.0(10) .
S21 AgC9 Ag5 106.2(8) .
S19 AgC9 Ag5 101.7(7) .
S21 AgC9 Ag10 122.5(9) .
S19 AgC9 Ag10 62.1(5) .
Ag5 AgC9 Ag10 63.3(4) .
S21 AgC9 Ag11 63.5(5) .
S19 AgC9 Ag11 123.3(8) .
Ag5 AgC9 Ag11 62.2(4) .
Ag10 AgC9 Ag11 62.5(4) .
S21 AgC9 Ag14 49.9(4) .
S19 AgC9 Ag14 160.1(8) .
Ag5 AgC9 Ag14 59.9(4) .
Ag10 AgC9 Ag14 110.5(6) .
Ag11 AgC9 Ag14 57.5(3) .
Ag7 Au1 Ag5 116.58(2) .
Ag7 Au1 Ag9 116.78(2) .
Ag5 Au1 Ag9 116.49(2) .
Ag7 Au1 Ag8 64.875(17) .
Ag5 Au1 Ag8 177.87(2) .
Ag9 Au1 Ag8 63.266(18) .
Ag7 Au1 Ag11 64.198(19) .
Ag5 Au1 Ag11 63.43(2) .
Ag9 Au1 Ag11 115.62(2) .
Ag8 Au1 Ag11 118.66(2) .
Ag7 Au1 Ag1 116.56(2) .
Ag5 Au1 Ag1 115.34(2) .
Ag9 Au1 Ag1 65.10(2) .
Ag8 Au1 Ag1 62.558(18) .
Ag11 Au1 Ag1 178.73(2) .
Ag7 Au1 Ag4 179.35(2) .
Ag5 Au1 Ag4 63.260(19) .
Ag9 Au1 Ag4 63.712(19) .
Ag8 Au1 Ag4 115.27(2) .
Ag11 Au1 Ag4 116.05(2) .
Ag1 Au1 Ag4 63.18(2) .
Ag7 Au1 Ag12 65.152(19) .
Ag5 Au1 Ag12 116.02(2) .
Ag9 Au1 Ag12 62.35(2) .
Ag8 Au1 Ag12 65.883(19) .
Ag11 Au1 Ag12 63.22(2) .
Ag1 Au1 Ag12 117.97(2) .
Ag4 Au1 Ag12 115.49(2) .
Ag7 Au1 Ag3 63.348(18) .
Ag5 Au1 Ag3 116.54(2) .
Ag9 Au1 Ag3 116.53(2) .
Ag8 Au1 Ag3 62.438(18) .
Ag11 Au1 Ag3 117.67(2) .
Ag1 Au1 Ag3 62.37(2) .
Ag4 Au1 Ag3 116.11(2) .
Ag12 Au1 Ag3 117.92(2) .
Ag7 Au1 Ag6 63.108(18) .
Ag5 Au1 Ag6 63.596(19) .
Ag9 Au1 Ag6 179.89(2) .
Ag8 Au1 Ag6 116.65(2) .
Ag11 Au1 Ag6 64.34(2) .
Ag1 Au1 Ag6 114.94(2) .
Ag4 Au1 Ag6 116.39(2) .
Ag12 Au1 Ag6 117.57(2) .
Ag3 Au1 Ag6 63.44(2) .
Ag7 Au1 Ag2 114.50(2) .
Ag5 Au1 Ag2 63.621(19) .
Ag9 Au1 Ag2 118.23(2) .
Ag8 Au1 Ag2 114.48(2) .
Ag11 Au1 Ag2 116.20(2) .
Ag1 Au1 Ag2 62.61(2) .
Ag4 Au1 Ag2 64.86(2) .
Ag12 Au1 Ag2 179.39(2) .
Ag3 Au1 Ag2 62.10(2) .
Ag6 Au1 Ag2 61.86(2) .
Ag7 Au1 Ag10 117.26(2) .
