#------------------------------------------------------------------------------
#$Date: 2021-11-23 12:39:32 +0200 (Tue, 23 Nov 2021) $
#$Revision: 270835 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/53/1565365.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1565365
loop_
_publ_author_name
'Shmakova, Alexandra A.'
'Sukhikh, Taisiya S.'
'Volchek, Victoria V.'
'Yanshole, Vadim'
'Stass, Dmitri V.'
'Filatov, Eugeniy Yu.'
'Glebov, Eugeniy M.'
'Abramov, Pavel A.'
'Sokolov, Maxim N.'
_publ_section_title
;
 Niobium uptake by {P2W12} polyoxoanion with [NbO(C2O4)2(H2O)2]− as
 Nb source
;
_journal_name_full               'Inorganica Chimica Acta'
_journal_page_first              119319
_journal_paper_doi               10.1016/j.ica.2019.119319
_journal_volume                  502
_journal_year                    2020
_chemical_formula_sum            'H0 K15.3 N0 Nb10 O160.9 P4 W26'
_chemical_formula_weight         9005.71
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                90
_cell_angle_beta                 101.214(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   43.2037(8)
_cell_length_b                   12.3001(2)
_cell_length_c                   29.4907(5)
_cell_measurement_reflns_used    28461
_cell_measurement_temperature    130(2)
_cell_measurement_theta_max      29.3640
_cell_measurement_theta_min      3.4470
_cell_volume                     15372.4(5)
_computing_cell_refinement       'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)'
_computing_data_collection       'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)'
_computing_data_reduction        'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)'
_computing_molecular_graphics    'ShelXle (Hübschle, 2011)'
_computing_publication_material  'CIFTAB-2014 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      130(2)
_diffrn_detector_area_resol_mean 10.6168
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.890
_diffrn_measurement_device_type  'New Xcalibur, AtlasS2'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0387
_diffrn_reflns_av_unetI/netI     0.0425
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.890
_diffrn_reflns_limit_h_max       59
_diffrn_reflns_limit_h_min       -59
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       41
_diffrn_reflns_limit_l_min       -38
_diffrn_reflns_number            72756
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.890
_diffrn_reflns_theta_full        25.500
_diffrn_reflns_theta_max         29.629
_diffrn_reflns_theta_min         3.313
_diffrn_source                   'sealed X-ray tube'
_exptl_absorpt_coefficient_mu    20.656
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.29753
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.891
_exptl_crystal_description       plate
_exptl_crystal_F_000             15888
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.050
_refine_diff_density_max         2.633
_refine_diff_density_min         -1.696
_refine_diff_density_rms         0.373
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     964
_refine_ls_number_reflns         19286
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.034
_refine_ls_R_factor_all          0.0619
_refine_ls_R_factor_gt           0.0415
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0467P)²+514.1895P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0998
_refine_ls_wR_factor_ref         0.1120
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                14741
_reflns_number_total             19286
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            ICA-2020-502-119319.cif
_cod_data_source_block           1_a
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'H0 K15.30 N0 Nb10 O160.90 P4 W26'
_cod_database_code               1565365
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.104
_shelx_estimated_absorpt_t_max   0.425
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O1 O 0.32712(19) 0.3881(6) 0.0760(2) 0.0251(17) Uani 1 1 d . . . . .
O00Y O 0.28816(16) 0.6687(6) 0.1753(2) 0.0174(14) Uani 1 1 d . . . . .
O2 O 0.36113(17) 0.5810(6) 0.0803(2) 0.0184(15) Uani 1 1 d . . . . .
O01C O 0.42508(16) 0.5922(5) 0.3274(2) 0.0133(13) Uani 1 1 d . . . . .
O01G O 0.35178(19) 0.9248(5) 0.2921(2) 0.0209(16) Uani 1 1 d . . . . .
O01J O 0.33471(17) 0.7888(6) 0.3515(2) 0.0195(15) Uani 1 1 d . . . . .
O01P O 0.41541(17) 0.6551(5) 0.1365(2) 0.0149(14) Uani 1 1 d . . . . .
O3 O 0.33277(17) 0.7746(6) 0.0871(2) 0.0202(15) Uani 1 1 d . . . . .
O02G O 0.500000 0.3672(11) 0.250000 0.042(3) Uani 1 2 d S T P . .
O5 O 0.39310(18) 0.7736(6) 0.0546(2) 0.0220(16) Uani 1 1 d . . . . .
O6 O 0.30321(17) 0.5898(6) 0.0994(2) 0.0193(15) Uani 1 1 d . . . . .
O7 O 0.32052(16) 0.4463(5) 0.1659(2) 0.0159(14) Uani 1 1 d . . . . .
O8 O 0.37698(17) 0.4379(5) 0.1493(2) 0.0168(14) Uani 1 1 d . . . . .
O9 O 0.41466(19) 0.2712(5) 0.1913(2) 0.0212(16) Uani 1 1 d . . . . .
O10 O 0.43816(17) 0.4761(5) 0.1869(2) 0.0174(14) Uani 1 1 d . . . . .
O11 O 0.36777(17) 0.3822(5) 0.2302(2) 0.0179(15) Uani 1 1 d . . . . .
O13 O 0.31692(18) 0.8494(6) 0.1671(2) 0.0218(16) Uani 1 1 d . . . . .
O14 O 0.28746(18) 0.4955(6) 0.2315(2) 0.0211(16) Uani 1 1 d . . . . .
O15 O 0.25029(18) 0.6762(6) 0.2398(2) 0.0250(17) Uani 1 1 d . . . . .
O015 O 0.42832(17) 0.4001(5) 0.2686(2) 0.0144(14) Uani 1 1 d . . . . .
O16 O 0.30594(19) 1.0108(6) 0.2254(2) 0.0238(17) Uani 1 1 d . . . . .
O17 O 0.30753(18) 0.7893(5) 0.2481(2) 0.0198(15) Uani 1 1 d . . . . .
O18 O 0.34164(16) 0.5934(5) 0.2370(2) 0.0144(14) Uani 1 1 d . . . . .
O19 O 0.39738(16) 0.5923(5) 0.2207(2) 0.0129(13) Uani 1 1 d . . . . .
O21 O 0.42697(19) 1.0131(6) 0.1881(2) 0.0239(17) Uani 1 1 d . . . . .
O1W O 0.4677(3) 0.1179(8) 0.6233(4) 0.062(3) Uani 1 1 d . . . . .
O22 O 0.2698(2) 0.7863(7) 0.0920(3) 0.033(2) Uani 1 1 d . . . . .
O022 O 0.28907(18) 0.6749(6) 0.3883(3) 0.0252(17) Uani 1 1 d . . . . .
O23 O 0.35177(16) 0.6516(5) 0.1601(2) 0.0132(13) Uiso 1 1 d . . . . .
O24 O 0.43544(17) 0.7845(5) 0.2110(2) 0.0165(14) Uani 1 1 d . . . . .
O25 O 0.46397(16) 0.6076(5) 0.2597(2) 0.0140(14) Uani 1 1 d . . . . .
O025 O 0.30895(18) 0.2836(6) 0.2231(2) 0.0223(16) Uani 1 1 d . . . . .
O26 O 0.48040(16) 0.6519(5) 0.1734(2) 0.0149(14) Uani 1 1 d . . . . .
O026 O 0.38717(19) 0.8499(5) 0.1447(2) 0.0224(16) Uani 1 1 d . . . . .
O27 O 0.33408(17) 0.4150(6) 0.2950(2) 0.0193(15) Uani 1 1 d . . . . .
O28 O 0.30275(18) 0.6271(6) 0.3038(2) 0.0206(16) Uani 1 1 d . . . . .
O29 O 0.34593(19) 0.2834(6) 0.3711(2) 0.0229(16) Uani 1 1 d . . . . .
O30 O 0.32526(17) 0.4953(6) 0.3759(2) 0.0205(16) Uani 1 1 d . . . . .
O2W O 0.4125(4) -0.0094(12) 0.5811(5) 0.027(3) Uiso 0.5 1 d . . P . .
O32 O 0.39452(18) 0.3807(5) 0.3339(2) 0.0180(15) Uani 1 1 d . . . . .
O33 O 0.45330(18) 0.2697(5) 0.3417(2) 0.0202(16) Uani 1 1 d . . . . .
O34 O 0.36522(18) 0.9776(6) 0.2088(2) 0.0219(16) Uani 1 1 d . . . . .
O35 O 0.37017(17) 0.7708(5) 0.2294(2) 0.0153(14) Uani 1 1 d . . . . .
O36 O 0.36881(17) 0.5923(5) 0.3416(2) 0.0171(14) Uani 1 1 d . . . . .
O37 O 0.39767(16) 0.7703(5) 0.3360(2) 0.0144(14) Uani 1 1 d . . . . .
O38 O 0.41419(16) 0.6487(5) 0.4042(2) 0.0148(14) Uani 1 1 d . . . . .
O39 O 0.38449(16) 0.4431(5) 0.4144(2) 0.0154(14) Uani 1 1 d . . . . .
O40 O 0.35169(18) 0.6659(6) 0.4244(2) 0.0200(15) Uani 1 1 d . . . . .
O3W O 0.3785(3) 1.1636(7) 0.2844(3) 0.047(3) Uani 1 1 d . . . . .
O41 O 0.44165(16) 0.4336(5) 0.3990(2) 0.0126(13) Uani 1 1 d . . . . .
O42 O 0.43284(18) 0.3822(6) 0.4881(2) 0.0203(15) Uani 1 1 d . . . . .
O43 O 0.40082(17) 0.5835(5) 0.4826(2) 0.0182(15) Uani 1 1 d . . . . .
O44 O 0.45989(17) 0.5773(5) 0.4680(2) 0.0177(15) Uani 1 1 d . . . . .
O45 O 0.37388(18) 0.7763(6) 0.5070(2) 0.0231(16) Uani 1 1 d . . . . .
O46 O 0.43141(17) 0.7703(6) 0.4777(2) 0.0178(15) Uani 1 1 d . . . . .
O47 O 0.49878(18) 0.7712(6) 0.4754(2) 0.0236(16) Uani 1 1 d . . . . .
O48 O 0.47997(15) 0.6532(5) 0.3917(2) 0.0133(13) Uani 1 1 d . . . . .
O49 O 0.38077(18) 0.8480(5) 0.4183(2) 0.0189(15) Uani 1 1 d . . . . .
O50 O 0.45200(18) 0.8489(5) 0.4000(2) 0.0184(15) Uani 1 1 d . . . . .
O4W O 0.500000 0.9120(14) 0.250000 0.072(5) Uiso 1 2 d S . P . .
O51 O 0.34413(18) 1.0106(6) 0.3747(2) 0.0220(16) Uani 1 1 d . . . . .
O52 O 0.40290(17) 0.9770(6) 0.3566(2) 0.0186(15) Uani 1 1 d . . . . .
O53 O 0.4659(2) 1.0117(6) 0.3415(3) 0.0262(17) Uani 1 1 d . . . . .
O54 O 0.41872(19) 0.9282(6) 0.2725(2) 0.0242(17) Uani 1 1 d . . . . .
O55 O 0.46273(16) 0.7836(5) 0.3171(2) 0.0136(13) Uani 1 1 d . . . . .
O56 O 0.47597(16) 0.4751(5) 0.3347(2) 0.0161(14) Uani 1 1 d . . . . .
O5W O 0.5185(2) 1.1345(8) 0.3230(4) 0.047(2) Uani 1 1 d . . . . .
O6W O 0.1587(3) 0.9435(11) 0.0166(3) 0.068(4) Uani 1 1 d . . . . .
O7W O 0.2020(4) 0.7124(12) 0.0132(5) 0.028(4) Uiso 0.5 1 d . . P . .
O8W O 0.2384(4) 0.9219(11) 0.1742(5) 0.086(4) Uiso 1 1 d . . . . .
O9W O 0.2239(4) 0.4358(14) 0.1901(6) 0.030(4) Uiso 0.5 1 d . . P . .
O10W O 0.2450(4) 0.9232(13) -0.0161(6) 0.034(4) Uiso 0.5 1 d . . P . .
O11W O 0.3268(3) 0.8591(9) -0.0712(4) 0.067(3) Uiso 1 1 d . . . . .
O12W O 0.2809(3) 0.8523(10) -0.1260(5) 0.075(4) Uiso 1 1 d . . . . .
O13W O 0.4231(5) 0.4545(16) 0.0799(6) 0.044(4) Uiso 0.55 1 d . . P . .
O14W O 0.4565(4) 0.1929(13) 0.0722(6) 0.031(4) Uiso 0.5 1 d . . P . .
