#------------------------------------------------------------------------------
#$Date: 2021-07-05 19:46:20 +0300 (Mon, 05 Jul 2021) $
#$Revision: 267058 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/55/96/1559665.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1559665
loop_
_publ_author_name
'Zhang, Jian'
'Xie, Zuowei'
_publ_section_title
;
 Tri-insertion with dearomatization of terminal arylalkynes using a
 carborane based frustrated Lewis pair template.
;
_journal_issue                   5
_journal_name_full               'Chemical science'
_journal_page_first              1745
_journal_page_last               1749
_journal_paper_doi               10.1039/d0sc05755j
_journal_volume                  12
_journal_year                    2020
_chemical_formula_sum            'C26 H30 B11 P'
_chemical_formula_weight         492.38
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2020-09-02 deposited with the CCDC.	2020-11-27 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 92.648(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.029(2)
_cell_length_b                   9.9593(19)
_cell_length_c                   20.562(3)
_cell_measurement_reflns_used    78
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      15
_cell_measurement_theta_min      15
_cell_volume                     2869.8(8)
_computing_cell_refinement       'BRUKER KAPPA APEXII DUO DIFFRACTOMETER'
_computing_data_collection       'BRUKER KAPPA APEXII DUO DIFFRACTOMETER'
_computing_data_reduction        'BRUKER KAPPA APEXII DUO DIFFRACTOMETER'
_computing_molecular_graphics    'SIEMENS SHELXTL'
_computing_publication_material  'SIEMENS SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'BRUKER KAPPA APEXII DUO DIFFRACTOMETER'
_diffrn_measurement_method       'PHI & OMEGA SCAN'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1232
_diffrn_reflns_av_sigmaI/netI    0.1054
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            22921
_diffrn_reflns_theta_full        25.25
_diffrn_reflns_theta_max         25.25
_diffrn_reflns_theta_min         1.45
_exptl_absorpt_coefficient_mu    0.112
_exptl_absorpt_correction_T_max  0.7217
_exptl_absorpt_correction_T_min  0.5495
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.140
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1024
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.30
_refine_diff_density_max         0.393
_refine_diff_density_min         -0.388
_refine_diff_density_rms         0.059
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     343
_refine_ls_number_reflns         5203
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.021
_refine_ls_R_factor_all          0.1142
_refine_ls_R_factor_gt           0.0636
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0950P)²+0.0362P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1547
_refine_ls_wR_factor_ref         0.1891
_reflns_number_gt                3173
_reflns_number_total             5203
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            d0sc05755j2.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Monoclinic' was changed to
'monoclinic' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 

 Adding full bibliography for 1559665--1559672.cif.

 Adding full bibliography for 1559665--1559672.cif.
;
_cod_original_cell_volume        2869.9(9)
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               1559665
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.69791(6) 0.79182(7) 0.10324(4) 0.0354(2) Uani 1 1 d . . .
C1 C 0.7679(2) 0.7949(3) 0.18117(14) 0.0329(7) Uani 1 1 d . . .
C2 C 0.79181(19) 0.9594(3) 0.17753(14) 0.0331(7) Uani 1 1 d . . .
C11 C 0.5802(2) 0.7192(3) 0.10800(15) 0.0381(7) Uani 1 1 d . . .
C12 C 0.5333(2) 0.6934(3) 0.04862(18) 0.0529(9) Uani 1 1 d . . .
H12A H 0.5653 0.7054 0.0104 0.063 Uiso 1 1 calc R . .
C13 C 0.4398(3) 0.6503(4) 0.0452(2) 0.0645(10) Uani 1 1 d . . .
H13A H 0.4093 0.6330 0.0049 0.077 Uiso 1 1 calc R . .
C14 C 0.3916(3) 0.6328(4) 0.1017(2) 0.0671(12) Uani 1 1 d . . .
H14A H 0.3283 0.6048 0.0995 0.081 Uiso 1 1 calc R . .
C15 C 0.4372(3) 0.6568(3) 0.1609(2) 0.0614(10) Uani 1 1 d . . .
H15A H 0.4048 0.6436 0.1988 0.074 Uiso 1 1 calc R . .
C16 C 0.5311(2) 0.7003(3) 0.16505(17) 0.0480(8) Uani 1 1 d . . .
H16A H 0.5613 0.7169 0.2055 0.058 Uiso 1 1 calc R . .
