#------------------------------------------------------------------------------
#$Date: 2021-05-17 12:05:26 +0300 (Mon, 17 May 2021) $
#$Revision: 265275 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/26/1562605.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1562605
loop_
_publ_author_name
'Liu, Guang-Zhen'
'Li, Xiao-Dong'
'Xin, Ling-Yun'
'Li, Xiao-Ling'
'Wang, Li-Ya'
_publ_section_title
;
 Diverse assemblies of the (4,4) grid layers exemplified in Zn(II)/Co(II)
 coordination polymers with dual linear ligands
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              106
_journal_page_last               113
_journal_paper_doi               10.1016/j.jssc.2013.03.053
_journal_volume                  203
_journal_year                    2013
_chemical_formula_sum            'C14 H10 N O4 Zn'
_chemical_formula_weight         321.60
_space_group_IT_number           13
_space_group_name_Hall           '-P 2yc'
_space_group_name_H-M_alt        'P 1 2/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 113.9270(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.0129(11)
_cell_length_b                   14.0992(16)
_cell_length_c                   11.0454(12)
_cell_measurement_reflns_used    4191
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.95
_cell_measurement_theta_min      2.48
_cell_volume                     1425.3(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0226
_diffrn_reflns_av_sigmaI/netI    0.0194
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            10441
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         2.48
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.733
_exptl_absorpt_correction_T_max  0.7689
_exptl_absorpt_correction_T_min  0.5821
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.499
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             652
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.16
_refine_diff_density_max         0.238
_refine_diff_density_min         -0.283
_refine_diff_density_rms         0.054
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     203
_refine_ls_number_reflns         2659
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.062
_refine_ls_R_factor_all          0.0282
_refine_ls_R_factor_gt           0.0238
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0323P)²+0.5872P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0637
_refine_ls_wR_factor_ref         0.0656
_reflns_number_gt                2309
_reflns_number_total             2659
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            JSSC-2013-203-106.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Monoclinic' was changed to
'monoclinic' in accordance with the built-in table derived from the
CIF Core dictionary named 'cif_core.dic' version 2.4.5 last updated
on 2014-11-21.

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 
;
_cod_original_sg_symbol_H-M      P2/c
_cod_database_code               1562605
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C14 C 0.4760(6) 0.9091(3) 0.1361(4) 0.0480(14) Uani 0.547(4) 1 d P A 1
H14A H 0.4602 0.8780 0.0572 0.058 Uiso 0.547(4) 1 calc PR A 1
C15 C 0.4756(6) 1.0066(3) 0.1409(4) 0.0484(14) Uani 0.547(4) 1 d P A 1
H15A H 0.4573 1.0398 0.0630 0.058 Uiso 0.547(4) 1 calc PR A 1
C14' C 0.6152(6) 0.9094(3) 0.2439(7) 0.0501(18) Uani 0.453(4) 1 d P A 2
H14B H 0.6948 0.8783 0.2390 0.060 Uiso 0.453(4) 1 calc PR A 2
C15' C 0.6107(6) 1.0073(3) 0.2452(6) 0.0477(17) Uani 0.453(4) 1 d P A 2
H15B H 0.6895 1.0408 0.2426 0.057 Uiso 0.453(4) 1 calc PR A 2
N2 N 0.5000 1.05596(16) 0.2500 0.0302(5) Uani 1 2 d S . .
Zn1 Zn 0.5000 0.20103(2) 0.2500 0.02364(10) Uani 1 2 d S . .
Zn2 Zn 0.5000 0.41038(2) 0.2500 0.02381(10) Uani 1 2 d S . .
O1 O 0.63614(16) 0.22922(11) 0.16011(15) 0.0382(4) Uani 1 1 d . . .
O2 O 0.62914(17) 0.38732(11) 0.14991(16) 0.0390(4) Uani 1 1 d . . .
O3 O 1.32185(16) 0.22065(11) 0.07162(15) 0.0388(4) Uani 1 1 d . . .
O4 O 1.31971(16) 0.37831(11) 0.08030(15) 0.0399(4) Uani 1 1 d . . .
N1 N 0.5000 0.55487(15) 0.2500 0.0245(5) Uani 1 2 d S . .
C1 C 0.6762(2) 0.30796(14) 0.13261(19) 0.0276(4) Uani 1 1 d . . .
