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#$Date: 2021-06-08 10:42:51 +0300 (Tue, 08 Jun 2021) $
#$Revision: 266256 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/32/1563210.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1563210
loop_
_publ_author_name
'Dürr, Ines'
'Schwarz, Michael'
'Röhr, Caroline'
_publ_section_title
;
 The binary tin-rich lanthanum stannides La2Sn5 and La3Sn7---A structural
 and bond theoretical study
;
_journal_issue                   8
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              2220
_journal_page_last               2230
_journal_paper_doi               10.1016/j.jssc.2011.06.035
_journal_volume                  184
_journal_year                    2011
_chemical_formula_sum            'La3 Sn7'
_chemical_formula_weight         1247.56
_space_group_IT_number           65
_space_group_name_Hall           '-C 2 2'
_space_group_name_H-M_alt        'C m m m'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'C m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   4.592(4)
_cell_length_b                   26.19(2)
_cell_length_c                   4.681(5)
_cell_measurement_temperature    293(2)
_cell_volume                     563.0(9)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.2954
_diffrn_reflns_av_sigmaI/netI    0.1299
_diffrn_reflns_limit_h_max       4
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       5
_diffrn_reflns_limit_l_min       -5
_diffrn_reflns_number            1905
_diffrn_reflns_theta_full        24.99
_diffrn_reflns_theta_max         24.99
_diffrn_reflns_theta_min         3.11
_exptl_absorpt_coefficient_mu    52.552
_exptl_crystal_density_diffrn    14.718
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2084
_refine_diff_density_max         9.558
_refine_diff_density_min         -5.646
_refine_diff_density_rms         2.216
_refine_ls_extinction_coef       0.0000(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.441
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     24
_refine_ls_number_reflns         329
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.441
_refine_ls_R_factor_all          0.3058
_refine_ls_R_factor_gt           0.2713
_refine_ls_shift/su_max          2.698
_refine_ls_shift/su_mean         0.112
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.4275
_refine_ls_wR_factor_ref         0.4543
_reflns_number_gt                137
_reflns_number_total             329
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            JSSC-2011-184-2220.cif
_cod_data_source_block           La3Sn7
_cod_original_cell_volume        563.0(8)
_cod_database_code               1563210
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'x, -y, -z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'x+1/2, -y+1/2, -z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, y, -z'
'-x, y, z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
La1 La 0.0000 0.0000 0.0000 0.079(5) Uani 1 8 d S . .
La2 La 0.0000 0.1833(5) 0.0000 0.090(4) Uani 1 4 d S . .
Sn1 Sn 0.5000 0.0000 0.5000 0.077(6) Uani 1 8 d S . .
Sn2 Sn 0.0000 0.4047(5) 0.0000 0.087(4) Uani 1 4 d S . .
Sn3 Sn 0.0000 0.0969(5) 0.5000 0.073(4) Uani 1 4 d S . .
Sn4 Sn 0.0000 0.2869(6) 0.5000 0.086(4) Uani 1 4 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
La La -0.2871 2.4523 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Sn1 La1 Sn1 180.0 1_454 .
Sn1 La1 Sn1 91.10(7) 1_454 1_455
Sn1 La1 Sn1 88.90(7) . 1_455
Sn1 La1 Sn1 88.90(7) 1_454 1_554
Sn1 La1 Sn1 91.10(7) . 1_554
Sn1 La1 Sn1 180.0 1_455 1_554
Sn1 La1 Sn2 118.31(10) 1_454 13
Sn1 La1 Sn2 61.69(10) . 13
Sn1 La1 Sn2 118.31(10) 1_455 13
Sn1 La1 Sn2 61.69(10) 1_554 13
Sn1 La1 Sn2 61.69(10) 1_454 5_445
Sn1 La1 Sn2 118.31(10) . 5_445
Sn1 La1 Sn2 61.69(10) 1_455 5_445
Sn1 La1 Sn2 118.31(10) 1_554 5_445
Sn2 La1 Sn2 180.0(3) 13 5_445
Sn1 La1 Sn2 61.69(10) 1_454 13_455
Sn1 La1 Sn2 118.31(10) . 13_455
Sn1 La1 Sn2 61.69(10) 1_455 13_455
Sn1 La1 Sn2 118.31(10) 1_554 13_455
Sn2 La1 Sn2 85.2(3) 13 13_455
Sn2 La1 Sn2 94.8(3) 5_445 13_455
Sn1 La1 Sn2 118.31(10) 1_454 5_545
Sn1 La1 Sn2 61.69(10) . 5_545
Sn1 La1 Sn2 118.31(10) 1_455 5_545
Sn1 La1 Sn2 61.69(10) 1_554 5_545
Sn2 La1 Sn2 94.8(3) 13 5_545
Sn2 La1 Sn2 85.2(3) 5_445 5_545
Sn2 La1 Sn2 180.0(3) 13_455 5_545
Sn1 La1 Sn3 61.06(9) 1_454 9
Sn1 La1 Sn3 118.94(9) . 9
Sn1 La1 Sn3 118.94(9) 1_455 9
Sn1 La1 Sn3 61.06(9) 1_554 9
Sn2 La1 Sn3 122.75(15) 13 9
Sn2 La1 Sn3 57.25(15) 5_445 9
Sn2 La1 Sn3 122.75(15) 13_455 9
Sn2 La1 Sn3 57.25(15) 5_545 9
Sn1 La1 Sn3 118.94(9) 1_454 .
Sn1 La1 Sn3 61.06(9) . .
Sn1 La1 Sn3 61.06(9) 1_455 .
Sn1 La1 Sn3 118.94(9) 1_554 .
Sn2 La1 Sn3 57.25(15) 13 .
Sn2 La1 Sn3 122.75(15) 5_445 .
Sn2 La1 Sn3 57.25(15) 13_455 .
Sn2 La1 Sn3 122.75(15) 5_545 .
Sn3 La1 Sn3 180.0(3) 9 .
