#------------------------------------------------------------------------------
#$Date: 2020-08-04 04:05:51 +0300 (Tue, 04 Aug 2020) $
#$Revision: 254752 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/55/87/1558743.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1558743
loop_
_publ_author_name
'Kephart, Jonathan'
'Romero, Catherine G.'
'Tseng, Chun-Chih'
'Anderton, Kevin J.'
'Yankowitz, Matthew'
'Kaminsky, Werner'
'Velian, Alexandra'
_publ_section_title
;
 Hierarchical Nanosheets Built from Superatomic Clusters: Properties,
 Exfoliation and Single-Crystal-to-Single-Crystal Intercalation
;
_journal_name_full               'Chemical Science'
_journal_paper_doi               10.1039/D0SC03506H
_journal_year                    2020
_chemical_formula_moiety         'C258 H228 Co18 N18 P12 Se16'
_chemical_formula_sum            'C258 H228 Co18 N18 P12 Se16'
_chemical_formula_weight         6276.31
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_audit_conform_dict_location     ftp://ftp.iucr.org/pub/cif_core.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.4.3
_audit_creation_date             2019-09-16T11:27:33-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_audit_update_record
;
2020-06-24 deposited with the CCDC.	2020-08-03 downloaded from the CCDC.
;
_cell_angle_alpha                109.902(5)
_cell_angle_beta                 97.084(5)
_cell_angle_gamma                102.271(4)
_cell_formula_units_Z            2
_cell_length_a                   19.0473(13)
_cell_length_b                   28.0304(18)
_cell_length_c                   30.824(3)
_cell_measurement_reflns_used    4337
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      15.14
_cell_measurement_theta_min      2.2
_cell_measurement_wavelength     0.71073
_cell_volume                     14774(2)
_computing_cell_refinement       'SAINT V8.34A integration software'
_computing_data_collection       'Bruker APEX2 software'
_computing_data_reduction        'SORTAV (Blessing, 1995)'
_computing_molecular_graphics    'ORTEP-3 for Windows (Farrugia, 2012)'
_computing_publication_material  'WinGX publication routines (Farrugia, 2012)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-2013/1 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector                 'APEX-II CCD'
_diffrn_measured_fraction_theta_full 0.911
_diffrn_measured_fraction_theta_max 0.881
_diffrn_measurement_device       'κ-geometry diffractometer'
_diffrn_measurement_device_type  'Bruker APEX-II'
_diffrn_measurement_method       'φ or ω oscillation scans'
_diffrn_orient_matrix_UB_11      0.009429
_diffrn_orient_matrix_UB_12      -0.005926
_diffrn_orient_matrix_UB_13      0.030147
_diffrn_orient_matrix_UB_21      0.041692
_diffrn_orient_matrix_UB_22      0.032895
_diffrn_orient_matrix_UB_23      0.013479
_diffrn_orient_matrix_UB_31      -0.034594
_diffrn_orient_matrix_UB_32      0.02093
_diffrn_orient_matrix_UB_33      0.012508
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.3504
_diffrn_reflns_av_unetI/netI     0.7904
_diffrn_reflns_Laue_measured_fraction_full 0.911
_diffrn_reflns_Laue_measured_fraction_max 0.881
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            87290
_diffrn_reflns_point_group_measured_fraction_full 0.911
_diffrn_reflns_point_group_measured_fraction_max 0.881
_diffrn_reflns_theta_full        25
_diffrn_reflns_theta_max         25.545
_diffrn_reflns_theta_min         1.353
_diffrn_source                   'sealed x-ray tube'
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.064
_exptl_absorpt_correction_T_max  0.745
_exptl_absorpt_correction_T_min  0.51
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2012/1 - Bruker AXS area detector scaling and absorption correction
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.411
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       piece
_exptl_crystal_F_000             6224
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.629
_refine_diff_density_min         -1.813
_refine_diff_density_rms         0.274
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.116
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     2407
_refine_ls_number_reflns         48703
_refine_ls_number_restraints     6251
_refine_ls_restrained_S_all      1.068
_refine_ls_R_factor_all          0.4204
_refine_ls_R_factor_gt           0.1683
_refine_ls_shift/su_max          0.007
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3907
_refine_ls_wR_factor_ref         0.5253
_reflns_Friedel_coverage         0
_reflns_number_gt                11662
_reflns_number_total             48703
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d0sc03506h2.cif
_cod_data_source_block           shelx_CCDC4
_cod_original_cell_volume        14773.8(19)
_cod_database_code               1558743
_shelx_estimated_absorpt_t_min   0.609
_shelx_estimated_absorpt_t_max   0.862
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Co13 Co 1.1728(3) -0.41254(19) 0.6521(2) 0.0508(17) Uani 1 1 d D . . . .
N13 N 1.1353(9) -0.3453(6) 0.6786(8) 0.056(6) Uani 1 1 d D U . . .
C229 C 1.1189(10) -0.3170(8) 0.6518(9) 0.058(6) Uani 1 1 d D U . . .
H229 H 1.1248 -0.3273 0.6201 0.069 Uiso 1 1 calc R U . . .
C230 C 1.0933(11) -0.2727(9) 0.6719(10) 0.062(6) Uani 1 1 d D U . . .
H230 H 1.082 -0.2533 0.6534 0.074 Uiso 1 1 calc R U . . .
C231 C 1.0840(12) -0.2566(9) 0.7182(10) 0.061(5) Uani 1 1 d D U . . .
C232 C 1.1008(13) -0.2856(9) 0.7450(9) 0.059(6) Uani 1 1 d D U . . .
H232 H 1.0951 -0.2757 0.7768 0.071 Uiso 1 1 calc R U . . .
C233 C 1.1260(12) -0.3290(9) 0.7243(8) 0.060(6) Uani 1 1 d D U . . .
H233 H 1.1374 -0.3486 0.7427 0.072 Uiso 1 1 calc R U . . .
P1 P 1.0807(5) -0.5091(3) 0.6643(4) 0.048(2) Uani 1 1 d D U . . .
N1 N 1.0862(9) -0.4697(7) 0.6330(7) 0.052(4) Uani 1 1 d D U . . .
C1 C 1.0270(11) -0.5755(5) 0.6226(6) 0.046(5) Uani 1 1 d DG U . . .
C2 C 0.9766(11) -0.6100(7) 0.6347(6) 0.059(6) Uani 1 1 d DG U . . .
H2 H 0.964 -0.5983 0.6647 0.071 Uiso 1 1 calc R U . . .
C3 C 0.9446(11) -0.6615(6) 0.6029(8) 0.050(6) Uani 1 1 d DG U . . .
H3 H 0.9102 -0.685 0.6111 0.06 Uiso 1 1 calc R U . . .
C4 C 0.9630(13) -0.6785(5) 0.5590(8) 0.065(7) Uani 1 1 d DG U . . .
H4 H 0.9412 -0.7137 0.5372 0.078 Uiso 1 1 calc R U . . .
C5 C 1.0134(13) -0.6441(8) 0.5469(6) 0.072(7) Uani 1 1 d DG U . . .
H5 H 1.026 -0.6557 0.5168 0.087 Uiso 1 1 calc R U . . .
C6 C 1.0454(11) -0.5926(7) 0.5787(7) 0.061(6) Uani 1 1 d DG U . . .
H6 H 1.0798 -0.569 0.5704 0.073 Uiso 1 1 calc R U . . .
C7 C 1.0242(11) -0.4875(8) 0.7081(6) 0.052(5) Uani 1 1 d DG U . . .
C8 C 1.0114(12) -0.5129(7) 0.7391(7) 0.048(5) Uani 1 1 d DG U . . .
H8 H 1.0265 -0.544 0.7355 0.058 Uiso 1 1 calc R U . . .
C9 C 0.9763(13) -0.4929(9) 0.7755(7) 0.068(6) Uani 1 1 d DG U . . .
H9 H 0.9675 -0.5103 0.7967 0.081 Uiso 1 1 calc R U . . .
C10 C 0.9542(12) -0.4474(10) 0.7808(7) 0.064(6) Uani 1 1 d DG U . . .
H10 H 0.9302 -0.4337 0.8057 0.077 Uiso 1 1 calc R U . . .
C11 C 0.9670(12) -0.4220(8) 0.7498(8) 0.070(6) Uani 1 1 d DG U . . .
H11 H 0.9519 -0.3909 0.7534 0.084 Uiso 1 1 calc R U . . .
C12 C 1.0021(12) -0.4420(8) 0.7134(7) 0.052(5) Uani 1 1 d DG U . . .
H12 H 1.0109 -0.4247 0.6922 0.062 Uiso 1 1 calc R U . . .
C13 C 1.0235(9) -0.4691(9) 0.6004(7) 0.055(5) Uani 1 1 d DG U . . .
C14 C 0.9529(10) -0.4998(8) 0.5950(7) 0.060(6) Uani 1 1 d DG U . . .
H14 H 0.9436 -0.519 0.6148 0.072 Uiso 1 1 calc R U . . .
C15 C 0.8960(8) -0.5025(8) 0.5606(8) 0.059(5) Uani 1 1 d DG U . . .
H15 H 0.8478 -0.5235 0.5569 0.071 Uiso 1 1 calc R U . . .
C16 C 0.9097(10) -0.4744(9) 0.5316(7) 0.058(6) Uani 1 1 d DG U . . .
C17 C 0.9803(11) -0.4437(8) 0.5370(7) 0.053(5) Uani 1 1 d DG U . . .
H17 H 0.9896 -0.4246 0.5172 0.063 Uiso 1 1 calc R U . . .
C18 C 1.0372(9) -0.4410(8) 0.5714(8) 0.059(5) Uani 1 1 d DG U . . .
H18 H 1.0854 -0.4201 0.5751 0.07 Uiso 1 1 calc R U . . .
C19 C 0.8477(15) -0.4737(15) 0.4951(12) 0.075(9) Uani 1 1 d D U . . .
H19A H 0.8443 -0.4375 0.5025 0.112 Uiso 1 1 d R U . . .
H19B H 0.801 -0.4959 0.496 0.112 Uiso 1 1 d R U . . .
H19C H 0.8579 -0.4874 0.4634 0.112 Uiso 1 1 d R U . . .
P2 P 1.3422(5) -0.3863(4) 0.6628(4) 0.051(2) Uani 1 1 d D U . . .
N2 N 1.2621(7) -0.3849(8) 0.6347(7) 0.056(4) Uani 1 1 d D U . . .
C20 C 1.4049(10) -0.3911(8) 0.6215(7) 0.058(5) Uani 1 1 d DG U . . .
C21 C 1.4602(11) -0.3476(7) 0.6256(7) 0.066(7) Uani 1 1 d DG U . . .
H21 H 1.4683 -0.315 0.6513 0.08 Uiso 1 1 calc R U . . .
C22 C 1.5037(11) -0.3518(9) 0.5922(9) 0.072(7) Uani 1 1 d DG U . . .
H22 H 1.5415 -0.3221 0.595 0.086 Uiso 1 1 calc R U . . .
C23 C 1.4918(13) -0.3996(10) 0.5547(7) 0.065(7) Uani 1 1 d DG U . . .
H23 H 1.5216 -0.4024 0.5318 0.078 Uiso 1 1 calc R U . . .
C24 C 1.4365(14) -0.4431(8) 0.5506(7) 0.069(7) Uani 1 1 d DG U . . .
H24 H 1.4284 -0.4757 0.525 0.082 Uiso 1 1 calc R U . . .
C25 C 1.3930(11) -0.4389(7) 0.5840(8) 0.072(7) Uani 1 1 d DG U . . .
H25 H 1.3552 -0.4686 0.5813 0.086 Uiso 1 1 calc R U . . .
C26 C 1.3850(10) -0.3226(7) 0.7128(6) 0.057(6) Uani 1 1 d DG U . . .
C27 C 1.3407(9) -0.2929(8) 0.7351(8) 0.069(7) Uani 1 1 d DG U . . .
H27 H 1.2898 -0.302 0.7215 0.083 Uiso 1 1 calc R U . . .
C28 C 1.3708(14) -0.2497(8) 0.7772(8) 0.083(7) Uani 1 1 d DG U . . .
H28 H 1.3405 -0.2294 0.7924 0.1 Uiso 1 1 calc R U . . .
C29 C 1.4453(15) -0.2363(8) 0.7971(6) 0.081(8) Uani 1 1 d DG U . . .
H29 H 1.4659 -0.2068 0.8259 0.097 Uiso 1 1 calc R U . . .
C30 C 1.4896(10) -0.2661(9) 0.7749(8) 0.070(7) Uani 1 1 d DG U . . .
H30 H 1.5405 -0.2569 0.7885 0.084 Uiso 1 1 calc R U . . .
C31 C 1.4595(10) -0.3092(8) 0.7327(7) 0.055(6) Uani 1 1 d DG U . . .
H31 H 1.4898 -0.3296 0.7175 0.066 Uiso 1 1 calc R U . . .
C32 C 1.2601(11) -0.3540(8) 0.6044(7) 0.057(6) Uani 1 1 d DG U . . .
C33 C 1.2168(12) -0.3801(7) 0.5591(7) 0.065(6) Uani 1 1 d DG U . . .
H33 H 1.1936 -0.4168 0.5479 0.078 Uiso 1 1 calc R U . . .
C34 C 1.2075(12) -0.3523(8) 0.5300(6) 0.064(6) Uani 1 1 d DG U . . .
H34 H 1.1779 -0.3701 0.499 0.077 Uiso 1 1 calc R U . . .
C35 C 1.2415(13) -0.2986(8) 0.5463(7) 0.063(6) Uani 1 1 d DG U . . .
C36 C 1.2847(12) -0.2725(6) 0.5916(8) 0.060(6) Uani 1 1 d DG U . . .
H36 H 1.308 -0.2358 0.6028 0.072 Uiso 1 1 calc R U . . .
C37 C 1.2940(11) -0.3002(8) 0.6207(6) 0.070(6) Uani 1 1 d DG U . . .
H37 H 1.3236 -0.2825 0.6517 0.084 Uiso 1 1 calc R U . . .
C38 C 1.225(2) -0.2656(12) 0.5172(12) 0.079(9) Uani 1 1 d D U . . .
H38A H 1.1938 -0.2437 0.5319 0.118 Uiso 1 1 d R U . . .
H38B H 1.1989 -0.2894 0.485 0.118 Uiso 1 1 d R U . . .
H38C H 1.2709 -0.2429 0.5161 0.118 Uiso 1 1 d R U . . .
Co14 Co 1.4592(3) -0.6025(2) 0.6835(2) 0.0563(18) Uani 1 1 d D . . . .
N14 N 1.4758(15) -0.6603(8) 0.7079(8) 0.065(6) Uani 1 1 d D U . . .
C234 C 1.470(2) -0.6559(12) 0.7532(10) 0.071(6) Uani 1 1 d D U . . .
H234 H 1.456 -0.6266 0.7729 0.086 Uiso 1 1 calc R U . . .
C235 C 1.484(2) -0.6940(13) 0.7706(10) 0.071(7) Uani 1 1 d D U . . .
H235 H 1.475 -0.692 0.8008 0.085 Uiso 1 1 calc R U . . .
C236 C 1.510(2) -0.7347(13) 0.7439(12) 0.079(7) Uani 1 1 d D U . . .
C237 C 1.512(2) -0.7402(12) 0.6976(12) 0.082(7) Uani 1 1 d D U . . .
H237 H 1.5238 -0.7701 0.6771 0.098 Uiso 1 1 calc R U . . .
C238 C 1.497(2) -0.7028(11) 0.6810(10) 0.076(7) Uani 1 1 d D U . . .
H238 H 1.5021 -0.7064 0.6497 0.091 Uiso 1 1 calc R U . . .
P3 P 1.3199(5) -0.6274(4) 0.6052(4) 0.051(2) Uani 1 1 d D U . . .
N3 N 1.4050(8) -0.6338(8) 0.6200(5) 0.050(4) Uani 1 1 d D U . . .
C39 C 1.2515(9) -0.6896(6) 0.5960(8) 0.058(5) Uani 1 1 d DG U . . .
C40 C 1.1773(10) -0.6950(7) 0.5813(8) 0.050(6) Uani 1 1 d DG U . . .
H40 H 1.1621 -0.6671 0.5757 0.06 Uiso 1 1 calc R U . . .
C41 C 1.1252(8) -0.7413(9) 0.5747(9) 0.066(6) Uani 1 1 d DG U . . .
H41 H 1.0745 -0.7451 0.5646 0.079 Uiso 1 1 calc R U . . .
C42 C 1.1474(12) -0.7822(7) 0.5829(10) 0.077(7) Uani 1 1 d DG U . . .
H42 H 1.1119 -0.8139 0.5784 0.092 Uiso 1 1 calc R U . . .
C43 C 1.2217(13) -0.7768(7) 0.5976(10) 0.078(7) Uani 1 1 d DG U . . .
H43 H 1.2369 -0.8048 0.6032 0.093 Uiso 1 1 calc R U . . .
C44 C 1.2737(9) -0.7305(8) 0.6042(9) 0.068(6) Uani 1 1 d DG U . . .
H44 H 1.3244 -0.7268 0.6143 0.082 Uiso 1 1 calc R U . . .
C45 C 1.3098(12) -0.6299(8) 0.5435(5) 0.051(5) Uani 1 1 d DG U . . .
C46 C 1.3161(12) -0.5837(7) 0.5350(6) 0.057(6) Uani 1 1 d DG U . . .
H46 H 1.3244 -0.551 0.5606 0.069 Uiso 1 1 calc R U . . .
C47 C 1.3104(13) -0.5853(8) 0.4891(8) 0.058(6) Uani 1 1 d DG U . . .
H47 H 1.3147 -0.5537 0.4833 0.07 Uiso 1 1 calc R U . . .
C48 C 1.2982(13) -0.6331(10) 0.4517(5) 0.067(7) Uani 1 1 d DG U . . .
H48 H 1.2943 -0.6343 0.4203 0.08 Uiso 1 1 calc R U . . .
C49 C 1.2919(13) -0.6794(8) 0.4601(6) 0.070(6) Uani 1 1 d DG U . . .
H49 H 1.2836 -0.7121 0.4346 0.084 Uiso 1 1 calc R U . . .
C50 C 1.2977(13) -0.6777(7) 0.5061(7) 0.069(6) Uani 1 1 d DG U . . .
H50 H 1.2934 -0.7093 0.5118 0.083 Uiso 1 1 calc R U . . .
C51 C 1.4510(10) -0.6442(8) 0.5846(7) 0.055(5) Uani 1 1 d DG U . . .
C52 C 1.4879(12) -0.6014(7) 0.5755(8) 0.068(6) Uani 1 1 d DG U . . .
H52 H 1.4728 -0.5699 0.5844 0.081 Uiso 1 1 calc R U . . .
C53 C 1.5471(12) -0.6048(8) 0.5535(9) 0.073(6) Uani 1 1 d DG U . . .
H53 H 1.5724 -0.5755 0.5473 0.087 Uiso 1 1 calc R U . . .
C54 C 1.5694(11) -0.6509(10) 0.5406(9) 0.077(7) Uani 1 1 d DG U . . .
C55 C 1.5324(12) -0.6937(8) 0.5497(9) 0.068(6) Uani 1 1 d DG U . . .
H55 H 1.5475 -0.7252 0.5408 0.082 Uiso 1 1 calc R U . . .
C56 C 1.4732(12) -0.6903(7) 0.5717(8) 0.067(6) Uani 1 1 d DG U . . .
H56 H 1.4479 -0.7196 0.5779 0.081 Uiso 1 1 calc R U . . .
C57 C 1.6397(17) -0.6554(15) 0.5206(16) 0.092(10) Uani 1 1 d D U . . .
H57A H 1.6829 -0.6324 0.5454 0.138 Uiso 1 1 d R U . . .
H57B H 1.6381 -0.6443 0.4937 0.138 Uiso 1 1 d R U . . .
H57C H 1.6426 -0.6919 0.5104 0.138 Uiso 1 1 d R U . . .
P4 P 1.5220(5) -0.4906(4) 0.7590(3) 0.047(2) Uani 1 1 d D U . . .