C2 C 0.7875(2) 0.30666(13) 0.0741(2) 0.0284(4) Uani 1 1 d . . .
C3 C 0.8619(3) 0.22452(17) 0.0735(3) 0.0472(6) Uani 1 1 d . . .
H3 H 0.8409 0.1691 0.1081 0.057 Uiso 1 1 calc R . .
C4 C 0.9669(3) 0.22291(18) 0.0223(3) 0.0494(7) Uani 1 1 d . . .
H4 H 1.0175 0.1670 0.0255 0.059 Uiso 1 1 calc R . .
C5 C 0.9978(2) 0.30311(15) -0.0334(2) 0.0314(5) Uani 1 1 d . . .
C6 C 0.9192(2) 0.38473(16) -0.0376(2) 0.0380(5) Uani 1 1 d . . .
H6 H 0.9351 0.4388 -0.0783 0.046 Uiso 1 1 calc R . .
C7 C 0.8175(2) 0.38737(15) 0.0176(2) 0.0356(5) Uani 1 1 d . . .
H7 H 0.7688 0.4437 0.0168 0.043 Uiso 1 1 calc R . .
C8 C 1.1174(2) 0.30233(17) -0.0847(2) 0.0369(5) Uani 1 1 d . . .
H8A H 1.1096 0.3584 -0.1380 0.044 Uiso 1 1 calc R . .
H8B H 1.1068 0.2469 -0.1399 0.044 Uiso 1 1 calc R . .
C9 C 1.2657(2) 0.30043(15) 0.03224(19) 0.0288(5) Uani 1 1 d . . .
C10 C 0.5613(2) 0.60396(14) 0.1819(2) 0.0294(5) Uani 1 1 d . . .
H10 H 0.6042 0.5707 0.1343 0.035 Uiso 1 1 calc R . .
C11 C 0.5634(2) 0.70179(13) 0.1796(2) 0.0301(5) Uani 1 1 d . . .
H11 H 0.6071 0.7333 0.1312 0.036 Uiso 1 1 calc R . .
C12 C 0.5000 0.75287(19) 0.2500 0.0243(6) Uani 1 2 d S . .
C13 C 0.5000 0.85781(19) 0.2500 0.0275(6) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C15 C14 C13 119.3(4) . .
C15 C14 H14A 120.4 . .
C13 C14 H14A 120.4 . .
N2 C15 C14 123.8(4) . .
N2 C15 H15A 118.1 . .
C14 C15 H15A 118.1 . .
C15' C14' C13 119.4(4) . .
C15' C14' H14B 120.3 . .
C13 C14' H14B 120.3 . .
N2 C15' C14' 123.4(4) . .
N2 C15' H15B 118.3 . .
C14' C15' H15B 118.3 . .
C15' N2 C15' 117.5(5) 2_655 .
C15' N2 C15 85.2(3) 2_655 .
C15' N2 C15 62.6(3) . .
C15' N2 C15 62.6(3) 2_655 2_655
C15' N2 C15 85.2(3) . 2_655
C15 N2 C15 116.7(4) . 2_655
C15' N2 Zn1 121.2(2) 2_655 1_565
C15' N2 Zn1 121.2(2) . 1_565
C15 N2 Zn1 121.66(19) . 1_565
C15 N2 Zn1 121.66(19) 2_655 1_565
O1 Zn1 O1 157.37(9) 2_655 .
O1 Zn1 N2 101.32(5) 2_655 1_545
O1 Zn1 N2 101.32(5) . 1_545
O1 Zn1 O3 87.07(6) 2_655 1_455
O1 Zn1 O3 89.93(6) . 1_455
N2 Zn1 O3 97.67(5) 1_545 1_455
O1 Zn1 O3 89.93(6) 2_655 2_755
O1 Zn1 O3 87.07(6) . 2_755
N2 Zn1 O3 97.67(5) 1_545 2_755
O3 Zn1 O3 164.65(9) 1_455 2_755
O1 Zn1 Zn2 78.68(5) 2_655 .
O1 Zn1 Zn2 78.68(5) . .
N2 Zn1 Zn2 180.0 1_545 .
O3 Zn1 Zn2 82.33(5) 1_455 .