C17 C 0.7599(2) 0.6757(3) 0.05219(15) 0.0379(7) Uani 1 1 d . . .
C18 C 0.8200(2) 0.7182(3) 0.00436(15) 0.0405(7) Uani 1 1 d . . .
H18A H 0.8243 0.8089 -0.0057 0.049 Uiso 1 1 calc R . .
C19 C 0.8733(2) 0.6250(3) -0.02813(16) 0.0480(8) Uani 1 1 d . . .
H19A H 0.9140 0.6541 -0.0596 0.058 Uiso 1 1 calc R . .
C20 C 0.8671(2) 0.4908(3) -0.01475(17) 0.0517(9) Uani 1 1 d . . .
H20A H 0.9041 0.4294 -0.0366 0.062 Uiso 1 1 calc R . .
C21 C 0.8061(3) 0.4475(3) 0.03110(18) 0.0595(10) Uani 1 1 d . . .
H21A H 0.8004 0.3562 0.0397 0.071 Uiso 1 1 calc R . .
C22 C 0.7530(3) 0.5388(3) 0.06445(17) 0.0539(9) Uani 1 1 d . . .
H22A H 0.7121 0.5084 0.0956 0.065 Uiso 1 1 calc R . .
C23 C 0.7808(2) 1.0487(3) 0.04451(15) 0.0369(7) Uani 1 1 d . . .
C24 C 0.7263(2) 1.0549(3) -0.01404(17) 0.0523(9) Uani 1 1 d . . .
H24A H 0.6617 1.0337 -0.0139 0.063 Uiso 1 1 calc R . .
C25 C 0.7650(3) 1.0915(4) -0.07221(18) 0.0634(10) Uani 1 1 d . . .
H25A H 0.7265 1.0938 -0.1103 0.076 Uiso 1 1 calc R . .
C26 C 0.8597(3) 1.1242(3) -0.0740(2) 0.0615(11) Uani 1 1 d . . .
H26A H 0.8862 1.1468 -0.1132 0.074 Uiso 1 1 calc R . .
C27 C 0.9154(3) 1.1232(3) -0.01658(19) 0.0564(10) Uani 1 1 d . . .
H27A H 0.9793 1.1480 -0.0167 0.068 Uiso 1 1 calc R . .
C28 C 0.8757(2) 1.0854(3) 0.04108(17) 0.0439(8) Uani 1 1 d . . .
H28A H 0.9144 1.0846 0.0791 0.053 Uiso 1 1 calc R . .
C29 C 0.6368(2) 1.0944(3) 0.12203(15) 0.0396(7) Uani 1 1 d . . .
C30 C 0.5418(2) 1.0654(3) 0.10787(17) 0.0519(9) Uani 1 1 d . . .
H30A H 0.5258 0.9827 0.0895 0.062 Uiso 1 1 calc R . .
C31 C 0.4693(3) 1.1558(4) 0.12022(19) 0.0637(10) Uani 1 1 d . . .
H31A H 0.4062 1.1327 0.1099 0.076 Uiso 1 1 calc R . .
C32 C 0.4899(3) 1.2783(4) 0.14743(19) 0.0619(11) Uani 1 1 d . . .
H32A H 0.4411 1.3379 0.1563 0.074 Uiso 1 1 calc R . .
C33 C 0.5831(3) 1.3120(3) 0.16142(19) 0.0621(11) Uani 1 1 d . . .
H33A H 0.5979 1.3956 0.1793 0.075 Uiso 1 1 calc R . .
C34 C 0.6561(2) 1.2220(3) 0.14910(17) 0.0510(9) Uani 1 1 d . . .
H34A H 0.7190 1.2468 0.1590 0.061 Uiso 1 1 calc R . .
B3 B 0.7139(2) 0.9004(3) 0.23438(17) 0.0358(8) Uani 1 1 d . . .
H3 H 0.6372 0.9243 0.2326 0.043 Uiso 1 1 calc R . .
B4 B 0.7575(3) 0.7371(4) 0.25914(17) 0.0415(9) Uani 1 1 d . . .
H4 H 0.7098 0.6557 0.2735 0.050 Uiso 1 1 calc R . .
B5 B 0.8613(2) 0.7028(4) 0.21498(18) 0.0416(9) Uani 1 1 d . . .