O15W O 0.4848(4) 0.4612(13) 0.0643(5) 0.041(4) Uiso 0.65 1 d . . P . .
O16W O 0.3022(5) 0.3059(17) -0.0112(7) 0.040(5) Uiso 0.5 1 d . . P . .
O17W O 0.3444(5) 0.8297(15) 0.6642(7) 0.036(4) Uiso 0.5 1 d . . P . .
O18W O 0.4086(4) 1.1754(14) 0.3959(6) 0.036(4) Uiso 0.5 1 d . . P . .
O19W O 0.3347(5) 0.9793(16) 0.4757(7) 0.049(5) Uiso 0.5 1 d . . P . .
O20W O 0.2812(7) 0.933(2) 0.4073(10) 0.036(7) Uiso 0.3 1 d . . P . .
O21W O 0.4953(3) -0.0005(9) 0.5591(4) 0.055(3) Uiso 1 1 d . . . . .
O22W O 0.3359(8) 0.985(3) 0.5722(11) 0.046(8) Uiso 0.3 1 d . . P . .
O23W O 0.2735(9) 0.869(3) 0.4630(12) 0.037(8) Uiso 0.25 1 d . . P . .
O24W O 0.2305(9) 0.785(3) 0.4127(13) 0.041(9) Uiso 0.25 1 d . . P . .
O25W O 0.2318(6) 0.374(2) 0.1876(8) 0.061(6) Uiso 0.5 1 d . . P . .
O26W O 0.4926(5) 0.4145(16) 0.0628(6) 0.013(4) Uiso 0.35 1 d . . P . .
O27W O 0.4157(4) 0.4045(13) 0.0815(5) 0.017(3) Uiso 0.45 1 d . . P . .
O28W O 0.4161(5) 1.1504(15) 0.4233(7) 0.044(5) Uiso 0.5 1 d . . P . .
O29W O 0.4357(8) 1.009(3) 0.4876(11) 0.088(9) Uiso 0.45 1 d . . P . .
O30W O 0.2377(9) 0.853(3) 0.3753(12) 0.054(9) Uiso 0.3 1 d . . P . .
O31W O 0.3368(9) 0.859(3) 0.6457(13) 0.048(9) Uiso 0.3 1 d . . P . .
O32W O 0.2695(9) 1.068(3) 0.0760(13) 0.093(11) Uiso 0.4 1 d . . P . .
O33W O 0.2957(7) 0.361(2) -0.0183(10) 0.054(7) Uiso 0.4 1 d . . P . .
P1 P 0.40082(6) 0.65162(18) 0.35045(8) 0.0099(4) Uiso 1 1 d . . . . .
P2 P 0.36571(6) 0.65221(18) 0.21378(8) 0.0106(5) Uiso 1 1 d . . . . .
K1 K 0.45455(11) 0.1460(3) 0.26184(11) 0.0644(11) Uani 1 1 d . . . . .
K2 K 0.47165(7) 0.3419(2) 0.13933(9) 0.0330(6) Uani 1 1 d . . . . .
K3 K 0.31377(6) 1.1473(2) 0.30205(9) 0.0276(5) Uani 1 1 d . . . . .
K4 K 0.23187(11) 0.6502(3) 0.33253(15) 0.0784(14) Uani 1 1 d . . . . .
K5 K 0.45557(7) 0.3177(3) 0.57440(8) 0.0365(7) Uani 1 1 d . . . . .
K6 K 0.2090(2) 0.8473(9) 0.0816(3) 0.072(2) Uani 0.5 1 d . . P . .
K7 K 0.21959(18) 0.9243(7) 0.0669(3) 0.0551(18) Uani 0.5 1 d . . P . .
K8 K 0.38065(19) 0.7796(5) 0.60047(18) 0.0432(16) Uani 0.5 1 d . . P . .
K9 K 0.47314(16) 0.7844(5) -0.06448(17) 0.0454(16) Uani 0.5 1 d . . P . .
K10 K 0.3729(2) 0.7751(6) -0.0376(2) 0.064(2) Uani 0.5 1 d . . P . .
K11 K 0.3933(7) 0.832(2) 0.6053(9) 0.057(6) Uiso 0.15 1 d . . P . .
Nb1 Nb 0.43884(2) 0.90483(5) 0.33595(2) 0.01240(13) Uani 0.75 1 d . . P . .
W14 W 0.43884(2) 0.90483(5) 0.33595(2) 0.01240(13) Uani 0.25 1 d . . P . .
Nb2 Nb 0.40599(2) 0.90626(5) 0.20683(2) 0.01378(14) Uani 0.75 1 d . . P . .
W15 W 0.40599(2) 0.90626(5) 0.20683(2) 0.01378(14) Uani 0.25 1 d . . P . .
Nb3 Nb 0.37931(2) 0.72958(6) 0.10368(2) 0.01714(14) Uani 0.75 1 d . . P . .
W16 W 0.37931(2) 0.72958(6) 0.10368(2) 0.01714(14) Uani 0.25 1 d . . P . .
Nb4 Nb 0.46391(2) 0.72743(5) 0.43945(2) 0.01504(14) Uani 0.75 1 d . . P . .
W17 W 0.46391(2) 0.72743(5) 0.43945(2) 0.01504(14) Uani 0.25 1 d . . P . .
Nb5 Nb 0.47557(2) 0.63887(7) 0.32490(3) 0.01158(17) Uani 1 1 d . . . . .
Nb6 Nb 0.44309(2) 0.63973(7) 0.19760(3) 0.01186(17) Uani 1 1 d . . . . .
W1 W 0.40581(2) 0.40179(3) 0.20570(2) 0.01385(9) Uani 1 1 d . . . . .
W2 W 0.33857(2) 0.49332(3) 0.11395(2) 0.01732(9) Uani 1 1 d . . . . .
W3 W 0.30419(2) 0.73633(4) 0.12435(2) 0.01929(9) Uani 1 1 d . . . . .
W4 W 0.32532(2) 0.41144(3) 0.22966(2) 0.01544(9) Uani 1 1 d . . . . .
W6 W 0.28919(2) 0.65018(3) 0.23878(2) 0.01759(9) Uani 1 1 d . . . . .
W7 W 0.33238(2) 0.90575(3) 0.22946(2) 0.01740(9) Uani 1 1 d . . . . .
W8 W 0.36501(2) 0.90495(3) 0.35802(2) 0.01636(9) Uani 1 1 d . . . . .
W9 W 0.35787(2) 0.41052(3) 0.35720(2) 0.01543(9) Uani 1 1 d . . . . .
W10 W 0.38879(2) 0.72720(3) 0.46111(2) 0.01533(9) Uani 1 1 d . . . . .
W11 W 0.42512(2) 0.48757(3) 0.44973(2) 0.01419(9) Uani 1 1 d . . . . .
W12 W 0.43883(2) 0.40044(3) 0.33402(2) 0.01347(8) Uani 1 1 d . . . . .
W13 W 0.32225(2) 0.64965(3) 0.36667(2) 0.01701(9) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nb Nb -2.0727 0.6215 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
W2 O1 K8 104.1(3) . 6_565
W6 O00Y W3 150.8(4) . .
W2 O2 Nb3 122.8(3) . .
P1 O01C Nb5 129.4(4) . .
P1 O01C W12 127.0(4) . .
Nb5 O01C W12 91.5(2) . .
W7 O01G W8 163.0(4) . .
W7 O01G K3 93.3(3) . .
W8 O01G K3 94.1(2) . .
W13 O01J W8 151.2(4) . .
Nb3 O01P Nb6 143.5(3) . .
Nb3 O01P K5 99.3(3) . 6_565
Nb6 O01P K5 105.6(3) . 6_565
W3 O3 Nb3 121.5(3) . .
K2 O02G K2 169.1(5) . 2_655
K2 O02G K1 86.2(2) . 2_655
K2 O02G K1 85.1(2) 2_655 2_655
K2 O02G K1 85.1(2) . .
K2 O02G K1 86.2(2) 2_655 .
K1 O02G K1 74.3(3) 2_655 .
Nb3 O5 K10 137.7(4) . .
Nb3 O5 K5 99.7(3) . 6_565
K10 O5 K5 108.4(3) . 6_565
W2 O6 W3 122.2(4) . .
W4 O7 W2 150.1(4) . .
W2 O8 W1 154.5(4) . .
W2 O8 K8 100.1(3) . 6_565
W1 O8 K8 97.0(3) . 6_565
W1 O9 K11 126.2(7) . 6_565
W1 O9 K8 109.6(4) . 6_565
K11 O9 K8 17.0(6) 6_565 6_565
W1 O9 K1 116.8(3) . .
K11 O9 K1 117.0(6) 6_565 .
K8 O9 K1 133.4(3) 6_565 .
W1 O9 K2 95.2(3) . .
K11 O9 K2 80.9(6) 6_565 .
K8 O9 K2 85.1(2) 6_565 .
K1 O9 K2 94.7(2) . .
W1 O10 Nb6 120.3(3) . .
W1 O10 K2 111.1(3) . .
Nb6 O10 K2 128.4(3) . .
W4 O11 W1 151.4(4) . .
W3 O13 W7 153.0(4) . .
W6 O14 W4 121.1(4) . .
W6 O15 K3 148.0(4) . 4_545
W6 O15 K4 115.3(3) . .
K3 O15 K4 88.5(2) 4_545 .
W12 O015 W1 163.8(4) . .
W12 O015 K1 92.6(2) . .
W1 O015 K1 93.8(2) . .
W7 O16 K4 145.9(4) . 4
W7 O16 K3 115.1(3) . .
K4 O16 K3 95.3(2) 4 .
W6 O17 W7 150.9(4) . .
P2 O18 W4 128.9(4) . .
P2 O18 W6 127.0(4) . .
W4 O18 W6 90.7(2) . .
P2 O19 Nb6 129.7(4) . .
P2 O19 W1 127.0(4) . .
Nb6 O19 W1 91.3(2) . .
Nb2 O21 K1 111.2(3) . 1_565
Nb2 O21 K11 120.0(6) . 6_575
K1 O21 K11 107.8(5) 1_565 6_575
W3 O22 K6 152.1(5) . .
W3 O22 K7 157.9(5) . .
K6 O22 K7 24.9(3) . .
W13 O022 K4 119.1(4) . .
W13 O022 K7 98.3(3) . 4_545
K4 O022 K7 88.7(2) . 4_545
P2 O23 W3 125.0(4) . .
P2 O23 W2 125.3(3) . .
W3 O23 W2 90.9(2) . .
P2 O23 Nb3 122.9(4) . .
W3 O23 Nb3 91.2(2) . .
W2 O23 Nb3 91.5(2) . .
Nb6 O24 Nb2 149.1(4) . .
Nb6 O25 Nb5 153.3(4) . .
W4 O025 K4 145.6(4) . 4_545
W4 O025 K3 119.0(3) . 1_545
K4 O025 K3 94.2(2) 4_545 1_545
Nb6 O26 Nb5 154.9(4) . 2_655
Nb6 O26 K5 102.3(3) . 6_565
Nb5 O26 K5 102.0(2) 2_655 6_565
Nb3 O026 Nb2 148.5(4) . .
W4 O27 W9 159.5(4) . .
W4 O27 K3 92.1(2) . 1_545
W9 O27 K3 90.6(2) . 1_545
W13 O28 W6 161.1(4) . .
W13 O28 K4 89.7(2) . .
W6 O28 K4 97.1(3) . .
W9 O29 K3 120.1(3) . 1_545
W9 O29 K10 111.9(4) . 6_566
K3 O29 K10 126.9(3) 1_545 6_566
W9 O29 K6 99.7(4) . 4_545
K3 O29 K6 99.5(3) 1_545 4_545
K10 O29 K6 81.0(3) 6_566 4_545
W9 O30 W13 122.0(3) . .
W9 O30 K6 105.0(4) . 4_545
W13 O30 K6 133.0(4) . 4_545
W9 O30 K7 127.4(4) . 4_545
W13 O30 K7 110.0(3) . 4_545
K6 O30 K7 23.4(2) 4_545 4_545
K11 O2W K8 7.9(7) 1_545 1_545
W9 O32 W12 151.6(4) . .
W12 O33 K9 112.6(3) . 6_566
W12 O33 K1 117.3(3) . .
K9 O33 K1 130.1(3) 6_566 .
W12 O33 K2 95.2(3) . 2_655
K9 O33 K2 78.2(2) 6_566 2_655
K1 O33 K2 96.2(2) . 2_655
W7 O34 Nb2 122.4(4) . .
P2 O35 W7 129.2(4) . .
P2 O35 Nb2 127.9(4) . .
W7 O35 Nb2 89.7(2) . .
P1 O36 W9 128.8(4) . .
