#------------------------------------------------------------------------------
#$Date: 2019-03-09 01:24:54 +0200 (Sat, 09 Mar 2019) $
#$Revision: 214055 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/55/07/1550726.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1550726
loop_
_publ_author_name
'Castells-Gil, Javier'
'Padial, Natalia M.'
'Almora-Barrios, Neyvis'
'da Silva, Ivan'
'Mateo, Diego'
'Albero, Josep'
'Garcia, Hermenegildo'
'Martí-Gastaldo, Carlos'
_publ_section_title
;
 De novo synthesis of mesoporous photoactive titanium(IV)-organic
 frameworks with MIL-100 topology
;
_journal_name_full               'Chemical Science'
_journal_paper_doi               10.1039/C8SC05218B
_journal_year                    2019
_chemical_formula_moiety         'C306 H102 O272 Ti51, 40.92(C2 H6 O)'
_chemical_formula_sum            'C387.84 H347.52 O312.92 Ti51'
_chemical_formula_weight         12456.26
_chemical_name_mineral           MIL-100(Ti)
_space_group_IT_number           227
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-F 4vw 2vw 3'
_symmetry_space_group_name_H-M   'F d -3 m :2'
_audit_update_record
;
2018-10-03 deposited with the CCDC.    2019-03-08 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   73.5168(16)
_cell_length_b                   73.5168(16)
_cell_length_c                   73.5168(16)
_cell_measurement_temperature    298
_cell_volume                     397338(15)
_diffrn_ambient_temperature      298
_diffrn_measurement_device_type  'PANalytical Empyrean'
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.540596
_diffrn_source                   'sealed X-ray tube'
_exptl_crystal_density_diffrn    0.83062
_pd_meas_scan_method             cont
_pd_proc_ls_prof_R_factor        3.85826177
_pd_proc_ls_prof_wR_expected     1.92590173
_pd_proc_ls_prof_wR_factor       5.24425273
_pd_spec_mounting                'borosilicate capillary'
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_refine_ls_goodness_of_fit_all   2.72301159
_refine_ls_R_factor_all          1.885114
_refine_ls_shift/su_max          0.001
_cod_data_source_file            c8sc05218b2.cif
_cod_data_source_block           MIL-100(Ti)
_cod_original_cell_volume        397340(30)
_cod_database_code               1550726
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z '
'-x, -z, -y '
'-x+1/4, -z-1/4, y+1/2 '
'-x+1/4, y+1/2, -z-1/4 '
'-x+1/2, z-1/4, y+1/4 '
'-x+1/2, y+1/4, z-1/4 '
'-x-1/4, -y+1/4, z+1/2 '
'-x-1/4, z+1/2, -y+1/4 '
'-y, -x, -z '
'-y, -z, -x '
'-y+1/4, -x-1/4, z+1/2 '
'-y+1/4, z+1/2, -x-1/4 '
'-y+1/2, z+1/4, x-1/4 '
'-y+1/2, x-1/4, z+1/4 '
'-y-1/4, -z+1/4, x+1/2 '
'-y-1/4, x+1/2, -z+1/4 '
'-z, -x, -y '
'-z, -y, -x '
'-z+1/4, -y-1/4, x+1/2 '
'-z+1/4, x+1/2, -y-1/4 '
'-z+1/2, y-1/4, x+1/4 '
'-z+1/2, x+1/4, y-1/4 '
'-z-1/4, -x+1/4, y+1/2 '
'-z-1/4, y+1/2, -x+1/4 '
'z, y, x '
'z, x, y '
'z+1/4, -y+1/2, x-1/4 '
'z+1/4, x-1/4, -y+1/2 '
'z+1/2, -x-1/4, -y+1/4 '
'z+1/2, -y+1/4, -x-1/4 '
'z-1/4, -x+1/2, y+1/4 '
'z-1/4, y+1/4, -x+1/2 '
'y, z, x '
'y, x, z '
'y+1/4, -x+1/2, z-1/4 '
'y+1/4, z-1/4, -x+1/2 '
'y+1/2, -x+1/4, -z-1/4 '
'y+1/2, -z-1/4, -x+1/4 '
'y-1/4, -z+1/2, x+1/4 '
'y-1/4, x+1/4, -z+1/2 '
'x, z, y '
'-x, -y, -z '
'x+1/4, -z+1/2, y-1/4 '
'x+1/4, y-1/4, -z+1/2 '
'x+1/2, -y-1/4, -z+1/4 '
'x+1/2, -z+1/4, -y-1/4 '
'x-1/4, -y+1/2, z+1/4 '
'x-1/4, z+1/4, -y+1/2 '