O3 Zn1 Zn2 82.33(5) 2_755 .
N1 Zn2 O2 99.17(4) . 2_655
N1 Zn2 O2 99.17(4) . .
O2 Zn2 O2 161.66(9) 2_655 .
N1 Zn2 O4 102.70(4) . 1_455
O2 Zn2 O4 86.78(6) 2_655 1_455
O2 Zn2 O4 89.20(6) . 1_455
N1 Zn2 O4 102.70(4) . 2_755
O2 Zn2 O4 89.20(6) 2_655 2_755
O2 Zn2 O4 86.78(6) . 2_755
O4 Zn2 O4 154.61(9) 1_455 2_755
N1 Zn2 Zn1 180.0 . .
O2 Zn2 Zn1 80.83(4) 2_655 .
O2 Zn2 Zn1 80.83(4) . .
O4 Zn2 Zn1 77.30(4) 1_455 .
O4 Zn2 Zn1 77.30(4) 2_755 .
C1 O1 Zn1 129.42(14) . .
C1 O2 Zn2 125.63(13) . .
C9 O3 Zn1 122.80(14) . 1_655
C9 O4 Zn2 130.68(14) . 1_655
C10 N1 C10 117.8(2) 2_655 .
C10 N1 Zn2 121.10(11) 2_655 .
C10 N1 Zn2 121.10(11) . .
O2 C1 O1 124.92(19) . .
O2 C1 C2 117.78(17) . .
O1 C1 C2 117.30(17) . .
C3 C2 C7 118.03(19) . .
C3 C2 C1 120.72(18) . .
C7 C2 C1 121.25(18) . .
C2 C3 C4 121.2(2) . .
C2 C3 H3 119.4 . .
C4 C3 H3 119.4 . .
C3 C4 C5 121.0(2) . .
C3 C4 H4 119.5 . .
C5 C4 H4 119.5 . .
C4 C5 C6 117.93(19) . .
C4 C5 C8 120.91(19) . .
C6 C5 C8 121.13(19) . .
C7 C6 C5 121.2(2) . .
C7 C6 H6 119.4 . .
C5 C6 H6 119.4 . .
C6 C7 C2 120.6(2) . .
C6 C7 H7 119.7 . .
C2 C7 H7 119.7 . .
C5 C8 C9 109.23(17) . .
C5 C8 H8A 109.8 . .
C9 C8 H8A 109.8 . .
C5 C8 H8B 109.8 . .
C9 C8 H8B 109.8 . .
H8A C8 H8B 108.3 . .
O4 C9 O3 126.0(2) . .
O4 C9 C8 116.88(19) . .
O3 C9 C8 117.11(19) . .
N1 C10 C11 122.74(19) . .
N1 C10 H10 118.6 . .
C11 C10 H10 118.6 . .
C10 C11 C12 119.61(19) . .
C10 C11 H11 120.2 . .
C12 C11 H11 120.2 . .
C11 C12 C11 117.5(2) . 2_655
C11 C12 C13 121.25(12) . .
C11 C12 C13 121.25(12) 2_655 .
C14 C13 C14 117.1(4) 2_655 .
C14 C13 C14' 85.9(3) 2_655 .
C14 C13 C14' 61.6(3) . .
C14 C13 C14' 61.6(3) 2_655 2_655
C14 C13 C14' 85.9(3) . 2_655
C14' C13 C14' 116.8(4) . 2_655
C14 C13 C12 121.47(19) 2_655 .
C14 C13 C12 121.47(19) . .
C14' C13 C12 121.6(2) . .
C14' C13 C12 121.6(2) 2_655 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C14 C15 1.376(5) .
C14 C13 1.385(4) .
C14 H14A 0.9300 .
C15 N2 1.326(4) .
C15 H15A 0.9300 .
C14' C15' 1.381(7) .
C14' C13 1.389(5) .
C14' H14B 0.9300 .
C15' N2 1.323(5) .
C15' H15B 0.9300 .
N2 C15' 1.323(5) 2_655
N2 C15 1.326(4) 2_655
N2 Zn1 2.045(2) 1_565
Zn1 O1 2.0248(14) 2_655
Zn1 O1 2.0248(14) .
Zn1 N2 2.045(2) 1_545
Zn1 O3 2.0711(15) 1_455
Zn1 O3 2.0711(15) 2_755
Zn1 Zn2 2.9515(5) .