P1 O36 W13 126.3(4) . .
W9 O36 W13 90.4(2) . .
P1 O37 W8 128.8(4) . .
P1 O37 Nb1 129.0(4) . .
W8 O37 Nb1 89.9(2) . .
P1 O38 W10 124.7(4) . .
P1 O38 W11 125.2(4) . .
W10 O38 W11 90.5(2) . .
P1 O38 Nb4 123.2(4) . .
W10 O38 Nb4 91.6(2) . .
W11 O38 Nb4 91.7(2) . .
W9 O39 W11 150.5(4) . .
W9 O39 K10 95.6(3) . 6_566
W11 O39 K10 102.0(3) . 6_566
W10 O40 W13 151.7(4) . .
W11 O41 W12 153.0(4) . .
W11 O41 K9 103.6(3) . 6_566
W12 O41 K9 95.8(2) . 6_566
W11 O42 K5 147.8(4) . .
W11 O42 K10 104.8(3) . 6_566
K5 O42 K10 100.2(2) . 6_566
W11 O42 K9 102.4(3) . 6_566
K5 O42 K9 97.7(2) . 6_566
K10 O42 K9 89.4(2) 6_566 6_566
W10 O43 W11 122.0(3) . .
W11 O44 Nb4 123.0(4) . .
W10 O45 K8 145.3(4) . .
W10 O45 K11 141.3(7) . .
K8 O45 K11 16.5(5) . .
W10 O46 Nb4 121.8(3) . .
Nb4 O47 K9 141.8(4) . 2_655
Nb4 O47 K5 99.6(3) . 5_666
K9 O47 K5 107.3(3) 2_655 5_666
Nb4 O48 Nb5 143.8(4) . .
Nb4 O48 K5 98.9(3) . 5_666
Nb5 O48 K5 105.5(3) . 5_666
W8 O49 W10 151.1(4) . .
Nb4 O50 Nb1 147.9(4) . .
W8 O51 K3 115.2(3) . .
W8 O52 Nb1 122.4(4) . .
Nb1 O53 K1 110.9(4) . 1_565
Nb2 O54 Nb1 160.5(4) . .
Nb2 O54 K1 94.0(3) . 1_565
Nb1 O54 K1 95.0(3) . 1_565
Nb5 O55 Nb1 148.6(4) . .
W12 O56 Nb5 120.5(3) . .
W12 O56 K2 111.7(3) . 2_655
Nb5 O56 K2 127.4(3) . 2_655
K2 O5W K1 103.8(3) 2_665 2_665
K2 O5W K1 104.4(3) 2_665 1_565
K1 O5W K1 87.5(3) 2_665 1_565
K7 O6W K6 23.9(2) . .
K7 O6W K10 103.0(4) . 7_565
K6 O6W K10 79.4(4) . 7_565
K6 O7W K7 21.8(3) . .
K6 O8W K4 109.4(5) . 4
K6 O8W K7 22.1(2) . .
K4 O8W K7 87.4(4) 4 .
O25W O9W K3 172(2) . 4_545
K10 O11W K6 92.9(5) . 7_565
K3 O12W K6 107.7(5) 6_575 7_565
O27W O13W K2 80(2) . .
O27W O13W K5 179(3) . 6_565
K2 O13W K5 100.6(6) . 6_565
K2 O14W K11 86.5(7) . 6_565
K2 O14W K9 83.7(5) . 5_665
K11 O14W K9 166.1(8) 6_565 5_665
O26W O15W K2 77(2) . .
O26W O15W K5 175(3) . 6_565
K2 O15W K5 103.8(5) . 6_565
O31W O17W K8 80(4) . .
O31W O17W K11 80(4) . .
K8 O17W K11 16.2(5) . .
O31W O17W K4 70(4) . 7_566
K8 O17W K4 137.6(7) . 7_566
K11 O17W K4 146.5(9) . 7_566
O28W O18W K10 65.1(18) . 6_576
O28W O18W K9 61.4(19) . 6_576
K10 O18W K9 107.8(6) 6_576 6_576
K11 O22W K8 15.3(5) . .
O30W O24W K4 70.7(19) . .
O9W O25W K4 172(2) . 4_545
O15W O26W K2 89(2) . .
O15W O26W K9 175(3) . 5_665
K2 O26W K9 87.7(6) . 5_665
O13W O27W K2 86(2) . .
O13W O27W K8 170(2) . 6_565
K2 O27W K8 95.2(5) . 6_565
O13W O27W K11 169(3) . 6_565
K2 O27W K11 82.9(7) . 6_565
K8 O27W K11 14.6(5) 6_565 6_565
O18W O28W K10 97(2) . 6_576
O18W O28W K9 101(2) . 6_576
K10 O28W K9 126.6(8) 6_576 6_576
O24W O30W K4 80(2) . .
O17W O31W K8 86(4) . .
O17W O31W K11 87(4) . .
K8 O31W K11 16.5(6) . .
O17W O31W K4 99(4) . 7_566
K8 O31W K4 149.9(14) . 7_566
K11 O31W K4 165.3(15) . 7_566
K7 O32W K4 99.1(12) . 4
O16W O33W K7 164(3) . 7_565
O37 P1 O01C 111.3(4) . .
O37 P1 O36 112.3(4) . .
O01C P1 O36 111.5(4) . .
O37 P1 O38 107.4(4) . .
O01C P1 O38 106.5(4) . .
O36 P1 O38 107.4(4) . .
O35 P2 O19 111.2(4) . .
O35 P2 O18 111.8(4) . .
O19 P2 O18 112.3(4) . .
O35 P2 O23 107.9(4) . .
O19 P2 O23 106.7(4) . .
O18 P2 O23 106.6(4) . .
O21 K1 O33 153.3(3) 1_545 .
O21 K1 O53 106.5(2) 1_545 1_545
O33 K1 O53 69.5(2) . 1_545
O21 K1 O9 69.2(2) 1_545 .
O33 K1 O9 102.1(2) . .
O53 K1 O9 153.4(3) 1_545 .
O21 K1 O5W 59.5(3) 1_545 2_645
O33 K1 O5W 143.9(3) . 2_645
O53 K1 O5W 129.7(3) 1_545 2_645
O9 K1 O5W 72.1(3) . 2_645
O21 K1 O5W 130.1(3) 1_545 1_545
O33 K1 O5W 71.8(2) . 1_545
O53 K1 O5W 58.8(3) 1_545 1_545
O9 K1 O5W 144.5(3) . 1_545
O5W K1 O5W 92.2(3) 2_645 1_545
O21 K1 O54 55.6(2) 1_545 1_545
O33 K1 O54 106.7(2) . 1_545
O53 K1 O54 55.2(2) 1_545 1_545
O9 K1 O54 106.9(2) . 1_545
O5W K1 O54 109.0(3) 2_645 1_545
O5W K1 O54 108.3(3) 1_545 1_545
O21 K1 O015 119.6(2) 1_545 .
O33 K1 O015 51.90(18) . .
O53 K1 O015 120.1(2) 1_545 .
O9 K1 O015 51.70(18) . .
O5W K1 O015 106.7(2) 2_645 .
O5W K1 O015 107.0(2) 1_545 .
O54 K1 O015 127.8(2) 1_545 .
O21 K1 O02G 123.57(19) 1_545 .
O33 K1 O02G 76.09(19) . .
O53 K1 O02G 122.6(2) 1_545 .
O9 K1 O02G 77.00(18) . .
O5W K1 O02G 67.9(2) 2_645 .
O5W K1 O02G 67.5(2) 1_545 .
O54 K1 O02G 174.3(2) 1_545 .
O015 K1 O02G 57.94(18) . .
O21 K1 Nb2 25.40(15) 1_545 1_545
O33 K1 Nb2 132.8(2) . 1_545
O53 K1 Nb2 83.90(17) 1_545 1_545
O9 K1 Nb2 84.44(17) . 1_545
O5W K1 Nb2 82.9(2) 2_645 1_545
O5W K1 Nb2 126.1(2) 1_545 1_545
O54 K1 Nb2 30.41(13) 1_545 1_545
O015 K1 Nb2 125.88(18) . 1_545
O02G K1 Nb2 148.97(11) . 1_545
O21 K1 Nb1 83.99(17) 1_545 1_545
O33 K1 Nb1 84.63(16) . 1_545
O53 K1 Nb1 25.26(16) 1_545 1_545
O9 K1 Nb1 132.9(2) . 1_545
O5W K1 Nb1 126.1(2) 2_645 1_545
O5W K1 Nb1 82.2(2) 1_545 1_545
O54 K1 Nb1 30.13(14) 1_545 1_545
O015 K1 Nb1 126.27(17) . 1_545
O02G K1 Nb1 147.86(12) . 1_545
Nb2 K1 Nb1 59.78(6) 1_545 1_545
O21 K1 W12 142.9(2) 1_545 .
O33 K1 W12 23.01(14) . .
O53 K1 W12 92.04(17) 1_545 .
O9 K1 W12 79.78(16) . .
O5W K1 W12 129.4(2) 2_645 .
O5W K1 W12 87.0(2) 1_545 .
O54 K1 W12 119.11(18) 1_545 .
O015 K1 W12 28.90(11) . .
O02G K1 W12 65.33(13) . .
Nb2 K1 W12 135.49(14) 1_545 .
Nb1 K1 W12 103.91(9) 1_545 .
O14W K2 O26W 71.8(5) . .
O14W K2 O10 135.1(4) . .
O26W K2 O10 121.0(5) . .
O14W K2 O56 132.5(4) . 2_655
O26W K2 O56 69.7(4) . 2_655
O10 K2 O56 89.2(2) . 2_655
O14W K2 O5W 70.4(4) . 2_645
O26W K2 O5W 125.4(5) . 2_645
O10 K2 O5W 113.7(3) . 2_645
O56 K2 O5W 112.2(3) 2_655 2_645
O14W K2 O27W 71.2(5) . .
O26W K2 O27W 77.9(6) . .
O10 K2 O27W 70.5(4) . .
O56 K2 O27W 124.7(4) 2_655 .
O5W K2 O27W 123.1(4) 2_645 .
O14W K2 O15W 80.4(5) . .
O26W K2 O15W 13.8(4) . .
O10 K2 O15W 107.2(4) . .
O56 K2 O15W 68.2(3) 2_655 .
O5W K2 O15W 139.1(4) 2_645 .
O27W K2 O15W 69.9(5) . .
O14W K2 O13W 80.3(5) . .
O26W K2 O13W 69.7(6) . .
O10 K2 O13W 67.7(4) . .
O56 K2 O13W 110.4(4) 2_655 .
O5W K2 O13W 137.4(5) 2_645 .
O27W K2 O13W 14.3(4) . .
O15W K2 O13W 59.5(5) . .
O14W K2 O9 93.8(4) . .
O26W K2 O9 151.0(5) . .
O10 K2 O9 53.18(19) . .
O56 K2 O9 132.6(2) 2_655 .
O5W K2 O9 68.8(2) 2_645 .
O27W K2 O9 73.5(4) . .
O15W K2 O9 142.9(4) . .
O13W K2 O9 83.4(4) . .
O14W K2 O02G 142.3(4) . .
O26W K2 O02G 132.2(4) . .
O10 K2 O02G 64.3(2) . .
O56 K2 O02G 62.8(2) 2_655 .
O5W K2 O02G 72.0(3) 2_645 .
O27W K2 O02G 134.2(3) . .
O15W K2 O02G 130.1(4) . .
O13W K2 O02G 131.5(4) . .
O9 K2 O02G 74.15(16) . .
O14W K2 O33 91.9(4) . 2_655
O26W K2 O33 75.9(5) . 2_655
O10 K2 O33 132.2(2) . 2_655
O56 K2 O33 52.52(19) 2_655 2_655
O5W K2 O33 67.5(2) 2_645 2_655
O27W K2 O33 152.3(4) . 2_655
O15W K2 O33 86.0(4) . 2_655
O13W K2 O33 145.4(4) . 2_655
O9 K2 O33 130.9(2) . 2_655
O02G K2 O33 72.06(15) . 2_655
O14W K2 W1 114.2(4) . .
O26W K2 W1 139.1(5) . .
O10 K2 W1 26.71(15) . .
O56 K2 W1 113.11(16) 2_655 .
O5W K2 W1 92.5(2) 2_645 .
O27W K2 W1 67.5(3) . .
O15W K2 W1 126.0(3) . .
O13W K2 W1 71.7(4) . .
O9 K2 W1 26.67(12) . .
O02G K2 W1 69.05(6) . .
O33 K2 W1 140.23(15) 2_655 .
O12W K3 O16 128.5(3) 6_576 .