'x+1/2, y+1/2, z '
'-x+1/2, -z+1/2, -y '
'-x-1/4, -z+1/4, y+1/2 '
'-x-1/4, y, -z-1/4 '
'-x, z+1/4, y+1/4 '
'-x, y-1/4, z-1/4 '
'-x+1/4, -y-1/4, z+1/2 '
'-x+1/4, z, -y+1/4 '
'-y+1/2, -x+1/2, -z '
'-y+1/2, -z+1/2, -x '
'-y-1/4, -x+1/4, z+1/2 '
'-y-1/4, z, -x-1/4 '
'-y, z-1/4, x-1/4 '
'-y, x+1/4, z+1/4 '
'-y+1/4, -z-1/4, x+1/2 '
'-y+1/4, x, -z+1/4 '
'-z+1/2, -x+1/2, -y '
'-z+1/2, -y+1/2, -x '
'-z-1/4, -y+1/4, x+1/2 '
'-z-1/4, x, -y-1/4 '
'-z, y+1/4, x+1/4 '
'-z, x-1/4, y-1/4 '
'-z+1/4, -x-1/4, y+1/2 '
'-z+1/4, y, -x+1/4 '
'z+1/2, y+1/2, x '
'z+1/2, x+1/2, y '
'z-1/4, -y, x-1/4 '
'z-1/4, x+1/4, -y+1/2 '
'z, -x+1/4, -y+1/4 '
'z, -y-1/4, -x-1/4 '
'z+1/4, -x, y+1/4 '
'z+1/4, y-1/4, -x+1/2 '
'y+1/2, z+1/2, x '
'y+1/2, x+1/2, z '
'y-1/4, -x, z-1/4 '
'y-1/4, z+1/4, -x+1/2 '
'y, -x-1/4, -z-1/4 '
'y, -z+1/4, -x+1/4 '
'y+1/4, -z, x+1/4 '
'y+1/4, x-1/4, -z+1/2 '
'x+1/2, z+1/2, y '
'-x+1/2, -y+1/2, -z '
'x-1/4, -z, y-1/4 '
'x-1/4, y+1/4, -z+1/2 '
'x, -y+1/4, -z+1/4 '
'x, -z-1/4, -y-1/4 '
'x+1/4, -y, z+1/4 '
'x+1/4, z-1/4, -y+1/2 '
'x+1/2, y, z+1/2 '
'-x+1/2, -z, -y+1/2 '
'-x-1/4, -z-1/4, y '
'-x-1/4, y+1/2, -z+1/4 '
'-x, z-1/4, y-1/4 '
'-x, y+1/4, z+1/4 '
'-x+1/4, -y+1/4, z '
'-x+1/4, z+1/2, -y-1/4 '
'-y+1/2, -x, -z+1/2 '
'-y+1/2, -z, -x+1/2 '
'-y-1/4, -x-1/4, z '
'-y-1/4, z+1/2, -x+1/4 '
'-y, z+1/4, x+1/4 '
'-y, x-1/4, z-1/4 '
'-y+1/4, -z+1/4, x '
'-y+1/4, x+1/2, -z-1/4 '
'-z+1/2, -x, -y+1/2 '
'-z+1/2, -y, -x+1/2 '
'-z-1/4, -y-1/4, x '
'-z-1/4, x+1/2, -y+1/4 '
'-z, y-1/4, x-1/4 '
'-z, x+1/4, y+1/4 '
'-z+1/4, -x+1/4, y '
'-z+1/4, y+1/2, -x-1/4 '
'z+1/2, y, x+1/2 '
'z+1/2, x, y+1/2 '
'z-1/4, -y+1/2, x+1/4 '
'z-1/4, x-1/4, -y '
'z, -x-1/4, -y-1/4 '
'z, -y+1/4, -x+1/4 '
'z+1/4, -x+1/2, y-1/4 '
'z+1/4, y+1/4, -x '
'y+1/2, z, x+1/2 '
'y+1/2, x, z+1/2 '
'y-1/4, -x+1/2, z+1/4 '
'y-1/4, z-1/4, -x '
'y, -x+1/4, -z+1/4 '
'y, -z-1/4, -x-1/4 '
'y+1/4, -z+1/2, x-1/4 '
'y+1/4, x+1/4, -z '
'x+1/2, z, y+1/2 '
'-x+1/2, -y, -z+1/2 '
'x-1/4, -z+1/2, y+1/4 '
'x-1/4, y-1/4, -z '
'x, -y-1/4, -z-1/4 '
'x, -z+1/4, -y+1/4 '
'x+1/4, -y+1/2, z-1/4 '
'x+1/4, z+1/4, -y '
'x, y+1/2, z+1/2 '
'-x, -z+1/2, -y+1/2 '
'-x+1/4, -z+1/4, y '
'-x+1/4, y, -z+1/4 '
'-x+1/2, z+1/4, y-1/4 '
'-x+1/2, y-1/4, z+1/4 '
'-x-1/4, -y-1/4, z '
'-x-1/4, z, -y-1/4 '
'-y, -x+1/2, -z+1/2 '
'-y, -z+1/2, -x+1/2 '
'-y+1/4, -x+1/4, z '
'-y+1/4, z, -x+1/4 '
'-y+1/2, z-1/4, x+1/4 '
'-y+1/2, x+1/4, z-1/4 '
'-y-1/4, -z-1/4, x '
'-y-1/4, x, -z-1/4 '
'-z, -x+1/2, -y+1/2 '
'-z, -y+1/2, -x+1/2 '
'-z+1/4, -y+1/4, x '
'-z+1/4, x, -y+1/4 '
'-z+1/2, y+1/4, x-1/4 '
'-z+1/2, x-1/4, y+1/4 '
'-z-1/4, -x-1/4, y '
'-z-1/4, y, -x-1/4 '
'z, y+1/2, x+1/2 '
'z, x+1/2, y+1/2 '
'z+1/4, -y, x+1/4 '
'z+1/4, x+1/4, -y '
'z+1/2, -x+1/4, -y-1/4 '
'z+1/2, -y-1/4, -x+1/4 '
'z-1/4, -x, y-1/4 '
'z-1/4, y-1/4, -x '
'y, z+1/2, x+1/2 '
'y, x+1/2, z+1/2 '
'y+1/4, -x, z+1/4 '
'y+1/4, z+1/4, -x '
'y+1/2, -x-1/4, -z+1/4 '
'y+1/2, -z+1/4, -x-1/4 '
'y-1/4, -z, x-1/4 '
'y-1/4, x-1/4, -z '
'x, z+1/2, y+1/2 '
'-x, -y+1/2, -z+1/2 '
'x+1/4, -z, y+1/4 '
'x+1/4, y+1/4, -z '
'x+1/2, -y+1/4, -z-1/4 '
'x+1/2, -z-1/4, -y+1/4 '
'x-1/4, -y, z-1/4 '
'x-1/4, z-1/4, -y '
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_B_iso_or_equiv
C1et1 C 192 0.3746(7) 0.1739(18) 0.5301(14) 1.00(3) 10(4)
C2et1 C 192 0.388(3) 0.166(4) 0.544(2) 1.00(3) 10(4)
O1et1 O 192 0.384(3) 0.183(3) 0.516(2) 1.00(3) 10(4)
