#------------------------------------------------------------------------------
#$Date: 2021-06-10 11:30:42 +0300 (Thu, 10 Jun 2021) $
#$Revision: 266354 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/32/1563286.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1563286
loop_
_publ_author_name
'Lei, Xiao-Wu'
_publ_section_title
;
 K2Mg5−xSn3 and K3Mg18Tt11 (Tt=Sn, pb) with two types of Mg--Sn/Pb
 frameworks
;
_journal_issue                   4
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              852
_journal_page_last               858
_journal_paper_doi               10.1016/j.jssc.2011.02.003
_journal_volume                  184
_journal_year                    2011
_chemical_formula_sum            'K2 Mg4.72 Sn3'
_chemical_formula_weight         549.01
_space_group_IT_number           139
_space_group_name_Hall           '-I 4 2'
_space_group_name_H-M_alt        'I 4/m m m'
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_H-M   'I 4/m m m'
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   4.9461(4)
_cell_length_b                   4.9461(4)
_cell_length_c                   23.403(3)
_cell_measurement_temperature    293(2)
_cell_volume                     572.53(10)
_computing_cell_refinement       'CrystalClear (Rigaku Corp., 2000)'
_computing_data_collection       'CrystalClear (Rigaku Corp., 2000)'
_computing_data_reduction        'CrystalClear (Rigaku Corp., 2000)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'Mercury70 (2x2 bin mode)'
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0353
_diffrn_reflns_av_sigmaI/netI    0.0198
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            2067
_diffrn_reflns_theta_full        27.44
_diffrn_reflns_theta_max         27.44
_diffrn_reflns_theta_min         3.48
_exptl_absorpt_coefficient_mu    7.409
_exptl_absorpt_correction_T_max  0.4761
_exptl_absorpt_correction_T_min  0.0712
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Gray
_exptl_crystal_density_diffrn    3.185
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       sheet
_exptl_crystal_F_000             489
_exptl_crystal_size_max          0.4000
_exptl_crystal_size_mid          0.4000
_exptl_crystal_size_min          0.1000
_refine_diff_density_max         0.928
_refine_diff_density_min         -1.121
_refine_diff_density_rms         0.148
_refine_ls_extinction_coef       0.0012(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.107
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     16
_refine_ls_number_reflns         240
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.107
_refine_ls_R_factor_all          0.0245
_refine_ls_R_factor_gt           0.0241
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0375P)²+2.1698P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0617
_refine_ls_wR_factor_ref         0.0620
_reflns_number_gt                236
_reflns_number_total             240
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            JSSC-2011-184-852.CIF
_cod_data_source_block           K2Mg4.72Sn3
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the built-in table derived
from the CIF Core dictionary named 'cif_core.dic' version 2.4.5 last
updated on 2014-11-21.

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 
;
_cod_original_cell_volume        572.52(10)
_cod_original_sg_symbol_H-M      I4/mmm
_cod_database_code               1563286
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-y, x, z'
'y, -x, z'
'-x, y, -z'
'x, -y, -z'
'y, x, -z'
'-y, -x, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-y+1/2, x+1/2, z+1/2'
'y+1/2, -x+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'y+1/2, x+1/2, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'y, -x, -z'
'-y, x, -z'
'x, -y, z'
'-x, y, z'
'-y, -x, z'
'y, x, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'-y+1/2, x+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
'-y+1/2, -x+1/2, z+1/2'
'y+1/2, x+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
K1 K 0.0000 0.0000 0.19932(9) 0.0270(5) Uani 1 8 d S . .
Mg1 Mg 0.5000 0.0000 0.07880(8) 0.0243(5) Uani 1 4 d S . .
Mg2 Mg 0.5000 0.5000 0.0000 0.0268(13) Uani 0.72 16 d SP . .
Sn1 Sn 0.0000 0.0000 0.0000 0.0158(3) Uani 1 16 d S . .