Zn2 N1 2.037(2) .
Zn2 O2 2.0394(14) 2_655
Zn2 O2 2.0394(14) .
Zn2 O4 2.0571(15) 1_455
Zn2 O4 2.0571(15) 2_755
O1 C1 1.259(2) .
O2 C1 1.258(2) .
O3 C9 1.254(2) .
O3 Zn1 2.0711(15) 1_655
O4 C9 1.244(2) .
O4 Zn2 2.0571(15) 1_655
N1 C10 1.340(2) 2_655
N1 C10 1.340(2) .
C1 C2 1.498(3) .
C2 C3 1.379(3) .
C2 C7 1.388(3) .
C3 C4 1.381(3) .
C3 H3 0.9300 .
C4 C5 1.381(3) .
C4 H4 0.9300 .
C5 C6 1.384(3) .
C5 C8 1.518(3) .
C6 C7 1.384(3) .
C6 H6 0.9300 .
C7 H7 0.9300 .
C8 C9 1.523(3) .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C10 C11 1.380(3) .
C10 H10 0.9300 .
C11 C12 1.388(2) .
C11 H11 0.9300 .
C12 C11 1.388(2) 2_655
C12 C13 1.480(4) .
C13 C14 1.385(4) 2_655
C13 C14' 1.389(5) 2_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
C13 C14 C15 N2 1.3(8) . . . .
C13 C14' C15' N2 -1.1(10) . . . .
C14' C15' N2 C15' 0.5(5) . . . 2_655
C14' C15' N2 C15 -67.3(6) . . . .
C14' C15' N2 C15 56.1(6) . . . 2_655
C14' C15' N2 Zn1 -179.5(5) . . . 1_565
C14 C15 N2 C15' -56.7(6) . . . 2_655
C14 C15 N2 C15' 67.8(5) . . . .
C14 C15 N2 C15 -0.7(4) . . . 2_655
C14 C15 N2 Zn1 179.3(4) . . . 1_565
O1 Zn1 Zn2 N1 -27(100) 2_655 . . .
O1 Zn1 Zn2 N1 153(100) . . . .
N2 Zn1 Zn2 N1 0(29) 1_545 . . .
O3 Zn1 Zn2 N1 61(100) 1_455 . . .
O3 Zn1 Zn2 N1 -119(100) 2_755 . . .
O1 Zn1 Zn2 O2 2.92(6) 2_655 . . 2_655
O1 Zn1 Zn2 O2 -177.08(6) . . . 2_655
N2 Zn1 Zn2 O2 -105(100) 1_545 . . 2_655
O3 Zn1 Zn2 O2 91.45(6) 1_455 . . 2_655
O3 Zn1 Zn2 O2 -88.55(6) 2_755 . . 2_655
O1 Zn1 Zn2 O2 -177.08(6) 2_655 . . .
O1 Zn1 Zn2 O2 2.92(6) . . . .
N2 Zn1 Zn2 O2 75(100) 1_545 . . .
O3 Zn1 Zn2 O2 -88.55(6) 1_455 . . .
O3 Zn1 Zn2 O2 91.45(6) 2_755 . . .
O1 Zn1 Zn2 O4 -85.82(7) 2_655 . . 1_455
O1 Zn1 Zn2 O4 94.18(7) . . . 1_455
N2 Zn1 Zn2 O4 166(100) 1_545 . . 1_455
O3 Zn1 Zn2 O4 2.71(6) 1_455 . . 1_455
O3 Zn1 Zn2 O4 -177.29(6) 2_755 . . 1_455
O1 Zn1 Zn2 O4 94.18(7) 2_655 . . 2_755
O1 Zn1 Zn2 O4 -85.82(7) . . . 2_755
N2 Zn1 Zn2 O4 -14(100) 1_545 . . 2_755
O3 Zn1 Zn2 O4 -177.29(6) 1_455 . . 2_755
O3 Zn1 Zn2 O4 2.71(6) 2_755 . . 2_755
O1 Zn1 O1 C1 -0.44(17) 2_655 . . .
N2 Zn1 O1 C1 179.56(17) 1_545 . . .
O3 Zn1 O1 C1 81.75(18) 1_455 . . .