H2aet1 H 192 0.382(5) 0.160(3) 0.5537(19) 1.00(3) 12(5)
H2bet1 H 192 0.395(3) 0.175(6) 0.550(3) 1.00(3) 12(5)
H2cet1 H 192 0.396(4) 0.157(5) 0.539(3) 1.00(3) 12(5)
H1aet1 H 192 0.368(2) 0.183(2) 0.5363(17) 1.00(3) 12(5)
H1bet1 H 192 0.367(2) 0.164(3) 0.526(2) 1.00(3) 12(5)
H1Oet1 H 192 0.389(4) 0.192(4) 0.521(4) 1.00(3) 12(5)
C1et2 C 192 0.035(2) 0.9413(15) 0.992(3) 0.63(2) 10(7)
C2et2 C 192 0.025(7) 0.958(4) 0.985(7) 0.63(2) 10(7)
O1et2 O 192 0.028(6) 0.925(3) 0.985(8) 0.63(2) 10(7)
H2aet2 H 192 0.030(10) 0.969(2) 0.990(10) 0.63(2) 12(8)
H2bet2 H 192 0.012(6) 0.958(7) 0.989(9) 0.63(2) 12(8)
H2cet2 H 192 0.025(11) 0.960(6) 0.973(7) 0.63(2) 12(8)
H1aet2 H 192 0.033(5) 0.940(5) 1.005(3) 0.63(2) 12(8)
H1bet2 H 192 0.048(3) 0.943(5) 0.989(6) 0.63(2) 12(8)
H1Oet2 H 192 0.017(6) 0.925(6) 0.989(10) 0.63(2) 12(8)
C1et3 C 192 0.0579(15) 0.2733(11) 0.431(2) 0.97(3) 10(5)
C2et3 C 192 0.040(3) 0.273(4) 0.420(5) 0.97(3) 10(5)
O1et3 O 192 0.066(3) 0.2908(18) 0.431(5) 0.97(3) 10(5)
H2aet3 H 192 0.034(4) 0.262(5) 0.420(7) 0.97(3) 12(6)
H2bet3 H 192 0.042(5) 0.276(7) 0.408(4) 0.97(3) 12(6)
H2cet3 H 192 0.031(2) 0.281(5) 0.425(7) 0.97(3) 12(6)
H1aet3 H 192 0.066(3) 0.265(2) 0.425(4) 0.97(3) 12(6)
H1bet3 H 192 0.055(3) 0.269(3) 0.443(3) 0.97(3) 12(6)
H1Oet3 H 192 0.069(4) 0.292(4) 0.419(6) 0.97(3) 12(6)
C1et4 C 192 0.630(3) 0.7762(11) 0.6641(9) 0.74(3) 10(6)
C2et4 C 192 0.631(18) 0.758(3) 0.654(4) 0.74(3) 10(6)
O1et4 O 192 0.625(10) 0.791(3) 0.652(3) 0.74(3) 10(6)
H2aet4 H 192 0.63(2) 0.748(4) 0.662(5) 0.74(3) 12(7)
H2bet4 H 192 0.64(2) 0.758(11) 0.644(3) 0.74(3) 12(7)
H2cet4 H 192 0.62(2) 0.755(7) 0.648(7) 0.74(3) 12(7)
H1aet4 H 192 0.642(5) 0.779(10) 0.668(4) 0.74(3) 12(7)
H1bet4 H 192 0.622(4) 0.775(8) 0.674(3) 0.74(3) 12(7)
H1Oet4 H 192 0.634(10) 0.791(7) 0.645(4) 0.74(3) 12(7)
Ti25 Ti 192 0.3803(5) 0.5893(5) 0.9859(5) 1 2.3(3)
Ti26 Ti 192 0.2974(5) 0.5566(5) 0.0224(5) 1 2.3(3)
Ti58 Ti 96 0.2879(7) 0.5707(6) 0.0707(6) 1 2.3(3)
Ti67 Ti 96 0.3926(5) 0.6126(8) 0.8574(5) 1 2.3(3)
Ti71 Ti 96 0.1610(5) 0.5890(5) 0.0556(6) 1 2.3(3)
Ti73 Ti 96 0.4242(5) 0.5758(5) 1 1 2.3(3)
Ti76 Ti 48 0.375 0.6530(10) 0.875 1 2.3(3)
O59 O 96 0.296(2) 0.5497(17) 0.0497(17) 1 2.3(3)
O74 O 96 0.4060(14) 0.5940(14) 1 1 2.3(3)
O77 O 48 0.375 0.625(4) 0.875 1 2.3(3)
O79 O 32 0.172(2) 0.578(2) 1.078(2) 1 2.3(3)
O29 O 192 0.2985(13) 0.5649(14) 0.9927(15) 1 2.3(3)
O60 O 96 0.282(2) 0.5875(15) 0.0875(15) 1 2.3(3)
O68 O 96 0.4083(14) 0.594(2) 0.8417(14) 1 2.3(3)
O72 O 96 0.1458(14) 0.6042(14) 0.0331(17) 1 2.3(3)
O78 O 48 0.375 0.682(3) 0.875 1 2.3(3)
O34 O 192 0.3624(13) 0.5853(14) 0.9753(14) 1 2.3(3)
O75 O 96 0.4416(14) 0.5584(14) 1 1 2.3(3)
C10 C 192 0.4018(3) 0.6683(4) 0.9499(4) 1 2.3(3)
C11 C 192 0.3930(4) 0.6629(4) 0.9331(4) 1 2.3(3)
C13 C 192 0.3844(3) 0.6452(4) 0.9317(4) 1 2.3(3)
C14 C 192 0.3846(3) 0.6329(4) 0.9471(4) 1 2.3(3)
C16 C 192 0.3934(4) 0.6383(4) 0.9639(4) 1 2.3(3)
C17 C 192 0.4020(3) 0.6560(4) 0.9653(4) 1 2.3(3)
H12 H 192 0.3929(4) 0.6707(5) 0.9233(5) 1 2.3(3)
H15 H 192 0.3791(4) 0.6217(4) 0.9462(5) 1 2.3(3)
H18 H 192 0.4076(4) 0.6594(5) 0.9760(4) 1 2.3(3)
C23 C 192 0.3936(5) 0.6250(5) 0.9806(5) 1 2.3(3)
O35 O 192 0.3853(13) 0.6103(8) 0.9781(8) 1 2.3(3)
O38 O 192 0.4017(12) 0.6299(9) 0.9946(7) 1 2.3(3)
C24 C 192 0.3749(5) 0.6394(6) 0.9135(5) 1 2.3(3)
O39 O 192 0.3683(11) 0.6237(8) 0.9135(7) 1 2.3(3)