Sn2 Sn 0.5000 0.5000 0.14090(3) 0.0227(3) Uani 1 8 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Sn2 K1 Mg1 138.76(3) 25 3_545
Sn2 K1 Mg1 138.76(3) 25 1_455
Mg1 K1 Mg1 55.57(4) 3_545 1_455
Sn2 K1 Mg1 138.76(3) 25 3
Mg1 K1 Mg1 82.49(6) 3_545 3
Mg1 K1 Mg1 55.57(4) 1_455 3
Sn2 K1 Mg1 138.76(3) 25 .
Mg1 K1 Mg1 55.57(4) 3_545 .
Mg1 K1 Mg1 82.49(6) 1_455 .
Mg1 K1 Mg1 55.57(4) 3 .
Sn2 K1 Sn2 111.35(3) 25 1_445
Mg1 K1 Sn2 44.933(16) 3_545 1_445
Mg1 K1 Sn2 44.933(16) 1_455 1_445
Mg1 K1 Sn2 99.23(4) 3 1_445
Mg1 K1 Sn2 99.23(4) . 1_445
Sn2 K1 Sn2 111.35(3) 25 .
Mg1 K1 Sn2 99.23(4) 3_545 .
Mg1 K1 Sn2 99.23(4) 1_455 .
Mg1 K1 Sn2 44.933(16) 3 .
Mg1 K1 Sn2 44.933(16) . .
Sn2 K1 Sn2 137.30(6) 1_445 .
Sn2 K1 Sn2 111.35(3) 25 1_455
Mg1 K1 Sn2 99.23(4) 3_545 1_455
Mg1 K1 Sn2 44.933(16) 1_455 1_455
Mg1 K1 Sn2 44.933(16) 3 1_455
Mg1 K1 Sn2 99.23(4) . 1_455
Sn2 K1 Sn2 82.38(2) 1_445 1_455
Sn2 K1 Sn2 82.38(2) . 1_455
Sn2 K1 Sn2 111.35(3) 25 1_545
Mg1 K1 Sn2 44.933(16) 3_545 1_545
Mg1 K1 Sn2 99.23(4) 1_455 1_545
Mg1 K1 Sn2 99.23(4) 3 1_545
Mg1 K1 Sn2 44.933(16) . 1_545
Sn2 K1 Sn2 82.38(2) 1_445 1_545
Sn2 K1 Sn2 82.38(2) . 1_545
Sn2 K1 Sn2 137.30(6) 1_455 1_545
Sn2 K1 K1 55.85(5) 25 25
Mg1 K1 K1 143.89(3) 3_545 25
Mg1 K1 K1 143.89(3) 1_455 25
Mg1 K1 K1 92.08(3) 3 25
Mg1 K1 K1 92.08(3) . 25
Sn2 K1 K1 167.20(7) 1_445 25
Sn2 K1 K1 55.50(2) . 25
Sn2 K1 K1 101.792(6) 1_455 25
Sn2 K1 K1 101.792(6) 1_545 25
Sn2 K1 K1 55.85(5) 25 25_445
Mg1 K1 K1 92.08(3) 3_545 25_445
Mg1 K1 K1 92.08(3) 1_455 25_445
Mg1 K1 K1 143.89(3) 3 25_445
Mg1 K1 K1 143.89(3) . 25_445
Sn2 K1 K1 55.50(2) 1_445 25_445
Sn2 K1 K1 167.20(7) . 25_445
Sn2 K1 K1 101.792(6) 1_455 25_445
Sn2 K1 K1 101.792(6) 1_545 25_445
K1 K1 K1 111.71(9) 25 25_445
Sn2 K1 K1 55.85(5) 25 25_545
Mg1 K1 K1 92.08(3) 3_545 25_545
Mg1 K1 K1 143.89(3) 1_455 25_545
Mg1 K1 K1 143.89(3) 3 25_545
Mg1 K1 K1 92.08(3) . 25_545
Sn2 K1 K1 101.792(6) 1_445 25_545
Sn2 K1 K1 101.792(6) . 25_545
Sn2 K1 K1 167.20(7) 1_455 25_545
Sn2 K1 K1 55.50(2) 1_545 25_545
K1 K1 K1 71.63(4) 25 25_545
K1 K1 K1 71.63(4) 25_445 25_545
Sn2 Mg1 Sn2 119.12(7) . 1_545
Sn2 Mg1 Mg2 173.73(6) . 1_545
Sn2 Mg1 Mg2 67.153(14) 1_545 1_545
Sn2 Mg1 Sn1 107.630(9) . .