Ag5 Au1 Ag10 63.628(19) .
Ag9 Au1 Ag10 62.926(19) .
Ag8 Au1 Ag10 117.37(2) .
Ag11 Au1 Ag10 63.05(2) .
Ag1 Au1 Ag10 116.91(2) .
Ag4 Au1 Ag10 63.29(2) .
Ag12 Au1 Ag10 62.35(2) .
Ag3 Au1 Ag10 179.28(2) .
Ag6 Au1 Ag10 117.10(2) .
Ag2 Au1 Ag10 117.65(2) .
O1 C1 C2 112.8(11) .
C3 C2 C1 117.6(12) .
O2 C4 C5 110.2(10) .
C6 C5 C4 112.2(12) .
O3 C7 C8 110.7(8) .
C7 C8 C9 111.4(9) .
O4 C10 C11 107.8(8) .
C10 C11 C12 112.9(11) .
C14 C13 O5 110.4(13) .
C13 C14 C15 93.3(16) .
O6 C16 C17 105.0(11) .
C18 C17 C16 107.4(15) .
C20 C19 O7 111.2(11) .
C19 C20 C21 112.2(12) .
O8 C22 C23 109.0(11) .
C22 C23 C24 119.7(14) .
O9 C25 C26 108.8(12) .
C25 C26 C27 99.5(12) .
O10 C28 C29 112.5(13) .
C30 C29 C28 106.7(15) .
O11 C31 C32 109.7(9) .
C31 C32 C33 113.2(10) .
O12 C34 C35 110.7(8) .
C34 C35 C36 110.4(9) .
O13 C37 C38 110.3(13) .
C37 C38 C39 114.0(16) .
O14 C40 C41 105.3(12) .
C42 C41 C40 105.7(14) .
O15 C43 C44 108.2(9) .
C43 C44 C45 114.4(10) .
O16 C46 C47 112.4(13) .
C46 C47 C48 111.9(14) .
O17 C49 C50 112.5(12) .
C51 C50 C49 120.1(15) .
O18 C52 C53 108.3(10) .
C54 C53 C52 108.6(13) .
O19 C55 C56 108.5(10) .
C55 C56 C57 113.1(12) .
O20 C58 C59 103.7(11) .
C60 C59 C58 117.7(18) .
O21 C61 C62 108.8(12) .
C63 C62 C61 111.8(15) .
O22 C64 C65 106.3(12) .
C66 C65 C64 109.9(14) .
C68 C67 O23 110.0(11) .
C67 C68 C69 101.6(14) .
O24 C70 C71 109.9(10) .
C70 C71 C72 112.3(12) .
C74 C73 C73 117(3) 3_676
C75 C74 C73 116(2) .
C1 O1 P1 122.9(7) .
C4 O2 P1 119.3(6) .
C7 O3 P2 118.4(5) .
C10 O4 P2 122.7(6) .
C13 O5 P3 119.1(9) .
C16 O6 P3 123.2(8) .
C19 O7 P4 120.2(7) .
C22 O8 P4 118.9(6) .
C25 O9 P5 120.5(9) .
C28 O10 P5 127.7(10) .
C31 O11 P6 120.7(6) .
C34 O12 P6 117.8(6) .
C37 O13 P7 127.5(11) .
C40 O14 P7 125.5(9) .
C43 O15 P8 121.1(6) .
C46 O16 P8 120.4(8) .
C49 O17 P9 125.9(7) .
C52 O18 P9 120.0(6) .
C55 O19 P10 121.6(7) .
C58 O20 P10 121.2(8) .
C61 O21 P11 122.6(7) .
C64 O22 P11 121.9(8) .
C67 O23 P12 119.0(6) .
C70 O24 P12 121.4(7) .
O2 P1 O1 101.9(4) .
O2 P1 S1 112.8(3) .
O1 P1 S1 108.4(3) .
O2 P1 S2 108.3(3) .
O1 P1 S2 109.9(3) .