O12W K3 O29 72.4(3) 6_576 1_565
O16 K3 O29 156.9(2) . 1_565
O12W K3 O15 74.3(3) 6_576 4
O16 K3 O15 76.6(2) . 4
O29 K3 O15 123.3(2) 1_565 4
O12W K3 O51 69.8(3) 6_576 .
O16 K3 O51 102.8(2) . .
O29 K3 O51 73.3(2) 1_565 .
O15 K3 O51 132.4(2) 4 .
O12W K3 O025 131.2(3) 6_576 1_565
O16 K3 O025 73.3(2) . 1_565
O29 K3 O025 101.0(2) 1_565 1_565
O15 K3 O025 70.0(2) 4 1_565
O51 K3 O025 156.6(2) . 1_565
O12W K3 O3W 141.2(4) 6_576 .
O16 K3 O3W 82.4(2) . .
O29 K3 O3W 74.5(2) 1_565 .
O15 K3 O3W 142.8(3) 4 .
O51 K3 O3W 81.9(2) . .
O025 K3 O3W 74.7(2) 1_565 .
O12W K3 O9W 65.8(4) 6_576 4
O16 K3 O9W 64.7(3) . 4
O29 K3 O9W 130.0(3) 1_565 4
O15 K3 O9W 69.8(4) 4 4
O51 K3 O9W 67.6(4) . 4
O025 K3 O9W 126.9(3) 1_565 4
O3W K3 O9W 126.9(4) . 4
O12W K3 O01G 114.6(3) 6_576 .
O16 K3 O01G 53.1(2) . .
O29 K3 O01G 112.6(2) 1_565 .
O15 K3 O01G 122.6(2) 4 .
O51 K3 O01G 53.04(19) . .
O025 K3 O01G 112.5(2) 1_565 .
O3W K3 O01G 61.7(2) . .
O9W K3 O01G 65.2(3) 4 .
O12W K3 O27 102.7(3) 6_576 1_565
O16 K3 O27 121.5(2) . 1_565
O29 K3 O27 50.96(18) 1_565 1_565
O15 K3 O27 95.3(2) 4 1_565
O51 K3 O27 122.0(2) . 1_565
O025 K3 O27 50.35(18) 1_565 1_565
O3W K3 O27 70.2(2) . 1_565
O9W K3 O27 162.9(3) 4 1_565
O01G K3 O27 131.9(2) . 1_565
O12W K3 W7 128.5(3) 6_576 .
O16 K3 W7 23.86(15) . .
O29 K3 W7 138.02(18) 1_565 .
O15 K3 W7 98.51(17) 4 .
O51 K3 W7 81.15(15) . .
O025 K3 W7 89.41(16) 1_565 .
O3W K3 W7 69.25(17) . .
O9W K3 W7 64.0(3) 4 .
O01G K3 W7 29.42(12) . .
O27 K3 W7 128.79(14) 1_565 .
O12W K3 W8 90.6(3) 6_576 .
O16 K3 W8 81.47(16) . .
O29 K3 W8 89.34(17) 1_565 .
O15 K3 W8 135.34(18) 4 .
O51 K3 W8 23.44(14) . .
O025 K3 W8 138.19(18) 1_565 .
O3W K3 W8 69.25(18) . .
O9W K3 W8 65.7(3) 4 .
O01G K3 W8 29.77(12) . .
O27 K3 W8 129.21(15) 1_565 .
W7 K3 W8 58.61(4) . .
O022 K4 O025 135.1(3) . 4
O022 K4 O16 144.7(3) . 4_545
O025 K4 O16 76.2(2) 4 4_545
O022 K4 O30W 68.4(8) . .
O025 K4 O30W 73.9(8) 4 .
O16 K4 O30W 146.9(8) 4_545 .
O022 K4 O32W 69.8(8) . 4_545
O025 K4 O32W 130.3(8) 4 4_545
O16 K4 O32W 104.2(8) 4_545 4_545
O30W K4 O32W 84.7(10) . 4_545
O022 K4 O24W 66.5(8) . .
O025 K4 O24W 91.9(8) 4 .
O16 K4 O24W 140.0(8) 4_545 .
O30W K4 O24W 29.7(10) . .
O32W K4 O24W 55.5(10) 4_545 .
O022 K4 O15 99.7(3) . .
O025 K4 O15 69.0(2) 4 .
O16 K4 O15 74.3(2) 4_545 .
O30W K4 O15 107.4(8) . .
O32W K4 O15 160.3(8) 4_545 .
O24W K4 O15 136.9(8) . .
O022 K4 O8W 78.5(3) . 4_545
O025 K4 O8W 137.3(3) 4 4_545
O16 K4 O8W 66.2(3) 4_545 4_545
O30W K4 O8W 146.7(8) . 4_545
O32W K4 O8W 80.0(8) 4_545 4_545
O24W K4 O8W 130.1(8) . 4_545
O15 K4 O8W 81.5(3) . 4_545
O022 K4 O31W 131.6(7) . 7_566
O025 K4 O31W 67.5(7) 4 7_566
O16 K4 O31W 68.5(7) 4_545 7_566
O30W K4 O31W 86.8(10) . 7_566
O32W K4 O31W 66.9(11) 4_545 7_566
O24W K4 O31W 71.7(10) . 7_566
O15 K4 O31W 127.8(7) . 7_566
O8W K4 O31W 113.5(7) 4_545 7_566
O022 K4 O25W 66.6(5) . 4
O025 K4 O25W 70.2(5) 4 4
O16 K4 O25W 131.6(5) 4_545 4
O30W K4 O25W 47.6(8) . 4
O32W K4 O25W 124.1(9) 4_545 4
O24W K4 O25W 75.7(8) . 4
O15 K4 O25W 61.7(4) . 4
O8W K4 O25W 121.9(5) 4_545 4
O31W K4 O25W 124.6(8) 7_566 4
O022 K4 O17W 140.1(4) . 7_566
O025 K4 O17W 56.1(4) 4 7_566
O16 K4 O17W 65.7(4) 4_545 7_566
O30W K4 O17W 85.6(8) . 7_566
O32W K4 O17W 78.4(9) 4_545 7_566
O24W K4 O17W 75.9(8) . 7_566
O15 K4 O17W 117.2(4) . 7_566
O8W K4 O17W 119.6(4) 4_545 7_566
O31W K4 O17W 11.7(7) 7_566 7_566
O25W K4 O17W 117.0(5) 4 7_566
O022 K4 O28 52.5(2) . .
O025 K4 O28 114.7(3) 4 .
O16 K4 O28 104.7(3) 4_545 .
O30W K4 O28 100.6(8) . .
O32W K4 O28 113.1(8) 4_545 .
O24W K4 O28 114.8(8) . .
O15 K4 O28 50.4(2) . .
O8W K4 O28 59.8(3) 4_545 .
O31W K4 O28 172.6(7) 7_566 .
O25W K4 O28 62.1(4) 4 .
O17W K4 O28 167.2(4) 7_566 .
O42 K5 O01P 115.6(2) . 6_566
O42 K5 O48 117.4(2) . 5_666
O01P K5 O48 117.1(2) 6_566 5_666
O42 K5 O1W 137.6(3) . .
O01P K5 O1W 81.2(3) 6_566 .
O48 K5 O1W 81.8(3) 5_666 .
O42 K5 O5 76.5(2) . 6_566
O01P K5 O5 59.9(2) 6_566 6_566
O48 K5 O5 162.5(2) 5_666 6_566
O1W K5 O5 80.7(3) . 6_566
O42 K5 O47 77.8(2) . 5_666
O01P K5 O47 162.8(2) 6_566 5_666
O48 K5 O47 60.0(2) 5_666 5_666
O1W K5 O47 81.6(3) . 5_666
O5 K5 O47 117.1(2) 6_566 5_666
O42 K5 O26 155.3(2) . 6_566
O01P K5 O26 58.8(2) 6_566 6_566
O48 K5 O26 58.75(19) 5_666 6_566
O1W K5 O26 67.1(3) . 6_566
O5 K5 O26 113.5(2) 6_566 6_566
O47 K5 O26 113.6(2) 5_666 6_566
O42 K5 O15W 73.9(3) . 6_566
O01P K5 O15W 106.4(3) 6_566 6_566
O48 K5 O15W 61.0(3) 5_666 6_566
O1W K5 O15W 141.6(4) . 6_566
O5 K5 O15W 136.2(3) 6_566 6_566
O47 K5 O15W 87.2(3) 5_666 6_566
O26 K5 O15W 84.5(3) 6_566 6_566
O42 K5 O13W 72.5(4) . 6_566
O01P K5 O13W 61.2(4) 6_566 6_566
O48 K5 O13W 106.9(4) 5_666 6_566
O1W K5 O13W 141.4(4) . 6_566
O5 K5 O13W 87.0(4) 6_566 6_566
O47 K5 O13W 135.7(4) 5_666 6_566
O26 K5 O13W 85.2(4) 6_566 6_566
O15W K5 O13W 53.6(4) 6_566 6_566
O42 K5 Nb3 95.31(18) . 6_566
O01P K5 Nb3 31.32(14) 6_566 6_566
O48 K5 Nb3 145.85(15) 5_666 6_566
O1W K5 Nb3 80.0(2) . 6_566
O5 K5 Nb3 28.60(13) 6_566 6_566
O47 K5 Nb3 143.53(18) 5_666 6_566
O26 K5 Nb3 87.51(15) 6_566 6_566
O15W K5 Nb3 125.7(3) 6_566 6_566
O13W K5 Nb3 72.3(3) 6_566 6_566
O42 K5 Nb4 96.98(17) . 5_666
O01P K5 Nb4 146.03(17) 6_566 5_666
O48 K5 Nb4 31.52(13) 5_666 5_666
O1W K5 Nb4 80.7(2) . 5_666
O5 K5 Nb4 143.22(17) 6_566 5_666
O47 K5 Nb4 28.44(15) 5_666 5_666
O26 K5 Nb4 87.62(15) 6_566 5_666
O15W K5 Nb4 72.5(3) 6_566 5_666
O13W K5 Nb4 126.0(3) 6_566 5_666
Nb3 K5 Nb4 160.51(10) 6_566 5_666
O42 K5 Nb5 142.14(19) . 5_666
O01P K5 Nb5 87.84(15) 6_566 5_666
O48 K5 Nb5 29.55(13) 5_666 5_666
O1W K5 Nb5 71.8(3) . 5_666
O5 K5 Nb5 140.56(16) 6_566 5_666
O47 K5 Nb5 86.71(16) 5_666 5_666
O26 K5 Nb5 29.20(14) 6_566 5_666
O15W K5 Nb5 71.0(3) 6_566 5_666
O13W K5 Nb5 97.1(3) 6_566 5_666
Nb3 K5 Nb5 116.52(7) 6_566 5_666
Nb4 K5 Nb5 59.21(5) 5_666 5_666
K7 K6 O7W 103.0(7) . .
K7 K6 O22 79.9(6) . .
O7W K6 O22 82.7(5) . .
K7 K6 O12W 148.5(7) . 7_565
O7W K6 O12W 77.5(5) . 7_565
O22 K6 O12W 68.8(4) . 7_565
K7 K6 O30 85.4(6) . 4
O7W K6 O30 141.0(5) . 4
O22 K6 O30 136.2(4) . 4
O12W K6 O30 114.4(4) 7_565 4
K7 K6 O6W 73.6(6) . .
O7W K6 O6W 77.6(5) . .
O22 K6 O6W 142.2(4) . .
O12W K6 O6W 135.3(6) 7_565 .
O30 K6 O6W 68.3(3) 4 .
K7 K6 O8W 87.9(7) . .
O7W K6 O8W 153.3(6) . .
O22 K6 O8W 75.2(4) . .
O12W K6 O8W 80.6(4) 7_565 .
O30 K6 O8W 63.2(4) 4 .
O6W K6 O8W 129.1(5) . .