Sn2 Mg1 Sn1 107.630(9) 1_545 .
Mg2 Mg1 Sn1 69.06(3) 1_545 .
Sn2 Mg1 Mg2 67.153(14) . .
Sn2 Mg1 Mg2 173.73(6) 1_545 .
Mg2 Mg1 Mg2 106.58(6) 1_545 .
Sn1 Mg1 Mg2 69.06(3) . .
Sn2 Mg1 Sn1 107.630(9) . 1_655
Sn2 Mg1 Sn1 107.630(9) 1_545 1_655
Mg2 Mg1 Sn1 69.06(3) 1_545 1_655
Sn1 Mg1 Sn1 106.58(6) . 1_655
Mg2 Mg1 Sn1 69.06(3) . 1_655
Sn2 Mg1 Mg1 52.437(16) . 3_655
Sn2 Mg1 Mg1 127.563(16) 1_545 3_655
Mg2 Mg1 Mg1 124.531(15) 1_545 3_655
Sn1 Mg1 Mg1 124.531(15) . 3_655
Mg2 Mg1 Mg1 55.469(15) . 3_655
Sn1 Mg1 Mg1 55.469(15) 1_655 3_655
Sn2 Mg1 Mg1 127.563(16) . 3_545
Sn2 Mg1 Mg1 52.437(16) 1_545 3_545
Mg2 Mg1 Mg1 55.469(15) 1_545 3_545
Sn1 Mg1 Mg1 55.469(15) . 3_545
Mg2 Mg1 Mg1 124.531(15) . 3_545
Sn1 Mg1 Mg1 124.531(15) 1_655 3_545
Mg1 Mg1 Mg1 180.0 3_655 3_545
Sn2 Mg1 Mg1 127.563(16) . 3_645
Sn2 Mg1 Mg1 52.437(16) 1_545 3_645
Mg2 Mg1 Mg1 55.469(15) 1_545 3_645
Sn1 Mg1 Mg1 124.531(15) . 3_645
Mg2 Mg1 Mg1 124.531(15) . 3_645
Sn1 Mg1 Mg1 55.469(15) 1_655 3_645
Mg1 Mg1 Mg1 90.0 3_655 3_645
Mg1 Mg1 Mg1 90.0 3_545 3_645
Sn2 Mg1 Mg1 52.437(16) . 3
Sn2 Mg1 Mg1 127.563(16) 1_545 3
Mg2 Mg1 Mg1 124.531(15) 1_545 3
Sn1 Mg1 Mg1 55.469(15) . 3
Mg2 Mg1 Mg1 55.469(15) . 3
Sn1 Mg1 Mg1 124.531(15) 1_655 3
Mg1 Mg1 Mg1 90.0 3_655 3
Mg1 Mg1 Mg1 90.0 3_545 3
Mg1 Mg1 Mg1 180.0 3_645 3
Sn2 Mg1 Mg1 120.44(4) . 17_655
Sn2 Mg1 Mg1 120.44(4) 1_545 17_655
Mg2 Mg1 Mg1 53.29(3) 1_545 17_655
Sn1 Mg1 Mg1 53.29(3) . 17_655
Mg2 Mg1 Mg1 53.29(3) . 17_655
Sn1 Mg1 Mg1 53.29(3) 1_655 17_655
Mg1 Mg1 Mg1 90.0 3_655 17_655
Mg1 Mg1 Mg1 90.0 3_545 17_655
Mg1 Mg1 Mg1 90.0 3_645 17_655
Mg1 Mg1 Mg1 90.0 3 17_655
Sn2 Mg1 K1 67.61(3) . 1_655
Sn2 Mg1 K1 67.61(3) 1_545 1_655