S1 P1 S2 114.81(15) .
O4 P2 O3 101.1(3) .
O4 P2 S3 107.5(3) .
O3 P2 S3 111.3(3) .
O4 P2 S4 111.8(3) .
O3 P2 S4 107.7(3) .
S3 P2 S4 116.40(14) .
O6 P3 O5 101.8(4) .
O6 P3 S5 107.2(3) .
O5 P3 S5 112.1(3) .
O6 P3 S6 112.1(3) .
O5 P3 S6 106.3(4) .
S5 P3 S6 116.48(16) .
O7 P4 O8 101.8(4) .
O7 P4 S8 109.0(3) .
O8 P4 S8 110.2(4) .
O7 P4 S7 111.8(3) .
O8 P4 S7 107.7(3) .
S8 P4 S7 115.51(16) .
O10 P5 O9 100.0(6) .
O10 P5 S9 106.0(6) .
O9 P5 S9 121.8(4) .
O10 P5 S10 107.3(5) .
O9 P5 S10 101.8(4) .
S9 P5 S10 117.9(2) .
O10 P5 S9B 119.7(6) .
O9 P5 S9B 101.1(4) .
S10 P5 S9B 122.3(2) .
O11 P6 O12 101.9(3) .
O11 P6 S12 108.3(3) .
O12 P6 S12 108.6(3) .
O11 P6 S11 113.1(3) .
O12 P6 S11 108.2(3) .
S12 P6 S11 115.74(14) .
O14 P7 O13 113.4(7) .
O14 P7 S13 110.8(4) .
O13 P7 S13 101.4(5) .
O14 P7 S14 101.3(4) .
O13 P7 S14 109.5(4) .
S13 P7 S14 120.93(17) .
O15 P8 O16 101.2(4) .
O15 P8 S16 108.1(3) .
O16 P8 S16 110.5(3) .
O15 P8 S15 110.0(3) .
O16 P8 S15 106.7(3) .
S16 P8 S15 118.95(15) .
O17 P9 O18 100.7(4) .
O17 P9 S17 113.1(3) .
O18 P9 S17 110.4(3) .
O17 P9 S18 104.7(3) .
O18 P9 S18 107.0(3) .
S17 P9 S18 119.12(15) .
O19 P10 O20 100.6(4) .
O19 P10 S19 113.7(3) .
O20 P10 S19 111.3(3) .
O19 P10 S20 105.9(3) .
O20 P10 S20 109.2(3) .
S19 P10 S20 115.11(16) .
O21 P11 O22 101.1(4) .
O21 P11 S21 112.4(4) .
O22 P11 S21 102.9(4) .
O21 P11 S22 108.5(3) .
O22 P11 S22 113.7(4) .
S21 P11 S22 117.00(16) .
O24 P12 O23 101.2(4) .
O24 P12 S24 108.8(3) .
O23 P12 S24 108.3(3) .
O24 P12 S23 112.7(3) .
O23 P12 S23 108.1(3) .
S24 P12 S23 116.51(16) .
P1 S1 Ag2 87.17(11) .
P1 S2 Ag13 96.96(12) .
P1 S2 Ag2 80.43(10) .
Ag13 S2 Ag2 68.95(6) .
P2 S3 Ag3 92.73(11) .
P2 S4 AgB9 126.8(5) .
P2 S4 Ag17 100.53(12) .
AgB9 S4 Ag17 95.5(4) .
P3 S5 Ag1 86.52(12) .
P3 S6 Ag15 100.87(13) .
P3 S6 Ag1 78.59(12) .
Ag15 S6 Ag1 69.89(7) .
P4 S7 Ag15 100.27(13) .
P4 S7 Ag4 84.19(12) .
Ag15 S7 Ag4 70.75(7) .
P4 S8 Ag16 102.87(13) .
P4 S8 Ag4 83.35(11) .
Ag16 S8 Ag4 72.53(6) .