N4 N 1.5423(8) -0.5417(6) 0.7195(7) 0.052(4) Uani 1 1 d D U . . .
C58 C 1.5538(12) -0.4927(8) 0.8174(5) 0.055(5) Uani 1 1 d DG U . . .
C59 C 1.5917(13) -0.5290(8) 0.8206(6) 0.057(6) Uani 1 1 d DG U . . .
H59 H 1.598 -0.5544 0.7928 0.068 Uiso 1 1 calc R U . . .
C60 C 1.6205(12) -0.5282(9) 0.8647(8) 0.065(6) Uani 1 1 d DG U . . .
H60 H 1.6464 -0.553 0.8669 0.078 Uiso 1 1 calc R U . . .
C61 C 1.6114(13) -0.4911(10) 0.9054(6) 0.064(7) Uani 1 1 d DG U . . .
H61 H 1.631 -0.4905 0.9355 0.077 Uiso 1 1 calc R U . . .
C62 C 1.5735(13) -0.4547(9) 0.9021(5) 0.069(6) Uani 1 1 d DG U . . .
H62 H 1.5672 -0.4293 0.93 0.083 Uiso 1 1 calc R U . . .
C63 C 1.5447(12) -0.4555(8) 0.8581(7) 0.058(6) Uani 1 1 d DG U . . .
H63 H 1.5188 -0.4307 0.8559 0.07 Uiso 1 1 calc R U . . .
C64 C 1.5747(11) -0.4279(6) 0.7592(7) 0.054(5) Uani 1 1 d DG U . . .
C65 C 1.6088(12) -0.3867(7) 0.8021(6) 0.053(6) Uani 1 1 d DG U . . .
H65 H 1.6061 -0.3917 0.8309 0.063 Uiso 1 1 calc R U . . .
C66 C 1.6467(12) -0.3382(6) 0.8029(7) 0.064(6) Uani 1 1 d DG U . . .
H66 H 1.67 -0.31 0.8322 0.077 Uiso 1 1 calc R U . . .
C67 C 1.6506(12) -0.3308(6) 0.7608(9) 0.058(7) Uani 1 1 d DG U . . .
H67 H 1.6766 -0.2976 0.7613 0.07 Uiso 1 1 calc R U . . .
C68 C 1.6166(13) -0.3720(9) 0.7179(8) 0.066(6) Uani 1 1 d DG U . . .
H68 H 1.6193 -0.367 0.6891 0.079 Uiso 1 1 calc R U . . .
C69 C 1.5786(12) -0.4206(7) 0.7171(6) 0.057(6) Uani 1 1 d DG U . . .
H69 H 1.5554 -0.4488 0.6878 0.068 Uiso 1 1 calc R U . . .
C70 C 1.6161(7) -0.5427(7) 0.7106(7) 0.043(6) Uani 1 1 d DG U . . .
C71 C 1.6185(9) -0.5848(7) 0.6711(7) 0.051(6) Uani 1 1 d DG U . . .
H71 H 1.5744 -0.6109 0.6526 0.061 Uiso 1 1 calc R U . . .
C72 C 1.6854(11) -0.5886(8) 0.6587(7) 0.059(7) Uani 1 1 d DG U . . .
H72 H 1.687 -0.6173 0.6317 0.07 Uiso 1 1 calc R U . . .
C73 C 1.7499(8) -0.5503(9) 0.6858(8) 0.065(7) Uani 1 1 d DG U . . .
C74 C 1.7475(8) -0.5083(8) 0.7253(8) 0.056(6) Uani 1 1 d DG U . . .
H74 H 1.7915 -0.4822 0.7438 0.068 Uiso 1 1 calc R U . . .
C75 C 1.6805(9) -0.5045(7) 0.7377(6) 0.044(6) Uani 1 1 d DG U . . .
H75 H 1.6789 -0.4758 0.7647 0.053 Uiso 1 1 calc R U . . .
C76 C 1.8232(14) -0.5505(15) 0.6698(14) 0.082(11) Uani 1 1 d D U . . .
H76A H 1.8543 -0.5143 0.68 0.123 Uiso 1 1 d R U . . .
H76B H 1.8136 -0.5673 0.6353 0.123 Uiso 1 1 d R U . . .
H76C H 1.8483 -0.5705 0.684 0.123 Uiso 1 1 d R U . . .
Co15 Co 1.2739(3) -0.5002(2) 0.8664(2) 0.0639(18) Uani 1 1 d D . . . .
N15 N 1.3536(12) -0.4992(9) 0.9195(7) 0.066(6) Uani 1 1 d D U . . .
C239 C 1.3638(16) -0.4641(13) 0.9651(8) 0.069(7) Uani 1 1 d D U . . .
H239 H 1.3315 -0.4428 0.9744 0.083 Uiso 1 1 calc R U . . .
C240 C 1.4243(17) -0.4619(13) 0.9964(9) 0.073(7) Uani 1 1 d D U . . .
H240 H 1.4385 -0.4344 1.0268 0.087 Uiso 1 1 calc DR U . . .
C241 C 1.4649(19) -0.4986(15) 0.9849(11) 0.078(7) Uani 1 1 d D U . . .
C242 C 1.4507(17) -0.5343(14) 0.9382(11) 0.077(8) Uani 1 1 d D U . . .
H242 H 1.4799 -0.5581 0.9289 0.092 Uiso 1 1 calc R U . . .
C243 C 1.3944(17) -0.5344(13) 0.9063(9) 0.080(8) Uani 1 1 d D U . . .
H243 H 1.3833 -0.5591 0.8747 0.097 Uiso 1 1 calc R U . . .
P5 P 1.2079(5) -0.6083(4) 0.7861(4) 0.053(2) Uani 1 1 d D U . . .
N5 N 1.2163(11) -0.5724(6) 0.8435(6) 0.057(4) Uani 1 1 d D U . . .
C77 C 1.2468(11) -0.6646(7) 0.7792(7) 0.047(5) Uani 1 1 d DG U . . .
C78 C 1.2789(13) -0.6724(8) 0.8184(6) 0.071(6) Uani 1 1 d DG U . . .
H78 H 1.2788 -0.6495 0.8493 0.085 Uiso 1 1 calc R U . . .
C79 C 1.3113(13) -0.7136(9) 0.8124(9) 0.072(6) Uani 1 1 d DG U . . .
H79 H 1.3332 -0.7189 0.8392 0.086 Uiso 1 1 calc R U . . .
C80 C 1.3115(13) -0.7470(8) 0.7672(10) 0.080(7) Uani 1 1 d DG U . . .
H80 H 1.3336 -0.7752 0.7631 0.097 Uiso 1 1 calc R U . . .
C81 C 1.2794(14) -0.7393(8) 0.7281(8) 0.075(6) Uani 1 1 d DG U . . .
H81 H 1.2795 -0.7621 0.6972 0.09 Uiso 1 1 calc R U . . .
C82 C 1.2470(12) -0.6981(8) 0.7341(6) 0.066(6) Uani 1 1 d DG U . . .
H82 H 1.2251 -0.6928 0.7073 0.079 Uiso 1 1 calc R U . . .
C83 C 1.1082(7) -0.6367(8) 0.7598(7) 0.062(6) Uani 1 1 d DG U . . .
C84 C 1.0592(10) -0.6128(8) 0.7830(7) 0.069(7) Uani 1 1 d DG U . . .
H84 H 1.0771 -0.5824 0.8114 0.083 Uiso 1 1 calc R U . . .
C85 C 0.9840(9) -0.6334(10) 0.7646(9) 0.065(7) Uani 1 1 d DG U . . .
H85 H 0.9505 -0.6171 0.7805 0.078 Uiso 1 1 calc R U . . .
C86 C 0.9577(7) -0.6778(10) 0.7231(10) 0.082(8) Uani 1 1 d DG U . . .
H86 H 0.9063 -0.6919 0.7106 0.098 Uiso 1 1 calc R U . . .
C87 C 1.0067(11) -0.7017(8) 0.7000(8) 0.078(7) Uani 1 1 d DG U . . .
H87 H 0.9888 -0.7321 0.6716 0.094 Uiso 1 1 calc R U . . .
C88 C 1.0820(10) -0.6811(8) 0.7183(7) 0.064(6) Uani 1 1 d DG U . . .
H88 H 1.1154 -0.6974 0.7025 0.077 Uiso 1 1 calc R U . . .
C89 C 1.1796(12) -0.5929(7) 0.8752(6) 0.053(6) Uani 1 1 d DG U . . .
C90 C 1.1852(13) -0.5583(7) 0.9210(7) 0.072(6) Uani 1 1 d DG U . . .
H90 H 1.2075 -0.5217 0.9301 0.086 Uiso 1 1 calc R U . . .
C91 C 1.1583(15) -0.5774(10) 0.9536(6) 0.089(7) Uani 1 1 d DG U . . .
H91 H 1.1622 -0.5538 0.9849 0.107 Uiso 1 1 calc R U . . .
C92 C 1.1257(16) -0.6310(10) 0.9403(8) 0.101(7) Uani 1 1 d DG U . . .
C93 C 1.1201(14) -0.6655(7) 0.8945(9) 0.087(6) Uani 1 1 d DG U . . .
H93 H 1.0978 -0.7022 0.8854 0.104 Uiso 1 1 calc R U . . .
C94 C 1.1470(13) -0.6465(7) 0.8619(7) 0.069(6) Uani 1 1 d DG U . . .
H94 H 1.1432 -0.6701 0.8306 0.083 Uiso 1 1 calc R U . . .
C95 C 1.101(3) -0.6557(16) 0.9758(13) 0.141(12) Uani 1 1 d D U . . .
H95A H 1.0473 -0.6702 0.9676 0.211 Uiso 1 1 d R U . . .
H95B H 1.1154 -0.628 1.0075 0.211 Uiso 1 1 d R U . . .
H95C H 1.1243 -0.6837 0.9751 0.211 Uiso 1 1 d R U . . .
P6 P 1.3036(5) -0.3936(4) 0.8527(4) 0.066(3) Uani 1 1 d D U . . .
N6 N 1.2702(11) -0.4284(5) 0.8851(6) 0.080(5) Uani 1 1 d D U . . .
C96 C 1.3979(7) -0.3534(8) 0.8842(8) 0.059(5) Uani 1 1 d DG U . . .
C97 C 1.4371(10) -0.3182(8) 0.8673(7) 0.056(6) Uani 1 1 d DG U . . .
H97 H 1.4132 -0.3111 0.8422 0.067 Uiso 1 1 calc R U . . .
C98 C 1.5112(10) -0.2933(8) 0.8873(9) 0.068(6) Uani 1 1 d DG U . . .
H98 H 1.538 -0.2692 0.8758 0.082 Uiso 1 1 calc R U . . .
C99 C 1.5461(8) -0.3037(9) 0.9241(9) 0.076(7) Uani 1 1 d DG U . . .
H99 H 1.5967 -0.2867 0.9378 0.091 Uiso 1 1 calc R U . . .
C100 C 1.5068(11) -0.3389(10) 0.9409(8) 0.080(6) Uani 1 1 d DG U . . .
H100 H 1.5307 -0.346 0.9661 0.096 Uiso 1 1 calc R U . . .
C101 C 1.4327(11) -0.3637(8) 0.9210(8) 0.079(6) Uani 1 1 d DG U . . .
H101 H 1.4059 -0.3878 0.9325 0.095 Uiso 1 1 calc R U . . .
C102 C 1.2486(10) -0.3454(7) 0.8565(9) 0.066(6) Uani 1 1 d DG U . . .
C103 C 1.1731(10) -0.3636(7) 0.8384(9) 0.065(7) Uani 1 1 d DG U . . .
H103 H 1.1508 -0.4002 0.8214 0.078 Uiso 1 1 calc R U . . .
C104 C 1.1305(9) -0.3282(10) 0.8451(9) 0.072(7) Uani 1 1 d DG U . . .
H104 H 1.0789 -0.3406 0.8328 0.086 Uiso 1 1 calc R U . . .
C105 C 1.1632(13) -0.2746(9) 0.8700(10) 0.071(7) Uani 1 1 d DG U . . .
H105 H 1.134 -0.2504 0.8746 0.085 Uiso 1 1 calc R U . . .
C106 C 1.2386(13) -0.2564(6) 0.8881(9) 0.077(7) Uani 1 1 d DG U . . .
H106 H 1.261 -0.2198 0.905 0.093 Uiso 1 1 calc R U . . .
C107 C 1.2813(9) -0.2918(7) 0.8813(9) 0.070(7) Uani 1 1 d DG U . . .
H107 H 1.3328 -0.2794 0.8937 0.084 Uiso 1 1 calc R U . . .
C108 C 1.2263(11) -0.4046(6) 0.9179(5) 0.097(7) Uani 1 1 d DG U . . .
C109 C 1.1518(11) -0.4290(8) 0.9102(8) 0.122(8) Uani 1 1 d DG U . . .
H109 H 1.1295 -0.4609 0.8838 0.147 Uiso 1 1 calc R U . . .
C110 C 1.1100(11) -0.4066(11) 0.9412(10) 0.143(8) Uani 1 1 d DG U . . .
H110 H 1.0591 -0.4233 0.936 0.171 Uiso 1 1 calc R U . . .
C111 C 1.1427(15) -0.3599(10) 0.9800(8) 0.145(9) Uani 1 1 d DG U . . .
C112 C 1.2172(15) -0.3356(8) 0.9877(7) 0.139(8) Uani 1 1 d DG U . . .
H112 H 1.2396 -0.3037 1.0141 0.167 Uiso 1 1 calc R U . . .
C113 C 1.2591(11) -0.3579(7) 0.9567(7) 0.119(8) Uani 1 1 d DG U . . .
H113 H 1.31 -0.3413 0.9619 0.143 Uiso 1 1 calc R U . . .
C114 C 1.101(2) -0.3325(14) 1.0160(11) 0.165(14) Uani 1 1 d D U . . .
H11A H 1.0483 -0.3423 1.0011 0.248 Uiso 1 1 d R U . . .
H11B H 1.1206 -0.2941 1.0272 0.248 Uiso 1 1 d R U . . .
H11C H 1.1058 -0.3436 1.0429 0.248 Uiso 1 1 d R U . . .
Co16 Co 0.6108(3) 0.0914(2) 0.8050(2) 0.068(2) Uani 1 1 d D . . . .
N16 N 0.5611(13) 0.1465(8) 0.7919(8) 0.116(8) Uani 1 1 d DG U . . .
C244 C 0.5238(13) 0.1330(9) 0.7458(7) 0.120(8) Uani 1 1 d DG U . . .
H244 H 0.5131 0.0977 0.7238 0.144 Uiso 1 1 calc DR U . . .
C245 C 0.5023(16) 0.1710(13) 0.7321(9) 0.122(8) Uani 1 1 d DG U . . .
H245 H 0.4769 0.1617 0.7006 0.146 Uiso 1 1 calc R U . . .
C246 C 0.5181(18) 0.2225(11) 0.7644(13) 0.118(8) Uani 1 1 d DG U . . .
C247 C 0.5554(17) 0.2361(7) 0.8104(12) 0.127(8) Uani 1 1 d DG U . . .
H247 H 0.5662 0.2713 0.8325 0.152 Uiso 1 1 calc R U . . .
C248 C 0.5769(15) 0.1981(8) 0.8242(8) 0.121(8) Uani 1 1 d DG U . . .
H248 H 0.6024 0.2074 0.8556 0.145 Uiso 1 1 calc R U . . .
P7 P 0.5599(9) -0.0128(6) 0.7192(5) 0.135(3) Uani 1 1 d D U . . .
N7 N 0.5379(10) 0.0261(7) 0.7678(5) 0.135(3) Uani 1 1 d D U . . .
C115 C 0.5120(14) -0.0048(10) 0.6673(8) 0.126(5) Uani 1 1 d DG U . . .
C116 C 0.4379(14) -0.0301(10) 0.6476(9) 0.135(7) Uani 1 1 d DG U . . .
H116 H 0.4136 -0.0581 0.6558 0.162 Uiso 1 1 calc R U . . .
C117 C 0.3995(13) -0.0145(13) 0.6160(10) 0.138(7) Uani 1 1 d DG U . . .
H117 H 0.3488 -0.0318 0.6025 0.166 Uiso 1 1 calc R U . . .
C118 C 0.4350(18) 0.0265(13) 0.6041(10) 0.123(7) Uani 1 1 d DG U . . .
H118 H 0.4087 0.0372 0.5824 0.148 Uiso 1 1 calc R U . . .
C119 C 0.5091(19) 0.0518(11) 0.6238(10) 0.125(7) Uani 1 1 d DG U . . .
H119 H 0.5334 0.0798 0.6156 0.15 Uiso 1 1 calc R U . . .
C120 C 0.5476(13) 0.0362(11) 0.6554(9) 0.125(7) Uani 1 1 d DG U . . .
H120 H 0.5982 0.0535 0.6688 0.15 Uiso 1 1 calc R U . . .
C121 C 0.5179(15) -0.0811(7) 0.7119(9) 0.135(6) Uani 1 1 d DG U . . .
C122 C 0.5090(12) -0.0907(11) 0.7525(9) 0.165(7) Uani 1 1 d DG U . . .
H122 H 0.5232 -0.0624 0.7824 0.198 Uiso 1 1 calc DR U . . .
C123 C 0.4792(17) -0.1419(13) 0.7494(13) 0.155(7) Uani 1 1 d DG U . . .
H123 H 0.4731 -0.1485 0.7771 0.186 Uiso 1 1 calc R U . . .
C124 C 0.4584(18) -0.1834(9) 0.7057(16) 0.159(8) Uani 1 1 d DG U . . .
H124 H 0.4381 -0.2183 0.7035 0.191 Uiso 1 1 calc R U . . .
C125 C 0.4673(16) -0.1737(8) 0.6650(12) 0.148(7) Uani 1 1 d DG U . . .
H125 H 0.4531 -0.2021 0.6352 0.177 Uiso 1 1 calc R U . . .
C126 C 0.4971(17) -0.1226(9) 0.6682(9) 0.138(7) Uani 1 1 d DG U . . .
H126 H 0.5032 -0.116 0.6404 0.166 Uiso 1 1 calc R U . . .
C127 C 0.4631(8) 0.0255(9) 0.7743(4) 0.135(3) Uani 1 1 d DG U . . .
C128 C 0.4455(12) 0.0732(8) 0.7841(7) 0.135(3) Uani 1 1 d DG U . . .
H128 H 0.4814 0.1037 0.7862 0.161 Uiso 1 1 calc DR U . . .
C129 C 0.3756(13) 0.0764(9) 0.7908(8) 0.135(3) Uani 1 1 d DG U . . .
H129 H 0.3636 0.109 0.7975 0.161 Uiso 1 1 calc R U . . .
C130 C 0.3231(9) 0.0318(11) 0.7876(7) 0.135(3) Uani 1 1 d DG U . . .
C131 C 0.3406(9) -0.0159(9) 0.7778(9) 0.135(3) Uani 1 1 d DG U . . .
H131 H 0.3048 -0.0464 0.7757 0.161 Uiso 1 1 calc R U . . .
C132 C 0.4106(10) -0.0191(8) 0.7712(8) 0.135(3) Uani 1 1 d DG U . . .
H132 H 0.4226 -0.0517 0.7645 0.161 Uiso 1 1 calc DR U . . .
C133 C 0.2454(8) 0.0335(15) 0.7948(10) 0.135(3) Uani 1 1 d D U . . .
H13A H 0.2121 0.0218 0.764 0.202 Uiso 1 1 d DR U . . .
H13B H 0.2465 0.0699 0.8136 0.202 Uiso 1 1 d DR U . . .
H13C H 0.228 0.0105 0.8112 0.202 Uiso 1 1 d DR U . . .
P8 P 0.7638(6) 0.1293(4) 0.8726(4) 0.080(3) Uani 1 1 d D U . . .
N8 N 0.6740(8) 0.1271(9) 0.8666(6) 0.080(5) Uani 1 1 d D U . . .
C134 C 0.7943(13) 0.1282(10) 0.9315(7) 0.091(6) Uani 1 1 d DG U . . .