Mg2 Mg1 K1 116.710(14) 1_545 1_655
Sn1 Mg1 K1 167.96(5) . 1_655
Mg2 Mg1 K1 116.710(14) . 1_655
Sn1 Mg1 K1 85.47(2) 1_655 1_655
Mg1 Mg1 K1 62.214(18) 3_655 1_655
Mg1 Mg1 K1 117.786(18) 3_545 1_655
Mg1 Mg1 K1 62.214(18) 3_645 1_655
Mg1 Mg1 K1 117.786(18) 3 1_655
Mg1 Mg1 K1 138.76(3) 17_655 1_655
Mg1 Mg2 Mg1 180.00(6) 19_565 3_655
Mg1 Mg2 Mg1 69.06(3) 19_565 17_655
Mg1 Mg2 Mg1 110.94(3) 3_655 17_655
Mg1 Mg2 Mg1 110.94(3) 19_565 1_565
Mg1 Mg2 Mg1 69.06(3) 3_655 1_565
Mg1 Mg2 Mg1 180.00(6) 17_655 1_565
Mg1 Mg2 Mg1 110.94(3) 19_565 .
Mg1 Mg2 Mg1 69.06(3) 3_655 .
Mg1 Mg2 Mg1 73.42(6) 17_655 .
Mg1 Mg2 Mg1 106.58(6) 1_565 .
Mg1 Mg2 Mg1 106.58(6) 19_565 19_665
Mg1 Mg2 Mg1 73.42(6) 3_655 19_665
Mg1 Mg2 Mg1 69.06(3) 17_655 19_665
Mg1 Mg2 Mg1 110.94(3) 1_565 19_665
Mg1 Mg2 Mg1 110.94(3) . 19_665
Mg1 Mg2 Mg1 69.06(3) 19_565 17_665
Mg1 Mg2 Mg1 110.94(3) 3_655 17_665
Mg1 Mg2 Mg1 106.58(6) 17_655 17_665
Mg1 Mg2 Mg1 73.42(6) 1_565 17_665
Mg1 Mg2 Mg1 180.00(6) . 17_665
Mg1 Mg2 Mg1 69.06(3) 19_665 17_665
Mg1 Mg2 Mg1 73.42(6) 19_565 3
Mg1 Mg2 Mg1 106.58(6) 3_655 3
Mg1 Mg2 Mg1 110.94(3) 17_655 3
Mg1 Mg2 Mg1 69.06(3) 1_565 3
Mg1 Mg2 Mg1 69.06(3) . 3
Mg1 Mg2 Mg1 180.00(6) 19_665 3
Mg1 Mg2 Mg1 110.94(3) 17_665 3
Mg1 Mg2 Sn2 53.29(3) 19_565 17_665
Mg1 Mg2 Sn2 126.71(3) 3_655 17_665
Mg1 Mg2 Sn2 53.29(3) 17_655 17_665
Mg1 Mg2 Sn2 126.71(3) 1_565 17_665
Mg1 Mg2 Sn2 126.71(3) . 17_665
Mg1 Mg2 Sn2 53.29(3) 19_665 17_665
Mg1 Mg2 Sn2 53.29(3) 17_665 17_665
Mg1 Mg2 Sn2 126.71(3) 3 17_665
Mg1 Mg2 Sn2 126.71(3) 19_565 .
Mg1 Mg2 Sn2 53.29(3) 3_655 .
Mg1 Mg2 Sn2 126.71(3) 17_655 .
Mg1 Mg2 Sn2 53.29(3) 1_565 .
Mg1 Mg2 Sn2 53.29(3) . .
Mg1 Mg2 Sn2 126.71(3) 19_665 .