P5 S9 Ag5 111.5(3) .
P5 S9B Ag5 102.5(3) .
P5 S10 Ag14 101.75(13) .
P5 S10 Ag13 97.48(15) .
Ag14 S10 Ag13 83.27(8) .
P6 S11 Ag13 107.60(12) .
P6 S11 Ag6 84.99(10) .
Ag13 S11 Ag6 69.25(6) .
P6 S12 Ag14 104.67(12) .
P6 S12 Ag6 82.95(11) .
Ag14 S12 Ag6 67.78(6) .
P7 S13 Ag7 100.54(14) .
P7 S13 Ag17 108.86(14) .
Ag7 S13 Ag17 70.78(6) .
P7 S14 Ag18 105.76(14) .
P7 S14 Ag19 103.76(15) .
Ag18 S14 Ag19 80.37(8) .
P8 S15 Ag18 103.74(12) .
P8 S15 Ag17 99.55(11) .
Ag18 S15 Ag17 76.93(7) .
P8 S16 Ag8 105.80(12) .
P9 S17 Ag9 103.60(12) .
P9 S18 Ag15 102.43(12) .
P9 S18 Ag16 103.45(12) .
Ag15 S18 Ag16 84.91(8) .
P10 S19 AgC9 137.7(6) .
P10 S19 Ag10 86.49(12) .
AgC9 S19 Ag10 72.4(5) .
P10 S20 Ag16 98.49(13) .
P10 S20 Ag10 80.80(11) .
Ag16 S20 Ag10 70.10(7) .
AgC9 S21 P11 150.9(6) .
AgC9 S21 Ag14 94.9(6) .
P11 S21 Ag14 102.44(13) .
AgC9 S21 Ag11 75.5(6) .
P11 S21 Ag11 88.26(12) .
Ag14 S21 Ag11 70.70(7) .
P11 S22 Ag19 109.60(13) .
P12 S23 Ag19 104.10(14) .
P12 S23 Ag12 83.14(12) .
Ag19 S23 Ag12 65.27(7) .
P12 S24 Ag18 105.92(13) .
P12 S24 Ag12 84.99(12) .
Ag18 S24 Ag12 68.34(6) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 S5 2.548(3) .
Ag1 Au1 2.7757(7) .
Ag1 AgB9 2.810(17) .
Ag1 S6 2.825(3) .
Ag1 Ag8 2.8716(8) .
Ag1 Ag3 2.8904(9) .
Ag1 Ag2 2.9024(9) .
Ag1 Ag4 2.9086(9) .
Ag1 Ag9 2.9749(9) .
Ag1 Ag15 3.0501(9) .
Ag2 S1 2.603(2) .
Ag2 Au1 2.8101(7) .
Ag2 S2 2.813(2) .
Ag2 Ag6 2.8874(9) .
Ag2 Ag3 2.8966(9) .
Ag2 Ag5 2.9268(9) .
Ag2 Ag4 2.9959(9) .
Ag2 Ag13 3.0263(10) .
Ag3 S3 2.505(2) .
Ag3 Au1 2.8060(7) .
Ag3 AgB9 2.866(17) .
Ag3 Ag8 2.8826(8) .
Ag3 Ag7 2.8923(8) .
Ag3 Ag6 2.9516(9) .
Ag3 Ag17 3.1010(9) .
Ag4 S7 2.703(3) .
Ag4 S8 2.750(2) .
Ag4 Au1 2.7766(7) .
Ag4 Ag5 2.8940(9) .
Ag4 Ag9 2.9187(9) .
Ag4 Ag10 2.9335(10) .
Ag4 Ag15 3.0248(10) .
Ag4 Ag16 3.1273(10) .
Ag5 S9 2.449(6) .
Ag5 S9B 2.498(6) .
Ag5 Au1 2.7415(6) .
Ag5 AgC9 2.782(19) .
Ag5 Ag11 2.8940(9) .