O43 O 192 0.3746(11) 0.6506(8) 0.9007(6) 1 2.3(3)
C9 C 192 0.4112(5) 0.6874(5) 0.9514(6) 1 2.3(3)
O44 O 192 0.4106(11) 0.6982(7) 0.9383(8) 1 2.3(3)
O31 O 192 0.4192(11) 0.6918(7) 0.9657(8) 1 2.3(3)
C48 C 96 0.4061(4) 0.5878(4) 0.9061(4) 1 2.3(3)
C3 C 192 0.4005(4) 0.5843(4) 0.9247(4) 1 2.3(3)
C2 C 192 0.4136(4) 0.5774(4) 0.9377(4) 1 2.3(3)
C46 C 96 0.4322(4) 0.5739(4) 0.9322(4) 1 2.3(3)
H4 H 192 0.3887(4) 0.5865(4) 0.9282(4) 1 2.3(3)
H47 H 96 0.4405(4) 0.5695(4) 0.9405(4) 1 2.3(3)
C1 C 192 0.4076(4) 0.5736(4) 0.9579(5) 1 2.3(3)
O41 O 192 0.4200(5) 0.5682(11) 0.9682(6) 1 2.3(3)
O37 O 192 0.3913(5) 0.5763(11) 0.9620(5) 1 2.3(3)
C49 C 96 0.3919(4) 0.5953(4) 0.8919(4) 1 2.3(3)
O40 O 192 0.3760(6) 0.5988(11) 0.8969(5) 1 2.3(3)
C7 C 192 0.3614(8) 0.5447(4) 0.0206(4) 1 2.3(3)
C6 C 192 0.3810(8) 0.5428(4) 0.0187(4) 1 2.3(3)
H8 H 192 0.3552(8) 0.5530(4) 0.0135(4) 1 2.3(3)
H51 H 96 0.4031(8) 0.5286(4) 0.0286(4) 1 2.3(3)
C5 C 192 0.3916(8) 0.5549(4) 0.0046(4) 1 2.3(3)
O42 O 192 0.4084(8) 0.5526(10) 0.0044(9) 1 2.3(3)
O36 O 192 0.3826(8) 0.5656(10) -0.0051(9) 1 2.3(3)
C53 C 96 0.3305(8) 0.5356(4) 0.0356(4) 1 2.3(3)
O32 O 192 0.3220(8) 0.5465(11) 0.0257(11) 1 2.3(3)
C52b C 96 0.352(3) 0.534(2) 0.034(2) 1 2.3(3)
C50b C 96 0.391(3) 0.530(2) 0.030(2) 1 2.3(3)
C65 C 96 0.2136(4) 0.5865(4) 0.0364(4) 1 2.3(3)
C21 C 192 0.2325(4) 0.5848(4) 0.0416(4) 1 2.3(3)
C20 C 192 0.2463(4) 0.5813(4) 0.0279(4) 1 2.3(3)
C63 C 96 0.2411(4) 0.5796(4) 0.0089(4) 1 2.3(3)
H22 H 192 0.2359(4) 0.5859(4) 0.0536(4) 1 2.3(3)
H64 H 96 0.2498(4) 0.5774(4) 0.0002(4) 1 2.3(3)
C19 C 192 0.2668(5) 0.5794(4) 0.0335(4) 1 2.3(3)
O33 O 192 0.2775(5) 0.5759(12) 0.0208(5) 1 2.3(3)
O45 O 192 0.2708(5) 0.5815(11) 0.0499(5) 1 2.3(3)
C66 C 96 0.1987(4) 0.5903(4) 0.0513(4) 1 2.3(3)
O27 O 192 0.1825(5) 0.5923(13) 0.0467(5) 1 2.3(3)
C61 C 96 0.25773(8) 0.51642(16) -0.00773(8) 1 2.3(3)
O30 O 192 0.2881(10) 0.5325(9) 0.0113(10) 1 2.3(3)
C55b C 96 0.265(2) 0.509(2) 0.009(2) 1 2.3(3)
C54b C 96 0.282(3) 0.518(2) 0.018(2) 1 2.3(3)
H62b H 96 0.263(13) 0.527(18) -0.013(13) 1 2.3(3)
H70 H 96 0.106(6) 0.567(6) 0.106(6) 1 2.3(3)
O28 O 192 0.135(8) 0.586(9) 0.065(9) 1 2.3(3)
C69b C 96 0.101(3) 0.577(4) 0.101(3) 1 2.3(3)
C57b C 96 0.110(3) 0.586(3) 0.086(3) 1 2.3(3)
C56b C 96 0.128(4) 0.578(2) 0.078(2) 1 2.3(3)
loop_
_pd_meas_2theta_scan
_pd_proc_intensity_total
_pd_calc_intensity_total
2.49407 10397.10153 10825.81885
2.50707 10261.82451 10738.00683
2.52007 10355.58360 10651.55486
2.53307 10283.90506 10566.47941
2.54607 10091.08650 10482.89901
2.55907 9945.23914 10400.76612
2.57207 10002.67790 10319.17683
2.58507 9744.45577 10238.76601
2.59807 9733.25446 10159.56531
2.61107 9815.79885 10081.56986
2.62407 9719.42780 10004.78038
2.63707 9655.88049 9929.20641
2.65007 9383.25295 9854.87451
2.66307 9434.83084 9781.85772
2.67607 9364.09544 9710.41849
2.68907 9367.62299 9640.56935
2.70207 9351.91376 9570.71772
2.71507 9206.09633 9501.56820
2.72807 9120.80757 9433.54719
2.74107 9164.39920 9366.66297
2.75407 9130.96091 9300.92756
2.76707 9036.45799 9236.35741
2.78007 8965.25795 9172.97420
2.79307 8914.72445 9110.80630
2.80607 8896.57088 9049.89089
2.81907 9002.21988 8990.27712
2.83207 9030.52311 8932.03237
2.84507 9105.48093 8875.26067
2.85807 9097.61757 8820.18285
2.87107 9057.82259 8766.87579
2.88407 9110.67880 8714.59243