Mg1 Mg2 Sn2 126.71(3) 17_665 .
Mg1 Mg2 Sn2 53.29(3) 3 .
Sn2 Mg2 Sn2 180.0 17_665 .
Mg1 Mg2 Sn1 55.469(15) 19_565 .
Mg1 Mg2 Sn1 124.531(15) 3_655 .
Mg1 Mg2 Sn1 55.469(15) 17_655 .
Mg1 Mg2 Sn1 124.531(15) 1_565 .
Mg1 Mg2 Sn1 55.469(15) . .
Mg1 Mg2 Sn1 124.531(15) 19_665 .
Mg1 Mg2 Sn1 124.531(15) 17_665 .
Mg1 Mg2 Sn1 55.469(15) 3 .
Sn2 Mg2 Sn1 90.0 17_665 .
Sn2 Mg2 Sn1 90.0 . .
Mg1 Mg2 Sn1 124.531(15) 19_565 1_665
Mg1 Mg2 Sn1 55.469(15) 3_655 1_665
Mg1 Mg2 Sn1 124.531(15) 17_655 1_665
Mg1 Mg2 Sn1 55.469(15) 1_565 1_665
Mg1 Mg2 Sn1 124.531(15) . 1_665
Mg1 Mg2 Sn1 55.469(15) 19_665 1_665
Mg1 Mg2 Sn1 55.469(15) 17_665 1_665
Mg1 Mg2 Sn1 124.531(15) 3 1_665
Sn2 Mg2 Sn1 90.0 17_665 1_665
Sn2 Mg2 Sn1 90.0 . 1_665
Sn1 Mg2 Sn1 180.0 . 1_665
Mg1 Sn1 Mg1 110.94(3) . 19
Mg1 Sn1 Mg1 69.06(3) . 3
Mg1 Sn1 Mg1 180.00(6) 19 3
Mg1 Sn1 Mg1 180.00(6) . 17
Mg1 Sn1 Mg1 69.06(3) 19 17
Mg1 Sn1 Mg1 110.94(3) 3 17
Mg1 Sn1 Mg1 110.94(3) . 19_565
Mg1 Sn1 Mg1 106.58(6) 19 19_565
Mg1 Sn1 Mg1 73.42(6) 3 19_565
Mg1 Sn1 Mg1 69.06(3) 17 19_565
Mg1 Sn1 Mg1 73.42(6) . 17_655
Mg1 Sn1 Mg1 69.06(3) 19 17_655
Mg1 Sn1 Mg1 110.94(3) 3 17_655
Mg1 Sn1 Mg1 106.58(6) 17 17_655
Mg1 Sn1 Mg1 69.06(3) 19_565 17_655
Mg1 Sn1 Mg1 69.06(3) . 3_545
Mg1 Sn1 Mg1 73.42(6) 19 3_545
Mg1 Sn1 Mg1 106.58(6) 3 3_545
Mg1 Sn1 Mg1 110.94(3) 17 3_545
Mg1 Sn1 Mg1 180.00(6) 19_565 3_545
Mg1 Sn1 Mg1 110.94(3) 17_655 3_545
Mg1 Sn1 Mg1 106.58(6) . 1_455
Mg1 Sn1 Mg1 110.94(3) 19 1_455
Mg1 Sn1 Mg1 69.06(3) 3 1_455
Mg1 Sn1 Mg1 73.42(6) 17 1_455
Mg1 Sn1 Mg1 110.94(3) 19_565 1_455
Mg1 Sn1 Mg1 180.00(6) 17_655 1_455
Mg1 Sn1 Mg1 69.06(3) 3_545 1_455
Mg1 Sn1 Mg2 124.531(15) . 1_445
Mg1 Sn1 Mg2 55.469(15) 19 1_445
Mg1 Sn1 Mg2 124.531(15) 3 1_445
Mg1 Sn1 Mg2 55.469(15) 17 1_445
Mg1 Sn1 Mg2 124.531(15) 19_565 1_445
Mg1 Sn1 Mg2 124.531(15) 17_655 1_445
Mg1 Sn1 Mg2 55.469(15) 3_545 1_445
Mg1 Sn1 Mg2 55.469(15) 1_455 1_445
Mg1 Sn1 Mg2 55.469(15) . .