H5 H 0.8799 0.5998 0.2010 0.050 Uiso 1 1 calc R . .
B6 B 0.8815(2) 0.8443(3) 0.16338(18) 0.0366(8) Uani 1 1 d . . .
H6 H 0.9132 0.8319 0.1158 0.044 Uiso 1 1 calc R . .
B7 B 0.8003(3) 1.0237(4) 0.25577(18) 0.0427(9) Uani 1 1 d . . .
H7 H 0.7803 1.1269 0.2685 0.051 Uiso 1 1 calc R . .
B8 B 0.7805(3) 0.8827(4) 0.30799(19) 0.0458(9) Uani 1 1 d . . .
H8 H 0.7478 0.8950 0.3552 0.055 Uiso 1 1 calc R . .
B9 B 0.8724(3) 0.7622(4) 0.29673(19) 0.0488(10) Uani 1 1 d . . .
H9 H 0.8996 0.6975 0.3368 0.059 Uiso 1 1 calc R . .
B10 B 0.9491(3) 0.8270(4) 0.23693(19) 0.0476(10) Uani 1 1 d . . .
H10 H 1.0258 0.8034 0.2380 0.057 Uiso 1 1 calc R . .
B11 B 0.9041(2) 0.9891(4) 0.21197(18) 0.0418(9) Uani 1 1 d . . .
H11 H 0.9510 1.0705 0.1966 0.050 Uiso 1 1 calc R . .
B12 B 0.8989(3) 0.9382(4) 0.2942(2) 0.0506(10) Uani 1 1 d . . .
H12 H 0.9436 0.9867 0.3328 0.061 Uiso 1 1 calc R . .
B13 B 0.7281(2) 0.9996(3) 0.10816(16) 0.0330(8) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11 P1 C17 103.90(13) . . ?
C11 P1 C1 114.26(14) . . ?
C17 P1 C1 105.34(13) . . ?
C11 P1 B13 124.73(13) . . ?
C17 P1 B13 123.53(13) . . ?
C1 P1 B13 81.05(12) . . ?
C2 C1 B4 113.3(2) . . ?
C2 C1 B3 61.67(17) . . ?
B4 C1 B3 63.35(19) . . ?
C2 C1 B5 112.9(2) . . ?
B4 C1 B5 62.56(19) . . ?
B3 C1 B5 114.8(2) . . ?
C2 C1 B6 61.43(16) . . ?
B4 C1 B6 114.4(2) . . ?
B3 C1 B6 113.6(2) . . ?
B5 C1 B6 62.82(19) . . ?
C2 C1 P1 94.45(16) . . ?
B4 C1 P1 138.0(2) . . ?
B3 C1 P1 109.37(19) . . ?
B5 C1 P1 135.1(2) . . ?
B6 C1 P1 106.33(19) . . ?
C1 C2 B13 99.7(2) . . ?
C1 C2 B11 109.4(2) . . ?
B13 C2 B11 137.9(2) . . ?
C1 C2 B7 109.0(2) . . ?
B13 C2 B7 134.8(2) . . ?
B11 C2 B7 62.09(19) . . ?
C1 C2 B6 60.68(17) . . ?
B13 C2 B6 111.9(2) . . ?
B11 C2 B6 61.74(19) . . ?
B7 C2 B6 112.4(2) . . ?
C1 C2 B3 60.40(16) . . ?
B13 C2 B3 108.7(2) . . ?
B11 C2 B3 111.9(2) . . ?
B7 C2 B3 61.23(19) . . ?
B6 C2 B3 111.9(2) . . ?
C12 C11 C16 118.8(3) . . ?
C12 C11 P1 115.1(2) . . ?
C16 C11 P1 125.8(2) . . ?
C13 C12 C11 121.1(3) . . ?
C12 C13 C14 119.8(4) . . ?
C15 C14 C13 119.9(3) . . ?
C14 C15 C16 120.9(4) . . ?
C15 C16 C11 119.5(3) . . ?
C18 C17 C22 118.4(3) . . ?
C18 C17 P1 122.6(2) . . ?
C22 C17 P1 118.8(2) . . ?
C19 C18 C17 119.8(3) . . ?
C20 C19 C18 121.2(3) . . ?
C19 C20 C21 119.5(3) . . ?
C20 C21 C22 120.2(3) . . ?