K7 K6 O11W 152.8(7) . 7_565
O7W K6 O11W 52.3(5) . 7_565
O22 K6 O11W 104.6(4) . 7_565
O12W K6 O11W 47.3(4) 7_565 7_565
O30 K6 O11W 107.1(4) 4 7_565
O6W K6 O11W 88.3(5) . 7_565
O8W K6 O11W 119.3(5) . 7_565
K7 K6 O29 140.0(7) . 4
O7W K6 O29 101.9(5) . 4
O22 K6 O29 134.3(4) . 4
O12W K6 O29 68.0(4) 7_565 4
O30 K6 O29 56.0(2) 4 4
O6W K6 O29 81.7(3) . 4
O8W K6 O29 83.7(4) . 4
O11W K6 O29 52.7(3) 7_565 4
K7 K6 W9 113.7(6) . 4
O7W K6 W9 121.4(5) . 4
O22 K6 W9 145.5(3) . 4
O12W K6 W9 91.3(4) 7_565 4
O30 K6 W9 29.42(18) 4 4
O6W K6 W9 71.5(3) . 4
O8W K6 W9 73.9(3) . 4
O11W K6 W9 78.0(3) 7_565 4
O29 K6 W9 26.72(14) 4 4
K7 K6 K10 126.4(6) . 7_565
O7W K6 K10 61.5(4) . 7_565
O22 K6 K10 138.2(4) . 7_565
O12W K6 K10 82.1(4) 7_565 7_565
O30 K6 K10 82.7(3) 4 7_565
O6W K6 K10 53.4(3) . 7_565
O8W K6 K10 130.0(4) . 7_565
O11W K6 K10 36.6(3) 7_565 7_565
O29 K6 K10 46.4(2) 4 7_565
W9 K6 K10 60.02(18) 4 7_565
K7 K6 K3 152.5(7) . 4_545
O7W K6 K3 103.6(5) . 4_545
O22 K6 K3 96.6(3) . 4_545
O12W K6 K3 36.1(3) 7_565 4_545
O30 K6 K3 78.5(3) 4 4_545
O6W K6 K3 119.2(4) . 4_545
O8W K6 K3 65.0(3) . 4_545
O11W K6 K3 54.6(3) 7_565 4_545
O29 K6 K3 37.84(18) 4 4_545
W9 K6 K3 56.27(13) 4 4_545
K10 K6 K3 73.6(2) 7_565 4_545
K6 K7 O22 75.2(6) . .
K6 K7 O32W 146.6(10) . .
O22 K7 O32W 78.9(8) . .
K6 K7 O6W 82.4(7) . .
O22 K7 O6W 144.9(5) . .
O32W K7 O6W 129.9(9) . .
K6 K7 O10W 123.7(7) . .
O22 K7 O10W 79.3(4) . .
O32W K7 O10W 70.4(9) . .
O6W K7 O10W 91.5(5) . .
K6 K7 O30 71.2(5) . 4
O22 K7 O30 127.2(4) . 4
O32W K7 O30 110.1(8) . 4
O6W K7 O30 67.5(3) . 4
O10W K7 O30 153.5(5) . 4
K6 K7 O33W 145.0(9) . 7_565
O22 K7 O33W 139.4(7) . 7_565
O32W K7 O33W 65.2(10) . 7_565
O6W K7 O33W 64.7(6) . 7_565
O10W K7 O33W 71.5(6) . 7_565
O30 K7 O33W 84.6(6) 4 7_565
K6 K7 O7W 55.2(6) . .
O22 K7 O7W 73.5(4) . .
O32W K7 O7W 134.8(9) . .
O6W K7 O7W 71.5(4) . .
O10W K7 O7W 69.7(5) . .
O30 K7 O7W 115.1(4) 4 .
O33W K7 O7W 119.3(7) 7_565 .
K6 K7 O8W 70.0(6) . .
O22 K7 O8W 71.5(4) . .
O32W K7 O8W 82.1(8) . .
O6W K7 O8W 125.3(4) . .
O10W K7 O8W 143.1(5) . .
O30 K7 O8W 59.3(3) 4 .
O33W K7 O8W 118.8(6) 7_565 .
O7W K7 O8W 120.4(5) . .
K6 K7 O022 120.5(6) . 4
O22 K7 O022 126.7(3) . 4
O32W K7 O022 61.7(8) . 4
O6W K7 O022 88.0(3) . 4
O10W K7 O022 115.1(4) . 4
O30 K7 O022 51.2(2) 4 4
O33W K7 O022 50.3(5) 7_565 4
O7W K7 O022 159.3(4) . 4
O8W K7 O022 68.9(3) . 4
K6 K7 W13 97.5(6) . 4
O22 K7 W13 134.6(3) . 4
O32W K7 W13 85.9(8) . 4
O6W K7 W13 74.4(3) . 4
O10W K7 W13 134.6(4) . 4
O30 K7 W13 26.65(16) 4 4
O33W K7 W13 63.3(5) 7_565 4
O7W K7 W13 138.4(4) . 4
O8W K7 W13 64.1(3) . 4
O022 K7 W13 24.85(14) 4 4
K6 K7 K4 116.1(6) . 4
O22 K7 K4 87.7(3) . 4
O32W K7 K4 41.6(8) . 4
O6W K7 K4 126.8(3) . 4
O10W K7 K4 112.0(4) . 4
O30 K7 K4 72.5(2) 4 4
O33W K7 K4 78.2(6) 7_565 4
O7W K7 K4 160.6(4) . 4
O8W K7 K4 46.3(3) . 4
O022 K7 K4 38.98(17) 4 4
W13 K7 K4 54.80(12) 4 4
K11 K8 O31W 98(2) . .
K11 K8 O45 97.0(19) . .
O31W K8 O45 124.0(9) . .
K11 K8 O17W 99(2) . .
O31W K8 O17W 14.3(8) . .
O45 K8 O17W 137.4(6) . .
K11 K8 O27W 107(2) . 6_566
O31W K8 O27W 146.8(9) . 6_566
O45 K8 O27W 75.2(4) . 6_566
O17W K8 O27W 135.5(6) . 6_566
K11 K8 O9 79.1(19) . 6_566
O31W K8 O9 84.2(9) . 6_566
O45 K8 O9 151.8(4) . 6_566
O17W K8 O9 70.4(5) . 6_566
O27W K8 O9 79.3(4) 6_566 6_566
K11 K8 O2W 22.0(19) . 1_565
O31W K8 O2W 99.9(8) . 1_565
O45 K8 O2W 77.6(4) . 1_565
O17W K8 O2W 106.0(5) . 1_565
O27W K8 O2W 111.4(5) 6_566 1_565
O9 K8 O2W 101.1(4) 6_566 1_565
K11 K8 O8 133(2) . 6_566
O31W K8 O8 88.7(8) . 6_566
O45 K8 O8 117.4(3) . 6_566
O17W K8 O8 77.6(5) . 6_566
O27W K8 O8 58.2(4) 6_566 6_566
O9 K8 O8 55.4(2) 6_566 6_566
O2W K8 O8 154.3(4) 1_565 6_566
K11 K8 O1 172(2) . 6_566
O31W K8 O1 77.9(8) . 6_566
O45 K8 O1 79.9(3) . 6_566
O17W K8 O1 79.0(5) . 6_566
O27W K8 O1 79.9(4) 6_566 6_566
O9 K8 O1 107.4(3) 6_566 6_566
O2W K8 O1 150.9(4) 1_565 6_566
O8 K8 O1 54.5(2) 6_566 6_566
K11 K8 O22W 77(2) . .
O31W K8 O22W 52.8(10) . .
O45 K8 O22W 78.8(6) . .
O17W K8 O22W 66.6(7) . .
O27W K8 O22W 154.0(7) 6_566 .
O9 K8 O22W 126.3(6) 6_566 .
O2W K8 O22W 63.3(7) 1_565 .
O8 K8 O22W 137.0(7) 6_566 .
O1 K8 O22W 94.5(7) 6_566 .
K11 K8 W1 104(2) . 6_566
O31W K8 W1 85.7(8) . 6_566
O45 K8 W1 141.0(3) . 6_566
O17W K8 W1 71.5(4) . 6_566
O27W K8 W1 67.3(3) 6_566 6_566
O9 K8 W1 25.26(15) 6_566 6_566
O2W K8 W1 125.8(4) 1_565 6_566
O8 K8 W1 30.18(14) 6_566 6_566
O1 K8 W1 83.18(19) 6_566 6_566
O22W K8 W1 137.7(6) . 6_566
K11 K8 W2 162(2) . 6_566
O31W K8 W2 82.7(8) . 6_566
O45 K8 W2 97.5(2) . 6_566
O17W K8 W2 77.5(4) . 6_566
O27W K8 W2 66.9(3) 6_566 6_566
O9 K8 W2 83.2(2) 6_566 6_566
O2W K8 W2 175.2(3) 1_565 6_566
O8 K8 W2 28.97(15) 6_566 6_566
O1 K8 W2 25.51(14) 6_566 6_566
O22W K8 W2 116.1(6) . 6_566
W1 K8 W2 58.25(9) 6_566 6_566
O28W K9 O47 113.5(5) 6_575 2_655
O28W K9 O33 80.4(5) 6_575 6_565
O47 K9 O33 160.9(3) 2_655 6_565
O28W K9 O18W 17.3(5) 6_575 6_575
O47 K9 O18W 129.3(5) 2_655 6_575
O33 K9 O18W 63.3(4) 6_565 6_575
O28W K9 O26W 139.1(6) 6_575 5_665
O47 K9 O26W 78.3(4) 2_655 5_665
O33 K9 O26W 82.6(4) 6_565 5_665
O18W K9 O26W 128.2(6) 6_575 5_665
O28W K9 O21W 98.5(5) 6_575 2_665
O47 K9 O21W 83.4(3) 2_655 2_665
O33 K9 O21W 108.2(3) 6_565 2_665
O18W K9 O21W 105.7(5) 6_575 2_665
O26W K9 O21W 122.1(5) 5_665 2_665
O28W K9 O41 82.9(5) 6_575 6_565
O47 K9 O41 111.9(3) 2_655 6_565
O33 K9 O41 54.9(2) 6_565 6_565
O18W K9 O41 71.3(4) 6_575 6_565
O26W K9 O41 57.1(4) 5_665 6_565
O21W K9 O41 162.8(3) 2_665 6_565
O28W K9 O14W 153.5(6) 6_575 5_665
O47 K9 O14W 79.3(4) 2_655 5_665
O33 K9 O14W 93.7(4) 6_565 5_665
O18W K9 O14W 148.0(5) 6_575 5_665
O26W K9 O14W 64.3(5) 5_665 5_665
O21W K9 O14W 58.5(4) 2_665 5_665
O41 K9 O14W 114.9(4) 6_565 5_665
O28W K9 O42 71.0(5) 6_575 6_565
O47 K9 O42 71.2(3) 2_655 6_565
O33 K9 O42 103.3(3) 6_565 6_565
O18W K9 O42 74.6(4) 6_575 6_565
O26W K9 O42 77.1(4) 5_665 6_565
O21W K9 O42 144.6(3) 2_665 6_565
O41 K9 O42 52.0(2) 6_565 6_565
O14W K9 O42 135.3(4) 5_665 6_565
O28W K9 W12 81.9(5) 6_575 6_565
O47 K9 W12 140.0(3) 2_655 6_565
O33 K9 W12 24.62(14) 6_565 6_565
O18W K9 W12 65.3(4) 6_575 6_565
O26W K9 W12 67.9(4) 5_665 6_565
O21W K9 W12 132.6(3) 2_665 6_565
O41 K9 W12 30.32(12) 6_565 6_565
O14W K9 W12 103.4(3) 5_665 6_565
O42 K9 W12 80.63(18) 6_565 6_565
O28W K9 K2 136.9(5) 6_575 5_665
O47 K9 K2 108.8(2) 2_655 5_665
O33 K9 K2 56.53(19) 6_565 5_665
O18W K9 K2 119.8(4) 6_575 5_665
O26W K9 K2 44.9(4) 5_665 5_665
O21W K9 K2 93.5(3) 2_665 5_665
O41 K9 K2 74.51(17) 6_565 5_665
O14W K9 K2 43.5(3) 5_665 5_665
O42 K9 K2 117.5(2) 6_565 5_665
W12 K9 K2 60.22(9) 6_565 5_665
O28W K9 W11 76.8(5) 6_575 6_565
O47 K9 W11 89.5(2) 2_655 6_565
O33 K9 W11 80.8(2) 6_565 6_565
O18W K9 W11 72.7(4) 6_575 6_565
O26W K9 W11 63.9(4) 5_665 6_565
O21W K9 W11 169.2(3) 2_665 6_565
O41 K9 W11 27.48(13) 6_565 6_565
O14W K9 W11 128.2(3) 5_665 6_565
O42 K9 W11 24.66(13) 6_565 6_565
W12 K9 W11 56.95(9) 6_565 6_565
K2 K9 W11 96.53(13) 5_665 6_565
O11W K10 O28W 107.1(6) . 6_575
O11W K10 O5 121.6(5) . .
O28W K10 O5 109.7(6) 6_575 .