Sn1 La1 Sn3 118.94(9) 1_454 9_556
Sn1 La1 Sn3 61.06(9) . 9_556
Sn1 La1 Sn3 61.06(9) 1_455 9_556
Sn1 La1 Sn3 118.94(9) 1_554 9_556
Sn2 La1 Sn3 122.75(15) 13 9_556
Sn2 La1 Sn3 57.25(15) 5_445 9_556
Sn2 La1 Sn3 122.75(15) 13_455 9_556
Sn2 La1 Sn3 57.25(15) 5_545 9_556
Sn3 La1 Sn3 85.4(3) 9 9_556
Sn3 La1 Sn3 94.6(3) . 9_556
Sn1 La1 Sn3 61.06(9) 1_454 1_554
Sn1 La1 Sn3 118.94(9) . 1_554
Sn1 La1 Sn3 118.94(9) 1_455 1_554
Sn1 La1 Sn3 61.06(9) 1_554 1_554
Sn2 La1 Sn3 57.25(15) 13 1_554
Sn2 La1 Sn3 122.75(15) 5_445 1_554
Sn2 La1 Sn3 57.25(15) 13_455 1_554
Sn2 La1 Sn3 122.75(15) 5_545 1_554
Sn3 La1 Sn3 94.6(3) 9 1_554
Sn3 La1 Sn3 85.4(3) . 1_554
Sn3 La1 Sn3 180.0(3) 9_556 1_554
Sn1 La1 La1 134.45(4) 1_454 1_655
Sn1 La1 La1 45.55(4) . 1_655
Sn1 La1 La1 134.45(4) 1_455 1_655
Sn1 La1 La1 45.55(4) 1_554 1_655
Sn2 La1 La1 47.38(17) 13 1_655
Sn2 La1 La1 132.62(17) 5_445 1_655
Sn2 La1 La1 132.62(17) 13_455 1_655
Sn2 La1 La1 47.38(17) 5_545 1_655
Sn3 La1 La1 90.0 9 1_655
Sn3 La1 La1 90.0 . 1_655
Sn3 La1 La1 90.0 9_556 1_655
Sn3 La1 La1 90.0 1_554 1_655
Sn1 La1 La1 45.55(4) 1_454 1_455
Sn1 La1 La1 134.45(4) . 1_455
Sn1 La1 La1 45.55(4) 1_455 1_455
Sn1 La1 La1 134.45(4) 1_554 1_455
Sn2 La1 La1 132.62(17) 13 1_455
Sn2 La1 La1 47.38(17) 5_445 1_455
Sn2 La1 La1 47.38(17) 13_455 1_455
Sn2 La1 La1 132.62(17) 5_545 1_455
Sn3 La1 La1 90.0 9 1_455
Sn3 La1 La1 90.0 . 1_455
Sn3 La1 La1 90.0 9_556 1_455
Sn3 La1 La1 90.0 1_554 1_455
La1 La1 La1 180.0 1_655 1_455
Sn1 La1 La1 44.45(4) 1_454 1_554
Sn1 La1 La1 135.55(4) . 1_554
Sn1 La1 La1 135.55(4) 1_455 1_554
Sn1 La1 La1 44.45(4) 1_554 1_554
Sn2 La1 La1 90.0 13 1_554
Sn2 La1 La1 90.0 5_445 1_554
Sn2 La1 La1 90.0 13_455 1_554
Sn2 La1 La1 90.0 5_545 1_554
Sn3 La1 La1 47.32(14) 9 1_554
Sn3 La1 La1 132.68(14) . 1_554
Sn3 La1 La1 132.68(14) 9_556 1_554
Sn3 La1 La1 47.32(14) 1_554 1_554
La1 La1 La1 90.0 1_655 1_554
La1 La1 La1 90.0 1_455 1_554
Sn1 La1 La1 135.55(4) 1_454 1_556
Sn1 La1 La1 44.45(4) . 1_556
Sn1 La1 La1 44.45(4) 1_455 1_556
Sn1 La1 La1 135.55(4) 1_554 1_556
Sn2 La1 La1 90.0 13 1_556
Sn2 La1 La1 90.0 5_445 1_556
Sn2 La1 La1 90.0 13_455 1_556
Sn2 La1 La1 90.0 5_545 1_556
Sn3 La1 La1 132.68(14) 9 1_556
Sn3 La1 La1 47.32(14) . 1_556
Sn3 La1 La1 47.32(14) 9_556 1_556
Sn3 La1 La1 132.68(14) 1_554 1_556
La1 La1 La1 90.0 1_655 1_556
La1 La1 La1 90.0 1_455 1_556
La1 La1 La1 180.0 1_554 1_556
Sn1 La1 La2 90.0 1_454 9
Sn1 La1 La2 90.0 . 9
Sn1 La1 La2 90.0 1_455 9
Sn1 La1 La2 90.0 1_554 9
Sn2 La1 La2 137.38(17) 13 9
Sn2 La1 La2 42.62(17) 5_445 9
Sn2 La1 La2 137.38(17) 13_455 9
Sn2 La1 La2 42.62(17) 5_545 9
Sn3 La1 La2 42.68(14) 9 9
Sn3 La1 La2 137.32(14) . 9
Sn3 La1 La2 42.68(14) 9_556 9
Sn3 La1 La2 137.32(14) 1_554 9
La1 La1 La2 90.0 1_655 9
La1 La1 La2 90.0 1_455 9
La1 La1 La2 90.0 1_554 9
La1 La1 La2 90.0 1_556 9
Sn1 La1 La2 90.0 1_454 .
Sn1 La1 La2 90.0 . .
Sn1 La1 La2 90.0 1_455 .
Sn1 La1 La2 90.0 1_554 .
Sn2 La1 La2 42.62(17) 13 .
Sn2 La1 La2 137.38(17) 5_445 .
Sn2 La1 La2 42.62(17) 13_455 .
Sn2 La1 La2 137.38(17) 5_545 .
Sn3 La1 La2 137.32(14) 9 .
Sn3 La1 La2 42.68(14) . .
Sn3 La1 La2 137.32(14) 9_556 .
Sn3 La1 La2 42.68(14) 1_554 .
La1 La1 La2 90.0 1_655 .
La1 La1 La2 90.0 1_455 .
La1 La1 La2 90.0 1_554 .
La1 La1 La2 90.0 1_556 .
La2 La1 La2 180.0 9 .
Sn2 La2 Sn2 89.8(5) 13_455 13
Sn2 La2 Sn3 60.5(3) 13_455 1_554
Sn2 La2 Sn3 60.5(3) 13 1_554
Sn2 La2 Sn3 60.5(3) 13_455 .
Sn2 La2 Sn3 60.5(3) 13 .
Sn3 La2 Sn3 91.9(5) 1_554 .
Sn2 La2 Sn4 130.1(3) 13_455 13_556
Sn2 La2 Sn4 71.5(2) 13 13_556
Sn3 La2 Sn4 131.3(3) 1_554 13_556
Sn3 La2 Sn4 70.2(3) . 13_556
Sn2 La2 Sn4 71.5(2) 13_455 13_455
Sn2 La2 Sn4 130.1(3) 13 13_455
Sn3 La2 Sn4 70.2(3) 1_554 13_455
Sn3 La2 Sn4 131.3(3) . 13_455
Sn4 La2 Sn4 153.2(7) 13_556 13_455
Sn2 La2 Sn4 71.5(2) 13_455 13_456
Sn2 La2 Sn4 130.1(3) 13 13_456
Sn3 La2 Sn4 131.3(3) 1_554 13_456
Sn3 La2 Sn4 70.2(3) . 13_456
Sn4 La2 Sn4 85.89(16) 13_556 13_456
Sn4 La2 Sn4 87.97(17) 13_455 13_456
Sn2 La2 Sn4 130.1(3) 13_455 13
Sn2 La2 Sn4 71.5(2) 13 13
Sn3 La2 Sn4 70.2(3) 1_554 13
Sn3 La2 Sn4 131.3(3) . 13
Sn4 La2 Sn4 87.97(17) 13_556 13
Sn4 La2 Sn4 85.89(16) 13_455 13
Sn4 La2 Sn4 153.2(7) 13_456 13
Sn2 La2 Sn4 122.44(16) 13_455 .
Sn2 La2 Sn4 122.44(16) 13 .
Sn3 La2 Sn4 174.8(4) 1_554 .
Sn3 La2 Sn4 93.2(2) . .
Sn4 La2 Sn4 51.0(3) 13_556 .
Sn4 La2 Sn4 106.2(3) 13_455 .
Sn4 La2 Sn4 51.0(3) 13_456 .
Sn4 La2 Sn4 106.2(3) 13 .