2.89707 9049.84734 8664.17058
2.91007 9084.50544 8615.90254
2.92307 9179.24352 8570.15599
2.93607 9297.34084 8527.49873
2.94907 9302.47732 8489.06855
2.96207 9483.41336 8458.55476
2.97507 9563.95176 8449.19172
2.98807 9751.03773 8493.51160
3.00107 9917.26692 8634.24896
3.01407 10021.35876 8888.24836
3.02707 10172.67445 9233.39194
3.04007 10453.82146 9637.07095
3.05307 10678.61367 10079.97236
3.06607 11000.19453 10556.01610
3.07907 11484.39386 11065.21091
3.09207 11667.42465 11609.67978
3.10507 11967.38220 12192.43166
3.11807 12272.56700 12817.12785
3.13107 12893.97463 13488.10963
3.14407 13567.20597 14210.49937
3.15707 14068.61590 14990.34873
3.17007 14781.26777 15834.84207
3.18307 15733.29891 16752.58245
3.19607 16501.80439 17753.89685
3.20907 17596.20312 18851.09080
3.22207 18929.75111 20059.53242
3.23507 20170.42443 21398.53417
3.24807 21630.65513 22892.31075
3.26107 23479.38971 24571.99491
3.27407 25546.23750 26478.44018
3.28707 28003.59256 28666.58395
3.30007 30999.65041 31212.55523
3.31307 34301.75552 34225.96610
3.32607 38221.92127 37873.07045
3.33907 43449.63868 42426.63978
3.35207 50109.75301 48392.98321
3.36507 59051.32330 56834.69163
3.37807 72353.60410 69741.07213
3.39107 91325.69442 88381.95983
3.40407 108613.51913 106378.08895
3.41707 106630.24847 106379.28574
3.43007 80141.66431 80051.64336
3.44307 46353.79559 46070.15357
3.45607 23005.65383 23518.29254
3.46907 12899.68109 13561.43037
3.48207 9765.07328 10029.79658
3.49507 8729.63877 8763.73924
3.50807 8238.91828 8180.13675
3.52107 7984.19183 7823.33619
3.53407 7838.78474 7572.31775
3.54707 7765.09456 7386.26263
3.56007 7918.72922 7245.22203
3.57307 8034.47862 7137.45867
3.58607 8069.83011 7056.07134
3.59907 8206.68819 6998.02218
3.61207 8451.80411 6967.17053
3.62507 8801.65918 6987.04708
3.63807 9177.29696 7117.68887
3.65107 9309.67431 7436.63671
3.66407 9623.06825 7973.90350
3.67707 10114.45596 8691.11271
3.69007 10617.96168 9531.10780
3.70307 11220.65282 10459.85645
3.71607 11843.85853 11467.43691
3.72907 12517.20224 12555.99747
3.74207 13394.93448 13732.62664
3.75507 14533.78293 15007.09703
3.76807 15652.63472 16391.63029
3.78107 16805.83846 17901.64538
3.79407 18362.17688 19555.82439
3.80707 19948.36947 21379.80535
3.82007 21804.79632 23414.48119
3.83307 24278.09839 25727.48188
3.84607 27081.39170 28403.58696
3.85907 30034.28226 31510.71067
3.87207 33304.88255 35101.40657
3.88507 37732.78603 39256.23837
3.89807 43067.90058 44117.29592
3.91107 49631.03939 49914.85203
3.92407 57308.24042 57027.38873
3.93707 67127.78729 66144.87167
3.95007 80926.68932 78697.74230
3.96307 100224.02141 97437.94030
3.97607 127941.41654 124628.72847
3.98907 156880.68490 153023.10799
4.00207 161463.09005 159372.32238
4.01507 130129.24842 128131.76347
4.02807 81379.38683 80356.23890
4.04107 44665.57656 45626.21276
4.05407 28009.31218 29913.84884
4.06707 23659.33010 25233.93644
4.08007 23816.62442 24993.77311
4.09307 25736.99725 26481.79392
4.10607 28713.02121 29008.52953
4.11907 32933.61996 32696.55727
4.13207 39249.76539 38240.04476
4.14507 48523.58311 47048.54850
4.15807 61431.95776 59839.04065
4.17107 71153.11306 71209.25309
4.18407 67944.09176 68273.85942
4.19707 49696.42125 47847.66737
4.21007 28359.03506 26246.18719
4.22307 14576.36686 14032.71345
4.23607 8754.03274 9131.56678
4.24907 6881.70502 7400.87906