O11W K10 O18W 98.7(5) . 6_575
O28W K10 O18W 18.0(5) 6_575 6_575
O5 K10 O18W 126.7(5) . 6_575
O11W K10 O29 62.5(4) . 6_565
O28W K10 O29 82.1(5) 6_575 6_565
O5 K10 O29 163.6(4) . 6_565
O18W K10 O29 64.2(4) 6_575 6_565
O11W K10 O39 113.3(4) . 6_565
O28W K10 O39 84.7(5) 6_575 6_565
O5 K10 O39 113.8(3) . 6_565
O18W K10 O39 73.1(4) 6_575 6_565
O29 K10 O39 54.5(2) 6_565 6_565
O11W K10 O6W 95.7(4) . 7_565
O28W K10 O6W 141.6(6) 6_575 7_565
O5 K10 O6W 82.1(3) . 7_565
O18W K10 O6W 130.4(5) 6_575 7_565
O29 K10 O6W 81.7(3) 6_565 7_565
O39 K10 O6W 57.7(3) 6_565 7_565
O11W K10 O42 165.9(4) . 6_565
O28W K10 O42 72.2(5) 6_575 6_565
O5 K10 O42 70.6(3) . 6_565
O18W K10 O42 76.4(4) 6_575 6_565
O29 K10 O42 103.7(3) 6_565 6_565
O39 K10 O42 52.7(2) 6_565 6_565
O6W K10 O42 78.3(3) 7_565 6_565
O11W K10 W9 85.6(4) . 6_565
O28W K10 W9 82.6(5) 6_575 6_565
O5 K10 W9 142.2(3) . 6_565
O18W K10 W9 65.6(4) 6_575 6_565
O29 K10 W9 24.82(16) 6_565 6_565
O39 K10 W9 29.63(14) 6_565 6_565
O6W K10 W9 68.6(2) 7_565 6_565
O42 K10 W9 80.3(2) 6_565 6_565
O11W K10 K6 50.5(4) . 7_565
O28W K10 K6 134.3(5) 6_575 7_565
O5 K10 K6 115.9(3) . 7_565
O18W K10 K6 116.7(5) 6_575 7_565
O29 K10 K6 52.6(2) 6_565 7_565
O39 K10 K6 74.2(2) 6_565 7_565
O6W K10 K6 47.2(3) 7_565 7_565
O42 K10 K6 119.6(3) 6_565 7_565
W9 K10 K6 59.24(16) 6_565 7_565
O11W K10 W11 141.6(4) . 6_565
O28W K10 W11 76.8(5) 6_575 6_565
O5 K10 W11 90.6(3) . 6_565
O18W K10 W11 73.2(4) 6_575 6_565
O29 K10 W11 80.8(2) 6_565 6_565
O39 K10 W11 28.30(15) 6_565 6_565
O6W K10 W11 66.4(2) 7_565 6_565
O42 K10 W11 24.40(14) 6_565 6_565
W9 K10 W11 56.57(11) 6_565 6_565
K6 K10 W11 98.7(2) 7_565 6_565
O11W K10 Nb3 112.2(4) . .
O28W K10 Nb3 126.1(5) 6_575 .
O5 K10 Nb3 16.47(17) . .
O18W K10 Nb3 142.7(5) 6_575 .
O29 K10 Nb3 149.3(3) 6_565 .
O39 K10 Nb3 110.7(2) 6_565 .
O6W K10 Nb3 68.5(2) 7_565 .
O42 K10 Nb3 77.77(19) 6_565 .
W9 K10 Nb3 134.7(2) 6_565 .
K6 K10 Nb3 99.4(2) 7_565 .
W11 K10 Nb3 93.19(16) 6_565 .
K8 K11 O2W 150(3) . 1_565
K8 K11 O9 84(2) . 6_566
O2W K11 O9 126.0(13) 1_565 6_566
K8 K11 O31W 66(2) . .
O2W K11 O31W 114.4(13) 1_565 .
O9 K11 O31W 80.7(10) 6_566 .
K8 K11 O45 66.5(18) . .
O2W K11 O45 86.7(9) 1_565 .
O9 K11 O45 139.6(11) 6_566 .
O31W K11 O45 109.0(12) . .
K8 K11 O17W 65.1(18) . .
O2W K11 O17W 122.1(12) 1_565 .
O9 K11 O17W 67.5(7) 6_566 .
O31W K11 O17W 13.2(7) . .
O45 K11 O17W 118.2(11) . .
K8 K11 O14W 117(2) . 6_566
O2W K11 O14W 65.8(8) 1_565 6_566
O9 K11 O14W 94.9(9) 6_566 6_566
O31W K11 O14W 174.5(13) . 6_566
O45 K11 O14W 76.4(7) . 6_566
O17W K11 O14W 162.2(11) . 6_566
K8 K11 O22W 88(2) . .
O2W K11 O22W 72.8(10) 1_565 .
O9 K11 O22W 130.8(11) 6_566 .
O31W K11 O22W 52.0(11) . .
O45 K11 O22W 76.9(9) . .
O17W K11 O22W 65.0(9) . .
O14W K11 O22W 131.4(11) 6_566 .
K8 K11 O27W 58.4(18) . 6_566
O2W K11 O27W 124.4(11) 1_565 6_566
O9 K11 O27W 74.2(7) 6_566 6_566
O31W K11 O27W 120.2(12) . 6_566
O45 K11 O27W 67.0(7) . 6_566
O17W K11 O27W 113.5(10) . 6_566
O14W K11 O27W 61.0(6) 6_566 6_566
O22W K11 O27W 137.6(12) . 6_566
K8 K11 O21 140(2) . 6_576
O2W K11 O21 66.0(8) 1_565 6_576
O9 K11 O21 64.1(6) 6_566 6_576
O31W K11 O21 85.1(10) . 6_576
O45 K11 O21 152.7(10) . 6_576
O17W K11 O21 80.3(8) . 6_576
O14W K11 O21 90.1(8) 6_566 6_576
O22W K11 O21 95.5(10) . 6_576
O27W K11 O21 126.6(9) 6_566 6_576
K8 K11 K2 97(2) . 6_566
O2W K11 K2 101.3(10) 1_565 6_566
O9 K11 K2 54.3(5) 6_566 6_566
O31W K11 K2 133.9(11) . 6_566
O45 K11 K2 100.9(7) . 6_566
O17W K11 K2 120.9(9) . 6_566
O14W K11 K2 42.5(5) 6_566 6_566
O22W K11 K2 173.7(11) . 6_566
O27W K11 K2 44.2(5) 6_566 6_566
O21 K11 K2 83.7(6) 6_576 6_566
K8 K11 W1 64.6(18) . 6_566
O2W K11 W1 145.2(12) 1_565 6_566
O9 K11 W1 19.9(3) 6_566 6_566
O31W K11 W1 77.7(9) . 6_566
O45 K11 W1 121.5(9) . 6_566
O17W K11 W1 65.2(6) . 6_566
O14W K11 W1 99.1(7) 6_566 6_566
O22W K11 W1 129.5(10) . 6_566
O27W K11 W1 60.9(5) 6_566 6_566
O21 K11 W1 83.7(6) 6_576 6_566
K2 K11 W1 56.7(4) 6_566 6_566
O53 Nb1 O54 98.4(3) . .
O53 Nb1 O55 102.7(3) . .
O54 Nb1 O55 90.0(3) . .
O53 Nb1 O52 100.6(3) . .
O54 Nb1 O52 89.9(3) . .
O55 Nb1 O52 156.4(3) . .
O53 Nb1 O50 96.3(3) . .
O54 Nb1 O50 165.3(3) . .
O55 Nb1 O50 86.4(3) . .
O52 Nb1 O50 87.7(3) . .
O53 Nb1 O37 171.8(3) . .
O54 Nb1 O37 84.9(3) . .
O55 Nb1 O37 84.7(2) . .
O52 Nb1 O37 71.8(3) . .
O50 Nb1 O37 80.7(3) . .
O53 Nb1 K1 43.9(3) . 1_565
O54 Nb1 K1 54.9(2) . 1_565
O55 Nb1 K1 105.5(2) . 1_565
O52 Nb1 K1 93.7(2) . 1_565
O50 Nb1 K1 139.7(2) . 1_565
O37 Nb1 K1 137.76(16) . 1_565
O21 Nb2 O54 98.6(3) . .
O21 Nb2 O24 103.0(3) . .
O54 Nb2 O24 89.4(3) . .
O21 Nb2 O34 101.3(3) . .
O54 Nb2 O34 89.5(3) . .
O24 Nb2 O34 155.6(3) . .
O21 Nb2 O026 96.6(3) . .
O54 Nb2 O026 164.8(3) . .
O24 Nb2 O026 86.2(3) . .
O34 Nb2 O026 88.5(3) . .
O21 Nb2 O35 172.3(3) . .
O54 Nb2 O35 83.9(3) . .
O24 Nb2 O35 84.3(3) . .
O34 Nb2 O35 71.4(3) . .
O026 Nb2 O35 81.2(3) . .
O21 Nb2 K1 43.4(2) . 1_565
O54 Nb2 K1 55.6(2) . 1_565
O24 Nb2 K1 105.6(2) . 1_565
O34 Nb2 K1 93.7(2) . 1_565
O026 Nb2 K1 139.6(2) . 1_565
O35 Nb2 K1 137.48(16) . 1_565
O5 Nb3 O026 103.8(3) . .
O5 Nb3 O01P 101.1(3) . .
O026 Nb3 O01P 91.3(3) . .
O5 Nb3 O3 101.2(3) . .
O026 Nb3 O3 89.3(3) . .
O01P Nb3 O3 156.9(3) . .
O5 Nb3 O2 99.6(3) . .
O026 Nb3 O2 156.3(3) . .
O01P Nb3 O2 88.0(3) . .
O3 Nb3 O2 82.4(3) . .
O5 Nb3 O23 168.3(3) . .
O026 Nb3 O23 85.5(3) . .
O01P Nb3 O23 85.6(3) . .
O3 Nb3 O23 71.4(2) . .
O2 Nb3 O23 70.8(2) . .
O5 Nb3 K5 51.7(3) . 6_565
O026 Nb3 K5 102.7(2) . 6_565
O01P Nb3 K5 49.4(2) . 6_565
O3 Nb3 K5 152.15(19) . 6_565
O2 Nb3 K5 94.8(2) . 6_565
O23 Nb3 K5 133.86(16) . 6_565
O5 Nb3 K10 25.8(3) . .
O026 Nb3 K10 120.2(2) . .
O01P Nb3 K10 117.6(2) . .
O3 Nb3 K10 81.6(2) . .
O2 Nb3 K10 80.6(2) . .
O23 Nb3 K10 142.6(2) . .
K5 Nb3 K10 70.65(13) 6_565 .
O47 Nb4 O50 103.2(3) . .
O47 Nb4 O48 101.5(3) . .
O50 Nb4 O48 91.0(3) . .
O47 Nb4 O46 100.9(3) . .
O50 Nb4 O46 90.1(3) . .
O48 Nb4 O46 156.6(3) . .
O47 Nb4 O44 99.2(3) . .
O50 Nb4 O44 157.5(3) . .
O48 Nb4 O44 86.8(3) . .
O46 Nb4 O44 83.3(3) . .
O47 Nb4 O38 168.2(3) . .
O50 Nb4 O38 86.5(3) . .
O48 Nb4 O38 84.9(3) . .
O46 Nb4 O38 71.9(2) . .
O44 Nb4 O38 71.0(3) . .
O47 Nb4 K5 51.9(2) . 5_666
O50 Nb4 K5 101.7(2) . 5_666
O48 Nb4 K5 49.6(2) . 5_666
O46 Nb4 K5 152.1(2) . 5_666
O44 Nb4 K5 93.9(2) . 5_666
O38 Nb4 K5 133.42(16) . 5_666
O47 Nb4 K9 23.2(3) . 2_655
O50 Nb4 K9 117.3(2) . 2_655
O48 Nb4 K9 117.4(2) . 2_655
O46 Nb4 K9 82.5(2) . 2_655
O44 Nb4 K9 83.2(2) . 2_655
O38 Nb4 K9 145.16(17) . 2_655
K5 Nb4 K9 69.63(11) 5_666 2_655
O55 Nb5 O26 101.3(3) . 2_655
O55 Nb5 O25 93.1(3) . .
O26 Nb5 O25 96.2(3) 2_655 .
O55 Nb5 O48 90.4(3) . .
O26 Nb5 O48 93.7(3) 2_655 .
O25 Nb5 O48 168.6(3) . .
O55 Nb5 O56 163.0(3) . .
O26 Nb5 O56 95.7(3) 2_655 .
O25 Nb5 O56 86.5(3) . .
O48 Nb5 O56 87.1(3) . .
O55 Nb5 O01C 88.9(3) . .
O26 Nb5 O01C 169.6(3) 2_655 .
O25 Nb5 O01C 85.3(3) . .