Sn2 La2 Sn4 122.44(16) 13_455 1_554
Sn2 La2 Sn4 122.44(16) 13 1_554
Sn3 La2 Sn4 93.2(2) 1_554 1_554
Sn3 La2 Sn4 174.8(4) . 1_554
Sn4 La2 Sn4 106.2(3) 13_556 1_554
Sn4 La2 Sn4 51.0(3) 13_455 1_554
Sn4 La2 Sn4 106.2(3) 13_456 1_554
Sn4 La2 Sn4 51.0(3) 13 1_554
Sn4 La2 Sn4 81.6(4) . 1_554
Sn2 La2 La2 168.4(4) 13_455 13
Sn2 La2 La2 101.80(19) 13 13
Sn3 La2 La2 125.50(13) 1_554 13
Sn3 La2 La2 125.50(12) . 13
Sn4 La2 La2 55.4(2) 13_556 13
Sn4 La2 La2 100.4(4) 13_455 13
Sn4 La2 La2 100.4(4) 13_456 13
Sn4 La2 La2 55.4(2) 13 13
Sn4 La2 La2 50.8(2) . 13
Sn4 La2 La2 50.8(2) 1_554 13
Sn2 La2 La2 101.80(19) 13_455 13_455
Sn2 La2 La2 168.4(4) 13 13_455
Sn3 La2 La2 125.50(12) 1_554 13_455
Sn3 La2 La2 125.50(12) . 13_455
Sn4 La2 La2 100.4(4) 13_556 13_455
Sn4 La2 La2 55.4(2) 13_455 13_455
Sn4 La2 La2 55.4(2) 13_456 13_455
Sn4 La2 La2 100.4(4) 13 13_455
Sn4 La2 La2 50.8(2) . 13_455
Sn4 La2 La2 50.8(2) 1_554 13_455
La2 La2 La2 66.7(4) 13 13_455
Sn2 La2 La2 45.1(2) 13_455 1_455
Sn2 La2 La2 134.9(2) 13 1_455
Sn3 La2 La2 90.0 1_554 1_455
Sn3 La2 La2 90.0 . 1_455
Sn4 La2 La2 132.94(8) 13_556 1_455
Sn4 La2 La2 47.06(8) 13_455 1_455
Sn4 La2 La2 47.06(8) 13_456 1_455
Sn4 La2 La2 132.94(8) 13 1_455
Sn4 La2 La2 90.0 . 1_455
Sn4 La2 La2 90.0 1_554 1_455
La2 La2 La2 123.33(19) 13 1_455
La2 La2 La2 56.67(19) 13_455 1_455
Sn2 La2 La2 134.9(2) 13_455 1_655
Sn2 La2 La2 45.1(2) 13 1_655
Sn3 La2 La2 90.0 1_554 1_655
Sn3 La2 La2 90.0 . 1_655
Sn4 La2 La2 47.06(8) 13_556 1_655
Sn4 La2 La2 132.94(8) 13_455 1_655
Sn4 La2 La2 132.94(8) 13_456 1_655
Sn4 La2 La2 47.06(8) 13 1_655
Sn4 La2 La2 90.0 . 1_655
Sn4 La2 La2 90.0 1_554 1_655
La2 La2 La2 56.67(19) 13 1_655
La2 La2 La2 123.33(19) 13_455 1_655
La2 La2 La2 180.0(6) 1_455 1_655
Sn2 La2 La2 90.0 13_455 1_556
Sn2 La2 La2 90.0 13 1_556
Sn3 La2 La2 136.0(2) 1_554 1_556
Sn3 La2 La2 44.0(2) . 1_556
Sn4 La2 La2 46.01(8) 13_556 1_556
Sn4 La2 La2 133.99(8) 13_455 1_556
Sn4 La2 La2 46.01(8) 13_456 1_556
Sn4 La2 La2 133.99(8) 13 1_556
Sn4 La2 La2 49.2(2) . 1_556
Sn4 La2 La2 130.8(2) 1_554 1_556
La2 La2 La2 90.0 13 1_556
La2 La2 La2 90.0 13_455 1_556
La2 La2 La2 90.0 1_455 1_556
La2 La2 La2 90.0 1_655 1_556
Sn2 La2 La2 90.000(1) 13_455 1_554
Sn2 La2 La2 90.0 13 1_554
Sn3 La2 La2 44.0(2) 1_554 1_554
Sn3 La2 La2 136.0(2) . 1_554
Sn4 La2 La2 133.99(8) 13_556 1_554
Sn4 La2 La2 46.01(8) 13_455 1_554
Sn4 La2 La2 133.99(8) 13_456 1_554
Sn4 La2 La2 46.01(8) 13 1_554
Sn4 La2 La2 130.8(2) . 1_554
Sn4 La2 La2 49.2(2) 1_554 1_554
La2 La2 La2 90.000(1) 13 1_554
La2 La2 La2 90.0 13_455 1_554
La2 La2 La2 90.0 1_455 1_554
La2 La2 La2 90.0 1_655 1_554
La2 La2 La2 180.0(6) 1_556 1_554
Sn2 La2 La1 44.9(2) 13_455 .
Sn2 La2 La1 44.9(2) 13 .
Sn3 La2 La1 46.0(2) 1_554 .
Sn3 La2 La1 46.0(2) . .
Sn4 La2 La1 103.4(3) 13_556 .
Sn4 La2 La1 103.4(3) 13_455 .
Sn4 La2 La1 103.4(3) 13_456 .
Sn4 La2 La1 103.4(3) 13 .
Sn4 La2 La1 139.2(2) . .
Sn4 La2 La1 139.2(2) 1_554 .
La2 La2 La1 146.67(19) 13 .
La2 La2 La1 146.67(19) 13_455 .
La2 La2 La1 90.0 1_455 .
La2 La2 La1 90.0 1_655 .
La2 La2 La1 90.0 1_556 .
La2 La2 La1 90.0 1_554 .
La1 Sn1 La1 180.0 1_656 .
La1 Sn1 La1 88.90(7) 1_656 1_556
La1 Sn1 La1 91.10(7) . 1_556
La1 Sn1 La1 91.10(7) 1_656 1_655
La1 Sn1 La1 88.90(7) . 1_655
La1 Sn1 La1 180.0 1_556 1_655
La1 Sn1 Sn2 60.76(10) 1_656 13_556
La1 Sn1 Sn2 119.24(10) . 13_556
La1 Sn1 Sn2 60.76(10) 1_556 13_556
La1 Sn1 Sn2 119.24(10) 1_655 13_556
La1 Sn1 Sn2 119.24(10) 1_656 5_545
La1 Sn1 Sn2 60.76(10) . 5_545
La1 Sn1 Sn2 119.24(10) 1_556 5_545
La1 Sn1 Sn2 60.76(10) 1_655 5_545
Sn2 Sn1 Sn2 180.0(3) 13_556 5_545
La1 Sn1 Sn2 119.24(10) 1_656 13
La1 Sn1 Sn2 60.76(10) . 13
La1 Sn1 Sn2 119.24(10) 1_556 13
La1 Sn1 Sn2 60.76(10) 1_655 13
Sn2 Sn1 Sn2 86.3(3) 13_556 13
Sn2 Sn1 Sn2 93.7(3) 5_545 13
La1 Sn1 Sn2 60.76(10) 1_656 5_546
La1 Sn1 Sn2 119.24(10) . 5_546
La1 Sn1 Sn2 60.76(10) 1_556 5_546
La1 Sn1 Sn2 119.24(10) 1_655 5_546
Sn2 Sn1 Sn2 93.7(3) 13_556 5_546
Sn2 Sn1 Sn2 86.3(3) 5_545 5_546
Sn2 Sn1 Sn2 180.0(3) 13 5_546
La1 Sn1 Sn3 118.02(9) 1_656 9_556
La1 Sn1 Sn3 61.98(8) . 9_556
La1 Sn1 Sn3 61.98(8) 1_556 9_556
La1 Sn1 Sn3 118.02(9) 1_655 9_556
Sn2 Sn1 Sn3 122.74(15) 13_556 9_556
Sn2 Sn1 Sn3 57.26(15) 5_545 9_556
Sn2 Sn1 Sn3 122.74(15) 13 9_556
Sn2 Sn1 Sn3 57.26(15) 5_546 9_556
La1 Sn1 Sn3 61.98(9) 1_656 1_655
La1 Sn1 Sn3 118.02(9) . 1_655
La1 Sn1 Sn3 118.02(8) 1_556 1_655
La1 Sn1 Sn3 61.98(9) 1_655 1_655
Sn2 Sn1 Sn3 57.26(15) 13_556 1_655
Sn2 Sn1 Sn3 122.74(15) 5_545 1_655
Sn2 Sn1 Sn3 57.26(15) 13 1_655
Sn2 Sn1 Sn3 122.74(15) 5_546 1_655
Sn3 Sn1 Sn3 180.0(3) 9_556 1_655
La1 Sn1 Sn3 61.98(9) 1_656 9_656
La1 Sn1 Sn3 118.02(9) . 9_656
La1 Sn1 Sn3 118.02(9) 1_556 9_656
La1 Sn1 Sn3 61.98(9) 1_655 9_656
Sn2 Sn1 Sn3 122.74(15) 13_556 9_656
Sn2 Sn1 Sn3 57.26(15) 5_545 9_656
Sn2 Sn1 Sn3 122.74(15) 13 9_656
Sn2 Sn1 Sn3 57.26(15) 5_546 9_656
Sn3 Sn1 Sn3 84.3(3) 9_556 9_656
Sn3 Sn1 Sn3 95.7(3) 1_655 9_656
La1 Sn1 Sn3 118.02(8) 1_656 .