Ag5 Ag6 2.9245(8) .
Ag5 Ag10 2.9296(9) .
Ag5 Ag13 3.0039(9) .
Ag5 Ag14 3.0728(10) .
Ag6 S11 2.709(2) .
Ag6 S12 2.791(3) .
Ag6 Au1 2.8076(7) .
Ag6 Ag7 2.8833(8) .
Ag6 Ag11 2.9663(9) .
Ag6 Ag14 2.9833(10) .
Ag6 Ag13 2.9903(9) .
Ag7 S13 2.510(2) .
Ag7 Au1 2.6995(6) .
Ag7 Ag11 2.9033(8) .
Ag7 Ag8 2.9259(8) .
Ag7 Ag17 2.9575(9) .
Ag7 Ag12 2.9582(8) .
Ag7 Ag18 2.9920(9) .
Ag7 Ag19 3.0036(10) .
Ag8 S16 2.470(2) .
Ag8 AgB9 2.657(16) .
Ag8 Au1 2.7548(6) .
Ag8 Ag9 2.8889(8) .
Ag8 Ag18 2.9903(9) .
Ag8 Ag17 3.0070(9) .
Ag8 Ag12 3.0168(9) .
Ag9 S17 2.473(2) .
Ag9 Au1 2.7533(6) .
Ag9 Ag12 2.8710(9) .
Ag9 Ag10 2.9066(9) .
Ag9 Ag15 3.0276(10) .
Ag9 Ag16 3.0390(9) .
Ag10 S19 2.600(3) .
Ag10 S20 2.782(3) .
Ag10 AgC9 2.804(19) .
Ag10 Au1 2.8146(7) .
Ag10 Ag12 2.9025(9) .
Ag10 Ag11 2.9167(9) .
Ag10 Ag16 3.0401(10) .
Ag11 S21 2.608(3) .
Ag11 Au1 2.7632(7) .
Ag11 AgC9 2.82(2) .
Ag11 Ag12 2.9122(9) .
Ag11 Ag19 2.9532(11) .
Ag11 Ag14 2.9772(10) .
Ag12 S24 2.752(3) .
Ag12 Au1 2.7927(7) .
Ag12 S23 2.818(3) .
Ag12 Ag19 2.8875(10) .
Ag12 Ag18 2.9678(10) .
Ag13 S2 2.516(3) .
Ag13 S10 2.535(3) .
Ag13 S11 2.549(2) .
Ag13 Ag14 3.3469(11) .
Ag14 S10 2.502(3) .
Ag14 S21 2.537(3) .
Ag14 S12 2.547(3) .
Ag14 AgC9 3.303(19) .
Ag15 S6 2.476(3) .
Ag15 S18 2.509(3) .
Ag15 S7 2.515(3) .
Ag16 S20 2.497(3) .
Ag16 S18 2.517(3) .
Ag16 S8 2.528(3) .
Ag17 S4 2.486(3) .
Ag17 S15 2.547(3) .
Ag17 S13 2.595(3) .
Ag17 Ag18 3.1669(10) .
Ag18 S24 2.521(3) .
Ag18 S14 2.541(3) .
Ag18 S15 2.545(3) .
Ag18 Ag19 3.2842(11) .
Ag19 S22 2.477(3) .
Ag19 S23 2.516(3) .
Ag19 S14 2.549(3) .
AgB9 S4 2.084(16) .
AgC9 S21 1.909(19) .
AgC9 S19 2.096(19) .
C1 O1 1.416(14) .
C1 C2 1.494(9) .
C2 C3 1.490(9) .
C4 O2 1.427(14) .
C4 C5 1.512(17) .
C5 C6 1.487(18) .
C7 O3 1.460(11) .
C7 C8 1.470(14) .
C8 C9 1.516(16) .
C10 O4 1.455(10) .
C10 C11 1.489(14) .
C11 C12 1.503(17) .
C13 C14 1.43(2) .