C135 C 0.8393(14) 0.1723(9) 0.9691(8) 0.109(7) Uani 1 1 d DG U . . .
H135 H 0.8576 0.2042 0.9647 0.131 Uiso 1 1 calc R U . . .
C136 C 0.8575(16) 0.1695(12) 1.0131(7) 0.111(7) Uani 1 1 d DG U . . .
H136 H 0.8882 0.1996 1.0388 0.133 Uiso 1 1 calc R U . . .
C137 C 0.8307(17) 0.1228(14) 1.0195(7) 0.116(8) Uani 1 1 d DG U . . .
H137 H 0.8432 0.121 1.0496 0.139 Uiso 1 1 calc R U . . .
C138 C 0.7858(17) 0.0788(11) 0.9819(10) 0.116(7) Uani 1 1 d DG U . . .
H138 H 0.7675 0.0468 0.9863 0.139 Uiso 1 1 calc R U . . .
C139 C 0.7676(14) 0.0815(9) 0.9379(8) 0.120(7) Uani 1 1 d DG U . . .
H139 H 0.7368 0.0514 0.9122 0.144 Uiso 1 1 calc R U . . .
C140 C 0.8135(11) 0.1947(8) 0.8751(10) 0.093(5) Uani 1 1 d DG U . . .
C141 C 0.8899(11) 0.2102(9) 0.8869(10) 0.099(6) Uani 1 1 d DG U . . .
H141 H 0.9157 0.1909 0.8997 0.118 Uiso 1 1 calc R U . . .
C142 C 0.9286(11) 0.2540(10) 0.8799(11) 0.108(7) Uani 1 1 d DG U . . .
H142 H 0.9808 0.2646 0.8879 0.129 Uiso 1 1 calc R U . . .
C143 C 0.8909(17) 0.2823(9) 0.8611(11) 0.109(7) Uani 1 1 d DG U . . .
H143 H 0.9174 0.3123 0.8563 0.13 Uiso 1 1 calc R U . . .
C144 C 0.8145(17) 0.2668(9) 0.8493(10) 0.104(7) Uani 1 1 d DG U . . .
H144 H 0.7887 0.2862 0.8365 0.125 Uiso 1 1 calc R U . . .
C145 C 0.7758(11) 0.2230(9) 0.8563(10) 0.095(7) Uani 1 1 d DG U . . .
H145 H 0.7236 0.2124 0.8483 0.114 Uiso 1 1 calc R U . . .
C146 C 0.6375(12) 0.1440(10) 0.9060(7) 0.090(7) Uani 1 1 d DG U . . .
C147 C 0.6693(11) 0.1927(10) 0.9426(8) 0.099(8) Uani 1 1 d DG U . . .
H147 H 0.7165 0.2131 0.9434 0.119 Uiso 1 1 calc R U . . .
C148 C 0.6321(15) 0.2114(9) 0.9781(8) 0.099(7) Uani 1 1 d DG U . . .
H148 H 0.6538 0.2447 1.0031 0.119 Uiso 1 1 calc R U . . .
C149 C 0.5630(16) 0.1816(12) 0.9769(9) 0.131(8) Uani 1 1 d DG U . . .
C150 C 0.5312(13) 0.1329(11) 0.9403(10) 0.128(8) Uani 1 1 d DG U . . .
H150 H 0.484 0.1125 0.9395 0.154 Uiso 1 1 calc R U . . .
C151 C 0.5684(13) 0.1142(9) 0.9048(8) 0.119(8) Uani 1 1 d DG U . . .
H151 H 0.5467 0.0809 0.8798 0.143 Uiso 1 1 calc R U . . .
C152 C 0.521(3) 0.2009(18) 1.0160(15) 0.158(13) Uani 1 1 d D U . . .
H15A H 0.5047 0.1726 1.0272 0.237 Uiso 1 1 d R U . . .
H15B H 0.4785 0.2108 1.0041 0.237 Uiso 1 1 d R U . . .
H15C H 0.5546 0.2316 1.042 0.237 Uiso 1 1 d R U . . .
Co17 Co 0.9426(4) -0.0705(2) 0.8108(2) 0.085(2) Uani 1 1 d D . . . .
N17 N 0.9937(10) -0.1292(7) 0.7816(7) 0.078(7) Uani 1 1 d D U . . .
C249 C 1.0511(11) -0.1371(8) 0.8081(8) 0.079(7) Uani 1 1 d D U . . .
H249 H 1.068 -0.1161 0.8408 0.095 Uiso 1 1 calc R U . . .
C250 C 1.0838(12) -0.1763(8) 0.7858(9) 0.067(6) Uani 1 1 d D U . . .
H250 H 1.1232 -0.1816 0.8041 0.08 Uiso 1 1 calc R U . . .
C251 C 1.0612(13) -0.2077(9) 0.7384(9) 0.067(6) Uani 1 1 d D U . . .
C252 C 1.0032(14) -0.1997(9) 0.7116(9) 0.064(6) Uani 1 1 d D U . . .
H252 H 0.9858 -0.2204 0.6789 0.077 Uiso 1 1 calc R U . . .
C253 C 0.9724(13) -0.1609(8) 0.7346(8) 0.068(7) Uani 1 1 d D U . . .
H253 H 0.9331 -0.1555 0.7164 0.082 Uiso 1 1 calc R U . . .
P9 P 0.7754(6) -0.1075(4) 0.8085(4) 0.075(3) Uani 1 1 d D U . . .
N9 N 0.8625(8) -0.1014(9) 0.8325(7) 0.084(5) Uani 1 1 d D U . . .
C153 C 0.7191(13) -0.1172(9) 0.8510(8) 0.093(5) Uani 1 1 d DG U . . .
C154 C 0.6801(15) -0.0826(9) 0.8729(10) 0.121(6) Uani 1 1 d DG U . . .
H154 H 0.6825 -0.0513 0.8669 0.145 Uiso 1 1 calc R U . . .
C155 C 0.6375(15) -0.0940(13) 0.9035(10) 0.118(6) Uani 1 1 d DG U . . .
H155 H 0.6108 -0.0704 0.9185 0.142 Uiso 1 1 calc R U . . .
C156 C 0.6340(16) -0.1399(14) 0.9122(10) 0.129(7) Uani 1 1 d DG U . . .
H156 H 0.6049 -0.1476 0.9331 0.155 Uiso 1 1 calc R U . . .
C157 C 0.6731(17) -0.1744(11) 0.8903(11) 0.106(6) Uani 1 1 d DG U . . .
H157 H 0.6707 -0.2057 0.8962 0.127 Uiso 1 1 calc R U . . .
C158 C 0.7157(15) -0.1630(9) 0.8597(10) 0.111(6) Uani 1 1 d DG U . . .
H158 H 0.7424 -0.1866 0.8447 0.133 Uiso 1 1 calc R U . . .
C159 C 0.7411(11) -0.1737(7) 0.7603(7) 0.076(6) Uani 1 1 d DG U . . .
C160 C 0.6663(11) -0.1921(8) 0.7401(8) 0.065(6) Uani 1 1 d DG U . . .
H160 H 0.6337 -0.1726 0.7531 0.078 Uiso 1 1 calc R U . . .
C161 C 0.6392(11) -0.2392(9) 0.7010(8) 0.082(7) Uani 1 1 d DG U . . .
H161 H 0.5881 -0.2518 0.6873 0.099 Uiso 1 1 calc R U . . .
C162 C 0.6870(16) -0.2678(7) 0.6821(7) 0.082(8) Uani 1 1 d DG U . . .
H162 H 0.6685 -0.2999 0.6554 0.098 Uiso 1 1 calc R U . . .
C163 C 0.7617(15) -0.2493(8) 0.7023(9) 0.092(8) Uani 1 1 d DG U . . .
H163 H 0.7944 -0.2689 0.6893 0.111 Uiso 1 1 calc R U . . .
C164 C 0.7888(10) -0.2023(9) 0.7414(8) 0.086(7) Uani 1 1 d DG U . . .
H164 H 0.8399 -0.1897 0.7551 0.103 Uiso 1 1 calc R U . . .
C165 C 0.8897(12) -0.1018(10) 0.8789(6) 0.084(6) Uani 1 1 d DG U . . .
C166 C 0.8907(14) -0.0590(9) 0.9188(8) 0.095(7) Uani 1 1 d DG U . . .
H166 H 0.8669 -0.0334 0.9159 0.114 Uiso 1 1 calc R U . . .
C167 C 0.9264(15) -0.0538(9) 0.9630(7) 0.099(6) Uani 1 1 d DG U . . .
H167 H 0.9271 -0.0245 0.9903 0.119 Uiso 1 1 calc R U . . .
C168 C 0.9612(15) -0.0913(11) 0.9673(7) 0.100(7) Uani 1 1 d DG U . . .
C169 C 0.9603(14) -0.1340(10) 0.9274(9) 0.100(7) Uani 1 1 d DG U . . .
H169 H 0.9841 -0.1597 0.9303 0.12 Uiso 1 1 calc R U . . .
C170 C 0.9245(14) -0.1393(9) 0.8832(7) 0.087(6) Uani 1 1 d DG U . . .
H170 H 0.9239 -0.1685 0.8559 0.105 Uiso 1 1 calc R U . . .
C171 C 0.989(3) -0.0919(18) 1.0160(10) 0.138(12) Uani 1 1 d D U . . .
H17A H 1.0397 -0.0947 1.0196 0.207 Uiso 1 1 d R U . . .
H17B H 0.9567 -0.1223 1.0189 0.207 Uiso 1 1 d R U . . .
H17C H 0.9868 -0.0594 1.0406 0.207 Uiso 1 1 d R U . . .
P10 P 1.0112(5) 0.0355(4) 0.8014(4) 0.081(3) Uani 1 1 d D U . . .
N10 N 1.0187(10) -0.0052(7) 0.8310(8) 0.102(5) Uani 1 1 d D U . . .
C172 C 1.0620(14) 0.0181(9) 0.7540(7) 0.100(5) Uani 1 1 d DG U . . .
C173 C 1.0945(15) -0.0231(9) 0.7468(9) 0.094(6) Uani 1 1 d DG U . . .
H173 H 1.0909 -0.0426 0.7667 0.113 Uiso 1 1 calc R U . . .
C174 C 1.1323(15) -0.0358(11) 0.7106(10) 0.105(6) Uani 1 1 d DG U . . .
H174 H 1.1546 -0.064 0.7057 0.126 Uiso 1 1 calc R U . . .
C175 C 1.1376(16) -0.0073(13) 0.6814(9) 0.120(7) Uani 1 1 d DG U . . .
H175 H 1.1635 -0.0159 0.6567 0.144 Uiso 1 1 calc R U . . .
C176 C 1.1051(17) 0.0339(13) 0.6886(9) 0.127(6) Uani 1 1 d DG U . . .
H176 H 1.1087 0.0534 0.6687 0.153 Uiso 1 1 calc R U . . .
C177 C 1.0672(16) 0.0466(10) 0.7248(9) 0.114(6) Uani 1 1 d DG U . . .
H177 H 1.045 0.0748 0.7297 0.137 Uiso 1 1 calc R U . . .
C178 C 1.0592(13) 0.1028(6) 0.8440(7) 0.090(6) Uani 1 1 d DG U . . .
C179 C 1.1173(14) 0.1346(9) 0.8347(8) 0.110(8) Uani 1 1 d DG U . . .
H179 H 1.1347 0.1211 0.8067 0.132 Uiso 1 1 calc R U . . .
C180 C 1.1498(13) 0.1860(8) 0.8665(10) 0.105(8) Uani 1 1 d DG U . . .
H180 H 1.1895 0.2077 0.8601 0.126 Uiso 1 1 calc R U . . .
C181 C 1.1244(16) 0.2057(6) 0.9075(9) 0.100(8) Uani 1 1 d DG U . . .
H181 H 1.1466 0.2409 0.9292 0.12 Uiso 1 1 calc R U . . .
C182 C 1.0663(15) 0.1739(9) 0.9169(7) 0.082(7) Uani 1 1 d DG U . . .
H182 H 1.0489 0.1873 0.9449 0.099 Uiso 1 1 calc R U . . .
C183 C 1.0338(13) 0.1224(8) 0.8851(8) 0.084(7) Uani 1 1 d DG U . . .
H183 H 0.9941 0.1007 0.8915 0.101 Uiso 1 1 calc R U . . .
C184 C 1.0871(4) 0.0059(5) 0.8650(4) 0.090(6) Uani 1 1 d DG U . . .
C185 C 1.0837(5) -0.0145(5) 0.9002(3) 0.108(6) Uani 1 1 d DG U . . .
H185 H 1.038 -0.0349 0.9018 0.13 Uiso 1 1 calc R U . . .
C186 C 1.1470(6) -0.0050(6) 0.9331(4) 0.114(7) Uani 1 1 d DG U . . .
H186 H 1.1446 -0.0189 0.9572 0.137 Uiso 1 1 calc R U . . .
C187 C 1.2137(5) 0.0248(6) 0.9308(5) 0.127(7) Uani 1 1 d DG U . . .
C188 C 1.2172(4) 0.0452(6) 0.8956(7) 0.114(6) Uani 1 1 d DG U . . .
H188 H 1.2628 0.0656 0.894 0.137 Uiso 1 1 calc R U . . .
C189 C 1.1539(4) 0.0357(7) 0.8627(7) 0.114(7) Uani 1 1 d DG U . . .
H189 H 1.1562 0.0496 0.8386 0.137 Uiso 1 1 calc R U . . .
C190 C 1.2871(15) 0.039(2) 0.9662(15) 0.163(12) Uani 1 1 d D U . . .
H19D H 1.3288 0.051 0.9532 0.245 Uiso 1 1 d R U . . .
H19E H 1.2918 0.0079 0.9728 0.245 Uiso 1 1 d R U . . .
H19F H 1.2868 0.0673 0.9956 0.245 Uiso 1 1 d R U . . .
Co18 Co 0.7741(3) 0.0092(2) 0.5993(2) 0.0528(17) Uani 1 1 d D . . . .
N18 N 0.6786(10) 0.0021(8) 0.5555(7) 0.072(6) Uani 1 1 d D U . . .
C254 C 0.6712(13) 0.0415(9) 0.5391(7) 0.075(7) Uani 1 1 d D U . . .
H254 H 0.713 0.0687 0.5419 0.09 Uiso 1 1 calc R U . . .
C255 C 0.6005(14) 0.0406(11) 0.5183(8) 0.088(8) Uani 1 1 d D U . . .
H255 H 0.5959 0.0677 0.5071 0.106 Uiso 1 1 calc R U . . .
C256 C 0.5377(13) 0.0022(12) 0.5133(9) 0.081(7) Uani 1 1 d D U . . .
C257 C 0.5460(13) -0.0370(11) 0.5298(10) 0.080(7) Uani 1 1 d D U . . .
H257 H 0.5045 -0.0643 0.5272 0.096 Uiso 1 1 calc R U . . .
C258 C 0.6151(12) -0.0357(9) 0.5501(8) 0.076(7) Uani 1 1 d D U . . .
H258 H 0.6195 -0.0629 0.5612 0.091 Uiso 1 1 calc R U . . .
P11 P 0.7899(5) -0.0932(3) 0.6149(4) 0.049(2) Uani 1 1 d D U . . .
N11 N 0.7964(11) -0.0571(6) 0.5811(7) 0.050(4) Uani 1 1 d D U . . .
C191 C 0.7042(8) -0.1480(7) 0.5887(8) 0.051(5) Uani 1 1 d DG U . . .
C192 C 0.6815(11) -0.1812(8) 0.6120(7) 0.071(6) Uani 1 1 d DG U . . .
H192 H 0.7124 -0.1783 0.64 0.085 Uiso 1 1 calc R U . . .
C193 C 0.6136(12) -0.2187(8) 0.5944(9) 0.083(7) Uani 1 1 d DG U . . .
H193 H 0.5981 -0.2413 0.6104 0.099 Uiso 1 1 calc R U . . .
C194 C 0.5684(9) -0.2229(9) 0.5535(10) 0.087(8) Uani 1 1 d DG U . . .
H194 H 0.5219 -0.2485 0.5415 0.104 Uiso 1 1 calc R U . . .
C195 C 0.5910(11) -0.1897(10) 0.5302(8) 0.083(7) Uani 1 1 d DG U . . .
H195 H 0.5601 -0.1926 0.5022 0.1 Uiso 1 1 calc R U . . .
C196 C 0.6589(11) -0.1522(8) 0.5477(7) 0.060(6) Uani 1 1 d DG U . . .
H196 H 0.6744 -0.1296 0.5318 0.072 Uiso 1 1 calc R U . . .
C197 C 0.8611(9) -0.1304(7) 0.6069(7) 0.043(5) Uani 1 1 d DG U . . .
C198 C 0.8412(9) -0.1800(7) 0.5709(7) 0.059(7) Uani 1 1 d DG U . . .
H198 H 0.7928 -0.194 0.5519 0.071 Uiso 1 1 calc R U . . .
C199 C 0.8921(12) -0.2092(7) 0.5627(7) 0.053(7) Uani 1 1 d DG U . . .
H199 H 0.8785 -0.2432 0.538 0.064 Uiso 1 1 calc R U . . .
C200 C 0.9629(11) -0.1888(8) 0.5904(9) 0.054(7) Uani 1 1 d DG U . . .
H200 H 0.9977 -0.2088 0.5848 0.065 Uiso 1 1 calc R U . . .
C201 C 0.9828(8) -0.1392(9) 0.6264(8) 0.053(7) Uani 1 1 d DG U . . .
H201 H 1.0312 -0.1253 0.6454 0.064 Uiso 1 1 calc R U . . .
C202 C 0.9319(10) -0.1100(7) 0.6347(7) 0.056(7) Uani 1 1 d DG U . . .
H202 H 0.9455 -0.0761 0.6593 0.067 Uiso 1 1 calc R U . . .
C203 C 0.8292(11) -0.0692(8) 0.5394(6) 0.060(6) Uani 1 1 d DG U . . .
C204 C 0.9046(11) -0.0629(9) 0.5467(6) 0.064(6) Uani 1 1 d DG U . . .
H204 H 0.9313 -0.0585 0.5766 0.077 Uiso 1 1 calc R U . . .
C205 C 0.9410(9) -0.0632(10) 0.5102(8) 0.076(6) Uani 1 1 d DG U . . .
H205 H 0.9926 -0.0589 0.5152 0.091 Uiso 1 1 calc R U . . .
C206 C 0.9020(12) -0.0698(10) 0.4665(7) 0.082(7) Uani 1 1 d DG U . . .
C207 C 0.8266(12) -0.0761(10) 0.4591(6) 0.073(6) Uani 1 1 d DG U . . .
H207 H 0.7999 -0.0806 0.4292 0.088 Uiso 1 1 calc R U . . .
C208 C 0.7901(9) -0.0758(9) 0.4956(7) 0.067(6) Uani 1 1 d DG U . . .
H208 H 0.7386 -0.0801 0.4906 0.08 Uiso 1 1 calc R U . . .
C209 C 0.9380(18) -0.0786(16) 0.4233(10) 0.080(9) Uani 1 1 d D U . . .
H20A H 0.9897 -0.0768 0.4332 0.12 Uiso 1 1 d R U . . .
H20B H 0.9349 -0.051 0.4111 0.12 Uiso 1 1 d R U . . .
H20C H 0.9129 -0.1132 0.3986 0.12 Uiso 1 1 d R U . . .
P12 P 0.8407(5) 0.1162(4) 0.6822(4) 0.054(2) Uani 1 1 d D U . . .
N12 N 0.8301(11) 0.0826(6) 0.6241(5) 0.050(4) Uani 1 1 d D U . . .
C210 C 0.7882(11) 0.1656(7) 0.6871(9) 0.074(7) Uani 1 1 d DG U . . .
C211 C 0.8135(11) 0.2189(7) 0.7155(8) 0.092(7) Uani 1 1 d DG U . . .
H211 H 0.8638 0.2339 0.7311 0.11 Uiso 1 1 calc DR U . . .