La1 Sn1 Sn3 61.98(9) . .
La1 Sn1 Sn3 61.98(8) 1_556 .
La1 Sn1 Sn3 118.02(8) 1_655 .
Sn2 Sn1 Sn3 57.26(15) 13_556 .
Sn2 Sn1 Sn3 122.74(15) 5_545 .
Sn2 Sn1 Sn3 57.26(15) 13 .
Sn2 Sn1 Sn3 122.74(15) 5_546 .
Sn3 Sn1 Sn3 95.7(3) 9_556 .
Sn3 Sn1 Sn3 84.3(3) 1_655 .
Sn3 Sn1 Sn3 180.0(3) 9_656 .
La1 Sn1 Sn1 45.55(4) 1_656 1_655
La1 Sn1 Sn1 134.45(4) . 1_655
La1 Sn1 Sn1 134.45(4) 1_556 1_655
La1 Sn1 Sn1 45.55(4) 1_655 1_655
Sn2 Sn1 Sn1 90.0 13_556 1_655
Sn2 Sn1 Sn1 90.0 5_545 1_655
Sn2 Sn1 Sn1 90.0 13 1_655
Sn2 Sn1 Sn1 90.0 5_546 1_655
Sn3 Sn1 Sn1 132.13(14) 9_556 1_655
Sn3 Sn1 Sn1 47.87(14) 1_655 1_655
Sn3 Sn1 Sn1 47.87(14) 9_656 1_655
Sn3 Sn1 Sn1 132.13(14) . 1_655
La1 Sn1 Sn1 134.45(4) 1_656 1_455
La1 Sn1 Sn1 45.55(4) . 1_455
La1 Sn1 Sn1 45.55(4) 1_556 1_455
La1 Sn1 Sn1 134.45(4) 1_655 1_455
Sn2 Sn1 Sn1 90.0 13_556 1_455
Sn2 Sn1 Sn1 90.0 5_545 1_455
Sn2 Sn1 Sn1 90.0 13 1_455
Sn2 Sn1 Sn1 90.0 5_546 1_455
Sn3 Sn1 Sn1 47.87(14) 9_556 1_455
Sn3 Sn1 Sn1 132.13(14) 1_655 1_455
Sn3 Sn1 Sn1 132.13(14) 9_656 1_455
Sn3 Sn1 Sn1 47.87(14) . 1_455
Sn1 Sn1 Sn1 180.0 1_655 1_455
La1 Sn1 Sn1 135.55(4) 1_656 1_554
La1 Sn1 Sn1 44.45(4) . 1_554
La1 Sn1 Sn1 135.55(4) 1_556 1_554
La1 Sn1 Sn1 44.45(4) 1_655 1_554
Sn2 Sn1 Sn1 133.17(17) 13_556 1_554
Sn2 Sn1 Sn1 46.83(17) 5_545 1_554
Sn2 Sn1 Sn1 46.83(17) 13 1_554
Sn2 Sn1 Sn1 133.17(17) 5_546 1_554
Sn3 Sn1 Sn1 90.0 9_556 1_554
Sn3 Sn1 Sn1 90.0 1_655 1_554
Sn3 Sn1 Sn1 90.0 9_656 1_554
Sn3 Sn1 Sn1 90.0 . 1_554
Sn1 Sn1 Sn1 90.0 1_655 1_554
Sn1 Sn1 Sn1 90.0 1_455 1_554
La1 Sn1 Sn1 44.45(4) 1_656 1_556
La1 Sn1 Sn1 135.55(4) . 1_556
La1 Sn1 Sn1 44.45(4) 1_556 1_556
La1 Sn1 Sn1 135.55(4) 1_655 1_556
Sn2 Sn1 Sn1 46.83(17) 13_556 1_556
Sn2 Sn1 Sn1 133.17(17) 5_545 1_556
Sn2 Sn1 Sn1 133.17(17) 13 1_556
Sn2 Sn1 Sn1 46.83(17) 5_546 1_556
Sn3 Sn1 Sn1 90.0 9_556 1_556
Sn3 Sn1 Sn1 90.0 1_655 1_556
Sn3 Sn1 Sn1 90.0 9_656 1_556
Sn3 Sn1 Sn1 90.0 . 1_556
Sn1 Sn1 Sn1 90.0 1_655 1_556
Sn1 Sn1 Sn1 90.0 1_455 1_556
Sn1 Sn1 Sn1 180.0 1_554 1_556
La2 Sn2 La2 89.8(5) 13_455 13
La2 Sn2 Sn3 119.0(3) 13_455 13_556
La2 Sn2 Sn3 59.77(19) 13 13_556
La2 Sn2 Sn3 59.77(19) 13_455 13_455
La2 Sn2 Sn3 119.0(3) 13 13_455
Sn3 Sn2 Sn3 178.5(5) 13_556 13_455
La2 Sn2 Sn3 59.77(19) 13_455 13_456
La2 Sn2 Sn3 119.0(3) 13 13_456
Sn3 Sn2 Sn3 88.89(7) 13_556 13_456
Sn3 Sn2 Sn3 91.09(7) 13_455 13_456
La2 Sn2 Sn3 119.0(3) 13_455 13
La2 Sn2 Sn3 59.77(19) 13 13
Sn3 Sn2 Sn3 91.09(7) 13_556 13
Sn3 Sn2 Sn3 88.89(7) 13_455 13
Sn3 Sn2 Sn3 178.5(5) 13_456 13
La2 Sn2 La1 177.7(4) 13_455 5
La2 Sn2 La1 92.50(17) 13 5
Sn3 Sn2 La1 62.32(16) 13_556 5
Sn3 Sn2 La1 118.9(3) 13_455 5
Sn3 Sn2 La1 118.9(3) 13_456 5
Sn3 Sn2 La1 62.32(16) 13 5
La2 Sn2 La1 92.50(17) 13_455 5_455
La2 Sn2 La1 177.7(4) 13 5_455
Sn3 Sn2 La1 118.9(3) 13_556 5_455
Sn3 Sn2 La1 62.32(16) 13_455 5_455
Sn3 Sn2 La1 62.32(16) 13_456 5_455
Sn3 Sn2 La1 118.9(3) 13 5_455
La1 Sn2 La1 85.2(3) 5 5_455
La2 Sn2 Sn1 121.12(10) 13_455 5_455
La2 Sn2 Sn1 121.12(10) 13 5_455
Sn3 Sn2 Sn1 61.40(16) 13_556 5_455
Sn3 Sn2 Sn1 119.9(3) 13_455 5_455
Sn3 Sn2 Sn1 61.40(16) 13_456 5_455
Sn3 Sn2 Sn1 119.9(3) 13 5_455
La1 Sn2 Sn1 57.5(2) 5 5_455
La1 Sn2 Sn1 57.5(2) 5_455 5_455
La2 Sn2 Sn1 121.12(10) 13_455 5_454
La2 Sn2 Sn1 121.12(10) 13 5_454
Sn3 Sn2 Sn1 119.9(3) 13_556 5_454
Sn3 Sn2 Sn1 61.40(16) 13_455 5_454
Sn3 Sn2 Sn1 119.9(3) 13_456 5_454
Sn3 Sn2 Sn1 61.40(16) 13 5_454
La1 Sn2 Sn1 57.5(2) 5 5_454
La1 Sn2 Sn1 57.5(2) 5_455 5_454
Sn1 Sn2 Sn1 86.3(3) 5_455 5_454
La2 Sn2 Sn4 55.6(2) 13_455 1_554
La2 Sn2 Sn4 55.6(2) 13 1_554
Sn3 Sn2 Sn4 114.9(3) 13_556 1_554
Sn3 Sn2 Sn4 63.8(2) 13_455 1_554
Sn3 Sn2 Sn4 114.9(3) 13_456 1_554
Sn3 Sn2 Sn4 63.8(2) 13 1_554
La1 Sn2 Sn4 125.89(10) 5 1_554
La1 Sn2 Sn4 125.89(10) 5_455 1_554
Sn1 Sn2 Sn4 174.0(3) 5_455 1_554
Sn1 Sn2 Sn4 99.65(17) 5_454 1_554
La2 Sn2 Sn4 55.6(2) 13_455 .