4.26207 6186.65880 6719.65336
4.27507 5736.34086 6355.30439
4.28807 5514.55493 6108.52076
4.30107 5400.94069 5924.46011
4.31407 5424.17762 5780.90663
4.32707 5249.15476 5665.57345
4.34007 5175.65724 5570.63336
4.35307 5167.75644 5490.91199
4.36607 5010.79606 5422.87156
4.37907 5001.93725 5364.02764
4.39207 5012.89484 5312.59748
4.40507 5032.99419 5267.28341
4.41807 4999.52941 5227.13658
4.43107 4971.76276 5191.47199
4.44407 5088.82963 5159.81632
4.45707 5034.79373 5131.88584
4.47007 4934.13142 5107.61248
4.48307 5032.43237 5087.37068
4.49607 5105.74586 5073.09139
4.50907 5121.23989 5071.37660
4.52207 5259.87025 5096.64846
4.53507 5288.91828 5166.35891
4.54807 5309.09820 5287.67495
4.56107 5443.24893 5453.20524
4.57407 5563.28878 5651.48300
4.58707 5772.85203 5875.76009
4.60007 5896.20266 6124.58504
4.61307 6016.51734 6399.48677
4.62607 6353.46382 6703.66130
4.63907 6606.10440 7041.79537
4.65207 6842.86149 7419.69274
4.66507 7231.99545 7844.45014
4.67807 7779.33589 8326.10313
4.69107 8456.61027 8877.85575
4.70407 9097.13592 9517.73457
4.71707 9940.90897 10271.34591
4.73007 11038.04527 11176.77085
4.74307 12324.48293 12294.59904
4.75607 13977.27059 13732.30999
4.76907 16256.08747 15708.90619
4.78207 19642.91800 18661.17421
4.79507 24218.87622 23060.74630
4.80807 29395.91650 28129.83062
4.82107 31728.14912 30350.97008
4.83407 27347.28525 26233.50944
4.84707 18731.67394 17924.96507
4.86007 11381.34725 10912.00430
4.87307 7291.83696 7230.22764
4.88607 5730.26516 5762.40236
4.89907 5151.14051 5230.34018
4.91207 4870.00444 5012.51874
4.92507 4871.72625 4894.05784
4.93807 4805.32607 4815.84710
4.95107 4764.06677 4762.05046
4.96407 4779.29529 4729.89195
4.97707 4828.35525 4725.68871
4.99007 4889.05192 4761.97834
5.00307 4914.31707 4845.07596
5.01607 4942.15735 4968.71613
5.02907 5040.09449 5122.67574
5.04207 5168.30426 5300.77156
5.05507 5290.98028 5502.72609
5.06807 5481.32936 5728.47390
5.08107 5703.35147 5983.41632
5.09407 5838.01979 6271.13830
5.10707 6239.16580 6597.95809
5.12007 6654.77853 6972.39768
5.13307 7018.06298 7406.16770
5.14607 7555.43670 7915.83398
5.15907 8240.10681 8525.81163
5.17207 8987.84437 9274.33496
5.18507 10025.56342 10227.44988
5.19807 11563.16302 11515.68191
5.21107 13664.03960 13405.15698
5.22407 16464.54624 16259.24455
5.23707 19967.03076 19865.13353
5.25007 21974.70238 22201.12299
5.26307 20136.35020 20368.33283
5.27607 14822.12321 14800.42827
5.28907 9669.13208 9489.63164
5.30207 6396.08278 6498.95415
5.31507 5151.10549 5249.87134
5.32807 4786.35455 4789.65359
5.34107 4607.03930 4606.11218
5.35407 4460.42256 4509.45635
5.36707 4485.45164 4445.62560
5.38007 4350.94276 4398.64830
5.39307 4342.19636 4362.46500
5.40607 4278.11729 4333.69106
5.41907 4260.02916 4310.20930
5.43207 4309.07124 4290.63331
5.44507 4309.33611 4274.02544
5.45807 4262.77930 4259.73544
5.47107 4306.64494 4247.30602
5.48407 4226.81386 4236.41415
5.49707 4223.83500 4226.76918
5.51007 4332.01563 4217.95729
5.52307 4300.20008 4210.05012
5.53607 4336.08076 4203.83574
5.54907 4278.08518 4198.42285
5.56207 4299.17602 4193.93465
5.57507 4264.09800 4190.42094
5.58807 4386.85721 4187.98513
5.60107 4415.58473 4186.80693
5.61407 4395.64259 4187.21800
5.62707 4392.02575 4190.09257
5.64007 4415.35875 4199.60957
5.65307 4567.31239 4223.91170
5.66607 4612.33286 4281.16853
5.67907 4613.23334 4381.96262