C212 C 0.7653(15) 0.2504(7) 0.7211(10) 0.099(7) Uani 1 1 d DG U . . .
H212 H 0.7827 0.2869 0.7405 0.119 Uiso 1 1 calc R U . . .
C213 C 0.6918(14) 0.2286(10) 0.6982(12) 0.118(8) Uani 1 1 d DG U . . .
H213 H 0.6588 0.2501 0.7021 0.142 Uiso 1 1 calc R U . . .
C214 C 0.6664(10) 0.1752(11) 0.6698(11) 0.112(8) Uani 1 1 d DG U . . .
H214 H 0.6162 0.1603 0.6542 0.134 Uiso 1 1 calc R U . . .
C215 C 0.7146(12) 0.1438(8) 0.6643(9) 0.096(7) Uani 1 1 d DG U . . .
H215 H 0.6973 0.1073 0.6448 0.116 Uiso 1 1 calc R U . . .
C216 C 0.9378(7) 0.1542(8) 0.7073(7) 0.050(6) Uani 1 1 d DG U . . .
C217 C 0.9912(10) 0.1411(8) 0.6821(6) 0.065(7) Uani 1 1 d DG U . . .
H217 H 0.9772 0.114 0.6514 0.078 Uiso 1 1 calc R U . . .
C218 C 1.0650(9) 0.1675(10) 0.7017(8) 0.067(7) Uani 1 1 d DG U . . .
H218 H 1.1014 0.1586 0.6844 0.08 Uiso 1 1 calc R U . . .
C219 C 1.0854(7) 0.2071(9) 0.7465(9) 0.066(7) Uani 1 1 d DG U . . .
H219 H 1.1358 0.2252 0.7599 0.08 Uiso 1 1 calc R U . . .
C220 C 1.0321(11) 0.2202(8) 0.7718(7) 0.068(7) Uani 1 1 d DG U . . .
H220 H 1.046 0.2472 0.8024 0.082 Uiso 1 1 calc R U . . .
C221 C 0.9583(9) 0.1937(8) 0.7522(6) 0.060(7) Uani 1 1 d DG U . . .
H221 H 0.9218 0.2027 0.7694 0.072 Uiso 1 1 calc DR U . . .
C222 C 0.8601(13) 0.1041(7) 0.5910(6) 0.057(6) Uani 1 1 d DG U . . .
C223 C 0.8516(12) 0.0681(6) 0.5454(7) 0.057(6) Uani 1 1 d DG U . . .
H223 H 0.8319 0.0315 0.5381 0.069 Uiso 1 1 calc R U . . .
C224 C 0.8718(13) 0.0857(8) 0.5105(6) 0.056(6) Uani 1 1 d DG U . . .
H224 H 0.866 0.0611 0.4793 0.067 Uiso 1 1 calc R U . . .
C225 C 0.9005(13) 0.1393(9) 0.5212(7) 0.061(6) Uani 1 1 d DG U . . .
C226 C 0.9090(13) 0.1753(6) 0.5669(8) 0.068(6) Uani 1 1 d DG U . . .
H226 H 0.9286 0.2119 0.5742 0.081 Uiso 1 1 calc R U . . .
C227 C 0.8888(13) 0.1577(7) 0.6018(6) 0.067(6) Uani 1 1 d DG U . . .
H227 H 0.8946 0.1823 0.633 0.08 Uiso 1 1 calc R U . . .
C228 C 0.923(2) 0.1604(13) 0.4835(10) 0.071(9) Uani 1 1 d D U . . .
H22A H 0.9047 0.1913 0.4866 0.107 Uiso 1 1 d R U . . .
H22B H 0.9006 0.1327 0.4523 0.107 Uiso 1 1 d R U . . .
H22C H 0.9766 0.1703 0.4873 0.107 Uiso 1 1 d R U . . .
Co1 Co 1.1875(3) -0.50752(18) 0.69647(19) 0.0373(14) Uani 1 1 d . . . . .
Co2 Co 1.3255(3) -0.44862(18) 0.68978(18) 0.0371(14) Uani 1 1 d . . . . .
Co3 Co 1.2945(2) -0.56383(18) 0.65940(19) 0.0339(14) Uani 1 1 d . . . . .
Co4 Co 1.4038(3) -0.49937(18) 0.74218(19) 0.0375(14) Uani 1 1 d . . . . .
Co5 Co 1.2599(3) -0.55663(18) 0.75270(19) 0.0389(15) Uani 1 1 d . . . . .
Co6 Co 1.3003(3) -0.44282(19) 0.7829(2) 0.0427(15) Uani 1 1 d . . . . .
Se1 Se 1.2373(2) -0.41491(14) 0.72806(15) 0.0386(11) Uani 1 1 d . . . . .
Se2 Se 1.23399(19) -0.51449(13) 0.62811(14) 0.0346(10) Uani 1 1 d . . . . .
Se3 Se 1.40244(19) -0.50279(13) 0.66576(14) 0.0357(11) Uani 1 1 d . . . . .
Se4 Se 1.35028(18) -0.59152(14) 0.71590(14) 0.0352(11) Uani 1 1 d . . . . .
Se5 Se 1.3605(2) -0.49340(15) 0.81192(15) 0.0409(11) Uani 1 1 d . . . . .
Se6 Se 1.18521(19) -0.50042(14) 0.77403(15) 0.0389(11) Uani 1 1 d . . . . .
Se7 Se 1.40903(19) -0.41014(13) 0.76325(14) 0.0354(11) Uani 1 1 d . . . . .
Se8 Se 1.18199(18) -0.59625(14) 0.67759(14) 0.0329(10) Uani 1 1 d . . . . .
Co7 Co 0.6739(3) -0.00179(18) 0.73088(19) 0.0398(15) Uani 1 1 d . . . . .
Co8 Co 0.7823(3) 0.0675(2) 0.8128(2) 0.0497(17) Uani 1 1 d . . . . .
Co9 Co 0.7694(3) -0.04576(19) 0.7813(2) 0.0434(15) Uani 1 1 d . . . . .
Co10 Co 0.8962(3) 0.02281(18) 0.77310(18) 0.0376(14) Uani 1 1 d . . . . .
Co11 Co 0.7880(3) -0.04708(18) 0.68705(19) 0.0384(15) Uani 1 1 d . . . . .
Co12 Co 0.8058(2) 0.06505(18) 0.71910(18) 0.0351(14) Uani 1 1 d . . . . .
Se9 Se 0.7112(2) 0.09106(15) 0.75901(15) 0.0486(12) Uani 1 1 d . . . . .
Se10 Se 0.7106(2) -0.00367(14) 0.66073(14) 0.0359(11) Uani 1 1 d . . . . .
Se11 Se 0.89098(19) 0.01884(14) 0.69557(14) 0.0367(11) Uani 1 1 d . . . . .
Se12 Se 0.8604(2) -0.07089(14) 0.74060(15) 0.0404(11) Uani 1 1 d . . . . .
Se13 Se 0.8556(2) 0.02404(14) 0.84214(14) 0.0418(11) Uani 1 1 d . . . . .
Se14 Se 0.6831(2) -0.00143(16) 0.80668(16) 0.0497(12) Uani 1 1 d . . . . .
Se15 Se 0.8867(2) 0.10840(14) 0.79260(14) 0.0410(11) Uani 1 1 d . . . . .
Se16 Se 0.6854(2) -0.08768(15) 0.70925(15) 0.0422(12) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Co13 N2 144.7(10) . . ?
N1 Co13 N13 104.0(8) . . ?
N2 Co13 N13 102.1(8) . . ?
N1 Co13 Se1 102.9(5) . . ?
N2 Co13 Se1 95.1(5) . . ?
N13 Co13 Se1 100.8(6) . . ?
C233 N13 C229 118.5(16) . . ?
C233 N13 Co13 118.8(14) . . ?
C229 N13 Co13 122.7(14) . . ?
N13 C229 C230 119.3(18) . . ?
N13 C229 H229 120.3 . . ?
C230 C229 H229 120.3 . . ?
C231 C230 C229 121.7(19) . . ?
C231 C230 H230 119.1 . . ?
C229 C230 H230 119.1 . . ?
C230 C231 C232 118.5(18) . . ?
C230 C231 C251 119(2) . . ?
C232 C231 C251 122(2) . . ?
C233 C232 C231 118.6(19) . . ?
C233 C232 H232 120.7 . . ?
C231 C232 H232 120.7 . . ?
N13 C233 C232 123.4(19) . . ?
N13 C233 H233 118.3 . . ?
C232 C233 H233 118.3 . . ?
N1 P1 C1 106.3(9) . . ?
N1 P1 C7 107.8(9) . . ?
C1 P1 C7 105.9(9) . . ?
N1 P1 Co1 111.1(7) . . ?
C1 P1 Co1 112.9(8) . . ?
C7 P1 Co1 112.4(8) . . ?
C13 N1 P1 124.2(11) . . ?
C13 N1 Co13 117.6(10) . . ?
P1 N1 Co13 116.7(9) . . ?
C2 C1 C6 120 . . ?
C2 C1 P1 123.6(11) . . ?
C6 C1 P1 116.0(11) . . ?
C3 C2 C1 120 . . ?
C3 C2 H2 120 . . ?
C1 C2 H2 120 . . ?
C2 C3 C4 120 . . ?
C2 C3 H3 120 . . ?
C4 C3 H3 120 . . ?
C5 C4 C3 120 . . ?
C5 C4 H4 120 . . ?
C3 C4 H4 120 . . ?
C4 C5 C6 120 . . ?
C4 C5 H5 120 . . ?
C6 C5 H5 120 . . ?
C5 C6 C1 120 . . ?
C5 C6 H6 120 . . ?
C1 C6 H6 120 . . ?
C8 C7 C12 120 . . ?
C8 C7 P1 120.1(10) . . ?
C12 C7 P1 119.5(10) . . ?
C9 C8 C7 120 . . ?
C9 C8 H8 120 . . ?
C7 C8 H8 120 . . ?
C10 C9 C8 120 . . ?
C10 C9 H9 120 . . ?
C8 C9 H9 120 . . ?
C9 C10 C11 120 . . ?
C9 C10 H10 120 . . ?
C11 C10 H10 120 . . ?
C12 C11 C10 120 . . ?
C12 C11 H11 120 . . ?
C10 C11 H11 120 . . ?
C11 C12 C7 120 . . ?
C11 C12 H12 120 . . ?
C7 C12 H12 120 . . ?
C14 C13 C18 120 . . ?
C14 C13 N1 121.3(11) . . ?
C18 C13 N1 118.4(12) . . ?
C13 C14 C15 120 . . ?
C13 C14 H14 120 . . ?
C15 C14 H14 120 . . ?
C14 C15 C16 120 . . ?
C14 C15 H15 120 . . ?
C16 C15 H15 120 . . ?
C17 C16 C15 120 . . ?
C17 C16 C19 118.1(14) . . ?
C15 C16 C19 121.8(14) . . ?
C16 C17 C18 120 . . ?
C16 C17 H17 120 . . ?
C18 C17 H17 120 . . ?
C17 C18 C13 120 . . ?
C17 C18 H18 120 . . ?
C13 C18 H18 120 . . ?
C16 C19 H19A 109.6 . . ?
C16 C19 H19B 109.1 . . ?
H19A C19 H19B 109.5 . . ?
C16 C19 H19C 109.7 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
N2 P2 C20 107.2(10) . . ?
N2 P2 C26 109.9(10) . . ?
C20 P2 C26 105.6(9) . . ?
N2 P2 Co2 110.6(7) . . ?
C20 P2 Co2 114.7(8) . . ?
C26 P2 Co2 108.8(9) . . ?
C32 N2 P2 121.0(12) . . ?
C32 N2 Co13 119.3(12) . . ?
P2 N2 Co13 118.6(9) . . ?
C21 C20 C25 120 . . ?
C21 C20 P2 121.5(11) . . ?
C25 C20 P2 118.4(11) . . ?
C22 C21 C20 120 . . ?
C22 C21 H21 120 . . ?
C20 C21 H21 120 . . ?
C21 C22 C23 120 . . ?
C21 C22 H22 120 . . ?
C23 C22 H22 120 . . ?
C24 C23 C22 120 . . ?
C24 C23 H23 120 . . ?
C22 C23 H23 120 . . ?
C23 C24 C25 120 . . ?
C23 C24 H24 120 . . ?
C25 C24 H24 120 . . ?
C24 C25 C20 120 . . ?
C24 C25 H25 120 . . ?
C20 C25 H25 120 . . ?
C27 C26 C31 120 . . ?
C27 C26 P2 119.6(11) . . ?
C31 C26 P2 119.5(11) . . ?
C26 C27 C28 120 . . ?
C26 C27 H27 120 . . ?
C28 C27 H27 120 . . ?
C27 C28 C29 120 . . ?
C27 C28 H28 120 . . ?
C29 C28 H28 120 . . ?
C30 C29 C28 120 . . ?
C30 C29 H29 120 . . ?
C28 C29 H29 120 . . ?
C31 C30 C29 120 . . ?
C31 C30 H30 120 . . ?
C29 C30 H30 120 . . ?
C30 C31 C26 120 . . ?
C30 C31 H31 120 . . ?
C26 C31 H31 120 . . ?
C33 C32 C37 120 . . ?
C33 C32 N2 116.9(13) . . ?
C37 C32 N2 122.9(13) . . ?
C34 C33 C32 120 . . ?
C34 C33 H33 120 . . ?
C32 C33 H33 120 . . ?
C33 C34 C35 120 . . ?
C33 C34 H34 120 . . ?
C35 C34 H34 120 . . ?
C34 C35 C36 120 . . ?
C34 C35 C38 121.1(14) . . ?
C36 C35 C38 118.5(15) . . ?
C37 C36 C35 120 . . ?
C37 C36 H36 120 . . ?
C35 C36 H36 120 . . ?
C36 C37 C32 120 . . ?
C36 C37 H37 120 . . ?
C32 C37 H37 120 . . ?
C35 C38 H38A 109.5 . . ?
C35 C38 H38B 109.1 . . ?
H38A C38 H38B 109.5 . . ?
C35 C38 H38C 109.8 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
N3 Co14 N4 135.7(9) . . ?
N3 Co14 N14 110.1(9) . . ?
N4 Co14 N14 104.6(9) . . ?
N3 Co14 Se4 93.4(5) . . ?
N4 Co14 Se4 109.9(5) . . ?
N14 Co14 Se4 95.8(8) . . ?
C238 N14 C234 117.5(16) . . ?
C238 N14 Co14 121.7(16) . . ?
C234 N14 Co14 120.7(15) . . ?
N14 C234 C235 121.0(19) . . ?
N14 C234 H234 119.5 . . ?
C235 C234 H234 119.5 . . ?
C236 C235 C234 121(2) . . ?
C236 C235 H235 119.7 . . ?
C234 C235 H235 119.7 . . ?
C237 C236 C235 117.3(19) . . ?
C237 C236 C246 124(10) . 1_645 ?
C235 C236 C246 117(10) . 1_645 ?
C238 C237 C236 121(2) . . ?
C238 C237 H237 119.6 . . ?
C236 C237 H237 119.6 . . ?
N14 C238 C237 122.4(19) . . ?
N14 C238 H238 118.8 . . ?
C237 C238 H238 118.8 . . ?
N3 P3 C39 108.5(9) . . ?
N3 P3 C45 106.0(9) . . ?
C39 P3 C45 100.5(9) . . ?
N3 P3 Co3 113.3(8) . . ?
C39 P3 Co3 107.6(9) . . ?
C45 P3 Co3 119.9(7) . . ?
C51 N3 P3 120.2(12) . . ?
C51 N3 Co14 114.0(12) . . ?
P3 N3 Co14 121.5(10) . . ?
C40 C39 C44 120 . . ?
C40 C39 P3 119.4(11) . . ?
C44 C39 P3 120.6(11) . . ?
C39 C40 C41 120 . . ?
C39 C40 H40 120 . . ?
C41 C40 H40 120 . . ?
C40 C41 C42 120 . . ?
C40 C41 H41 120 . . ?
C42 C41 H41 120 . . ?
C43 C42 C41 120 . . ?
C43 C42 H42 120 . . ?
C41 C42 H42 120 . . ?
C44 C43 C42 120 . . ?
C44 C43 H43 120 . . ?
C42 C43 H43 120 . . ?
C43 C44 C39 120 . . ?
C43 C44 H44 120 . . ?
C39 C44 H44 120 . . ?
C46 C45 C50 120 . . ?
C46 C45 P3 119.9(11) . . ?
C50 C45 P3 120.0(11) . . ?
C45 C46 C47 120 . . ?
C45 C46 H46 120 . . ?
C47 C46 H46 120 . . ?
C46 C47 C48 120 . . ?
C46 C47 H47 120 . . ?
C48 C47 H47 120 . . ?
C47 C48 C49 120 . . ?
C47 C48 H48 120 . . ?
C49 C48 H48 120 . . ?
C50 C49 C48 120 . . ?
C50 C49 H49 120 . . ?
C48 C49 H49 120 . . ?
C49 C50 C45 120 . . ?
C49 C50 H50 120 . . ?
C45 C50 H50 120 . . ?
C52 C51 C56 120 . . ?
C52 C51 N3 117.3(13) . . ?
C56 C51 N3 120.1(13) . . ?
C53 C52 C51 120 . . ?
C53 C52 H52 120 . . ?
C51 C52 H52 120 . . ?
C52 C53 C54 120 . . ?
C52 C53 H53 120 . . ?
C54 C53 H53 120 . . ?
C55 C54 C53 120 . . ?
C55 C54 C57 117.1(15) . . ?
C53 C54 C57 122.6(15) . . ?
C56 C55 C54 120 . . ?
C56 C55 H55 120 . . ?
C54 C55 H55 120 . . ?
C55 C56 C51 120 . . ?
C55 C56 H56 120 . . ?
C51 C56 H56 120 . . ?
C54 C57 H57A 109 . . ?
C54 C57 H57B 109.5 . . ?
H57A C57 H57B 109.5 . . ?
C54 C57 H57C 110 . . ?
H57A C57 H57C 109.5 . . ?
H57B C57 H57C 109.5 . . ?
N4 P4 C64 110.8(9) . . ?
N4 P4 C58 105.4(10) . . ?
C64 P4 C58 107.1(9) . . ?
N4 P4 Co4 109.3(7) . . ?
C64 P4 Co4 110.9(8) . . ?
C58 P4 Co4 113.3(8) . . ?
C70 N4 P4 125.2(11) . . ?
C70 N4 Co14 119.4(10) . . ?
P4 N4 Co14 115.4(9) . . ?
C59 C58 C63 120 . . ?
C59 C58 P4 119.7(11) . . ?
C63 C58 P4 120.1(11) . . ?
C58 C59 C60 120 . . ?
C58 C59 H59 120 . . ?
C60 C59 H59 120 . . ?
C61 C60 C59 120 . . ?
C61 C60 H60 120 . . ?
C59 C60 H60 120 . . ?
C62 C61 C60 120 . . ?
C62 C61 H61 120 . . ?
C60 C61 H61 120 . . ?
C63 C62 C61 120 . . ?
C63 C62 H62 120 . . ?
C61 C62 H62 120 . . ?
C62 C63 C58 120 . . ?
C62 C63 H63 120 . . ?
C58 C63 H63 120 . . ?
C65 C64 C69 120 . . ?
C65 C64 P4 119.4(11) . . ?
C69 C64 P4 120.6(11) . . ?
C64 C65 C66 120 . . ?
C64 C65 H65 120 . . ?
C66 C65 H65 120 . . ?
C67 C66 C65 120 . . ?
C67 C66 H66 120 . . ?
C65 C66 H66 120 . . ?
C68 C67 C66 120 . . ?
C68 C67 H67 120 . . ?
C66 C67 H67 120 . . ?
C69 C68 C67 120 . . ?
C69 C68 H68 120 . . ?
C67 C68 H68 120 . . ?
C68 C69 C64 120 . . ?
C68 C69 H69 120 . . ?
C64 C69 H69 120 . . ?
C71 C70 C75 120 . . ?
C71 C70 N4 115.4(11) . . ?
C75 C70 N4 124.5(11) . . ?