La2 Sn2 Sn4 55.6(2) 13 .
Sn3 Sn2 Sn4 63.8(2) 13_556 .
Sn3 Sn2 Sn4 114.9(3) 13_455 .
Sn3 Sn2 Sn4 63.8(2) 13_456 .
Sn3 Sn2 Sn4 114.9(3) 13 .
La1 Sn2 Sn4 125.89(10) 5 .
La1 Sn2 Sn4 125.89(10) 5_455 .
Sn1 Sn2 Sn4 99.65(17) 5_455 .
Sn1 Sn2 Sn4 174.0(3) 5_454 .
Sn4 Sn2 Sn4 74.4(4) 1_554 .
La2 Sn2 Sn2 45.1(2) 13_455 1_455
La2 Sn2 Sn2 134.9(2) 13 1_455
Sn3 Sn2 Sn2 134.45(4) 13_556 1_455
Sn3 Sn2 Sn2 45.55(4) 13_455 1_455
Sn3 Sn2 Sn2 45.55(4) 13_456 1_455
Sn3 Sn2 Sn2 134.45(4) 13 1_455
La1 Sn2 Sn2 132.62(17) 5 1_455
La1 Sn2 Sn2 47.38(17) 5_455 1_455
Sn1 Sn2 Sn2 90.0 5_455 1_455
Sn1 Sn2 Sn2 90.0 5_454 1_455
Sn4 Sn2 Sn2 90.0 1_554 1_455
Sn4 Sn2 Sn2 90.0 . 1_455
La2 Sn2 Sn2 134.9(2) 13_455 1_655
La2 Sn2 Sn2 45.1(2) 13 1_655
Sn3 Sn2 Sn2 45.55(4) 13_556 1_655
Sn3 Sn2 Sn2 134.45(4) 13_455 1_655
Sn3 Sn2 Sn2 134.45(4) 13_456 1_655
Sn3 Sn2 Sn2 45.55(4) 13 1_655
La1 Sn2 Sn2 47.38(17) 5 1_655
La1 Sn2 Sn2 132.62(17) 5_455 1_655
Sn1 Sn2 Sn2 90.0 5_455 1_655
Sn1 Sn2 Sn2 90.0 5_454 1_655
Sn4 Sn2 Sn2 90.0 1_554 1_655
Sn4 Sn2 Sn2 90.0 . 1_655
Sn2 Sn2 Sn2 180.0(7) 1_455 1_655
La2 Sn2 Sn2 90.0 13_455 1_556
La2 Sn2 Sn2 90.0 13 1_556
Sn3 Sn2 Sn2 44.46(4) 13_556 1_556
Sn3 Sn2 Sn2 135.54(4) 13_455 1_556
Sn3 Sn2 Sn2 44.46(4) 13_456 1_556
Sn3 Sn2 Sn2 135.54(4) 13 1_556
La1 Sn2 Sn2 90.0 5 1_556
La1 Sn2 Sn2 90.0 5_455 1_556
Sn1 Sn2 Sn2 46.83(17) 5_455 1_556
Sn1 Sn2 Sn2 133.17(17) 5_454 1_556
Sn4 Sn2 Sn2 127.18(18) 1_554 1_556
Sn4 Sn2 Sn2 52.82(18) . 1_556
Sn2 Sn2 Sn2 90.0 1_455 1_556
Sn2 Sn2 Sn2 90.0 1_655 1_556
La2 Sn2 Sn2 90.0 13_455 1_554
La2 Sn2 Sn2 90.0 13 1_554
Sn3 Sn2 Sn2 135.54(4) 13_556 1_554
Sn3 Sn2 Sn2 44.46(4) 13_455 1_554
Sn3 Sn2 Sn2 135.54(4) 13_456 1_554
Sn3 Sn2 Sn2 44.46(4) 13 1_554
La1 Sn2 Sn2 90.0 5 1_554
La1 Sn2 Sn2 90.0 5_455 1_554
Sn1 Sn2 Sn2 133.17(17) 5_455 1_554
Sn1 Sn2 Sn2 46.83(17) 5_454 1_554
Sn4 Sn2 Sn2 52.82(18) 1_554 1_554
Sn4 Sn2 Sn2 127.18(18) . 1_554
Sn2 Sn2 Sn2 90.0 1_455 1_554
Sn2 Sn2 Sn2 90.0 1_655 1_554
Sn2 Sn2 Sn2 180.0(7) 1_556 1_554
La2 Sn2 Sn2 135.1(2) 13_455 9_565
La2 Sn2 Sn2 135.1(2) 13 9_565
Sn3 Sn2 Sn2 90.8(2) 13_556 9_565
Sn3 Sn2 Sn2 90.8(2) 13_455 9_565
Sn3 Sn2 Sn2 90.8(2) 13_456 9_565
Sn3 Sn2 Sn2 90.8(2) 13 9_565
La1 Sn2 Sn2 42.62(17) 5 9_565
La1 Sn2 Sn2 42.62(17) 5_455 9_565
Sn1 Sn2 Sn2 43.17(17) 5_455 9_565
Sn1 Sn2 Sn2 43.17(17) 5_454 9_565
Sn4 Sn2 Sn2 142.82(18) 1_554 9_565
Sn4 Sn2 Sn2 142.82(18) . 9_565
Sn2 Sn2 Sn2 90.0 1_455 9_565
Sn2 Sn2 Sn2 90.0 1_655 9_565
Sn2 Sn2 Sn2 90.0 1_556 9_565
Sn2 Sn2 Sn2 90.0 1_554 9_565
La2 Sn3 La2 91.9(5) 1_556 .