5.69207 4658.49979 4525.87890
5.70507 4829.04923 4704.43356
5.71807 4980.36118 4911.09135
5.73107 5192.35067 5144.57188
5.74407 5364.87342 5407.53289
5.75707 5475.05411 5705.22387
5.77007 5744.64566 6045.21071
5.78307 6159.69497 6437.99046
5.79607 6658.64876 6898.41859
5.80907 7242.87802 7448.35207
5.82207 7758.36803 8122.30681
5.83507 8580.88418 8981.03224
5.84807 9969.15814 10142.48318
5.86107 11740.63656 11847.08909
5.87407 14189.54528 14403.86476
5.88707 17158.20721 17559.27494
5.90007 18664.97357 19489.71885
5.91307 17003.08574 17829.01312
5.92607 12903.30265 13137.92506
5.93907 8717.60015 8680.01229
5.95207 6159.68859 6103.38820
5.96507 5109.83676 4989.72545
5.97807 4795.96917 4576.69128
5.99107 4681.54462 4424.30412
6.00407 4686.05390 4360.02124
6.01707 4781.36408 4342.35588
6.03007 4847.42359 4382.08562
6.04307 4968.87621 4505.75568
6.05607 5054.92926 4724.04856
6.06907 5270.80193 5024.59928
6.08207 5536.50583 5390.65287
6.09507 5773.10228 5814.57198
6.10807 6085.07270 6298.52268
6.12107 6569.25034 6851.61782
6.13407 7080.41265 7488.61680
6.14707 7716.48183 8230.82083
6.16007 8632.78040 9109.20166
6.17307 9766.07690 10170.88457
6.18607 11059.19270 11492.35627
6.19907 12883.53759 13213.39577
6.21207 15479.73104 15628.35716
6.22507 19222.99118 19306.46254
6.23807 24576.34621 24666.29037
6.25107 29079.65869 30010.41958
6.26407 29521.97645 30548.74001
6.27707 23906.66265 24053.34704
6.29007 15730.94484 15429.58134
6.30307 9575.08571 9345.86764
6.31607 6340.23704 6313.07449
6.32907 5080.81506 5080.30281
6.34207 4653.69184 4613.14806
6.35507 4437.47225 4407.55940
6.36807 4344.77154 4288.53453
6.38107 4292.05650 4206.78715
6.39407 4210.24439 4146.67985
6.40707 4193.88334 4100.87579
6.42007 4193.69735 4065.03353
6.43307 4119.73197 4036.37480
6.44607 4020.18222 4013.03253
6.45907 4100.23270 3993.84637
6.47207 4130.18875 3977.75264
6.48507 4091.99905 3964.63604
6.49807 4076.99082 3953.75794
6.51107 4120.18065 3944.84231
6.52407 4076.43623 3937.73130
6.53707 4059.32254 3932.37973
6.55007 4107.91300 3928.87518
6.56307 4071.23434 3927.56468
6.57607 4110.43370 3929.70024
6.58907 4139.57066 3939.51271
6.60207 4209.56692 3967.10816
6.61507 4337.63952 4026.39911
6.62807 4332.14612 4125.11988
6.64107 4477.00081 4260.48081
6.65407 4574.15973 4426.48849
6.66707 4765.05788 4620.59583
6.68007 4813.07388 4844.76171
6.69307 4981.50802 5104.68599
6.70607 5234.44740 5409.63250
6.71907 5536.40397 5773.50271
6.73207 5948.77529 6218.14048
6.74507 6545.78795 6780.78349
6.75807 7321.57698 7533.85832
6.77107 8372.27489 8624.87908
6.78407 9968.37936 10266.96987
6.79707 12137.66243 12395.91506
6.81007 13285.12938 13962.98244
6.82307 12595.07089 13294.18574
6.83607 9986.82972 10394.75962
6.84907 7377.29953 7353.07742
6.86207 5471.72834 5435.01260
6.87507 4589.87687 4532.74323
6.88807 4313.58633 4177.21497
6.90107 4220.11564 4045.60508
6.91407 4239.40298 3993.71407
6.92707 4151.54617 3983.23725
6.94007 4122.24606 4012.27451
6.95307 4208.90280 4081.52611
6.96607 4268.42688 4186.19032
6.97907 4306.41672 4320.84772
6.99207 4377.05747 4483.65828
7.00507 4520.59792 4676.94742
7.01807 4706.54215 4907.10139
7.03107 4917.97706 5184.86672
7.04407 5043.21619 5527.37844
7.05707 5395.24427 5963.74005
7.07007 5837.11116 6550.54200
7.08307 6491.47267 7401.36377
7.09607 7466.50131 8671.26922