O3 Zn1 O1 C1 -83.19(18) 2_755 . . .
Zn2 Zn1 O1 C1 -0.44(17) . . . .
N1 Zn2 O2 C1 173.03(16) . . . .
O2 Zn2 O2 C1 -6.97(16) 2_655 . . .
O4 Zn2 O2 C1 -84.24(17) 1_455 . . .
O4 Zn2 O2 C1 70.68(17) 2_755 . . .
Zn1 Zn2 O2 C1 -6.97(16) . . . .
O2 Zn2 N1 C10 6.67(11) 2_655 . . 2_655
O2 Zn2 N1 C10 -173.33(11) . . . 2_655
O4 Zn2 N1 C10 95.42(12) 1_455 . . 2_655
O4 Zn2 N1 C10 -84.58(12) 2_755 . . 2_655
Zn1 Zn2 N1 C10 37(100) . . . 2_655
O2 Zn2 N1 C10 -173.33(11) 2_655 . . .
O2 Zn2 N1 C10 6.67(11) . . . .
O4 Zn2 N1 C10 -84.58(12) 1_455 . . .
O4 Zn2 N1 C10 95.42(12) 2_755 . . .
Zn1 Zn2 N1 C10 -143(100) . . . .
Zn2 O2 C1 O1 9.3(3) . . . .
Zn2 O2 C1 C2 -171.08(13) . . . .
Zn1 O1 C1 O2 -4.8(3) . . . .
Zn1 O1 C1 C2 175.62(13) . . . .
O2 C1 C2 C3 168.8(2) . . . .
O1 C1 C2 C3 -11.6(3) . . . .
O2 C1 C2 C7 -12.1(3) . . . .
O1 C1 C2 C7 167.5(2) . . . .
C7 C2 C3 C4 2.2(4) . . . .
C1 C2 C3 C4 -178.6(2) . . . .
C2 C3 C4 C5 -1.9(4) . . . .
C3 C4 C5 C6 -0.7(4) . . . .
C3 C4 C5 C8 177.6(2) . . . .
C4 C5 C6 C7 2.9(3) . . . .
C8 C5 C6 C7 -175.3(2) . . . .
C5 C6 C7 C2 -2.6(3) . . . .
C3 C2 C7 C6 0.0(3) . . . .
C1 C2 C7 C6 -179.1(2) . . . .
C4 C5 C8 C9 -72.5(3) . . . .
C6 C5 C8 C9 105.7(2) . . . .
Zn2 O4 C9 O3 -8.8(3) 1_655 . . .
Zn2 O4 C9 C8 170.87(13) 1_655 . . .
Zn1 O3 C9 O4 12.4(3) 1_655 . . .
Zn1 O3 C9 C8 -167.27(13) 1_655 . . .
C5 C8 C9 O4 -87.1(2) . . . .
C5 C8 C9 O3 92.5(2) . . . .
C10 N1 C10 C11 0.01(16) 2_655 . . .
Zn2 N1 C10 C11 -179.99(16) . . . .
N1 C10 C11 C12 0.0(3) . . . .
C10 C11 C12 C11 0.01(15) . . . 2_655
C10 C11 C12 C13 -179.99(15) . . . .
C15 C14 C13 C14 -0.6(4) . . . 2_655
C15 C14 C13 C14' -69.1(5) . . . .
C15 C14 C13 C14' 54.5(5) . . . 2_655
C15 C14 C13 C12 179.4(4) . . . .
C15' C14' C13 C14 -54.7(6) . . . 2_655
C15' C14' C13 C14 69.1(6) . . . .
C15' C14' C13 C14' 0.5(4) . . . 2_655
C15' C14' C13 C12 -179.5(4) . . . .
C11 C12 C13 C14 -140.0(3) . . . 2_655
C11 C12 C13 C14 40.0(3) 2_655 . . 2_655
C11 C12 C13 C14 40.0(3) . . . .
C11 C12 C13 C14 -140.0(3) 2_655 . . .
C11 C12 C13 C14' -33.8(4) . . . .
C11 C12 C13 C14' 146.2(4) 2_655 . . .
C11 C12 C13 C14' 146.2(4) . . . 2_655
C11 C12 C13 C14' -33.8(4) 2_655 . . 2_655