La2 Sn3 Sn2 59.7(2) 1_556 13_556
La2 Sn3 Sn2 121.5(3) . 13_556
La2 Sn3 Sn2 121.5(3) 1_556 13_455
La2 Sn3 Sn2 59.7(2) . 13_455
Sn2 Sn3 Sn2 178.5(5) 13_556 13_455
La2 Sn3 Sn2 59.7(2) 1_556 13_456
La2 Sn3 Sn2 121.5(3) . 13_456
Sn2 Sn3 Sn2 88.89(7) 13_556 13_456
Sn2 Sn3 Sn2 91.09(7) 13_455 13_456
La2 Sn3 Sn2 121.5(3) 1_556 13
La2 Sn3 Sn2 59.7(2) . 13
Sn2 Sn3 Sn2 91.09(7) 13_556 13
Sn2 Sn3 Sn2 88.89(7) 13_455 13
Sn2 Sn3 Sn2 178.5(5) 13_456 13
La2 Sn3 Sn1 121.03(11) 1_556 1_455
La2 Sn3 Sn1 121.03(11) . 1_455
Sn2 Sn3 Sn1 117.4(2) 13_556 1_455
Sn2 Sn3 Sn1 61.34(19) 13_455 1_455
Sn2 Sn3 Sn1 61.34(19) 13_456 1_455
Sn2 Sn3 Sn1 117.4(2) 13 1_455
La2 Sn3 Sn1 121.03(11) 1_556 .
La2 Sn3 Sn1 121.03(11) . .
Sn2 Sn3 Sn1 61.34(19) 13_556 .
Sn2 Sn3 Sn1 117.4(2) 13_455 .
Sn2 Sn3 Sn1 117.4(2) 13_456 .
Sn2 Sn3 Sn1 61.34(19) 13 .
Sn1 Sn3 Sn1 84.3(3) 1_455 .
La2 Sn3 La1 176.7(3) 1_556 .
La2 Sn3 La1 91.35(18) . .
Sn2 Sn3 La1 118.3(3) 13_556 .
Sn2 Sn3 La1 60.42(19) 13_455 .
Sn2 Sn3 La1 118.3(3) 13_456 .
Sn2 Sn3 La1 60.42(19) 13 .
Sn1 Sn3 La1 56.96(16) 1_455 .
Sn1 Sn3 La1 56.96(16) . .
La2 Sn3 La1 91.35(18) 1_556 1_556
La2 Sn3 La1 176.7(3) . 1_556
Sn2 Sn3 La1 60.42(19) 13_556 1_556
Sn2 Sn3 La1 118.3(3) 13_455 1_556
Sn2 Sn3 La1 60.42(19) 13_456 1_556
Sn2 Sn3 La1 118.3(3) 13 1_556
Sn1 Sn3 La1 56.96(16) 1_455 1_556
Sn1 Sn3 La1 56.96(16) . 1_556
La1 Sn3 La1 85.4(3) . 1_556
La2 Sn3 Sn4 56.3(2) 1_556 13_556
La2 Sn3 Sn4 56.3(2) . 13_556
Sn2 Sn3 Sn4 65.7(2) 13_556 13_556
Sn2 Sn3 Sn4 115.6(3) 13_455 13_556
Sn2 Sn3 Sn4 115.6(3) 13_456 13_556
Sn2 Sn3 Sn4 65.7(2) 13 13_556
Sn1 Sn3 Sn4 174.9(3) 1_455 13_556
Sn1 Sn3 Sn4 100.83(16) . 13_556
La1 Sn3 Sn4 125.93(9) . 13_556
La1 Sn3 Sn4 125.93(9) 1_556 13_556
La2 Sn3 Sn4 56.3(2) 1_556 13_456
La2 Sn3 Sn4 56.3(2) . 13_456
Sn2 Sn3 Sn4 115.6(3) 13_556 13_456
Sn2 Sn3 Sn4 65.7(2) 13_455 13_456
Sn2 Sn3 Sn4 65.7(2) 13_456 13_456
Sn2 Sn3 Sn4 115.6(3) 13 13_456
Sn1 Sn3 Sn4 100.83(16) 1_455 13_456
Sn1 Sn3 Sn4 174.9(3) . 13_456
La1 Sn3 Sn4 125.93(9) . 13_456
La1 Sn3 Sn4 125.93(9) 1_556 13_456
Sn4 Sn3 Sn4 74.1(4) 13_556 13_456
La2 Sn3 Sn3 90.0 1_556 1_655
La2 Sn3 Sn3 90.0 . 1_655
Sn2 Sn3 Sn3 45.55(4) 13_556 1_655
Sn2 Sn3 Sn3 134.45(4) 13_455 1_655
Sn2 Sn3 Sn3 134.45(4) 13_456 1_655
Sn2 Sn3 Sn3 45.55(4) 13 1_655
Sn1 Sn3 Sn3 132.13(14) 1_455 1_655
Sn1 Sn3 Sn3 47.87(14) . 1_655
La1 Sn3 Sn3 90.0 . 1_655
La1 Sn3 Sn3 90.0 1_556 1_655
Sn4 Sn3 Sn3 52.96(18) 13_556 1_655
Sn4 Sn3 Sn3 127.04(18) 13_456 1_655
La2 Sn3 Sn3 90.0 1_556 1_455
La2 Sn3 Sn3 90.0 . 1_455
Sn2 Sn3 Sn3 134.45(4) 13_556 1_455
Sn2 Sn3 Sn3 45.55(4) 13_455 1_455
Sn2 Sn3 Sn3 45.55(4) 13_456 1_455
Sn2 Sn3 Sn3 134.45(4) 13 1_455
Sn1 Sn3 Sn3 47.87(14) 1_455 1_455
Sn1 Sn3 Sn3 132.13(14) . 1_455
La1 Sn3 Sn3 90.0 . 1_455
La1 Sn3 Sn3 90.0 1_556 1_455
Sn4 Sn3 Sn3 127.04(18) 13_556 1_455
Sn4 Sn3 Sn3 52.96(18) 13_456 1_455
Sn3 Sn3 Sn3 180.0(6) 1_655 1_455
La2 Sn3 Sn3 136.0(2) 1_556 1_554
La2 Sn3 Sn3 44.0(2) . 1_554
Sn2 Sn3 Sn3 135.54(4) 13_556 1_554
Sn2 Sn3 Sn3 44.46(4) 13_455 1_554
Sn2 Sn3 Sn3 135.54(4) 13_456 1_554
Sn2 Sn3 Sn3 44.46(4) 13 1_554
Sn1 Sn3 Sn3 90.0 1_455 1_554
Sn1 Sn3 Sn3 90.0 . 1_554
La1 Sn3 Sn3 47.32(14) . 1_554
La1 Sn3 Sn3 132.68(14) 1_556 1_554
Sn4 Sn3 Sn3 90.0 13_556 1_554
Sn4 Sn3 Sn3 90.0 13_456 1_554
Sn3 Sn3 Sn3 90.0 1_655 1_554
Sn3 Sn3 Sn3 90.0 1_455 1_554
La2 Sn3 Sn3 44.0(2) 1_556 1_556
La2 Sn3 Sn3 136.0(2) . 1_556
Sn2 Sn3 Sn3 44.46(4) 13_556 1_556
Sn2 Sn3 Sn3 135.54(4) 13_455 1_556
Sn2 Sn3 Sn3 44.46(4) 13_456 1_556
Sn2 Sn3 Sn3 135.54(4) 13 1_556
Sn1 Sn3 Sn3 90.0 1_455 1_556
Sn1 Sn3 Sn3 90.0 . 1_556
La1 Sn3 Sn3 132.68(14) . 1_556
La1 Sn3 Sn3 47.32(14) 1_556 1_556
Sn4 Sn3 Sn3 90.000(1) 13_556 1_556
Sn4 Sn3 Sn3 90.0 13_456 1_556
Sn3 Sn3 Sn3 90.0 1_655 1_556
Sn3 Sn3 Sn3 90.0 1_455 1_556
Sn3 Sn3 Sn3 180.0(3) 1_554 1_556
La2 Sn3 Sn4 46.0(2) 1_556 .
La2 Sn3 Sn4 46.0(2) . .
Sn2 Sn3 Sn4 90.8(2) 13_556 .
Sn2 Sn3 Sn4 90.8(2) 13_455 .
Sn2 Sn3 Sn4 90.8(2) 13_456 .
Sn2 Sn3 Sn4 90.8(2) 13 .