C21 C22 C17 120.9(3) . . ?
C28 C23 C24 115.7(3) . . ?
C28 C23 B13 126.9(3) . . ?
C24 C23 B13 117.4(3) . . ?
C25 C24 C23 122.3(3) . . ?
C26 C25 C24 120.4(4) . . ?
C25 C26 C27 119.0(3) . . ?
C28 C27 C26 119.9(3) . . ?
C27 C28 C23 122.7(3) . . ?
C30 C29 C34 115.9(3) . . ?
C30 C29 B13 127.0(3) . . ?
C34 C29 B13 117.1(3) . . ?
C29 C30 C31 122.2(3) . . ?
C32 C31 C30 120.6(4) . . ?
C31 C32 C33 119.1(3) . . ?
C32 C33 C34 120.5(3) . . ?
C33 C34 C29 121.6(3) . . ?
C1 B3 C2 57.93(16) . . ?
C1 B3 B8 104.8(2) . . ?
C2 B3 B8 106.7(2) . . ?
C1 B3 B7 105.4(2) . . ?
C2 B3 B7 59.15(18) . . ?
B8 B3 B7 61.5(2) . . ?
C1 B3 B4 58.27(17) . . ?
C2 B3 B4 106.2(2) . . ?
B8 B3 B4 60.3(2) . . ?
B7 B3 B4 109.7(3) . . ?
C1 B4 B9 104.2(2) . . ?
C1 B4 B5 58.83(18) . . ?
B9 B4 B5 60.1(2) . . ?
C1 B4 B8 103.4(2) . . ?
B9 B4 B8 60.2(2) . . ?
B5 B4 B8 108.2(3) . . ?
C1 B4 B3 58.37(18) . . ?
B9 B4 B3 106.6(3) . . ?
B5 B4 B3 107.7(2) . . ?
B8 B4 B3 58.4(2) . . ?
C1 B5 B9 103.6(2) . . ?
C1 B5 B4 58.61(18) . . ?
B9 B5 B4 59.6(2) . . ?
C1 B5 B10 103.7(2) . . ?
B9 B5 B10 60.2(2) . . ?
B4 B5 B10 107.9(3) . . ?
C1 B5 B6 58.68(18) . . ?
B9 B5 B6 106.7(3) . . ?
B4 B5 B6 107.8(2) . . ?
B10 B5 B6 58.7(2) . . ?
C1 B6 C2 57.89(16) . . ?
C1 B6 B10 104.9(2) . . ?
C2 B6 B10 106.7(2) . . ?
C1 B6 B11 104.8(2) . . ?
C2 B6 B11 58.76(18) . . ?
B10 B6 B11 61.3(2) . . ?
C1 B6 B5 58.50(18) . . ?
C2 B6 B5 106.5(2) . . ?
B10 B6 B5 60.5(2) . . ?
B11 B6 B5 109.5(3) . . ?
C2 B7 B3 59.62(18) . . ?
C2 B7 B12 104.7(2) . . ?
B3 B7 B12 106.7(3) . . ?
C2 B7 B11 58.72(18) . . ?
B3 B7 B11 107.9(2) . . ?
B12 B7 B11 59.6(2) . . ?
C2 B7 B8 105.1(2) . . ?
B3 B7 B8 58.8(2) . . ?
B12 B7 B8 59.9(2) . . ?
B11 B7 B8 107.6(3) . . ?
B3 B8 B9 108.4(3) . . ?
B3 B8 B4 61.3(2) . . ?
B9 B8 B4 59.6(2) . . ?
B3 B8 B12 107.2(3) . . ?
B9 B8 B12 60.3(2) . . ?
B4 B8 B12 107.9(3) . . ?
B3 B8 B7 59.7(2) . . ?
B9 B8 B7 108.4(3) . . ?
B4 B8 B7 109.1(3) . . ?
B12 B8 B7 59.5(2) . . ?
B4 B9 B5 60.3(2) . . ?
B4 B9 B8 60.2(2) . . ?
B5 B9 B8 108.3(3) . . ?
B4 B9 B10 108.3(3) . . ?
B5 B9 B10 60.1(2) . . ?
B8 B9 B10 107.9(3) . . ?
B4 B9 B12 108.1(3) . . ?
B5 B9 B12 107.8(3) . . ?
B8 B9 B12 59.9(2) . . ?