Mg1 Sn1 Mg2 124.531(15) 19 .
Mg1 Sn1 Mg2 55.469(15) 3 .
Mg1 Sn1 Mg2 124.531(15) 17 .
Mg1 Sn1 Mg2 55.469(15) 19_565 .
Mg1 Sn1 Mg2 55.469(15) 17_655 .
Mg1 Sn1 Mg2 124.531(15) 3_545 .
Mg1 Sn1 Mg2 124.531(15) 1_455 .
Mg2 Sn1 Mg2 180.0 1_445 .
Mg1 Sn1 Mg2 124.531(15) . 1_455
Mg1 Sn1 Mg2 124.531(15) 19 1_455
Mg1 Sn1 Mg2 55.469(15) 3 1_455
Mg1 Sn1 Mg2 55.469(15) 17 1_455
Mg1 Sn1 Mg2 55.469(15) 19_565 1_455
Mg1 Sn1 Mg2 124.531(15) 17_655 1_455
Mg1 Sn1 Mg2 124.531(15) 3_545 1_455
Mg1 Sn1 Mg2 55.469(15) 1_455 1_455
Mg2 Sn1 Mg2 90.0 1_445 1_455
Mg2 Sn1 Mg2 90.0 . 1_455
Mg1 Sn1 Mg2 55.469(15) . 1_545
Mg1 Sn1 Mg2 55.469(15) 19 1_545
Mg1 Sn1 Mg2 124.531(15) 3 1_545
Mg1 Sn1 Mg2 124.531(15) 17 1_545
Mg1 Sn1 Mg2 124.531(15) 19_565 1_545
Mg1 Sn1 Mg2 55.469(15) 17_655 1_545
Mg1 Sn1 Mg2 55.469(15) 3_545 1_545
Mg1 Sn1 Mg2 124.531(15) 1_455 1_545
Mg2 Sn1 Mg2 90.0 1_445 1_545
Mg2 Sn1 Mg2 90.0 . 1_545
Mg2 Sn1 Mg2 180.0 1_455 1_545
Mg1 Sn2 Mg1 75.13(3) 3 .
Mg1 Sn2 Mg1 119.12(7) 3 3_655
Mg1 Sn2 Mg1 75.13(3) . 3_655
Mg1 Sn2 Mg1 75.13(3) 3 1_565
Mg1 Sn2 Mg1 119.12(7) . 1_565
Mg1 Sn2 Mg1 75.13(3) 3_655 1_565
Mg1 Sn2 Mg2 59.56(4) 3 .
Mg1 Sn2 Mg2 59.56(4) . .
Mg1 Sn2 Mg2 59.56(4) 3_655 .
Mg1 Sn2 Mg2 59.56(4) 1_565 .
Mg1 Sn2 K1 120.44(4) 3 25
Mg1 Sn2 K1 120.44(4) . 25
Mg1 Sn2 K1 120.44(4) 3_655 25
Mg1 Sn2 K1 120.44(4) 1_565 25
Mg2 Sn2 K1 180.0 . 25
Mg1 Sn2 K1 138.786(11) 3 1_665
Mg1 Sn2 K1 138.786(11) . 1_665
Mg1 Sn2 K1 67.46(3) 3_655 1_665
Mg1 Sn2 K1 67.46(3) 1_565 1_665
Mg2 Sn2 K1 111.35(3) . 1_665
K1 Sn2 K1 68.65(3) 25 1_665
Mg1 Sn2 K1 67.46(3) 3 .
Mg1 Sn2 K1 67.46(3) . .
Mg1 Sn2 K1 138.786(11) 3_655 .
Mg1 Sn2 K1 138.786(11) 1_565 .