C72 C71 C70 120 . . ?
C72 C71 H71 120 . . ?
C70 C71 H71 120 . . ?
C71 C72 C73 120 . . ?
C71 C72 H72 120 . . ?
C73 C72 H72 120 . . ?
C74 C73 C72 120 . . ?
C74 C73 C76 118.9(14) . . ?
C72 C73 C76 120.8(14) . . ?
C73 C74 C75 120 . . ?
C73 C74 H74 120 . . ?
C75 C74 H74 120 . . ?
C74 C75 C70 120 . . ?
C74 C75 H75 120 . . ?
C70 C75 H75 120 . . ?
C73 C76 H76A 110.2 . . ?
C73 C76 H76B 109.4 . . ?
H76A C76 H76B 109.5 . . ?
C73 C76 H76C 108.7 . . ?
H76A C76 H76C 109.5 . . ?
H76B C76 H76C 109.5 . . ?
N6 Co15 N5 144.9(9) . . ?
N6 Co15 N15 104.2(8) . . ?
N5 Co15 N15 100.5(9) . . ?
N6 Co15 Se5 95.1(5) . . ?
N5 Co15 Se5 107.5(6) . . ?
N15 Co15 Se5 94.6(8) . . ?
C243 N15 C239 123.1(15) . . ?
C243 N15 Co15 116.6(15) . . ?
C239 N15 Co15 120.3(15) . . ?
N15 C239 C240 115.8(18) . . ?
N15 C239 H239 122.1 . . ?
C240 C239 H239 122.1 . . ?
C239 C240 C241 122(2) . . ?
C239 C240 H240 118.9 . . ?
C241 C240 H240 118.9 . . ?
C240 C241 C242 118.8(19) . . ?
C240 C241 C241 129(3) . 2_847 ?
C242 C241 C241 111(3) . 2_847 ?
C243 C242 C241 119(2) . . ?
C243 C242 H242 120.5 . . ?
C241 C242 H242 120.5 . . ?
C242 C243 N15 120.5(19) . . ?
C242 C243 H243 119.8 . . ?
N15 C243 H243 119.8 . . ?
N5 P5 C77 110.6(10) . . ?
N5 P5 C83 107.1(10) . . ?
C77 P5 C83 106.4(10) . . ?
N5 P5 Co5 108.7(7) . . ?
C77 P5 Co5 112.8(8) . . ?
C83 P5 Co5 111.2(9) . . ?
C89 N5 P5 123.2(11) . . ?
C89 N5 Co15 120.2(11) . . ?
P5 N5 Co15 116.5(10) . . ?
C78 C77 C82 120 . . ?
C78 C77 P5 121.0(11) . . ?
C82 C77 P5 118.9(11) . . ?
C79 C78 C77 120 . . ?
C79 C78 H78 120 . . ?
C77 C78 H78 120 . . ?
C78 C79 C80 120 . . ?
C78 C79 H79 120 . . ?
C80 C79 H79 120 . . ?
C81 C80 C79 120 . . ?
C81 C80 H80 120 . . ?
C79 C80 H80 120 . . ?
C80 C81 C82 120 . . ?
C80 C81 H81 120 . . ?
C82 C81 H81 120 . . ?
C81 C82 C77 120 . . ?
C81 C82 H82 120 . . ?
C77 C82 H82 120 . . ?
C84 C83 C88 120 . . ?
C84 C83 P5 118.5(11) . . ?
C88 C83 P5 121.5(11) . . ?
C83 C84 C85 120 . . ?
C83 C84 H84 120 . . ?
C85 C84 H84 120 . . ?
C86 C85 C84 120 . . ?
C86 C85 H85 120 . . ?
C84 C85 H85 120 . . ?
C85 C86 C87 120 . . ?
C85 C86 H86 120 . . ?
C87 C86 H86 120 . . ?
C88 C87 C86 120 . . ?
C88 C87 H87 120 . . ?
C86 C87 H87 120 . . ?
C87 C88 C83 120 . . ?
C87 C88 H88 120 . . ?
C83 C88 H88 120 . . ?
C90 C89 C94 120 . . ?
C90 C89 N5 118.3(12) . . ?
C94 C89 N5 121.3(12) . . ?
C91 C90 C89 120 . . ?
C91 C90 H90 120 . . ?
C89 C90 H90 120 . . ?
C92 C91 C90 120 . . ?
C92 C91 H91 120 . . ?
C90 C91 H91 120 . . ?
C93 C92 C91 120 . . ?
C93 C92 C95 116.9(16) . . ?
C91 C92 C95 122.8(16) . . ?
C92 C93 C94 120 . . ?
C92 C93 H93 120 . . ?
C94 C93 H93 120 . . ?
C93 C94 C89 120 . . ?
C93 C94 H94 120 . . ?
C89 C94 H94 120 . . ?
C92 C95 H95A 109.9 . . ?
C92 C95 H95B 108.4 . . ?
H95A C95 H95B 109.5 . . ?
C92 C95 H95C 110.1 . . ?
H95A C95 H95C 109.5 . . ?
H95B C95 H95C 109.5 . . ?
N6 P6 C96 107.6(10) . . ?
N6 P6 C102 105.6(10) . . ?
C96 P6 C102 105.2(10) . . ?
N6 P6 Co6 112.4(7) . . ?
C96 P6 Co6 111.9(9) . . ?
C102 P6 Co6 113.6(9) . . ?
C108 N6 P6 116.2(8) . . ?
C108 N6 Co15 124.6(9) . . ?
P6 N6 Co15 117.7(9) . . ?
C97 C96 C101 120 . . ?
C97 C96 P6 120.3(11) . . ?
C101 C96 P6 119.1(11) . . ?
C98 C97 C96 120 . . ?
C98 C97 H97 120 . . ?
C96 C97 H97 120 . . ?
C97 C98 C99 120 . . ?
C97 C98 H98 120 . . ?
C99 C98 H98 120 . . ?
C100 C99 C98 120 . . ?
C100 C99 H99 120 . . ?
C98 C99 H99 120 . . ?
C101 C100 C99 120 . . ?
C101 C100 H100 120 . . ?
C99 C100 H100 120 . . ?
C100 C101 C96 120 . . ?
C100 C101 H101 120 . . ?
C96 C101 H101 120 . . ?
C103 C102 C107 120 . . ?
C103 C102 P6 119.5(11) . . ?
C107 C102 P6 120.2(11) . . ?
C104 C103 C102 120 . . ?
C104 C103 H103 120 . . ?
C102 C103 H103 120 . . ?
C103 C104 C105 120 . . ?
C103 C104 H104 120 . . ?
C105 C104 H104 120 . . ?
C106 C105 C104 120 . . ?
C106 C105 H105 120 . . ?
C104 C105 H105 120 . . ?
C107 C106 C105 120 . . ?
C107 C106 H106 120 . . ?
C105 C106 H106 120 . . ?
C106 C107 C102 120 . . ?
C106 C107 H107 120 . . ?
C102 C107 H107 120 . . ?
C109 C108 C113 120 . . ?
C109 C108 N6 119.8(12) . . ?
C113 C108 N6 120.2(12) . . ?
C110 C109 C108 120 . . ?
C110 C109 H109 120 . . ?
C108 C109 H109 120 . . ?
C109 C110 C111 120 . . ?
C109 C110 H110 120 . . ?
C111 C110 H110 120 . . ?
C112 C111 C110 120 . . ?
C112 C111 C114 116.6(16) . . ?
C110 C111 C114 123.4(16) . . ?
C111 C112 C113 120 . . ?
C111 C112 H112 120 . . ?
C113 C112 H112 120 . . ?
C112 C113 C108 120 . . ?
C112 C113 H113 120 . . ?
C108 C113 H113 120 . . ?
C111 C114 H11A 109.5 . . ?
C111 C114 H11B 109.7 . . ?
H11A C114 H11B 109.5 . . ?
C111 C114 H11C 109.2 . . ?
H11A C114 H11C 109.5 . . ?
H11B C114 H11C 109.5 . . ?
N8 Co16 N7 140.4(10) . . ?
N8 Co16 N16 106.3(9) . . ?
N7 Co16 N16 101.7(9) . . ?
N8 Co16 Se9 96.6(6) . . ?
N7 Co16 Se9 103.6(5) . . ?
N16 Co16 Se9 103.3(7) . . ?
C244 N16 C248 120 . . ?
C244 N16 Co16 116.6(12) . . ?
C248 N16 Co16 122.0(12) . . ?
C245 C244 N16 120 . . ?
C245 C244 H244 120 . . ?
N16 C244 H244 120 . . ?
C244 C245 C246 120 . . ?
C244 C245 H245 120 . . ?
C246 C245 H245 120 . . ?
C247 C246 C245 120 . . ?
C247 C246 C236 121(3) . 1_465 ?
C245 C246 C236 117(3) . 1_465 ?
C246 C247 C248 120 . . ?
C246 C247 H247 120 . . ?
C248 C247 H247 120 . . ?
C247 C248 N16 120 . . ?
C247 C248 H248 120 . . ?
N16 C248 H248 120 . . ?
N7 P7 C121 106.6(11) . . ?
N7 P7 C115 108.2(12) . . ?
C121 P7 C115 105.1(11) . . ?
N7 P7 Co7 109.6(10) . . ?
C121 P7 Co7 107.0(11) . . ?
C115 P7 Co7 119.7(11) . . ?
C127 N7 P7 125.0(10) . . ?
C127 N7 Co16 114.7(11) . . ?
P7 N7 Co16 115.9(11) . . ?
C116 C115 C120 120 . . ?
C116 C115 P7 121.5(14) . . ?
C120 C115 P7 117.0(14) . . ?
C117 C116 C115 120 . . ?
C117 C116 H116 120 . . ?
C115 C116 H116 120 . . ?
C116 C117 C118 120 . . ?
C116 C117 H117 120 . . ?
C118 C117 H117 120 . . ?
C117 C118 C119 120 . . ?
C117 C118 H118 120 . . ?
C119 C118 H118 120 . . ?
C120 C119 C118 120 . . ?
C120 C119 H119 120 . . ?
C118 C119 H119 120 . . ?
C119 C120 C115 120 . . ?
C119 C120 H120 120 . . ?
C115 C120 H120 120 . . ?
C122 C121 C126 120 . . ?
C122 C121 P7 117.3(14) . . ?
C126 C121 P7 122.7(14) . . ?
C121 C122 C123 120 . . ?
C121 C122 H122 120 . . ?
C123 C122 H122 120 . . ?
C124 C123 C122 120 . . ?
C124 C123 H123 120 . . ?
C122 C123 H123 120 . . ?
C123 C124 C125 120 . . ?
C123 C124 H124 120 . . ?
C125 C124 H124 120 . . ?
C126 C125 C124 120 . . ?
C126 C125 H125 120 . . ?
C124 C125 H125 120 . . ?
C125 C126 C121 120 . . ?
C125 C126 H126 120 . . ?
C121 C126 H126 120 . . ?
C128 C127 C132 120 . . ?
C128 C127 N7 116.0(13) . . ?
C132 C127 N7 124.0(13) . . ?
C127 C128 C129 120 . . ?
C127 C128 H128 120 . . ?
C129 C128 H128 120 . . ?
C128 C129 C130 120 . . ?
C128 C129 H129 120 . . ?
C130 C129 H129 120 . . ?
C131 C130 C129 120 . . ?
C131 C130 C133 118.3(16) . . ?
C129 C130 C133 121.7(16) . . ?
C130 C131 C132 120 . . ?
C130 C131 H131 120 . . ?
C132 C131 H131 120 . . ?
C131 C132 C127 120 . . ?
C131 C132 H132 120 . . ?
C127 C132 H132 120 . . ?
C130 C133 H13A 109.5 . . ?
C130 C133 H13B 108.9 . . ?
H13A C133 H13B 109.5 . . ?
C130 C133 H13C 109.9 . . ?
H13A C133 H13C 109.5 . . ?
H13B C133 H13C 109.5 . . ?
N8 P8 C140 107.1(11) . . ?
N8 P8 C134 106.9(11) . . ?
C140 P8 C134 105.9(11) . . ?
N8 P8 Co8 110.9(9) . . ?
C140 P8 Co8 109.8(11) . . ?
C134 P8 Co8 115.9(10) . . ?
C146 N8 P8 124.4(13) . . ?
C146 N8 Co16 116.1(12) . . ?
P8 N8 Co16 118.9(10) . . ?
C135 C134 C139 120 . . ?
C135 C134 P8 122.8(13) . . ?
C139 C134 P8 117.1(13) . . ?
C134 C135 C136 120 . . ?
C134 C135 H135 120 . . ?
C136 C135 H135 120 . . ?
C135 C136 C137 120 . . ?
C135 C136 H136 120 . . ?
C137 C136 H136 120 . . ?
C138 C137 C136 120 . . ?
C138 C137 H137 120 . . ?
C136 C137 H137 120 . . ?
C139 C138 C137 120 . . ?
C139 C138 H138 120 . . ?
C137 C138 H138 120 . . ?
C138 C139 C134 120 . . ?
C138 C139 H139 120 . . ?
C134 C139 H139 120 . . ?
C141 C140 C145 120 . . ?
C141 C140 P8 119.3(12) . . ?
C145 C140 P8 119.5(12) . . ?
C140 C141 C142 120 . . ?
C140 C141 H141 120 . . ?
C142 C141 H141 120 . . ?
C143 C142 C141 120 . . ?
C143 C142 H142 120 . . ?
C141 C142 H142 120 . . ?
C144 C143 C142 120 . . ?
C144 C143 H143 120 . . ?
C142 C143 H143 120 . . ?
C143 C144 C145 120 . . ?
C143 C144 H144 120 . . ?
C145 C144 H144 120 . . ?
C144 C145 C140 120 . . ?
C144 C145 H145 120 . . ?
C140 C145 H145 120 . . ?
C147 C146 C151 120 . . ?
C147 C146 N8 119.3(14) . . ?
C151 C146 N8 120.4(14) . . ?
C148 C147 C146 120 . . ?
C148 C147 H147 120 . . ?
C146 C147 H147 120 . . ?
C149 C148 C147 120 . . ?
C149 C148 H148 120 . . ?
C147 C148 H148 120 . . ?
C148 C149 C150 120 . . ?
C148 C149 C152 121.1(16) . . ?
C150 C149 C152 118.9(16) . . ?
C149 C150 C151 120 . . ?
C149 C150 H150 120 . . ?
C151 C150 H150 120 . . ?
C150 C151 C146 120 . . ?
C150 C151 H151 120 . . ?
C146 C151 H151 120 . . ?
C149 C152 H15A 108.7 . . ?
C149 C152 H15B 111 . . ?
H15A C152 H15B 109.5 . . ?
C149 C152 H15C 108.7 . . ?
H15A C152 H15C 109.5 . . ?
H15B C152 H15C 109.5 . . ?
N9 Co17 N10 138.8(10) . . ?
N9 Co17 N17 107.0(9) . . ?
N10 Co17 N17 105.0(9) . . ?
N9 Co17 Se12 93.1(6) . . ?
N10 Co17 Se12 103.9(5) . . ?
N17 Co17 Se12 103.7(6) . . ?
C253 N17 C249 117.2(15) . . ?
C253 N17 Co17 120.7(14) . . ?
C249 N17 Co17 122.1(14) . . ?
N17 C249 C250 118.9(17) . . ?
N17 C249 H249 120.6 . . ?
C250 C249 H249 120.6 . . ?
C251 C250 C249 122.7(18) . . ?
C251 C250 H250 118.7 . . ?
C249 C250 H250 118.7 . . ?
C250 C251 C252 118.5(18) . . ?
C250 C251 C231 121(2) . . ?
C252 C251 C231 119(2) . . ?
C253 C252 C251 117.2(19) . . ?
C253 C252 H252 121.4 . . ?
C251 C252 H252 121.4 . . ?
C252 C253 N17 125.5(19) . . ?
C252 C253 H253 117.2 . . ?
N17 C253 H253 117.2 . . ?
N9 P9 C153 106.9(11) . . ?
N9 P9 C159 106.8(11) . . ?
C153 P9 C159 100.1(10) . . ?
N9 P9 Co9 111.2(9) . . ?
C153 P9 Co9 119.8(9) . . ?
C159 P9 Co9 110.8(10) . . ?
C165 N9 P9 127.0(13) . . ?
C165 N9 Co17 109.2(12) . . ?
P9 N9 Co17 121.0(11) . . ?
C154 C153 C158 120 . . ?
C154 C153 P9 124.1(13) . . ?
C158 C153 P9 115.9(13) . . ?
C155 C154 C153 120 . . ?
C155 C154 H154 120 . . ?
C153 C154 H154 120 . . ?
C154 C155 C156 120 . . ?
C154 C155 H155 120 . . ?
C156 C155 H155 120 . . ?
C155 C156 C157 120 . . ?
C155 C156 H156 120 . . ?
C157 C156 H156 120 . . ?
C158 C157 C156 120 . . ?
C158 C157 H157 120 . . ?
C156 C157 H157 120 . . ?
C157 C158 C153 120 . . ?
C157 C158 H158 120 . . ?
C153 C158 H158 120 . . ?
C160 C159 C164 120 . . ?
C160 C159 P9 118.1(12) . . ?
C164 C159 P9 121.6(12) . . ?
C161 C160 C159 120 . . ?
C161 C160 H160 120 . . ?
C159 C160 H160 120 . . ?
C160 C161 C162 120 . . ?
C160 C161 H161 120 . . ?
C162 C161 H161 120 . . ?
C161 C162 C163 120 . . ?
C161 C162 H162 120 . . ?
C163 C162 H162 120 . . ?
C164 C163 C162 120 . . ?
C164 C163 H163 120 . . ?
C162 C163 H163 120 . . ?
C163 C164 C159 120 . . ?
C163 C164 H164 120 . . ?
C159 C164 H164 120 . . ?
C166 C165 C170 120 . . ?
C166 C165 N9 118.2(14) . . ?
C170 C165 N9 121.0(14) . . ?
C165 C166 C167 120 . . ?
C165 C166 H166 120 . . ?
C167 C166 H166 120 . . ?
C166 C167 C168 120 . . ?
C166 C167 H167 120 . . ?
C168 C167 H167 120 . . ?
C169 C168 C167 120 . . ?
C169 C168 C171 118.3(16) . . ?
C167 C168 C171 120.8(16) . . ?
C168 C169 C170 120 . . ?
C168 C169 H169 120 . . ?
C170 C169 H169 120 . . ?
C169 C170 C165 120 . . ?
C169 C170 H170 120 . . ?
C165 C170 H170 120 . . ?
C168 C171 H17A 111.4 . . ?
C168 C171 H17B 107.7 . . ?
H17A C171 H17B 109.5 . . ?
C168 C171 H17C 109.2 . . ?
H17A C171 H17C 109.5 . . ?
H17B C171 H17C 109.5 . . ?
N10 P10 C172 106.6(11) . . ?
N10 P10 C178 105.8(10) . . ?
C172 P10 C178 108.7(10) . . ?
N10 P10 Co10 108.9(7) . . ?
C172 P10 Co10 111.2(10) . . ?
C178 P10 Co10 115.3(10) . . ?
C184 N10 P10 119.8(9) . . ?
C184 N10 Co17 121.9(9) . . ?
P10 N10 Co17 117.6(8) . . ?
C173 C172 C177 120 . . ?
C173 C172 P10 120.9(13) . . ?
C177 C172 P10 119.1(13) . . ?
C172 C173 C174 120 . . ?
C172 C173 H173 120 . . ?
C174 C173 H173 120 . . ?
C175 C174 C173 120 . . ?
C175 C174 H174 120 . . ?
C173 C174 H174 120 . . ?
C174 C175 C176 120 . . ?
C174 C175 H175 120 . . ?
C176 C175 H175 120 . . ?
C175 C176 C177 120 . . ?
C175 C176 H176 120 . . ?
C177 C176 H176 120 . . ?
C176 C177 C172 120 . . ?
C176 C177 H177 120 . . ?
C172 C177 H177 120 . . ?
C179 C178 C183 120 . . ?