Sn1 Sn3 Sn4 137.87(14) 1_455 .
Sn1 Sn3 Sn4 137.87(14) . .
La1 Sn3 Sn4 137.32(14) . .
La1 Sn3 Sn4 137.32(14) 1_556 .
Sn4 Sn3 Sn4 37.04(18) 13_556 .
Sn4 Sn3 Sn4 37.04(18) 13_456 .
Sn3 Sn3 Sn4 90.0 1_655 .
Sn3 Sn3 Sn4 90.0 1_455 .
Sn3 Sn3 Sn4 90.0 1_554 .
Sn3 Sn3 Sn4 90.0 1_556 .
La2 Sn3 Sn3 134.0(2) 1_556 9_556
La2 Sn3 Sn3 134.0(2) . 9_556
Sn2 Sn3 Sn3 89.2(2) 13_556 9_556
Sn2 Sn3 Sn3 89.2(2) 13_455 9_556
Sn2 Sn3 Sn3 89.2(2) 13_456 9_556
Sn2 Sn3 Sn3 89.2(2) 13 9_556
Sn1 Sn3 Sn3 42.13(14) 1_455 9_556
Sn1 Sn3 Sn3 42.13(14) . 9_556
La1 Sn3 Sn3 42.68(14) . 9_556
La1 Sn3 Sn3 42.68(14) 1_556 9_556
Sn4 Sn3 Sn3 142.96(18) 13_556 9_556
Sn4 Sn3 Sn3 142.96(18) 13_456 9_556
Sn3 Sn3 Sn3 90.0 1_655 9_556
Sn3 Sn3 Sn3 90.0 1_455 9_556
Sn3 Sn3 Sn3 90.0 1_554 9_556
Sn3 Sn3 Sn3 90.0 1_556 9_556
Sn4 Sn3 Sn3 180.0 . 9_556
Sn4 Sn4 Sn4 99.8(9) 13_456 13_556
Sn4 Sn4 La2 132.1(4) 13_456 13_556
Sn4 Sn4 La2 68.1(2) 13_556 13_556
Sn4 Sn4 La2 68.1(2) 13_456 13_455
Sn4 Sn4 La2 132.1(4) 13_556 13_455
La2 Sn4 La2 153.2(7) 13_556 13_455
Sn4 Sn4 La2 68.1(2) 13_456 13_456
Sn4 Sn4 La2 132.1(4) 13_556 13_456
La2 Sn4 La2 85.89(16) 13_556 13_456
La2 Sn4 La2 87.97(17) 13_455 13_456
Sn4 Sn4 La2 132.1(4) 13_456 13
Sn4 Sn4 La2 68.1(2) 13_556 13
La2 Sn4 La2 87.97(17) 13_556 13
La2 Sn4 La2 85.89(16) 13_455 13
La2 Sn4 La2 153.2(7) 13_456 13
Sn4 Sn4 La2 60.8(4) 13_456 .
Sn4 Sn4 La2 60.8(4) 13_556 .
La2 Sn4 La2 129.0(3) 13_556 .
La2 Sn4 La2 73.8(3) 13_455 .
La2 Sn4 La2 129.0(3) 13_456 .
La2 Sn4 La2 73.8(3) 13 .
Sn4 Sn4 La2 60.8(4) 13_456 1_556
Sn4 Sn4 La2 60.8(4) 13_556 1_556
La2 Sn4 La2 73.8(3) 13_556 1_556
La2 Sn4 La2 129.0(3) 13_455 1_556
La2 Sn4 La2 73.8(3) 13_456 1_556
La2 Sn4 La2 129.0(3) 13 1_556
La2 Sn4 La2 81.6(4) . 1_556
Sn4 Sn4 Sn3 167.1(6) 13_456 13_556
Sn4 Sn4 Sn3 93.0(3) 13_556 13_556
La2 Sn4 Sn3 53.5(2) 13_556 13_556
La2 Sn4 Sn3 103.0(4) 13_455 13_556
La2 Sn4 Sn3 103.0(4) 13_456 13_556
La2 Sn4 Sn3 53.5(2) 13 13_556
La2 Sn4 Sn3 127.18(11) . 13_556
La2 Sn4 Sn3 127.18(11) 1_556 13_556
Sn4 Sn4 Sn3 93.0(3) 13_456 13_456
Sn4 Sn4 Sn3 167.1(6) 13_556 13_456
La2 Sn4 Sn3 103.0(4) 13_556 13_456
La2 Sn4 Sn3 53.5(2) 13_455 13_456
La2 Sn4 Sn3 53.5(2) 13_456 13_456
La2 Sn4 Sn3 103.0(4) 13 13_456
La2 Sn4 Sn3 127.18(11) . 13_456
La2 Sn4 Sn3 127.18(11) 1_556 13_456
Sn3 Sn4 Sn3 74.1(4) 13_556 13_456
Sn4 Sn4 Sn2 120.9(3) 13_456 1_556
Sn4 Sn4 Sn2 120.9(3) 13_556 1_556
La2 Sn4 Sn2 52.8(2) 13_556 1_556
La2 Sn4 Sn2 103.6(4) 13_455 1_556
La2 Sn4 Sn2 52.8(2) 13_456 1_556
La2 Sn4 Sn2 103.6(4) 13 1_556
La2 Sn4 Sn2 176.4(3) . 1_556
La2 Sn4 Sn2 102.0(2) 1_556 1_556
Sn3 Sn4 Sn2 50.5(2) 13_556 1_556
Sn3 Sn4 Sn2 50.5(2) 13_456 1_556
Sn4 Sn4 Sn2 120.9(3) 13_456 .
Sn4 Sn4 Sn2 120.9(3) 13_556 .
La2 Sn4 Sn2 103.6(4) 13_556 .
La2 Sn4 Sn2 52.8(2) 13_455 .
La2 Sn4 Sn2 103.6(4) 13_456 .
La2 Sn4 Sn2 52.8(2) 13 .
La2 Sn4 Sn2 102.0(2) . .
La2 Sn4 Sn2 176.4(3) 1_556 .
Sn3 Sn4 Sn2 50.5(2) 13_556 .
Sn3 Sn4 Sn2 50.5(2) 13_456 .
Sn2 Sn4 Sn2 74.4(4) 1_556 .