Mg2 Sn2 K1 111.35(3) . .
K1 Sn2 K1 68.65(3) 25 .
K1 Sn2 K1 137.30(6) 1_665 .
Mg1 Sn2 K1 67.46(3) 3 1_565
Mg1 Sn2 K1 138.786(11) . 1_565
Mg1 Sn2 K1 138.786(11) 3_655 1_565
Mg1 Sn2 K1 67.46(3) 1_565 1_565
Mg2 Sn2 K1 111.35(3) . 1_565
K1 Sn2 K1 68.65(3) 25 1_565
K1 Sn2 K1 82.38(2) 1_665 1_565
K1 Sn2 K1 82.38(2) . 1_565
Mg1 Sn2 K1 138.786(11) 3 1_655
Mg1 Sn2 K1 67.46(3) . 1_655
Mg1 Sn2 K1 67.46(3) 3_655 1_655
Mg1 Sn2 K1 138.786(11) 1_565 1_655
Mg2 Sn2 K1 111.35(3) . 1_655
K1 Sn2 K1 68.65(3) 25 1_655
K1 Sn2 K1 82.38(2) 1_665 1_655
K1 Sn2 K1 82.38(2) . 1_655
K1 Sn2 K1 137.30(6) 1_565 1_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
K1 Sn2 3.739(2) 25
K1 Mg1 3.751(2) 3_545
K1 Mg1 3.751(2) 1_455
K1 Mg1 3.751(2) 3
K1 Mg1 3.751(2) .
K1 Sn2 3.7552(8) 1_445
K1 Sn2 3.7552(8) .
K1 Sn2 3.7552(8) 1_455
K1 Sn2 3.7552(8) 1_545
K1 K1 4.226(2) 25
K1 K1 4.226(2) 25_445
K1 K1 4.226(2) 25_545
Mg1 Sn2 2.8685(11) .
Mg1 Sn2 2.8685(11) 1_545
Mg1 Mg2 3.0849(12) 1_545
Mg1 Sn1 3.0849(12) .
Mg1 Mg2 3.0849(12) .
Mg1 Sn1 3.0849(12) 1_655
Mg1 Mg1 3.4974(3) 3_655
Mg1 Mg1 3.4974(3) 3_545
Mg1 Mg1 3.4974(3) 3_645
Mg1 Mg1 3.4974(3) 3
Mg1 Mg1 3.688(4) 17_655
Mg1 K1 3.751(2) 1_655
Mg2 Mg1 3.0849(12) 19_565
Mg2 Mg1 3.0849(12) 3_655
Mg2 Mg1 3.0849(12) 17_655
Mg2 Mg1 3.0849(12) 1_565
Mg2 Mg1 3.0849(12) 19_665
Mg2 Mg1 3.0849(12) 17_665
Mg2 Mg1 3.0849(12) 3
Mg2 Sn2 3.2975(8) 17_665
Mg2 Sn2 3.2975(8) .
Mg2 Sn1 3.4974(3) .
Mg2 Sn1 3.4974(3) 1_665
Sn1 Mg1 3.0849(12) 19
Sn1 Mg1 3.0849(12) 3
Sn1 Mg1 3.0849(12) 17
Sn1 Mg1 3.0849(12) 19_565
Sn1 Mg1 3.0849(12) 17_655
Sn1 Mg1 3.0849(12) 3_545
Sn1 Mg1 3.0849(12) 1_455
Sn1 Mg2 3.4974(3) 1_445
Sn1 Mg2 3.4974(3) 1_455
Sn1 Mg2 3.4974(3) 1_545
Sn2 Mg1 2.8685(11) 3
Sn2 Mg1 2.8685(11) 3_655
Sn2 Mg1 2.8685(11) 1_565
Sn2 K1 3.739(2) 25
Sn2 K1 3.7552(8) 1_665
Sn2 K1 3.7552(8) 1_565
Sn2 K1 3.7552(8) 1_655