C179 C178 P10 121.4(12) . . ?
C183 C178 P10 118.5(12) . . ?
C178 C179 C180 120 . . ?
C178 C179 H179 120 . . ?
C180 C179 H179 120 . . ?
C179 C180 C181 120 . . ?
C179 C180 H180 120 . . ?
C181 C180 H180 120 . . ?
C182 C181 C180 120 . . ?
C182 C181 H181 120 . . ?
C180 C181 H181 120 . . ?
C181 C182 C183 120 . . ?
C181 C182 H182 120 . . ?
C183 C182 H182 120 . . ?
C182 C183 C178 120 . . ?
C182 C183 H183 120 . . ?
C178 C183 H183 120 . . ?
C185 C184 C189 120 . . ?
C185 C184 N10 118.1(7) . . ?
C189 C184 N10 121.9(7) . . ?
C184 C185 C186 120 . . ?
C184 C185 H185 120 . . ?
C186 C185 H185 120 . . ?
C187 C186 C185 120 . . ?
C187 C186 H186 120 . . ?
C185 C186 H186 120 . . ?
C186 C187 C188 120 . . ?
C186 C187 C190 124.5(15) . . ?
C188 C187 C190 115.5(15) . . ?
C189 C188 C187 120 . . ?
C189 C188 H188 120 . . ?
C187 C188 H188 120 . . ?
C188 C189 C184 120 . . ?
C188 C189 H189 120 . . ?
C184 C189 H189 120 . . ?
C187 C190 H19D 110.5 . . ?
C187 C190 H19E 109.2 . . ?
H19D C190 H19E 109.5 . . ?
C187 C190 H19F 108.7 . . ?
H19D C190 H19F 109.5 . . ?
H19E C190 H19F 109.5 . . ?
N11 Co18 N12 135.9(9) . . ?
N11 Co18 N18 109.3(8) . . ?
N12 Co18 N18 107.5(8) . . ?
N11 Co18 Se10 94.9(5) . . ?
N12 Co18 Se10 106.4(5) . . ?
N18 Co18 Se10 93.3(7) . . ?
C258 N18 C254 116.8(16) . . ?
C258 N18 Co18 120.6(14) . . ?
C254 N18 Co18 121.1(14) . . ?
N18 C254 C255 118.8(18) . . ?
N18 C254 H254 120.6 . . ?
C255 C254 H254 120.6 . . ?
C256 C255 C254 123.2(19) . . ?
C256 C255 H255 118.4 . . ?
C254 C255 H255 118.4 . . ?
C255 C256 C257 117.3(18) . . ?
C255 C256 C256 124(3) . 2_656 ?
C257 C256 C256 119(3) . 2_656 ?
C258 C257 C256 119(2) . . ?
C258 C257 H257 120.5 . . ?
C256 C257 H257 120.5 . . ?
C257 C258 N18 124.9(19) . . ?
C257 C258 H258 117.5 . . ?
N18 C258 H258 117.5 . . ?
N11 P11 C191 108.4(10) . . ?
N11 P11 C197 108.6(9) . . ?
C191 P11 C197 101.1(9) . . ?
N11 P11 Co11 112.3(7) . . ?
C191 P11 Co11 109.3(8) . . ?
C197 P11 Co11 116.4(8) . . ?
C203 N11 P11 123.9(12) . . ?
C203 N11 Co18 113.7(11) . . ?
P11 N11 Co18 121.9(10) . . ?
C192 C191 C196 120 . . ?
C192 C191 P11 120.5(11) . . ?
C196 C191 P11 119.2(11) . . ?
C191 C192 C193 120 . . ?
C191 C192 H192 120 . . ?
C193 C192 H192 120 . . ?
C192 C193 C194 120 . . ?
C192 C193 H193 120 . . ?
C194 C193 H193 120 . . ?
C195 C194 C193 120 . . ?
C195 C194 H194 120 . . ?
C193 C194 H194 120 . . ?
C194 C195 C196 120 . . ?
C194 C195 H195 120 . . ?
C196 C195 H195 120 . . ?
C195 C196 C191 120 . . ?
C195 C196 H196 120 . . ?
C191 C196 H196 120 . . ?
C198 C197 C202 120 . . ?
C198 C197 P11 117.2(10) . . ?
C202 C197 P11 122.8(10) . . ?
C197 C198 C199 120 . . ?
C197 C198 H198 120 . . ?
C199 C198 H198 120 . . ?
C200 C199 C198 120 . . ?
C200 C199 H199 120 . . ?
C198 C199 H199 120 . . ?
C201 C200 C199 120 . . ?
C201 C200 H200 120 . . ?
C199 C200 H200 120 . . ?
C200 C201 C202 120 . . ?
C200 C201 H201 120 . . ?
C202 C201 H201 120 . . ?
C201 C202 C197 120 . . ?
C201 C202 H202 120 . . ?
C197 C202 H202 120 . . ?
C204 C203 C208 120 . . ?
C204 C203 N11 117.5(13) . . ?
C208 C203 N11 121.2(13) . . ?
C203 C204 C205 120 . . ?
C203 C204 H204 120 . . ?
C205 C204 H204 120 . . ?
C204 C205 C206 120 . . ?
C204 C205 H205 120 . . ?
C206 C205 H205 120 . . ?
C207 C206 C205 120 . . ?
C207 C206 C209 118.1(15) . . ?
C205 C206 C209 121.3(15) . . ?
C206 C207 C208 120 . . ?
C206 C207 H207 120 . . ?
C208 C207 H207 120 . . ?
C207 C208 C203 120 . . ?
C207 C208 H208 120 . . ?
C203 C208 H208 120 . . ?
C206 C209 H20A 108.9 . . ?
C206 C209 H20B 109.1 . . ?
H20A C209 H20B 109.5 . . ?
C206 C209 H20C 110.3 . . ?
H20A C209 H20C 109.5 . . ?
H20B C209 H20C 109.5 . . ?
N12 P12 C216 109.3(9) . . ?
N12 P12 C210 105.6(10) . . ?
C216 P12 C210 105.9(9) . . ?
N12 P12 Co12 112.3(7) . . ?
C216 P12 Co12 110.4(8) . . ?
C210 P12 Co12 113.1(10) . . ?
C222 N12 P12 125.3(11) . . ?
C222 N12 Co18 117.8(10) . . ?
P12 N12 Co18 116.8(9) . . ?
C211 C210 C215 120 . . ?
C211 C210 P12 125.8(11) . . ?
C215 C210 P12 113.7(11) . . ?
C212 C211 C210 120 . . ?
C212 C211 H211 120 . . ?
C210 C211 H211 120 . . ?
C213 C212 C211 120 . . ?
C213 C212 H212 120 . . ?
C211 C212 H212 120 . . ?
C214 C213 C212 120 . . ?
C214 C213 H213 120 . . ?
C212 C213 H213 120 . . ?
C213 C214 C215 120 . . ?
C213 C214 H214 120 . . ?
C215 C214 H214 120 . . ?
C214 C215 C210 120 . . ?
C214 C215 H215 120 . . ?
C210 C215 H215 120 . . ?
C217 C216 C221 120 . . ?
C217 C216 P12 119.4(11) . . ?
C221 C216 P12 120.5(11) . . ?
C218 C217 C216 120 . . ?
C218 C217 H217 120 . . ?
C216 C217 H217 120 . . ?
C219 C218 C217 120 . . ?
C219 C218 H218 120 . . ?
C217 C218 H218 120 . . ?
C218 C219 C220 120 . . ?
C218 C219 H219 120 . . ?
C220 C219 H219 120 . . ?
C221 C220 C219 120 . . ?
C221 C220 H220 120 . . ?
C219 C220 H220 120 . . ?
C220 C221 C216 120 . . ?
C220 C221 H221 120 . . ?
C216 C221 H221 120 . . ?
C223 C222 C227 120 . . ?
C223 C222 N12 116.0(12) . . ?
C227 C222 N12 123.7(12) . . ?
C222 C223 C224 120 . . ?
C222 C223 H223 120 . . ?
C224 C223 H223 120 . . ?
C225 C224 C223 120 . . ?
C225 C224 H224 120 . . ?
C223 C224 H224 120 . . ?
C224 C225 C226 120 . . ?
C224 C225 C228 121.6(14) . . ?
C226 C225 C228 118.3(14) . . ?
C227 C226 C225 120 . . ?
C227 C226 H226 120 . . ?
C225 C226 H226 120 . . ?
C226 C227 C222 120 . . ?
C226 C227 H227 120 . . ?
C222 C227 H227 120 . . ?
C225 C228 H22A 108.9 . . ?
C225 C228 H22B 108.5 . . ?
H22A C228 H22B 109.5 . . ?
C225 C228 H22C 111 . . ?
H22A C228 H22C 109.5 . . ?
H22B C228 H22C 109.5 . . ?
P1 Co1 Se8 103.7(3) . . ?
P1 Co1 Se6 107.6(4) . . ?
Se8 Co1 Se6 88.0(2) . . ?
P1 Co1 Se2 93.4(3) . . ?
Se8 Co1 Se2 86.9(2) . . ?
Se6 Co1 Se2 159.0(2) . . ?
P1 Co1 Se1 97.2(3) . . ?
Se8 Co1 Se1 159.1(3) . . ?
Se6 Co1 Se1 86.5(2) . . ?
Se2 Co1 Se1 91.0(2) . . ?
P1 Co1 Co2 126.7(3) . . ?
Se8 Co1 Co2 112.0(2) . . ?
Se6 Co1 Co2 111.7(2) . . ?
Se2 Co1 Co2 52.27(17) . . ?
Se1 Co1 Co2 52.31(16) . . ?
P1 Co1 Co5 141.1(3) . . ?
Se8 Co1 Co5 51.25(16) . . ?
Se6 Co1 Co5 50.78(16) . . ?
Se2 Co1 Co5 111.6(2) . . ?
Se1 Co1 Co5 111.1(2) . . ?
Co2 Co1 Co5 92.15(18) . . ?
P1 Co1 Co6 138.6(3) . . ?
Se8 Co1 Co6 109.7(2) . . ?
Se6 Co1 Co6 51.38(17) . . ?
Se2 Co1 Co6 111.9(2) . . ?
Se1 Co1 Co6 52.19(16) . . ?
Co2 Co1 Co6 60.51(17) . . ?
Co5 Co1 Co6 59.01(16) . . ?
P1 Co1 Co3 131.8(4) . . ?
Se8 Co1 Co3 51.46(15) . . ?
Se6 Co1 Co3 111.1(2) . . ?
Se2 Co1 Co3 51.01(15) . . ?
Se1 Co1 Co3 112.5(2) . . ?
Co2 Co1 Co3 60.84(15) . . ?
Co5 Co1 Co3 60.83(16) . . ?
Co6 Co1 Co3 88.82(18) . . ?
P2 Co2 Se3 111.2(3) . . ?
P2 Co2 Se2 100.6(3) . . ?
Se3 Co2 Se2 85.7(2) . . ?
P2 Co2 Se1 89.5(3) . . ?
Se3 Co2 Se1 159.3(3) . . ?
Se2 Co2 Se1 91.6(2) . . ?
P2 Co2 Se7 102.7(3) . . ?
Se3 Co2 Se7 86.1(2) . . ?
Se2 Co2 Se7 156.7(2) . . ?
Se1 Co2 Se7 88.4(2) . . ?
P2 Co2 Co1 126.5(3) . . ?
Se3 Co2 Co1 111.2(2) . . ?
Se2 Co2 Co1 52.49(17) . . ?
Se1 Co2 Co1 52.86(16) . . ?
Se7 Co2 Co1 111.3(2) . . ?
P2 Co2 Co6 128.3(4) . . ?
Se3 Co2 Co6 109.8(2) . . ?
Se2 Co2 Co6 112.6(2) . . ?
Se1 Co2 Co6 52.54(16) . . ?
Se7 Co2 Co6 50.71(16) . . ?
Co1 Co2 Co6 61.07(18) . . ?
P2 Co2 Co3 141.9(4) . . ?
Se3 Co2 Co3 50.53(15) . . ?
Se2 Co2 Co3 51.09(15) . . ?
Se1 Co2 Co3 113.1(2) . . ?
Se7 Co2 Co3 107.9(2) . . ?
Co1 Co2 Co3 60.93(16) . . ?
Co6 Co2 Co3 89.18(19) . . ?
P2 Co2 Co4 142.8(3) . . ?
Se3 Co2 Co4 50.40(16) . . ?
Se2 Co2 Co4 108.5(2) . . ?
Se1 Co2 Co4 111.9(2) . . ?
Se7 Co2 Co4 50.68(15) . . ?
Co1 Co2 Co4 90.13(18) . . ?
Co6 Co2 Co4 59.68(16) . . ?
Co3 Co2 Co4 57.59(15) . . ?
P3 Co3 Se3 93.1(3) . . ?
P3 Co3 Se2 112.7(3) . . ?
Se3 Co3 Se2 86.15(19) . . ?
P3 Co3 Se8 109.7(3) . . ?
Se3 Co3 Se8 157.2(3) . . ?
Se2 Co3 Se8 86.46(19) . . ?
P3 Co3 Se4 87.8(3) . . ?
Se3 Co3 Se4 92.9(2) . . ?
Se2 Co3 Se4 159.5(3) . . ?
Se8 Co3 Se4 86.59(19) . . ?
P3 Co3 Co4 119.2(3) . . ?
Se3 Co3 Co4 52.31(17) . . ?
Se2 Co3 Co4 112.4(2) . . ?
Se8 Co3 Co4 111.7(2) . . ?
Se4 Co3 Co4 53.26(16) . . ?
P3 Co3 Co2 136.9(3) . . ?
Se3 Co3 Co2 51.06(15) . . ?
Se2 Co3 Co2 51.10(15) . . ?
Se8 Co3 Co2 108.6(2) . . ?
Se4 Co3 Co2 113.7(2) . . ?
Co4 Co3 Co2 61.47(16) . . ?
P3 Co3 Co1 149.8(3) . . ?
Se3 Co3 Co1 109.1(2) . . ?
Se2 Co3 Co1 51.24(16) . . ?
Se8 Co3 Co1 50.68(15) . . ?
Se4 Co3 Co1 110.5(2) . . ?
Co4 Co3 Co1 90.8(2) . . ?
Co2 Co3 Co1 58.23(15) . . ?
P3 Co3 Co5 130.4(3) . . ?
Se3 Co3 Co5 113.0(2) . . ?
Se2 Co3 Co5 110.6(2) . . ?
Se8 Co3 Co5 50.51(16) . . ?
Se4 Co3 Co5 51.26(16) . . ?
Co4 Co3 Co5 61.63(17) . . ?
Co2 Co3 Co5 89.84(19) . . ?
Co1 Co3 Co5 59.53(16) . . ?
P4 Co4 Se3 94.4(3) . . ?
P4 Co4 Se7 98.0(3) . . ?
Se3 Co4 Se7 86.8(2) . . ?
P4 Co4 Se5 106.8(3) . . ?
Se3 Co4 Se5 158.5(2) . . ?
Se7 Co4 Se5 86.5(2) . . ?
P4 Co4 Se4 103.9(3) . . ?
Se3 Co4 Se4 92.6(2) . . ?
Se7 Co4 Se4 158.1(2) . . ?
Se5 Co4 Se4 86.2(2) . . ?
P4 Co4 Co3 131.4(3) . . ?
Se3 Co4 Co3 52.19(16) . . ?
Se7 Co4 Co3 111.8(2) . . ?
Se5 Co4 Co3 112.3(2) . . ?
Se4 Co4 Co3 52.99(16) . . ?
P4 Co4 Co6 136.7(3) . . ?
Se3 Co4 Co6 110.2(2) . . ?
Se7 Co4 Co6 50.79(16) . . ?
Se5 Co4 Co6 50.89(16) . . ?
Se4 Co4 Co6 109.7(2) . . ?
Co3 Co4 Co6 91.14(19) . . ?
P4 Co4 Co2 128.5(3) . . ?
Se3 Co4 Co2 50.81(16) . . ?
Se7 Co4 Co2 51.22(16) . . ?
Se5 Co4 Co2 110.2(2) . . ?
Se4 Co4 Co2 113.0(2) . . ?
Co3 Co4 Co2 60.95(16) . . ?
Co6 Co4 Co2 59.65(16) . . ?
P4 Co4 Co5 142.0(3) . . ?
Se3 Co4 Co5 112.7(2) . . ?
Se7 Co4 Co5 109.2(2) . . ?
Se5 Co4 Co5 51.13(17) . . ?
Se4 Co4 Co5 51.15(15) . . ?
Co3 Co4 Co5 61.48(17) . . ?
Co6 Co4 Co5 58.70(16) . . ?
Co2 Co4 Co5 89.48(18) . . ?
P5 Co5 Se6 93.0(3) . . ?
P5 Co5 Se8 99.4(3) . . ?
Se6 Co5 Se8 87.8(2) . . ?
P5 Co5 Se5 105.2(4) . . ?
Se6 Co5 Se5 90.5(2) . . ?
Se8 Co5 Se5 155.4(3) . . ?
P5 Co5 Se4 109.1(3) . . ?
Se6 Co5 Se4 157.8(3) . . ?
Se8 Co5 Se4 86.5(2) . . ?
Se5 Co5 Se4 85.8(2) . . ?
P5 Co5 Co6 130.9(4) . . ?
Se6 Co5 Co6 52.14(16) . . ?
Se8 Co5 Co6 110.7(2) . . ?
Se5 Co5 Co6 51.27(16) . . ?
Se4 Co5 Co6 110.5(2) . . ?
P5 Co5 Co1 127.5(3) . . ?
Se6 Co5 Co1 51.07(16) . . ?
Se8 Co5 Co1 50.78(15) . . ?
Se5 Co5 Co1 111.0(2) . . ?
Se4 Co5 Co1 110.2(2) . . ?
Co6 Co5 Co1 60.51(16) . . ?
P5 Co5 Co3 139.2(3) . . ?
Se6 Co5 Co3 110.2(2) . . ?
Se8 Co5 Co3 50.82(16) . . ?
Se5 Co5 Co3 107.5(2) . . ?
Se4 Co5 Co3 50.84(15) . . ?
Co6 Co5 Co3 88.99(19) . . ?
Co1 Co5 Co3 59.64(16) . . ?
P5 Co5 Co4 144.2(3) . . ?
Se6 Co5 Co4 111.0(2) . . ?
Se8 Co5 Co4 107.3(2) . . ?
Se5 Co5 Co4 50.80(17) . . ?
Se4 Co5 Co4 50.99(16) . . ?
Co6 Co5 Co4 59.68(16) . . ?
Co1 Co5 Co4 88.13(18) . . ?
Co3 Co5 Co4 56.90(16) . . ?
P6 Co6 Se7 107.4(4) . . ?
P6 Co6 Se5 89.7(3) . . ?
Se7 Co6 Se5 87.7(2) . . ?
P6 Co6 Se6 94.6(3) . . ?
Se7 Co6 Se6 158.0(3) . . ?
Se5 Co6 Se6 91.0(2) . . ?
P6 Co6 Se1 110.2(3) . . ?
Se7 Co6 Se1 88.2(2) . . ?
Se5 Co6 Se1 160.0(3) . . ?
Se6 Co6 Se1 85.6(2) . . ?
P6 Co6 Co5 121.6(3) . . ?
Se7 Co6 Co5 112.6(2) . . ?
Se5 Co6 Co5 52.68(16) . . ?
Se6 Co6 Co5 51.38(16) . . ?
Se1 Co6 Co5 111.8(2) . . ?
P6 Co6 Co2 146.6(4) . . ?
Se7 Co6 Co2 51.79(17) . . ?
Se5 Co6 Co2 112.3(2) . . ?
Se6 Co6 Co2 109.2(2) . . ?
Se1 Co6 Co2 51.21(16) . . ?
Co5 Co6 Co2 91.8(2) . . ?
P6 Co6 Co4 131.5(3) . . ?
Se7 Co6 Co4 51.33(15) . . ?
Se5 Co6 Co4 51.93(16) . . ?
Se6 Co6 Co4 112.1(2) . . ?