C13 O5 1.473(15) .
C14 C15 1.67(3) .
C16 O6 1.438(14) .
C16 C17 1.564(19) .
C17 C18 1.52(2) .
C19 C20 1.449(18) .
C19 O7 1.468(15) .
C20 C21 1.534(19) .
C22 O8 1.457(13) .
C22 C23 1.492(9) .
C23 C24 1.494(10) .
C25 O9 1.397(9) .
C25 C26 1.503(9) .
C26 C27 1.511(9) .
C28 O10 1.405(9) .
C28 C29 1.504(9) .
C29 C30 1.500(10) .
C31 O11 1.475(11) .
C31 C32 1.491(14) .
C32 C33 1.510(17) .
C34 O12 1.459(11) .
C34 C35 1.484(14) .
C35 C36 1.515(14) .
C37 O13 1.393(9) .
C37 C38 1.497(9) .
C38 C39 1.509(10) .
C40 O14 1.413(15) .
C40 C41 1.522(9) .
C41 C42 1.497(9) .
C43 O15 1.447(11) .
C43 C44 1.489(15) .
C44 C45 1.494(17) .
C46 O16 1.426(14) .
C46 C47 1.495(9) .
C47 C48 1.509(10) .
C49 O17 1.465(13) .
C49 C50 1.507(9) .
C50 C51 1.501(10) .
C52 O18 1.442(14) .
C52 C53 1.513(9) .
C53 C54 1.507(9) .
C55 O19 1.444(12) .
C55 C56 1.479(17) .
C56 C57 1.50(2) .
C58 O20 1.460(14) .
C58 C59 1.54(2) .
C59 C60 1.44(2) .
C61 O21 1.438(14) .
C61 C62 1.51(2) .
C62 C63 1.48(2) .
C64 O22 1.420(16) .
C64 C65 1.519(9) .
C65 C66 1.505(10) .
C67 C68 1.437(17) .
C67 O23 1.457(13) .
C68 C69 1.68(3) .
C70 O24 1.468(13) .
C70 C71 1.474(16) .
C71 C72 1.497(17) .
C73 C74 1.48(3) .
C73 C73 1.50(4) 3_676
C74 C75 1.47(3) .
O1 P1 1.621(8) .
O2 P1 1.576(8) .
O3 P2 1.591(6) .
O4 P2 1.581(6) .
O5 P3 1.579(8) .
O6 P3 1.561(7) .
O7 P4 1.568(7) .
O8 P4 1.583(7) .
O9 P5 1.556(9) .
O10 P5 1.551(10) .
O11 P6 1.566(7) .
O12 P6 1.588(6) .
O13 P7 1.602(11) .
O14 P7 1.592(11) .
O15 P8 1.583(6) .
O16 P8 1.584(7) .
O17 P9 1.570(7) .
O18 P9 1.584(7) .
O19 P10 1.578(7) .
O20 P10 1.595(8) .
O21 P11 1.582(8) .
O22 P11 1.592(8) .
O23 P12 1.580(7) .
O24 P12 1.577(7) .
P1 S1 1.963(3) .
P1 S2 2.025(4) .
P2 S3 1.973(3) .
P2 S4 2.009(3) .
P3 S5 1.981(4) .
P3 S6 2.020(4) .
P4 S8 1.994(4) .
P4 S7 2.016(4) .
P5 S9 1.888(7) .
P5 S10 2.014(5) .
P5 S9B 2.107(7) .
P6 S12 1.999(3) .
P6 S11 2.006(3) .
P7 S13 2.006(4) .
P7 S14 2.008(4) .
P8 S16 1.970(3) .
P8 S15 2.029(3) .
P9 S17 1.975(3) .
P9 S18 2.027(3) .
P10 S19 1.967(4) .
P10 S20 2.014(4) .
P11 S21 1.992(4) .
P11 S22 1.994(4) .
P12 S24 1.997(4) .
P12 S23 2.002(4) .