O48 Nb5 O01C 84.0(2) . .
O56 Nb5 O01C 74.1(3) . .
O55 Nb5 K5 97.5(2) . 5_666
O26 Nb5 K5 48.82(19) 2_655 5_666
O25 Nb5 K5 144.8(2) . 5_666
O48 Nb5 K5 44.9(2) . 5_666
O56 Nb5 K5 92.5(2) . 5_666
O01C Nb5 K5 128.26(16) . 5_666
O24 Nb6 O26 101.7(3) . .
O24 Nb6 O25 93.7(3) . .
O26 Nb6 O25 95.7(3) . .
O24 Nb6 O01P 90.0(3) . .
O26 Nb6 O01P 93.3(3) . .
O25 Nb6 O01P 169.3(3) . .
O24 Nb6 O10 162.8(3) . .
O26 Nb6 O10 95.2(3) . .
O25 Nb6 O10 87.7(3) . .
O01P Nb6 O10 85.8(3) . .
O24 Nb6 O19 89.0(3) . .
O26 Nb6 O19 168.9(3) . .
O25 Nb6 O19 86.4(3) . .
O01P Nb6 O19 83.7(3) . .
O10 Nb6 O19 74.0(3) . .
O24 Nb6 K5 97.7(2) . 6_565
O26 Nb6 K5 48.7(2) . 6_565
O25 Nb6 K5 144.2(2) . 6_565
O01P Nb6 K5 44.6(2) . 6_565
O10 Nb6 K5 91.01(19) . 6_565
O19 Nb6 K5 127.54(17) . 6_565
O9 W1 O10 99.8(3) . .
O9 W1 O015 97.6(3) . .
O10 W1 O015 91.4(3) . .
O9 W1 O8 98.0(3) . .
O10 W1 O8 91.5(3) . .
O015 W1 O8 163.4(3) . .
O9 W1 O11 102.8(3) . .
O10 W1 O11 157.4(3) . .
O015 W1 O11 86.9(3) . .
O8 W1 O11 84.2(3) . .
O9 W1 O19 173.7(3) . .
O10 W1 O19 74.1(3) . .
O015 W1 O19 84.3(2) . .
O8 W1 O19 80.8(2) . .
O11 W1 O19 83.3(3) . .
O9 W1 K8 45.1(3) . 6_565
O10 W1 K8 99.1(2) . 6_565
O015 W1 K8 142.4(2) . 6_565
O8 W1 K8 52.9(2) . 6_565
O11 W1 K8 95.9(2) . 6_565
O19 W1 K8 133.29(18) . 6_565
O9 W1 K2 58.1(3) . .
O10 W1 K2 42.2(2) . .
O015 W1 K2 101.8(2) . .
O8 W1 K2 91.3(2) . .
O11 W1 K2 159.6(2) . .
O19 W1 K2 115.61(16) . .
K8 W1 K2 65.96(12) 6_565 .
O9 W1 K1 40.3(2) . .
O10 W1 K1 98.5(2) . .
O015 W1 K1 57.30(19) . .
O8 W1 K1 138.2(2) . .
O11 W1 K1 99.6(2) . .
O19 W1 K1 141.02(16) . .
K8 W1 K1 85.39(12) 6_565 .
K2 W1 K1 70.93(7) . .
O9 W1 K11 33.9(5) . 6_565
O10 W1 K11 97.6(4) . 6_565
O015 W1 K11 131.5(5) . 6_565
O8 W1 K11 64.2(5) . 6_565
O11 W1 K11 100.4(4) . 6_565
O19 W1 K11 143.9(4) . 6_565
K8 W1 K11 11.5(4) 6_565 6_565
K2 W1 K11 60.0(4) . 6_565
K1 W1 K11 74.2(4) . 6_565
O1 W2 O2 101.7(3) . .
O1 W2 O8 101.3(3) . .
O2 W2 O8 90.5(3) . .
O1 W2 O6 101.8(3) . .
O2 W2 O6 90.0(3) . .
O8 W2 O6 156.3(3) . .
O1 W2 O7 100.5(3) . .
O2 W2 O7 157.8(3) . .
O8 W2 O7 84.4(3) . .
O6 W2 O7 86.3(3) . .
O1 W2 O23 173.9(3) . .
O2 W2 O23 74.9(3) . .
O8 W2 O23 83.9(3) . .
O6 W2 O23 73.3(3) . .
O7 W2 O23 83.1(2) . .
O1 W2 K8 50.4(3) . 6_565
O2 W2 K8 98.2(2) . 6_565
O8 W2 K8 50.9(2) . 6_565
O6 W2 K8 152.0(2) . 6_565
O7 W2 K8 95.2(2) . 6_565
O23 W2 K8 134.61(19) . 6_565
O22 W3 O3 100.5(4) . .
O22 W3 O13 102.5(4) . .
O3 W3 O13 93.8(3) . .
O22 W3 O6 99.7(3) . .
O3 W3 O6 88.8(3) . .
O13 W3 O6 156.7(3) . .
O22 W3 O00Y 100.4(4) . .
O3 W3 O00Y 158.8(3) . .
O13 W3 O00Y 84.4(3) . .
O6 W3 O00Y 84.9(3) . .
O22 W3 O23 172.1(3) . .
O3 W3 O23 75.9(3) . .
O13 W3 O23 84.9(3) . .
O6 W3 O23 73.3(3) . .
O00Y W3 O23 83.0(3) . .
O025 W4 O11 102.0(3) . .
O025 W4 O27 97.6(3) . .
O11 W4 O27 89.6(3) . .
O025 W4 O7 97.6(3) . .
O11 W4 O7 88.3(3) . .
O27 W4 O7 164.8(3) . .
O025 W4 O14 99.2(3) . .
O11 W4 O14 158.9(3) . .
O27 W4 O14 87.9(3) . .
O7 W4 O14 88.7(3) . .
O025 W4 O18 173.4(3) . .
O11 W4 O18 84.6(3) . .
O27 W4 O18 83.5(3) . .
O7 W4 O18 81.3(2) . .
O14 W4 O18 74.3(3) . .
O025 W4 K3 38.8(2) . 1_545
O11 W4 K3 93.6(2) . 1_545
O27 W4 K3 59.5(2) . 1_545
O7 W4 K3 135.7(2) . 1_545
O14 W4 K3 103.1(2) . 1_545
O18 W4 K3 142.98(16) . 1_545
O15 W6 O00Y 99.2(3) . .
O15 W6 O17 102.3(3) . .
O00Y W6 O17 87.8(3) . .
O15 W6 O28 96.9(3) . .
O00Y W6 O28 163.7(3) . .
O17 W6 O28 87.2(3) . .
O15 W6 O14 99.8(3) . .
O00Y W6 O14 90.9(3) . .
O17 W6 O14 157.7(3) . .
O28 W6 O14 87.9(3) . .
O15 W6 O18 173.7(3) . .
O00Y W6 O18 81.5(3) . .
O17 W6 O18 83.9(3) . .
O28 W6 O18 82.6(3) . .
O14 W6 O18 73.9(3) . .
O15 W6 K4 42.2(2) . .
O00Y W6 K4 141.3(2) . .
O17 W6 K4 101.3(2) . .
O28 W6 K4 54.9(2) . .
O14 W6 K4 93.5(2) . .
O18 W6 K4 136.47(16) . .
O16 W7 O34 99.1(3) . .
O16 W7 O01G 98.0(3) . .
O34 W7 O01G 92.3(3) . .
O16 W7 O17 100.3(3) . .
O34 W7 O17 160.2(3) . .
O01G W7 O17 88.8(3) . .
O16 W7 O13 95.7(3) . .
O34 W7 O13 90.1(3) . .
O01G W7 O13 165.5(3) . .
O17 W7 O13 84.1(3) . .
O16 W7 O35 174.6(3) . .
O34 W7 O35 76.1(3) . .
O01G W7 O35 84.9(3) . .
O17 W7 O35 84.3(3) . .
O13 W7 O35 81.9(3) . .
O16 W7 K3 41.1(2) . .
O34 W7 K3 94.1(2) . .
O01G W7 K3 57.3(2) . .
O17 W7 K3 103.1(2) . .
O13 W7 K3 136.7(2) . .
O35 W7 K3 140.81(17) . .
O51 W8 O52 99.2(3) . .
O51 W8 O49 97.1(3) . .
O52 W8 O49 92.3(3) . .
O51 W8 O01J 101.9(3) . .
O52 W8 O01J 158.8(3) . .
O49 W8 O01J 86.2(3) . .
O51 W8 O01G 97.1(3) . .
O52 W8 O01G 90.3(3) . .
O49 W8 O01G 164.9(3) . .
O01J W8 O01G 86.0(3) . .
O51 W8 O37 174.8(3) . .
O52 W8 O37 75.7(3) . .
O49 W8 O37 82.7(3) . .
O01J W8 O37 83.2(3) . .
O01G W8 O37 83.5(3) . .
O51 W8 K3 41.3(2) . .
O52 W8 K3 93.2(2) . .
O49 W8 K3 138.4(2) . .
O01J W8 K3 101.9(2) . .
O01G W8 K3 56.2(2) . .
O37 W8 K3 138.37(15) . .
O29 W9 O32 102.9(3) . .
O29 W9 O39 98.0(3) . .
O32 W9 O39 87.6(3) . .
O29 W9 O30 98.9(3) . .
O32 W9 O30 158.3(3) . .
O39 W9 O30 88.9(3) . .
O29 W9 O27 97.1(3) . .
O32 W9 O27 89.3(3) . .
O39 W9 O27 164.9(3) . .
O30 W9 O27 88.4(3) . .
O29 W9 O36 173.0(3) . .
O32 W9 O36 84.2(3) . .
O39 W9 O36 82.0(3) . .
O30 W9 O36 74.1(3) . .
O27 W9 O36 82.9(3) . .
O29 W9 K6 53.6(3) . 4_545
O32 W9 K6 155.8(3) . 4_545
O39 W9 K6 90.4(2) . 4_545
O30 W9 K6 45.6(3) . 4_545
O27 W9 K6 98.4(2) . 4_545
O36 W9 K6 119.4(2) . 4_545
O29 W9 K10 43.3(3) . 6_566
O32 W9 K10 99.2(2) . 6_566
O39 W9 K10 54.7(2) . 6_566
O30 W9 K10 96.3(2) . 6_566
O27 W9 K10 140.4(2) . 6_566
O36 W9 K10 136.2(2) . 6_566
K6 W9 K10 60.7(2) 4_545 6_566
O29 W9 K3 37.7(2) . 1_545
O32 W9 K3 93.6(2) . 1_545
O39 W9 K3 134.7(2) . 1_545
O30 W9 K3 104.0(2) . 1_545
O27 W9 K3 60.3(2) . 1_545
O36 W9 K3 143.17(17) . 1_545
K6 W9 K3 71.02(15) 4_545 1_545
K10 W9 K3 80.53(13) 6_566 1_545
O45 W10 O46 101.2(3) . .
O45 W10 O40 100.6(3) . .
O46 W10 O40 158.2(3) . .
O45 W10 O43 100.6(3) . .
O46 W10 O43 89.2(3) . .
O40 W10 O43 88.1(3) . .
O45 W10 O49 101.4(3) . .
O46 W10 O49 89.8(3) . .
O40 W10 O49 84.7(3) . .
O43 W10 O49 157.8(3) . .
O45 W10 O38 173.1(3) . .
O46 W10 O38 74.7(3) . .
O40 W10 O38 83.7(3) . .
O43 W10 O38 74.1(2) . .
O49 W10 O38 84.2(2) . .
O42 W11 O44 102.4(3) . .
O42 W11 O41 101.6(3) . .
O44 W11 O41 91.7(3) . .
O42 W11 O39 100.5(3) . .
O44 W11 O39 157.0(3) . .
O41 W11 O39 85.3(3) . .
O42 W11 O43 100.6(3) . .
O44 W11 O43 88.8(3) . .
O41 W11 O43 157.1(3) . .
O39 W11 O43 85.4(3) . .
O42 W11 O38 172.9(3) . .
O44 W11 O38 74.4(3) . .
O41 W11 O38 84.9(2) . .
O39 W11 O38 82.7(2) . .
O43 W11 O38 73.3(2) . .
O42 W11 K10 50.8(3) . 6_566
O44 W11 K10 153.1(2) . 6_566
O41 W11 K10 95.5(2) . 6_566
O39 W11 K10 49.7(2) . 6_566
O43 W11 K10 94.2(2) . 6_566
O38 W11 K10 131.99(19) . 6_566
O42 W11 K9 52.9(2) . 6_566
O44 W11 K9 96.9(2) . 6_566
O41 W11 K9 48.93(19) . 6_566
O39 W11 K9 98.1(2) . 6_566
O43 W11 K9 153.5(2) . 6_566
O38 W11 K9 133.22(17) . 6_566
K10 W11 K9 69.40(15) 6_566 6_566
O33 W12 O56 99.8(3) . .