Se1 Co6 Co4 111.5(2) . . ?
Co5 Co6 Co4 61.62(16) . . ?
Co2 Co6 Co4 60.67(17) . . ?
P6 Co6 Co1 137.1(3) . . ?
Se7 Co6 Co1 109.7(2) . . ?
Se5 Co6 Co1 112.3(2) . . ?
Se6 Co6 Co1 50.93(17) . . ?
Se1 Co6 Co1 51.39(16) . . ?
Co5 Co6 Co1 60.47(16) . . ?
Co2 Co6 Co1 58.42(17) . . ?
Co4 Co6 Co1 89.2(2) . . ?
Co2 Se1 Co1 74.8(2) . . ?
Co2 Se1 Co6 76.3(2) . . ?
Co1 Se1 Co6 76.4(2) . . ?
Co2 Se1 Co13 90.5(2) . . ?
Co1 Se1 Co13 88.7(2) . . ?
Co6 Se1 Co13 162.1(2) . . ?
Co3 Se2 Co2 77.80(19) . . ?
Co3 Se2 Co1 77.75(19) . . ?
Co2 Se2 Co1 75.2(2) . . ?
Co3 Se3 Co4 75.5(2) . . ?
Co3 Se3 Co2 78.4(2) . . ?
Co4 Se3 Co2 78.8(2) . . ?
Co3 Se4 Co4 73.74(19) . . ?
Co3 Se4 Co5 77.90(19) . . ?
Co4 Se4 Co5 77.9(2) . . ?
Co3 Se4 Co14 97.2(2) . . ?
Co4 Se4 Co14 86.8(2) . . ?
Co5 Se4 Co14 164.6(2) . . ?
Co6 Se5 Co4 77.2(2) . . ?
Co6 Se5 Co5 76.0(2) . . ?
Co4 Se5 Co5 78.1(2) . . ?
Co6 Se5 Co15 92.3(2) . . ?
Co4 Se5 Co15 160.7(2) . . ?
Co5 Se5 Co15 83.7(2) . . ?
Co5 Se6 Co1 78.1(2) . . ?
Co5 Se6 Co6 76.5(2) . . ?
Co1 Se6 Co6 77.7(2) . . ?
Co6 Se7 Co4 77.9(2) . . ?
Co6 Se7 Co2 77.5(2) . . ?
Co4 Se7 Co2 78.1(2) . . ?
Co1 Se8 Co5 78.0(2) . . ?
Co1 Se8 Co3 77.86(19) . . ?
Co5 Se8 Co3 78.7(2) . . ?
P7 Co7 Se14 93.8(5) . . ?
P7 Co7 Se16 103.3(5) . . ?
Se14 Co7 Se16 85.6(2) . . ?
P7 Co7 Se10 107.7(5) . . ?
Se14 Co7 Se10 158.1(2) . . ?
Se16 Co7 Se10 85.6(2) . . ?
P7 Co7 Se9 98.6(4) . . ?
Se14 Co7 Se9 92.3(2) . . ?
Se16 Co7 Se9 158.1(3) . . ?
Se10 Co7 Se9 88.4(2) . . ?
P7 Co7 Co8 128.3(5) . . ?
Se14 Co7 Co8 52.60(18) . . ?
Se16 Co7 Co8 110.5(2) . . ?
Se10 Co7 Co8 112.8(2) . . ?
Se9 Co7 Co8 53.11(17) . . ?
P7 Co7 Co12 139.4(5) . . ?
Se14 Co7 Co12 113.1(2) . . ?
Se16 Co7 Co12 108.4(2) . . ?
Se10 Co7 Co12 51.68(17) . . ?
Se9 Co7 Co12 52.62(16) . . ?
Co8 Co7 Co12 61.48(18) . . ?
P7 Co7 Co9 130.8(5) . . ?
Se14 Co7 Co9 50.25(16) . . ?
Se16 Co7 Co9 50.37(16) . . ?
Se10 Co7 Co9 109.8(2) . . ?
Se9 Co7 Co9 113.0(2) . . ?
Co8 Co7 Co9 60.52(16) . . ?
Co12 Co7 Co9 89.41(18) . . ?
P7 Co7 Co11 140.9(5) . . ?
Se14 Co7 Co11 109.7(2) . . ?
Se16 Co7 Co11 50.53(15) . . ?
Se10 Co7 Co11 50.30(15) . . ?
Se9 Co7 Co11 110.7(2) . . ?
Co8 Co7 Co11 90.50(19) . . ?
Co12 Co7 Co11 58.28(15) . . ?
Co9 Co7 Co11 59.65(16) . . ?
P8 Co8 Se13 108.2(4) . . ?
P8 Co8 Se14 98.2(4) . . ?
Se13 Co8 Se14 85.9(2) . . ?
P8 Co8 Se15 105.2(4) . . ?
Se13 Co8 Se15 87.2(2) . . ?
Se14 Co8 Se15 156.6(3) . . ?
P8 Co8 Se9 90.9(3) . . ?
Se13 Co8 Se9 160.9(3) . . ?
Se14 Co8 Se9 91.7(2) . . ?
Se15 Co8 Se9 87.5(2) . . ?
P8 Co8 Co7 125.5(4) . . ?
Se13 Co8 Co7 112.7(2) . . ?
Se14 Co8 Co7 52.07(18) . . ?
Se15 Co8 Co7 111.2(3) . . ?
Se9 Co8 Co7 52.86(17) . . ?
P8 Co8 Co10 143.4(4) . . ?
Se13 Co8 Co10 51.57(16) . . ?
Se14 Co8 Co10 108.7(2) . . ?
Se15 Co8 Co10 50.84(16) . . ?
Se9 Co8 Co10 112.1(3) . . ?
Co7 Co8 Co10 90.9(2) . . ?
P8 Co8 Co9 138.2(4) . . ?
Se13 Co8 Co9 50.98(17) . . ?
Se14 Co8 Co9 50.77(16) . . ?
Se15 Co8 Co9 108.7(2) . . ?
Se9 Co8 Co9 114.0(3) . . ?
Co7 Co8 Co9 61.85(17) . . ?
Co10 Co8 Co9 58.21(17) . . ?
P8 Co8 Co12 131.1(4) . . ?
Se13 Co8 Co12 111.3(2) . . ?
Se14 Co8 Co12 112.0(3) . . ?
Se15 Co8 Co12 50.68(17) . . ?
Se9 Co8 Co12 52.32(17) . . ?
Co7 Co8 Co12 60.89(18) . . ?
Co10 Co8 Co12 59.99(17) . . ?
Co9 Co8 Co12 89.8(2) . . ?
P9 Co9 Se14 113.9(4) . . ?
P9 Co9 Se13 98.1(4) . . ?
Se14 Co9 Se13 86.2(2) . . ?
P9 Co9 Se16 105.4(4) . . ?
Se14 Co9 Se16 85.7(2) . . ?
Se13 Co9 Se16 156.4(3) . . ?
P9 Co9 Se12 86.4(4) . . ?
Se14 Co9 Se12 159.6(3) . . ?
Se13 Co9 Se12 92.3(2) . . ?
Se16 Co9 Se12 87.6(2) . . ?
P9 Co9 Co10 122.8(4) . . ?
Se14 Co9 Co10 111.7(2) . . ?
Se13 Co9 Co10 52.75(17) . . ?
Se16 Co9 Co10 110.6(2) . . ?
Se12 Co9 Co10 53.36(16) . . ?
P9 Co9 Co8 141.6(4) . . ?
Se14 Co9 Co8 51.20(17) . . ?
Se13 Co9 Co8 50.93(16) . . ?
Se16 Co9 Co8 107.8(2) . . ?
Se12 Co9 Co8 113.4(2) . . ?
Co10 Co9 Co8 60.75(17) . . ?
P9 Co9 Co11 127.2(4) . . ?
Se14 Co9 Co11 110.4(2) . . ?
Se13 Co9 Co11 112.2(2) . . ?
Se16 Co9 Co11 50.93(17) . . ?
Se12 Co9 Co11 51.65(16) . . ?
Co10 Co9 Co11 60.32(18) . . ?
Co8 Co9 Co11 89.3(2) . . ?
P9 Co9 Co7 146.6(4) . . ?
Se14 Co9 Co7 50.18(17) . . ?
Se13 Co9 Co7 108.4(2) . . ?
Se16 Co9 Co7 50.60(16) . . ?
Se12 Co9 Co7 111.8(2) . . ?
Co10 Co9 Co7 89.94(19) . . ?
Co8 Co9 Co7 57.62(16) . . ?
Co11 Co9 Co7 60.41(17) . . ?
P10 Co10 Se15 102.1(4) . . ?
P10 Co10 Se11 104.9(4) . . ?
Se15 Co10 Se11 86.9(2) . . ?
P10 Co10 Se13 96.2(4) . . ?
Se15 Co10 Se13 87.3(2) . . ?
Se11 Co10 Se13 158.8(3) . . ?
P10 Co10 Se12 98.7(3) . . ?
Se15 Co10 Se12 159.1(3) . . ?
Se11 Co10 Se12 87.0(2) . . ?
Se13 Co10 Se12 91.3(2) . . ?
P10 Co10 Co9 129.9(3) . . ?
Se15 Co10 Co9 112.2(2) . . ?
Se11 Co10 Co9 112.1(2) . . ?
Se13 Co10 Co9 52.17(18) . . ?
Se12 Co10 Co9 52.60(17) . . ?
P10 Co10 Co11 137.0(4) . . ?
Se15 Co10 Co11 109.7(2) . . ?
Se11 Co10 Co11 50.63(16) . . ?
Se13 Co10 Co11 113.1(2) . . ?
Se12 Co10 Co11 52.15(16) . . ?
Co9 Co10 Co11 61.76(18) . . ?
P10 Co10 Co8 132.6(4) . . ?
Se15 Co10 Co8 51.51(17) . . ?
Se11 Co10 Co8 110.8(2) . . ?
Se13 Co10 Co8 50.97(16) . . ?
Se12 Co10 Co8 113.0(2) . . ?
Co9 Co10 Co8 61.04(17) . . ?
Co11 Co10 Co8 90.21(19) . . ?
P10 Co10 Co12 138.2(3) . . ?
Se15 Co10 Co12 51.08(16) . . ?
Se11 Co10 Co12 50.56(16) . . ?
Se13 Co10 Co12 111.3(2) . . ?
Se12 Co10 Co12 110.9(2) . . ?
Co9 Co10 Co12 91.83(19) . . ?
Co11 Co10 Co12 58.99(16) . . ?
Co8 Co10 Co12 60.60(16) . . ?
P11 Co11 Se11 93.8(3) . . ?
P11 Co11 Se10 90.9(3) . . ?
Se11 Co11 Se10 91.5(2) . . ?
P11 Co11 Se16 110.1(3) . . ?
Se11 Co11 Se16 156.0(3) . . ?
Se10 Co11 Se16 85.58(19) . . ?
P11 Co11 Se12 110.2(3) . . ?
Se11 Co11 Se12 87.7(2) . . ?
Se10 Co11 Se12 158.9(3) . . ?
Se16 Co11 Se12 86.6(2) . . ?
P11 Co11 Co12 121.6(3) . . ?
Se11 Co11 Co12 51.61(15) . . ?
Se10 Co11 Co12 52.60(16) . . ?
Se16 Co11 Co12 110.0(2) . . ?
Se12 Co11 Co12 112.7(2) . . ?
P11 Co11 Co10 136.6(3) . . ?
Se11 Co11 Co10 51.65(17) . . ?
Se10 Co11 Co10 112.4(2) . . ?
Se16 Co11 Co10 107.8(2) . . ?
Se12 Co11 Co10 52.09(16) . . ?
Co12 Co11 Co10 60.86(16) . . ?
P11 Co11 Co9 147.7(3) . . ?
Se11 Co11 Co9 109.3(2) . . ?
Se10 Co11 Co9 110.2(2) . . ?
Se16 Co11 Co9 50.47(17) . . ?
Se12 Co11 Co9 50.88(16) . . ?
Co12 Co11 Co9 90.7(2) . . ?
Co10 Co11 Co9 57.92(17) . . ?
P11 Co11 Co7 132.6(3) . . ?
Se11 Co11 Co7 110.9(2) . . ?
Se10 Co11 Co7 50.45(16) . . ?
Se16 Co11 Co7 50.31(16) . . ?
Se12 Co11 Co7 110.6(2) . . ?
Co12 Co11 Co7 60.14(16) . . ?
Co10 Co11 Co7 88.3(2) . . ?
Co9 Co11 Co7 59.94(17) . . ?
P12 Co12 Se11 91.4(3) . . ?
P12 Co12 Se15 102.1(3) . . ?
Se11 Co12 Se15 87.1(2) . . ?
P12 Co12 Se10 102.1(3) . . ?
Se11 Co12 Se10 90.5(2) . . ?
Se15 Co12 Se10 155.8(3) . . ?
P12 Co12 Se9 110.0(3) . . ?
Se11 Co12 Se9 158.5(3) . . ?
Se15 Co12 Se9 86.7(2) . . ?
Se10 Co12 Se9 86.7(2) . . ?
P12 Co12 Co11 127.1(4) . . ?
Se11 Co12 Co11 51.30(16) . . ?
Se15 Co12 Co11 110.4(2) . . ?
Se10 Co12 Co11 51.69(15) . . ?
Se9 Co12 Co11 112.5(2) . . ?
P12 Co12 Co10 128.6(3) . . ?
Se11 Co12 Co10 51.27(16) . . ?
Se15 Co12 Co10 50.61(16) . . ?
Se10 Co12 Co10 110.8(2) . . ?
Se9 Co12 Co10 110.3(2) . . ?
Co11 Co12 Co10 60.15(16) . . ?
P12 Co12 Co7 142.2(3) . . ?
Se11 Co12 Co7 112.0(2) . . ?
Se15 Co12 Co7 108.1(2) . . ?
Se10 Co12 Co7 50.95(17) . . ?
Se9 Co12 Co7 51.13(16) . . ?
Co11 Co12 Co7 61.58(16) . . ?
Co10 Co12 Co7 88.71(18) . . ?
P12 Co12 Co8 142.0(3) . . ?
Se11 Co12 Co8 110.3(2) . . ?
Se15 Co12 Co8 50.87(17) . . ?
Se10 Co12 Co8 108.2(2) . . ?
Se9 Co12 Co8 51.08(16) . . ?
Co11 Co12 Co8 90.20(19) . . ?
Co10 Co12 Co8 59.42(16) . . ?
Co7 Co12 Co8 57.64(18) . . ?
Co7 Se9 Co8 74.0(2) . . ?
Co7 Se9 Co12 76.2(2) . . ?
Co8 Se9 Co12 76.6(2) . . ?
Co7 Se9 Co16 87.8(2) . . ?
Co8 Se9 Co16 90.5(2) . . ?
Co12 Se9 Co16 161.7(2) . . ?
Co11 Se10 Co7 79.3(2) . . ?
Co11 Se10 Co12 75.72(19) . . ?
Co7 Se10 Co12 77.4(2) . . ?
Co11 Se10 Co18 96.5(2) . . ?
Co7 Se10 Co18 167.1(3) . . ?
Co12 Se10 Co18 89.8(2) . . ?
Co11 Se11 Co12 77.1(2) . . ?
Co11 Se11 Co10 77.7(2) . . ?
Co12 Se11 Co10 78.2(2) . . ?
Co9 Se12 Co10 74.0(2) . . ?
Co9 Se12 Co11 77.5(2) . . ?
Co10 Se12 Co11 75.76(19) . . ?
Co9 Se12 Co17 95.1(2) . . ?
Co10 Se12 Co17 89.3(2) . . ?
Co11 Se12 Co17 164.6(2) . . ?
Co8 Se13 Co9 78.1(2) . . ?
Co8 Se13 Co10 77.5(2) . . ?
Co9 Se13 Co10 75.1(2) . . ?
Co7 Se14 Co9 79.6(2) . . ?
Co7 Se14 Co8 75.3(2) . . ?
Co9 Se14 Co8 78.0(2) . . ?
Co10 Se15 Co12 78.3(2) . . ?
Co10 Se15 Co8 77.6(2) . . ?
Co12 Se15 Co8 78.4(2) . . ?
Co9 Se16 Co7 79.0(2) . . ?
Co9 Se16 Co11 78.6(2) . . ?
Co7 Se16 Co11 79.2(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co13 N1 1.904(14) . ?
Co13 N2 1.931(14) . ?
Co13 N13 2.098(14) . ?
Co13 Se1 2.535(7) . ?
N13 C233 1.374(16) . ?
N13 C229 1.376(16) . ?
C229 C230 1.403(16) . ?
C229 H229 0.95 . ?
C230 C231 1.387(17) . ?
C230 H230 0.95 . ?
C231 C232 1.394(17) . ?
C231 C251 1.48(3) . ?
C232 C233 1.382(16) . ?
C232 H232 0.95 . ?
C233 H233 0.95 . ?
P1 N1 1.693(13) . ?
P1 C1 1.843(12) . ?
P1 C7 1.851(12) . ?
P1 Co1 2.134(10) . ?
N1 C13 1.470(14) . ?
C1 C2 1.39 . ?
C1 C6 1.39 . ?
C2 C3 1.39 . ?
C2 H2 0.95 . ?
C3 C4 1.39 . ?
C3 H3 0.95 . ?
C4 C5 1.39 . ?
C4 H4 0.95 . ?
C5 C6 1.39 . ?
C5 H5 0.95 . ?
C6 H6 0.95 . ?
C7 C8 1.39 . ?
C7 C12 1.39 . ?
C8 C9 1.39 . ?
C8 H8 0.95 . ?
C9 C10 1.39 . ?
C9 H9 0.95 . ?
C10 C11 1.39 . ?
C10 H10 0.95 . ?
C11 C12 1.39 . ?
C11 H11 0.95 . ?
C12 H12 0.95 . ?
C13 C14 1.39 . ?
C13 C18 1.39 . ?
C14 C15 1.39 . ?
C14 H14 0.95 . ?
C15 C16 1.39 . ?
C15 H15 0.95 . ?
C16 C17 1.39 . ?
C16 C19 1.537(16) . ?
C17 C18 1.39 . ?
C17 H17 0.95 . ?
C18 H18 0.95 . ?
C19 H19A 0.98 . ?
C19 H19B 0.98 . ?
C19 H19C 0.98 . ?
P2 N2 1.674(14) . ?
P2 C20 1.841(12) . ?
P2 C26 1.850(12) . ?
P2 Co2 2.158(10) . ?
N2 C32 1.477(14) . ?
C20 C21 1.39 . ?
C20 C25 1.39 . ?
C21 C22 1.39 . ?
C21 H21 0.95 . ?
C22 C23 1.39 . ?
C22 H22 0.95 . ?
C23 C24 1.39 . ?
C23 H23 0.95 . ?
C24 C25 1.39 . ?
C24 H24 0.95 . ?
C25 H25 0.95 . ?
C26 C27 1.39 . ?
C26 C31 1.39 . ?
C27 C28 1.39 . ?
C27 H27 0.95 . ?
C28 C29 1.39 . ?
C28 H28 0.95 . ?
C29 C30 1.39 . ?
C29 H29 0.95 . ?
C30 C31 1.39 . ?
C30 H30 0.95 . ?
C31 H31 0.95 . ?
C32 C33 1.39 . ?
C32 C37 1.39 . ?
C33 C34 1.39 . ?
C33 H33 0.95 . ?
C34 C35 1.39 . ?
C34 H34 0.95 . ?
C35 C36 1.39 . ?
C35 C38 1.542(16) . ?
C36 C37 1.39 . ?
C36 H36 0.95 . ?
C37 H37 0.95 . ?
C38 H38A 0.98 . ?
C38 H38B 0.98 . ?
C38 H38C 0.9801 . ?
Co14 N3 1.901(14) . ?
Co14 N4 1.943(14) . ?
Co14 N14 2.069(15) . ?
Co14 Se4 2.443(6) . ?
N14 C238 1.376(16) . ?
N14 C234 1.381(16) . ?
C234 C235 1.406(16) . ?
C234 H234 0.95 . ?