Sn4 Sn4 Sn4 139.9(5) 13_456 1_655
Sn4 Sn4 Sn4 40.1(5) 13_556 1_655
La2 Sn4 Sn4 47.06(8) 13_556 1_655
La2 Sn4 Sn4 132.94(8) 13_455 1_655
La2 Sn4 Sn4 132.94(8) 13_456 1_655
La2 Sn4 Sn4 47.06(8) 13 1_655
La2 Sn4 Sn4 90.0 . 1_655
La2 Sn4 Sn4 90.0 1_556 1_655
Sn3 Sn4 Sn4 52.96(18) 13_556 1_655
Sn3 Sn4 Sn4 127.04(18) 13_456 1_655
Sn2 Sn4 Sn4 90.0 1_556 1_655
Sn2 Sn4 Sn4 90.0 . 1_655
Sn4 Sn4 Sn4 40.1(5) 13_456 1_455
Sn4 Sn4 Sn4 139.9(5) 13_556 1_455
La2 Sn4 Sn4 132.94(8) 13_556 1_455
La2 Sn4 Sn4 47.06(8) 13_455 1_455
La2 Sn4 Sn4 47.06(8) 13_456 1_455
La2 Sn4 Sn4 132.94(8) 13 1_455
La2 Sn4 Sn4 90.0 . 1_455
La2 Sn4 Sn4 90.0 1_556 1_455
Sn3 Sn4 Sn4 127.04(18) 13_556 1_455
Sn3 Sn4 Sn4 52.96(18) 13_456 1_455
Sn2 Sn4 Sn4 90.0 1_556 1_455
Sn2 Sn4 Sn4 90.0 . 1_455
Sn4 Sn4 Sn4 180.0(8) 1_655 1_455
Sn4 Sn4 Sn4 90.0 13_456 1_554
Sn4 Sn4 Sn4 90.0 13_556 1_554
La2 Sn4 Sn4 133.99(8) 13_556 1_554
La2 Sn4 Sn4 46.01(8) 13_455 1_554
La2 Sn4 Sn4 133.99(8) 13_456 1_554
La2 Sn4 Sn4 46.01(8) 13 1_554
La2 Sn4 Sn4 49.2(2) . 1_554
La2 Sn4 Sn4 130.8(2) 1_556 1_554
Sn3 Sn4 Sn4 90.0 13_556 1_554
Sn3 Sn4 Sn4 90.0 13_456 1_554
Sn2 Sn4 Sn4 127.18(18) 1_556 1_554
Sn2 Sn4 Sn4 52.82(18) . 1_554
Sn4 Sn4 Sn4 90.000(1) 1_655 1_554
Sn4 Sn4 Sn4 90.0 1_455 1_554
Sn4 Sn4 Sn4 90.0 13_456 1_556
Sn4 Sn4 Sn4 90.0 13_556 1_556
La2 Sn4 Sn4 46.01(8) 13_556 1_556
La2 Sn4 Sn4 133.99(8) 13_455 1_556
La2 Sn4 Sn4 46.01(8) 13_456 1_556
La2 Sn4 Sn4 133.99(8) 13 1_556
La2 Sn4 Sn4 130.8(2) . 1_556
La2 Sn4 Sn4 49.2(2) 1_556 1_556
Sn3 Sn4 Sn4 90.0 13_556 1_556
Sn3 Sn4 Sn4 90.0 13_456 1_556
Sn2 Sn4 Sn4 52.82(18) 1_556 1_556
Sn2 Sn4 Sn4 127.18(18) . 1_556
Sn4 Sn4 Sn4 90.000(1) 1_655 1_556
Sn4 Sn4 Sn4 90.0 1_455 1_556
Sn4 Sn4 Sn4 180.0(4) 1_554 1_556
Sn4 Sn4 Sn3 49.9(5) 13_456 .
Sn4 Sn4 Sn3 49.9(5) 13_556 .
La2 Sn4 Sn3 103.4(3) 13_556 .
La2 Sn4 Sn3 103.4(3) 13_455 .
La2 Sn4 Sn3 103.4(3) 13_456 .
La2 Sn4 Sn3 103.4(3) 13 .
La2 Sn4 Sn3 40.8(2) . .
La2 Sn4 Sn3 40.8(2) 1_556 .
Sn3 Sn4 Sn3 142.96(18) 13_556 .
Sn3 Sn4 Sn3 142.96(18) 13_456 .
Sn2 Sn4 Sn3 142.82(18) 1_556 .
Sn2 Sn4 Sn3 142.82(18) . .
Sn4 Sn4 Sn3 90.0 1_655 .
Sn4 Sn4 Sn3 90.0 1_455 .
Sn4 Sn4 Sn3 90.0 1_554 .
Sn4 Sn4 Sn3 90.0 1_556 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
La1 Sn1 3.279(2) 1_454
La1 Sn1 3.279(2) .
La1 Sn1 3.279(2) 1_455
La1 Sn1 3.279(2) 1_554
La1 Sn2 3.391(11) 13
La1 Sn2 3.391(11) 5_445
La1 Sn2 3.391(11) 13_455
La1 Sn2 3.391(11) 5_545
La1 Sn3 3.453(9) 9
La1 Sn3 3.453(9) .
La1 Sn3 3.453(9) 9_556
La1 Sn3 3.453(9) 1_554
La1 La1 4.592(4) 1_655
La1 La1 4.592(4) 1_455
La1 La1 4.681(5) 1_554
La1 La1 4.681(5) 1_556
La1 La2 4.801(13) 9
La1 La2 4.801(13) .
La2 Sn2 3.254(13) 13_455
La2 Sn2 3.254(13) 13
La2 Sn3 3.256(13) 1_554
La2 Sn3 3.256(13) .
La2 Sn4 3.370(5) 13_556
La2 Sn4 3.370(5) 13_455
La2 Sn4 3.370(5) 13_456
La2 Sn4 3.370(5) 13
La2 Sn4 3.583(15) .
La2 Sn4 3.583(15) 1_554
La2 La2 4.18(2) 13
La2 La2 4.18(2) 13_455
La2 La2 4.592(4) 1_455
La2 La2 4.592(4) 1_655
La2 La2 4.681(5) 1_556
La2 La2 4.681(5) 1_554
Sn1 La1 3.279(2) 1_656
Sn1 La1 3.279(2) 1_556
Sn1 La1 3.279(2) 1_655
Sn1 Sn2 3.421(11) 13_556
Sn1 Sn2 3.421(11) 5_545
Sn1 Sn2 3.421(11) 13
Sn1 Sn2 3.421(11) 5_546
Sn1 Sn3 3.423(9) 9_556
Sn1 Sn3 3.423(9) 1_655
Sn1 Sn3 3.423(9) 9_656
Sn1 Sn3 3.423(9) .
Sn1 Sn1 4.592(4) 1_655
Sn1 Sn1 4.592(4) 1_455
Sn1 Sn1 4.681(5) 1_554
Sn1 Sn1 4.681(4) 1_556
Sn2 La2 3.254(13) 13_455
Sn2 La2 3.254(13) 13
Sn2 Sn3 3.279(2) 13_556
Sn2 Sn3 3.279(2) 13_455
Sn2 Sn3 3.279(2) 13_456
Sn2 Sn3 3.279(2) 13
Sn2 La1 3.391(11) 5
Sn2 La1 3.391(11) 5_455
Sn2 Sn1 3.421(11) 5_455
Sn2 Sn1 3.421(11) 5_454
Sn2 Sn4 3.873(16) 1_554
Sn2 Sn4 3.873(16) .
Sn2 Sn2 4.592(4) 1_455
Sn2 Sn2 4.592(4) 1_655
Sn2 Sn2 4.681(5) 1_556
Sn2 Sn2 4.681(5) 1_554
Sn2 Sn2 4.99(3) 9_565
Sn3 La2 3.256(13) 1_556
Sn3 Sn2 3.279(2) 13_556
Sn3 Sn2 3.279(2) 13_455
Sn3 Sn2 3.279(2) 13_456
Sn3 Sn2 3.279(2) 13
Sn3 Sn1 3.423(9) 1_455
Sn3 La1 3.453(9) 1_556
Sn3 Sn4 3.812(16) 13_556
Sn3 Sn4 3.812(16) 13_456
Sn3 Sn3 4.592(4) 1_655
Sn3 Sn3 4.592(4) 1_455
Sn3 Sn3 4.681(5) 1_554
Sn3 Sn3 4.681(4) 1_556
Sn3 Sn4 4.98(2) .
Sn3 Sn3 5.08(2) 9_556
Sn4 Sn4 3.00(2) 13_456
Sn4 Sn4 3.00(2) 13_556
Sn4 La2 3.370(5) 13_556
Sn4 La2 3.370(5) 13_455
Sn4 La2 3.370(5) 13_456
Sn4 La2 3.370(5) 13
Sn4 La2 3.583(15) 1_556
Sn4 Sn3 3.812(16) 13_556
Sn4 Sn3 3.812(16) 13_456
Sn4 Sn2 3.873(16) 1_556
Sn4 Sn4 4.592(4) 1_655
Sn4 Sn4 4.592(4) 1_455
Sn4 Sn4 4.681(5) 1_554
Sn4 Sn4 4.681(4) 1_556