O33 W12 O015 98.1(3) . .
O56 W12 O015 92.8(3) . .
O33 W12 O32 102.5(3) . .
O56 W12 O32 157.4(3) . .
O015 W12 O32 87.5(3) . .
O33 W12 O41 96.5(3) . .
O56 W12 O41 89.8(3) . .
O015 W12 O41 164.4(3) . .
O32 W12 O41 84.3(3) . .
O33 W12 O01C 172.8(3) . .
O56 W12 O01C 73.5(3) . .
O015 W12 O01C 85.1(2) . .
O32 W12 O01C 84.0(3) . .
O41 W12 O01C 80.9(2) . .
O33 W12 K9 42.8(3) . 6_566
O56 W12 K9 94.8(2) . 6_566
O015 W12 K9 140.9(2) . 6_566
O32 W12 K9 99.2(2) . 6_566
O41 W12 K9 53.9(2) . 6_566
O01C W12 K9 133.75(18) . 6_566
O33 W12 K2 58.4(3) . 2_655
O56 W12 K2 41.9(2) . 2_655
O015 W12 K2 103.8(2) . 2_655
O32 W12 K2 158.6(2) . 2_655
O41 W12 K2 88.3(2) . 2_655
O01C W12 K2 114.64(16) . 2_655
K9 W12 K2 60.59(11) 6_566 2_655
O33 W12 K1 39.7(2) . .
O56 W12 K1 99.3(2) . .
O015 W12 K1 58.5(2) . .
O32 W12 K1 100.1(2) . .
O41 W12 K1 136.09(18) . .
O01C W12 K1 142.86(15) . .
K9 W12 K1 82.45(11) 6_566 .
K2 W12 K1 71.88(8) 2_655 .
O022 W13 O01J 103.0(3) . .
O022 W13 O28 98.4(3) . .
O01J W13 O28 89.6(3) . .
O022 W13 O30 99.5(3) . .
O01J W13 O30 157.3(3) . .
O28 W13 O30 90.0(3) . .
O022 W13 O40 96.3(3) . .
O01J W13 O40 86.9(3) . .
O28 W13 O40 165.4(3) . .
O30 W13 O40 87.8(3) . .
O022 W13 O36 172.5(3) . .
O01J W13 O36 84.1(3) . .
O28 W13 O36 84.0(3) . .
O30 W13 O36 73.3(3) . .
O40 W13 O36 81.5(3) . .
O022 W13 K4 38.0(3) . .
O01J W13 K4 105.1(2) . .
O28 W13 K4 60.6(2) . .
O30 W13 K4 94.4(2) . .
O40 W13 K4 134.0(2) . .
O36 W13 K4 142.85(18) . .
O022 W13 K7 56.9(3) . 4_545
O01J W13 K7 157.4(2) . 4_545
O28 W13 K7 102.6(2) . 4_545
O30 W13 K7 43.4(2) . 4_545
O40 W13 K7 85.6(2) . 4_545
O36 W13 K7 115.7(2) . 4_545
K4 W13 K7 66.31(13) . 4_545
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
O1 W2 1.720(7) .
O1 K8 3.078(11) 6_565
O00Y W6 1.879(7) .
O00Y W3 1.957(7) .
O2 W2 1.864(7) .
O2 Nb3 2.055(7) .
O01C P1 1.540(7) .
O01C Nb5 2.271(7) .
O01C W12 2.431(6) .
O01G W7 1.888(7) .
O01G W8 1.933(7) .
O01G K3 3.234(7) .
O01J W13 1.875(7) .
O01J W8 1.921(7) .
O01P Nb3 1.903(7) .
O01P Nb6 1.968(7) .
O01P K5 2.778(7) 6_565
O3 W3 1.865(7) .
O3 Nb3 2.051(7) .
O02G K2 3.270(3) .
O02G K2 3.270(3) 2_655
O02G K1 3.413(11) 2_655
O02G K1 3.413(11) .
O5 Nb3 1.754(7) .
O5 K10 2.692(10) .
O5 K5 2.876(8) 6_565
O6 W2 1.916(7) .
O6 W3 1.944(7) .
O7 W4 1.899(6) .
O7 W2 1.939(6) .
O8 W2 1.906(7) .
O8 W1 1.927(7) .
O8 K8 3.056(9) 6_565
O9 W1 1.724(7) .
O9 K11 2.83(3) 6_565
O9 K8 2.862(9) 6_565
O9 K1 2.876(8) .
O9 K2 3.261(8) .
O10 W1 1.843(7) .
O10 Nb6 2.042(7) .
O10 K2 2.752(7) .
O11 W4 1.866(8) .
O11 W1 1.935(7) .
O13 W3 1.886(7) .
O13 W7 1.957(7) .
O14 W6 1.915(7) .
O14 W4 1.944(8) .
O15 W6 1.717(8) .
O15 K3 2.825(8) 4_545
O15 K4 3.011(9) .
O015 W12 1.895(6) .
O015 W1 1.919(6) .
O015 K1 3.344(7) .
O16 W7 1.713(7) .
O16 K4 2.728(8) 4
O16 K3 2.783(8) .
O17 W6 1.884(7) .
O17 W7 1.932(7) .
O18 P2 1.533(7) .
O18 W4 2.344(6) .
O18 W6 2.382(7) .
O19 P2 1.533(7) .
O19 Nb6 2.286(7) .
O19 W1 2.425(6) .
O21 Nb2 1.747(7) .
O21 K1 2.796(8) 1_565
O21 K11 3.21(3) 6_575
O1W K5 2.846(12) .
O22 W3 1.718(8) .
O22 K6 2.690(12) .
O22 K7 2.739(11) .
O022 W13 1.707(7) .
O022 K4 2.706(9) .
O022 K7 3.403(11) 4_545
O23 P2 1.581(7) .
O23 W3 2.362(7) .
O23 W2 2.380(6) .
O23 Nb3 2.423(6) .
O24 Nb6 1.867(6) .
O24 Nb2 1.953(7) .
O25 Nb6 1.918(6) .
O25 Nb5 1.930(6) .
O025 W4 1.719(7) .
O025 K4 2.715(8) 4_545
O025 K3 2.844(7) 1_545
O26 Nb6 1.892(7) .
O26 Nb5 1.900(7) 2_655
O26 K5 2.932(7) 6_565
O026 Nb3 1.900(7) .
O026 Nb2 1.979(7) .
O27 W4 1.890(6) .
O27 W9 1.922(7) .
O27 K3 3.425(7) 1_545
O28 W13 1.901(7) .
O28 W6 1.915(7) .
O28 K4 3.344(9) .
O29 W9 1.721(7) .
O29 K3 2.789(8) 1_545
O29 K10 2.810(10) 6_566
O29 K6 3.080(12) 4_545
O30 W9 1.918(7) .
O30 W13 1.919(7) .
O30 K6 2.792(10) 4_545
O30 K7 2.939(10) 4_545
O2W K11 2.29(3) 1_545
O2W K8 3.044(17) 1_545
O32 W9 1.881(7) .
O32 W12 1.929(7) .
O33 W12 1.724(6) .
O33 K9 2.812(8) 6_566
O33 K1 2.815(8) .
O33 K2 3.303(8) 2_655
O34 W7 1.872(7) .
O34 Nb2 1.978(7) .
O35 P2 1.531(7) .
O35 W7 2.329(7) .
O35 Nb2 2.453(7) .
O36 P1 1.540(7) .
O36 W9 2.349(7) .
O36 W13 2.381(7) .
O37 P1 1.519(7) .
O37 W8 2.348(6) .
O37 Nb1 2.430(7) .
O38 P1 1.579(7) .
O38 W10 2.381(6) .
O38 W11 2.389(6) .
O38 Nb4 2.401(7) .
O39 W9 1.890(7) .
O39 W11 1.938(7) .
O39 K10 3.120(10) 6_566
O40 W10 1.907(7) .
O40 W13 1.927(7) .
O3W K3 2.949(11) .
O41 W11 1.899(6) .
O41 W12 1.939(6) .
O41 K9 3.103(9) 6_566
O42 W11 1.709(7) .
O42 K5 2.665(7) .
O42 K10 3.205(12) 6_566
O42 K9 3.269(10) 6_566
O43 W10 1.916(7) .
O43 W11 1.957(7) .
O44 W11 1.857(7) .
O44 Nb4 2.051(7) .
O45 W10 1.717(7) .
O45 K8 2.717(9) .
O45 K11 2.94(3) .
O46 W10 1.887(7) .
O46 Nb4 2.034(7) .
O47 Nb4 1.750(7) .
O47 K9 2.676(9) 2_655
O47 K5 2.893(8) 5_666
O48 Nb4 1.917(6) .
O48 Nb5 1.951(6) .
O48 K5 2.793(7) 5_666
O49 W8 1.908(7) .
O49 W10 1.937(7) .
O50 Nb4 1.902(7) .
O50 Nb1 1.986(7) .
O51 W8 1.708(7) .
O51 K3 2.836(8) .
O52 W8 1.869(7) .
O52 Nb1 1.984(7) .
O53 Nb1 1.746(7) .
O53 K1 2.836(8) 1_565
O54 Nb2 1.926(7) .
O54 Nb1 1.926(7) .
O54 K1 3.140(9) 1_565
O55 Nb5 1.865(6) .
O55 Nb1 1.955(6) .
O56 W12 1.845(7) .
O56 Nb5 2.035(7) .
O56 K2 2.778(7) 2_655
O5W K2 2.781(10) 2_665
O5W K1 2.962(11) 2_665
O5W K1 2.995(11) 1_565
O6W K7 2.769(13) .
O6W K6 2.860(13) .
O6W K10 3.130(16) 7_565
O7W K6 2.584(18) .
O7W K7 3.067(17) .
O8W K6 2.927(17) .
O8W K4 3.111(15) 4
O8W K7 3.112(16) .
O9W O25W 0.84(2) .
O9W K3 3.100(18) 4_545
O10W K7 2.870(18) .
O11W K10 2.288(15) .
O11W K6 2.959(16) 7_565
O12W K3 2.774(14) 6_575
O12W K6 2.778(16) 7_565
O13W O27W 0.70(2) .
O13W K2 2.822(19) .
O13W K5 3.15(2) 6_565
O14W K2 2.683(16) .
O14W K11 3.09(3) 6_565
O14W K9 3.107(18) 5_665
O15W O26W 0.67(2) .
O15W K2 2.805(15) .
O15W K5 3.038(17) 6_565
O16W O33W 0.75(3) .
O17W O31W 0.68(4) .
O17W K8 2.74(2) .
O17W K11 2.98(3) .
O17W K4 3.33(2) 7_566
O18W O28W 0.87(2) .
O18W K10 2.788(19) 6_576
O18W K9 2.85(2) 6_576
O21W K9 2.966(13) 2_645
O22W K11 3.11(4) .
O22W K8 3.19(3) .
O24W O30W 1.46(5) .
O24W K4 2.90(4) .
O25W K4 3.28(3) 4_545
O26W K2 2.738(19) .
O26W K9 2.86(2) 5_665
O27W K2 2.783(16) .
O27W K8 2.839(18) 6_565
O27W K11 3.19(3) 6_565
O28W K10 2.55(2) 6_576
O28W K9 2.55(2) 6_576
O30W K4 2.78(3) .
O31W K8 2.70(4) .
O31W K11 2.94(5) .
O31W K4 3.15(4) 7_566
O32W K7 2.76(4) .
O32W K4 2.89(4) 4
O33W K7 3.01(3) 7_565
K1 Nb2 3.795(4) 1_545
K1 Nb1 3.823(4) 1_545
K1 W12 3.918(4) .
K2 W1 3.825(3) .
K3 W7 3.837(2) .
K3 W8 3.884(3) .
K5 Nb3 3.612(3) 6_566
K5 Nb4 3.623(3) 5_666
K5 Nb5 3.811(3) 5_666
K6 K7 1.171(11) .
K6 W9 3.773(8) 4
K6 K10 3.830(13) 7_565
K7 W13 4.021(7) 4
K8 K11 0.84(3) .
K8 W1 3.805(5) 6_566
K8 W2 3.874(7) 6_566
K9 W12 3.821(5) 6_565
K9 W11 4.001(7) 6_565
K10 W9 3.803(6) 6_565
K10 W11 4.000(9) 6_565
K10 Nb3 4.160(7) .
K11 W1 4.09(3) 6_566