C235 C236 1.395(17) . ?
C235 H235 0.95 . ?
C236 C237 1.389(17) . ?
C236 C246 1.6(4) 1_645 ?
C237 C238 1.380(17) . ?
C237 H237 0.95 . ?
C238 H238 0.95 . ?
P3 N3 1.692(13) . ?
P3 C39 1.851(12) . ?
P3 C45 1.863(12) . ?
P3 Co3 2.179(11) . ?
N3 C51 1.472(14) . ?
C39 C40 1.39 . ?
C39 C44 1.39 . ?
C40 C41 1.39 . ?
C40 H40 0.95 . ?
C41 C42 1.39 . ?
C41 H41 0.95 . ?
C42 C43 1.39 . ?
C42 H42 0.95 . ?
C43 C44 1.39 . ?
C43 H43 0.95 . ?
C44 H44 0.95 . ?
C45 C46 1.39 . ?
C45 C50 1.39 . ?
C46 C47 1.39 . ?
C46 H46 0.95 . ?
C47 C48 1.39 . ?
C47 H47 0.95 . ?
C48 C49 1.39 . ?
C48 H48 0.95 . ?
C49 C50 1.39 . ?
C49 H49 0.95 . ?
C50 H50 0.95 . ?
C51 C52 1.39 . ?
C51 C56 1.39 . ?
C52 C53 1.39 . ?
C52 H52 0.95 . ?
C53 C54 1.39 . ?
C53 H53 0.95 . ?
C54 C55 1.39 . ?
C54 C57 1.552(16) . ?
C55 C56 1.39 . ?
C55 H55 0.95 . ?
C56 H56 0.95 . ?
C57 H57A 0.9801 . ?
C57 H57B 0.98 . ?
C57 H57C 0.98 . ?
P4 N4 1.686(13) . ?
P4 C64 1.826(11) . ?
P4 C58 1.851(12) . ?
P4 Co4 2.188(10) . ?
N4 C70 1.468(14) . ?
C58 C59 1.39 . ?
C58 C63 1.39 . ?
C59 C60 1.39 . ?
C59 H59 0.95 . ?
C60 C61 1.39 . ?
C60 H60 0.95 . ?
C61 C62 1.39 . ?
C61 H61 0.95 . ?
C62 C63 1.39 . ?
C62 H62 0.95 . ?
C63 H63 0.95 . ?
C64 C65 1.39 . ?
C64 C69 1.39 . ?
C65 C66 1.39 . ?
C65 H65 0.95 . ?
C66 C67 1.39 . ?
C66 H66 0.95 . ?
C67 C68 1.39 . ?
C67 H67 0.95 . ?
C68 C69 1.39 . ?
C68 H68 0.95 . ?
C69 H69 0.95 . ?
C70 C71 1.39 . ?
C70 C75 1.39 . ?
C71 C72 1.39 . ?
C71 H71 0.95 . ?
C72 C73 1.39 . ?
C72 H72 0.95 . ?
C73 C74 1.39 . ?
C73 C76 1.537(16) . ?
C74 C75 1.39 . ?
C74 H74 0.95 . ?
C75 H75 0.95 . ?
C76 H76A 0.98 . ?
C76 H76B 0.98 . ?
C76 H76C 0.98 . ?
Co15 N6 1.915(13) . ?
Co15 N5 1.921(14) . ?
Co15 N15 2.079(15) . ?
Co15 Se5 2.518(7) . ?
N15 C243 1.369(16) . ?
N15 C239 1.374(16) . ?
C239 C240 1.385(16) . ?
C239 H239 0.95 . ?
C240 C241 1.395(17) . ?
C240 H240 0.95 . ?
C241 C242 1.396(17) . ?
C241 C241 1.56(4) 2_847 ?
C242 C243 1.363(16) . ?
C242 H242 0.95 . ?
C243 H243 0.95 . ?
P5 N5 1.680(14) . ?
P5 C77 1.841(11) . ?
P5 C83 1.854(12) . ?
P5 Co5 2.191(11) . ?
N5 C89 1.466(14) . ?
C77 C78 1.39 . ?
C77 C82 1.39 . ?
C78 C79 1.39 . ?
C78 H78 0.95 . ?
C79 C80 1.39 . ?
C79 H79 0.95 . ?
C80 C81 1.39 . ?
C80 H80 0.95 . ?
C81 C82 1.39 . ?
C81 H81 0.95 . ?
C82 H82 0.95 . ?
C83 C84 1.39 . ?
C83 C88 1.39 . ?
C84 C85 1.39 . ?
C84 H84 0.95 . ?
C85 C86 1.39 . ?
C85 H85 0.95 . ?
C86 C87 1.39 . ?
C86 H86 0.95 . ?
C87 C88 1.39 . ?
C87 H87 0.95 . ?
C88 H88 0.95 . ?
C89 C90 1.39 . ?
C89 C94 1.39 . ?
C90 C91 1.39 . ?
C90 H90 0.95 . ?
C91 C92 1.39 . ?
C91 H91 0.95 . ?
C92 C93 1.39 . ?
C92 C95 1.549(17) . ?
C93 C94 1.39 . ?
C93 H93 0.95 . ?
C94 H94 0.95 . ?
C95 H95A 0.98 . ?
C95 H95B 0.98 . ?
C95 H95C 0.98 . ?
P6 N6 1.705(13) . ?
P6 C96 1.845(12) . ?
P6 C102 1.862(12) . ?
P6 Co6 2.107(13) . ?
N6 C108 1.467(14) . ?
C96 C97 1.39 . ?
C96 C101 1.39 . ?
C97 C98 1.39 . ?
C97 H97 0.95 . ?
C98 C99 1.39 . ?
C98 H98 0.95 . ?
C99 C100 1.39 . ?
C99 H99 0.95 . ?
C100 C101 1.39 . ?
C100 H100 0.95 . ?
C101 H101 0.95 . ?
C102 C103 1.39 . ?
C102 C107 1.39 . ?
C103 C104 1.39 . ?
C103 H103 0.95 . ?
C104 C105 1.39 . ?
C104 H104 0.95 . ?
C105 C106 1.39 . ?
C105 H105 0.95 . ?
C106 C107 1.39 . ?
C106 H106 0.95 . ?
C107 H107 0.95 . ?
C108 C109 1.39 . ?
C108 C113 1.39 . ?
C109 C110 1.39 . ?
C109 H109 0.95 . ?
C110 C111 1.39 . ?
C110 H110 0.95 . ?
C111 C112 1.39 . ?
C111 C114 1.542(17) . ?
C112 C113 1.39 . ?
C112 H112 0.95 . ?
C113 H113 0.95 . ?
C114 H11A 0.98 . ?
C114 H11B 0.98 . ?
C114 H11C 0.98 . ?
Co16 N8 1.919(15) . ?
Co16 N7 1.922(15) . ?
Co16 N16 2.096(13) . ?
Co16 Se9 2.515(7) . ?
N16 C244 1.39 . ?
N16 C248 1.39 . ?
C244 C245 1.39 . ?
C244 H244 0.95 . ?
C245 C246 1.39 . ?
C245 H245 0.95 . ?
C246 C247 1.39 . ?
C246 C236 1.56(3) 1_465 ?
C247 C248 1.39 . ?
C247 H247 0.95 . ?
C248 H248 0.95 . ?
P7 N7 1.686(14) . ?
P7 C121 1.834(13) . ?
P7 C115 1.849(13) . ?
P7 Co7 2.094(16) . ?
N7 C127 1.462(15) . ?
C115 C116 1.39 . ?
C115 C120 1.39 . ?
C116 C117 1.39 . ?
C116 H116 0.95 . ?
C117 C118 1.39 . ?
C117 H117 0.95 . ?
C118 C119 1.39 . ?
C118 H118 0.95 . ?
C119 C120 1.39 . ?
C119 H119 0.95 . ?
C120 H120 0.95 . ?
C121 C122 1.39 . ?
C121 C126 1.39 . ?
C122 C123 1.39 . ?
C122 H122 0.95 . ?
C123 C124 1.39 . ?
C123 H123 0.95 . ?
C124 C125 1.39 . ?
C124 H124 0.95 . ?
C125 C126 1.39 . ?
C125 H125 0.95 . ?
C126 H126 0.95 . ?
C127 C128 1.39 . ?
C127 C132 1.39 . ?
C128 C129 1.39 . ?
C128 H128 0.95 . ?
C129 C130 1.39 . ?
C129 H129 0.95 . ?
C130 C131 1.39 . ?
C130 C133 1.532(14) . ?
C131 C132 1.39 . ?
C131 H131 0.95 . ?
C132 H132 0.95 . ?
C133 H13A 0.98 . ?
C133 H13B 0.98 . ?
C133 H13C 0.98 . ?
P8 N8 1.683(14) . ?
P8 C140 1.847(12) . ?
P8 C134 1.850(12) . ?
P8 Co8 2.185(13) . ?
N8 C146 1.464(15) . ?
C134 C135 1.39 . ?
C134 C139 1.39 . ?
C135 C136 1.39 . ?
C135 H135 0.95 . ?
C136 C137 1.39 . ?
C136 H136 0.95 . ?
C137 C138 1.39 . ?
C137 H137 0.95 . ?
C138 C139 1.39 . ?
C138 H138 0.95 . ?
C139 H139 0.95 . ?
C140 C141 1.39 . ?
C140 C145 1.39 . ?
C141 C142 1.39 . ?
C141 H141 0.95 . ?
C142 C143 1.39 . ?
C142 H142 0.95 . ?
C143 C144 1.39 . ?
C143 H143 0.95 . ?
C144 C145 1.39 . ?
C144 H144 0.95 . ?
C145 H145 0.95 . ?
C146 C147 1.39 . ?
C146 C151 1.39 . ?
C147 C148 1.39 . ?
C147 H147 0.95 . ?
C148 C149 1.39 . ?
C148 H148 0.95 . ?
C149 C150 1.39 . ?
C149 C152 1.534(17) . ?
C150 C151 1.39 . ?
C150 H150 0.95 . ?
C151 H151 0.95 . ?
C152 H15A 0.9799 . ?
C152 H15B 0.98 . ?
C152 H15C 0.98 . ?
Co17 N9 1.900(15) . ?
Co17 N10 1.928(14) . ?
Co17 N17 2.084(14) . ?
Co17 Se12 2.505(7) . ?
N17 C253 1.371(16) . ?
N17 C249 1.384(16) . ?
C249 C250 1.396(16) . ?
C249 H249 0.95 . ?
C250 C251 1.380(17) . ?
C250 H250 0.95 . ?
C251 C252 1.399(17) . ?
C252 C253 1.371(17) . ?
C252 H252 0.95 . ?
C253 H253 0.95 . ?
P9 N9 1.679(14) . ?
P9 C153 1.843(12) . ?
P9 C159 1.858(12) . ?
P9 Co9 2.181(12) . ?
N9 C165 1.464(15) . ?
C153 C154 1.39 . ?
C153 C158 1.39 . ?
C154 C155 1.39 . ?
C154 H154 0.95 . ?
C155 C156 1.39 . ?
C155 H155 0.95 . ?
C156 C157 1.39 . ?
C156 H156 0.95 . ?
C157 C158 1.39 . ?
C157 H157 0.95 . ?
C158 H158 0.95 . ?
C159 C160 1.39 . ?
C159 C164 1.39 . ?
C160 C161 1.39 . ?
C160 H160 0.95 . ?
C161 C162 1.39 . ?
C161 H161 0.95 . ?
C162 C163 1.39 . ?
C162 H162 0.95 . ?
C163 C164 1.39 . ?
C163 H163 0.95 . ?
C164 H164 0.95 . ?
C165 C166 1.39 . ?
C165 C170 1.39 . ?
C166 C167 1.39 . ?
C166 H166 0.95 . ?
C167 C168 1.39 . ?
C167 H167 0.95 . ?
C168 C169 1.39 . ?
C168 C171 1.537(17) . ?
C169 C170 1.39 . ?
C169 H169 0.95 . ?
C170 H170 0.95 . ?
C171 H17A 0.98 . ?
C171 H17B 0.98 . ?
C171 H17C 0.98 . ?
P10 N10 1.702(13) . ?
P10 C172 1.836(12) . ?
P10 C178 1.846(12) . ?
P10 Co10 2.160(10) . ?
N10 C184 1.471(14) . ?
C172 C173 1.39 . ?
C172 C177 1.39 . ?
C173 C174 1.39 . ?
C173 H173 0.95 . ?
C174 C175 1.39 . ?
C174 H174 0.95 . ?
C175 C176 1.39 . ?
C175 H175 0.95 . ?
C176 C177 1.39 . ?
C176 H176 0.95 . ?
C177 H177 0.95 . ?
C178 C179 1.39 . ?
C178 C183 1.39 . ?
C179 C180 1.39 . ?
C179 H179 0.95 . ?
C180 C181 1.39 . ?
C180 H180 0.95 . ?
C181 C182 1.39 . ?
C181 H181 0.95 . ?
C182 C183 1.39 . ?
C182 H182 0.95 . ?
C183 H183 0.95 . ?
C184 C185 1.39 . ?
C184 C189 1.39 . ?
C185 C186 1.39 . ?
C185 H185 0.95 . ?
C186 C187 1.39 . ?
C186 H186 0.95 . ?
C187 C188 1.39 . ?
C187 C190 1.547(17) . ?
C188 C189 1.39 . ?
C188 H188 0.95 . ?
C189 H189 0.95 . ?
C190 H19D 0.98 . ?
C190 H19E 0.98 . ?
C190 H19F 0.98 . ?
Co18 N11 1.907(14) . ?
Co18 N12 1.936(14) . ?
Co18 N18 2.056(14) . ?
Co18 Se10 2.456(7) . ?
N18 C258 1.377(16) . ?
N18 C254 1.388(16) . ?
C254 C255 1.408(16) . ?
C254 H254 0.95 . ?
C255 C256 1.381(17) . ?
C255 H255 0.95 . ?
C256 C257 1.389(17) . ?
C256 C256 1.52(5) 2_656 ?
C257 C258 1.372(17) . ?
C257 H257 0.95 . ?
C258 H258 0.95 . ?
P11 N11 1.680(14) . ?
P11 C191 1.854(12) . ?
P11 C197 1.868(11) . ?
P11 Co11 2.168(12) . ?
N11 C203 1.467(14) . ?
C191 C192 1.39 . ?
C191 C196 1.39 . ?
C192 C193 1.39 . ?
C192 H192 0.95 . ?
C193 C194 1.39 . ?
C193 H193 0.95 . ?
C194 C195 1.39 . ?
C194 H194 0.95 . ?
C195 C196 1.39 . ?
C195 H195 0.95 . ?
C196 H196 0.95 . ?
C197 C198 1.39 . ?
C197 C202 1.39 . ?
C198 C199 1.39 . ?
C198 H198 0.95 . ?
C199 C200 1.39 . ?
C199 H199 0.95 . ?
C200 C201 1.39 . ?
C200 H200 0.95 . ?
C201 C202 1.39 . ?
C201 H201 0.95 . ?
C202 H202 0.95 . ?
C203 C204 1.39 . ?
C203 C208 1.39 . ?
C204 C205 1.39 . ?
C204 H204 0.95 . ?
C205 C206 1.39 . ?
C205 H205 0.95 . ?
C206 C207 1.39 . ?
C206 C209 1.539(16) . ?
C207 C208 1.39 . ?
C207 H207 0.95 . ?
C208 H208 0.95 . ?
C209 H20A 0.98 . ?
C209 H20B 0.98 . ?
C209 H20C 0.98 . ?
P12 N12 1.680(14) . ?
P12 C216 1.845(12) . ?
P12 C210 1.851(12) . ?
P12 Co12 2.163(11) . ?
N12 C222 1.464(14) . ?
C210 C211 1.39 . ?
C210 C215 1.39 . ?
C211 C212 1.39 . ?
C211 H211 0.95 . ?
C212 C213 1.39 . ?
C212 H212 0.95 . ?
C213 C214 1.39 . ?
C213 H213 0.95 . ?
C214 C215 1.39 . ?
C214 H214 0.95 . ?
C215 H215 0.95 . ?
C216 C217 1.39 . ?
C216 C221 1.39 . ?
C217 C218 1.39 . ?
C217 H217 0.95 . ?
C218 C219 1.39 . ?
C218 H218 0.95 . ?
C219 C220 1.39 . ?
C219 H219 0.95 . ?
C220 C221 1.39 . ?
C220 H220 0.95 . ?
C221 H221 0.95 . ?
C222 C223 1.39 . ?
C222 C227 1.39 . ?
C223 C224 1.39 . ?
C223 H223 0.95 . ?
C224 C225 1.39 . ?
C224 H224 0.95 . ?
C225 C226 1.39 . ?
C225 C228 1.538(16) . ?
C226 C227 1.39 . ?
C226 H226 0.95 . ?
C227 H227 0.95 . ?
C228 H22A 0.98 . ?
C228 H22B 0.98 . ?
C228 H22C 0.98 . ?
Co1 Se8 2.329(5) . ?
Co1 Se6 2.337(7) . ?
Co1 Se2 2.349(6) . ?
Co1 Se1 2.365(6) . ?
Co1 Co2 2.863(7) . ?
Co1 Co5 2.940(6) . ?
Co1 Co6 2.941(7) . ?
Co1 Co3 2.944(6) . ?
Co2 Se3 2.335(6) . ?
Co2 Se2 2.342(6) . ?
Co2 Se1 2.347(6) . ?
Co2 Se7 2.355(6) . ?
Co2 Co6 2.925(8) . ?
Co2 Co3 2.941(6) . ?
Co2 Co4 2.955(6) . ?
Co3 Se3 2.318(6) . ?
Co3 Se2 2.341(5) . ?
Co3 Se8 2.355(6) . ?
Co3 Se4 2.362(6) . ?
Co3 Co4 2.840(7) . ?
Co3 Co5 2.979(7) . ?
Co4 Se3 2.321(7) . ?
Co4 Se7 2.337(6) . ?
Co4 Se5 2.363(7) . ?
Co4 Se4 2.371(6) . ?
Co4 Co6 2.926(7) . ?
Co4 Co5 2.983(7) . ?
Co5 Se6 2.328(5) . ?
Co5 Se8 2.345(6) . ?
Co5 Se5 2.374(6) . ?
Co5 Se4 2.376(6) . ?
Co5 Co6 2.897(7) . ?
Co6 Se7 2.319(6) . ?
Co6 Se5 2.329(6) . ?
Co6 Se6 2.352(6) . ?
Co6 Se1 2.391(6) . ?
Co7 Se14 2.318(7) . ?
Co7 Se16 2.336(6) . ?
Co7 Se10 2.340(7) . ?
Co7 Se9 2.357(6) . ?
Co7 Co8 2.843(8) . ?
Co7 Co12 2.940(7) . ?
Co7 Co9 2.968(6) . ?
Co7 Co11 2.982(7) . ?
Co8 Se13 2.325(5) . ?
Co8 Se14 2.335(7) . ?
Co8 Se15 2.341(7) . ?
Co8 Se9 2.365(6) . ?
Co8 Co10 2.922(7) . ?
Co8 Co9 2.930(7) . ?
Co8 Co12 2.957(8) . ?
Co9 Se14 2.320(6) . ?
Co9 Se13 2.327(7) . ?
Co9 Se16 2.329(7) . ?
Co9 Se12 2.352(6) . ?
Co9 Co10 2.847(7) . ?
Co9 Co11 2.960(8) . ?
Co10 Se15 2.319(5) . ?
Co10 Se11 2.343(7) . ?
Co10 Se13 2.345(7) . ?
Co10 Se12 2.376(6) . ?
Co10 Co11 2.919(7) . ?
Co10 Co12 2.939(6) . ?
Co11 Se11 2.309(6) . ?
Co11 Se10 2.335(5) . ?
Co11 Se16 2.344(6) . ?
Co11 Se12 2.378(6) . ?
Co11 Co12 2.884(6) . ?
Co12 Se11 2.319(5) . ?
Co12 Se15 2.335(6) . ?
Co12 Se10 2.364(6) . ?
Co12 Se9 2.406(6) . ?