B10 B9 B12 59.7(2) . . ?
B6 B10 B12 107.1(3) . . ?
B6 B10 B5 60.8(2) . . ?
B12 B10 B5 107.9(3) . . ?
B6 B10 B9 108.0(3) . . ?
B12 B10 B9 60.2(2) . . ?
B5 B10 B9 59.7(2) . . ?
B6 B10 B11 59.9(2) . . ?
B12 B10 B11 59.2(2) . . ?
B5 B10 B11 108.7(3) . . ?
B9 B10 B11 107.7(3) . . ?
C2 B11 B12 105.5(2) . . ?
C2 B11 B6 59.51(18) . . ?
B12 B11 B6 106.9(3) . . ?
C2 B11 B7 59.18(19) . . ?
B12 B11 B7 60.1(2) . . ?
B6 B11 B7 108.2(2) . . ?
C2 B11 B10 105.4(2) . . ?
B12 B11 B10 60.0(2) . . ?
B6 B11 B10 58.9(2) . . ?
B7 B11 B10 108.3(3) . . ?
B11 B12 B7 60.2(2) . . ?
B11 B12 B10 60.8(2) . . ?
B7 B12 B10 109.0(3) . . ?
B11 B12 B8 108.6(3) . . ?
B7 B12 B8 60.6(2) . . ?
B10 B12 B8 108.1(3) . . ?
B11 B12 B9 109.0(3) . . ?
B7 B12 B9 108.8(3) . . ?
B10 B12 B9 60.1(2) . . ?
B8 B12 B9 59.8(2) . . ?
C23 B13 C29 111.2(2) . . ?
C23 B13 C2 120.8(2) . . ?
C29 B13 C2 112.2(2) . . ?
C23 B13 P1 110.9(2) . . ?
C29 B13 P1 114.8(2) . . ?
C2 B13 P1 84.59(16) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P1 C11 1.809(3) . ?
P1 C17 1.811(3) . ?
P1 C1 1.840(3) . ?
P1 B13 2.113(3) . ?
C1 C2 1.674(4) . ?
C1 B4 1.716(4) . ?
C1 B3 1.718(4) . ?
C1 B5 1.720(4) . ?
C1 B6 1.724(4) . ?
C2 B13 1.696(4) . ?
C2 B11 1.722(4) . ?
C2 B7 1.731(4) . ?
C2 B6 1.736(4) . ?
C2 B3 1.739(4) . ?
C11 C12 1.384(4) . ?
C11 C16 1.400(4) . ?
C12 C13 1.378(5) . ?
C13 C14 1.382(6) . ?
C14 C15 1.370(5) . ?
C15 C16 1.386(5) . ?
C17 C18 1.390(4) . ?
C17 C22 1.391(4) . ?
C18 C19 1.383(4) . ?
C19 C20 1.368(4) . ?
C20 C21 1.373(5) . ?
C21 C22 1.377(4) . ?
C23 C28 1.386(4) . ?
C23 C24 1.398(4) . ?
C23 B13 1.609(4) . ?
C24 C25 1.385(5) . ?
C25 C26 1.371(5) . ?
C26 C27 1.385(5) . ?
C27 C28 1.385(4) . ?
C29 C30 1.381(4) . ?
C29 C34 1.409(4) . ?
C29 B13 1.626(4) . ?
C30 C31 1.391(4) . ?
C31 C32 1.367(5) . ?
C32 C33 1.369(5) . ?
C33 C34 1.392(4) . ?
B3 B8 1.751(5) . ?
B3 B7 1.767(5) . ?
B3 B4 1.803(5) . ?
B4 B9 1.772(5) . ?
B4 B5 1.784(5) . ?
B4 B8 1.785(5) . ?
B5 B9 1.782(5) . ?
B5 B10 1.789(5) . ?
B5 B6 1.795(5) . ?
B6 B10 1.756(5) . ?
B6 B11 1.774(5) . ?
B7 B12 1.779(6) . ?
B7 B11 1.781(5) . ?
B7 B8 1.798(5) . ?
B8 B9 1.784(5) . ?
B8 B12 1.786(5) . ?
B9 B10 1.792(5) . ?
B9 B12 1.793(6) . ?
B10 B12 1.785(6) . ?
B10 B11 1.800(5) . ?
B11 B12 1.770(6) . ?