7.10907 8762.69212 10290.21233
7.12207 9472.09534 11464.65058
7.13507 9068.03169 10983.31542
7.14807 7670.86201 8860.96910
7.16107 6044.02256 6600.70845
7.17407 4919.31004 5138.40744
7.18707 4358.78023 4444.52887
7.20007 4246.17481 4198.18099
7.21307 4204.13095 4143.40976
7.22607 4101.98642 4118.98792
7.23907 4053.26053 4044.33801
7.25207 4042.94516 3928.89237
7.26507 4001.84201 3825.64171
7.27807 3893.26124 3758.69580
7.29107 3861.88759 3721.40394
7.30407 3937.68706 3700.49779
7.31707 3930.31595 3686.92926
7.33007 3872.30355 3676.42348
7.34307 3832.96672 3667.52419
7.35607 3823.64692 3659.70194
7.36907 3858.38393 3652.70146
7.38207 3818.88634 3646.37178
7.39507 3861.92887 3640.61460
7.40807 3881.12184 3635.40103
7.42107 3880.38673 3631.02644
7.43407 3816.80690 3628.01240
7.44707 3783.09394 3626.87433
7.46007 3888.02769 3627.74916
7.47307 3913.24149 3630.45028
7.48607 3795.08631 3634.81006
7.49907 3806.30077 3640.86725
7.51207 3821.13390 3648.88776
7.52507 3804.40927 3659.45692
7.53807 3753.82608 3673.38761
7.55107 3779.06693 3692.63187
7.56407 3797.16928 3720.25631
7.57707 3792.35350 3762.69491
7.59007 3822.62042 3827.04656
7.60307 3982.98699 3903.54959
7.61607 3983.78770 3944.81064
7.62907 3972.78759 3899.51026
7.64207 3900.41963 3788.18526
7.65507 3805.21753 3680.33538
7.66807 3806.06308 3610.90103
7.68107 3799.97981 3575.66956
7.69407 3791.01123 3559.90442
7.70707 3733.16425 3552.76938
7.72007 3815.53604 3549.29345
7.73307 3730.30998 3548.09416
7.74607 3661.92302 3548.97659
7.75907 3650.52519 3551.85281
7.77207 3752.83576 3556.85611
7.78507 3764.70293 3564.86762
7.79807 3700.82412 3578.78886
7.81107 3747.00227 3604.78879
7.82407 3783.00505 3650.30993
7.83707 3845.70133 3719.66434
7.85007 3846.83732 3814.56832
7.86307 3962.78435 3938.47163
7.87607 3989.13520 4094.96731
7.88907 4064.92765 4272.79731
7.90207 4133.31374 4438.83380
7.91507 4145.47122 4588.17291
7.92807 4432.43703 4779.06705
7.94107 4667.57179 5090.22798
7.95407 5005.28871 5611.12891
7.96707 5516.37783 6389.64374
7.98007 6059.32766 7173.90708
7.99307 6070.99356 7304.17916
8.00607 5630.95271 6477.39262
8.01907 4911.68752 5311.97761
8.03207 4256.20792 4403.57037
8.04507 3773.68990 3886.19123
8.05807 3632.22733 3648.06285
8.07107 3646.28832 3551.45331
8.08407 3609.75485 3509.16521
8.09707 3581.48020 3485.07250
8.11007 3567.01881 3468.22486
8.12307 3468.70020 3455.38369
8.13607 3535.13624 3445.24961
8.14907 3464.34272 3437.28658
8.16207 3497.02475 3431.78948
8.17507 3592.09317 3429.96334
8.18807 3557.34495 3433.00364
8.20107 3544.25614 3441.47034
8.21407 3559.74495 3455.14129
8.22707 3542.56064 3473.76051
8.24007 3542.02495 3497.54639
8.25307 3555.54431 3527.55774
8.26607 3543.63366 3565.91165
8.27907 3615.96510 3616.57719
8.29207 3666.42574 3687.66563
8.30507 3756.38035 3794.62389
8.31807 3882.77584 3951.88241
8.33107 3994.16540 4128.57091
8.34407 4014.38218 4209.96081
8.35707 3954.46287 4098.02314
8.37007 3823.28970 3859.47294
8.38307 3595.17500 3635.14421
8.39607 3456.61861 3490.04133
8.40907 3434.66490 3418.22261
8.42207 3500.60891 3394.30156
8.43507 3559.18525 3400.76310
8.44807 3572.61584 3431.25169
8.46107 3598.14431 3483.68000
8.47407 3546.46891 3555.80505
8.48707 3562.82054 3646.78488
8.50007 3624.04457 3758.20884
8.51307 3787.72541 3894.86505
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