#------------------------------------------------------------------------------
#$Date: 2022-02-06 06:45:20 +0200 (Sun, 06 Feb 2022) $
#$Revision: 272821 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/59/1565983.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1565983
loop_
_publ_author_name
'Hu, Qifa'
'Wen, Bin'
'Fan, Changzeng'
_publ_section_title
;
 The Al~61.49~Mn~11.35~Ni₄ phase in the Al--Mn--Ni system
;
_journal_coeditor_code           WM4158
_journal_issue                   1
_journal_name_full               IUCrData
_journal_page_first              x220038
_journal_paper_doi               10.1107/S2414314622000384
_journal_volume                  7
_journal_year                    2022
_chemical_formula_sum            'Al61.49 Mn11.35 Ni4'
_chemical_formula_weight         2517.49
_space_group_crystal_system      orthorhombic
_space_group_IT_number           63
_space_group_name_Hall           '-C 2c 2'
_space_group_name_H-M_alt        'C m c m'
_audit_creation_method           SHELXL-2016/6
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   7.6135(3)
_cell_length_b                   23.9582(11)
_cell_length_c                   12.4828(6)
_cell_measurement_reflns_used    8707
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      30.60
_cell_measurement_theta_min      2.36
_cell_volume                     2276.93(18)
_computing_cell_refinement
;
SAINT (Bruker, 2015)
;
_computing_data_collection
;
APEX3 (Bruker, 2015)
;
_computing_data_reduction
;
SAINT (Bruker, 2015)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg & Putz, 2017)
;
_computing_publication_material
;
publCIF (Westrip, 2010)
;
_computing_structure_refinement
;
SHELXL (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 Venture Photon 100 CMOS'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0897
_diffrn_reflns_av_unetI/netI     0.0293
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            40442
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         28.272
_diffrn_reflns_theta_min         2.356
_exptl_absorpt_coefficient_mu    5.854
_exptl_absorpt_correction_T_max  0.7461
_exptl_absorpt_correction_T_min  0.6481
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour            metallic
_exptl_crystal_density_diffrn    3.672
_exptl_crystal_description       fragment
_exptl_crystal_F_000             2390
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.847
_refine_diff_density_min         -1.026
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_matrix_type           full
_refine_ls_number_parameters     114
_refine_ls_number_reflns         1584
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.062
_refine_ls_R_factor_all          0.0556
_refine_ls_R_factor_gt           0.0390
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0463P)²+17.4467P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0876
_refine_ls_wR_factor_ref         0.0945
_reflns_number_gt                1269
_reflns_number_total             1584
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            wm4158sup1.cif
_cod_data_source_block           I
_cod_depositor_comments          'Adding full bibliography for 1565983.cif.'
_cod_database_code               1565983
_cod_database_fobs_code          1565983
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni Ni1 0.000000 0.91273(3) 0.06707(7) 0.0123(2) Uani d 1 . .
Mn Mn1 0.000000 0.54113(5) 0.750000 0.0070(3) Uani d 1 A .
Mn Mn2 0.000000 0.92062(7) 0.750000 0.0071(6) Uani d 0.677(5) A .
Mn Mn3 0.000000 0.63847(3) 0.05426(6) 0.00525(19) Uani d 1 . .
Mn Mn4 0.18574(11) 0.71395(3) 0.750000 0.00517(19) Uani d 1 . .
Al Al1 0.000000 0.81074(10) 0.750000 0.0081(5) Uani d 1 A .
Al Al2 0.000000 0.79366(10) 0.250000 0.0083(5) Uani d 1 . .
Al Al3 0.000000 0.63386(10) 0.250000 0.0111(5) Uani d 1 . .
Al Al4 0.000000 0.63837(6) 0.84947(13) 0.0066(3) Uani d 1 A .
Al Al5 0.000000 0.73945(7) 0.93387(13) 0.0076(3) Uani d 1 A .
Al Al6 0.000000 0.53869(7) 0.11718(14) 0.0129(4) Uani d 1 . .
Al Al7A 0.000000 0.98517(9) 0.9064(2) 0.0170(8) Uani d 0.811(8) A 1
Al Al7B 0.000000 0.000000 0.000000 0.0170(8) Uani d 0.121(7) B 2
Al Al8 0.2272(3) 0.01406(8) 0.250000 0.0250(5) Uani d 1 . .
Al Al9 0.1846(2) 0.89615(7) 0.250000 0.0094(4) Uani d 1 . .
Al Al10 0.18981(16) 0.55406(5) 0.93399(9) 0.0075(3) Uani d 1 . .
Al Al11 0.19159(16) 0.82804(5) 0.06539(9) 0.0074(3) Uani d 1 . .
Al Al12 0.18747(16) 0.71601(5) 0.12610(9) 0.0080(3) Uani d 1 . .
Al Al13 0.18943(17) 0.89124(5) 0.88587(11) 0.0135(3) Uani d 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Al7A Ni1 Al10 9_576 13_566 71.59(3) ?
Al7A Ni1 Al10 9_576 8_466 71.59(3) ?
Al10 Ni1 Al10 13_566 8_466 142.75(6) ?
Al7B Ni1 Al11 1_565 . 138.65(3) ?
Al7A Ni1 Al11 9_576 . 143.68(3) ?
Al10 Ni1 Al11 13_566 . 72.91(4) ?
Al10 Ni1 Al11 8_466 . 144.33(5) ?
Al7A Ni1 Al11 9_576 12 143.68(3) ?
Al10 Ni1 Al11 13_566 12 144.33(5) ?
Al10 Ni1 Al11 8_466 12 72.91(4) ?
Al11 Ni1 Al11 . 12 71.42(6) ?
Al7A Ni1 Al7A 9_576 1_554 56.83(10) ?
Al10 Ni1 Al7A 13_566 1_554 77.70(3) ?
Al10 Ni1 Al7A 8_466 1_554 77.70(3) ?
Al11 Ni1 Al7A . 1_554 121.67(5) ?
Al11 Ni1 Al7A 12 1_554 121.67(5) ?
Al7B Ni1 Al9 1_565 . 116.69(4) ?
Al7A Ni1 Al9 9_576 . 91.85(7) ?
Al10 Ni1 Al9 13_566 . 63.89(4) ?
Al10 Ni1 Al9 8_466 . 122.86(5) ?
Al11 Ni1 Al9 . . 65.51(4) ?
Al11 Ni1 Al9 12 . 101.00(5) ?
Al7A Ni1 Al9 1_554 . 137.13(5) ?
Al7A Ni1 Al9 9_576 3 91.85(7) ?
Al10 Ni1 Al9 13_566 3 122.86(5) ?
Al10 Ni1 Al9 8_466 3 63.89(4) ?
Al11 Ni1 Al9 . 3 100.99(5) ?
Al11 Ni1 Al9 12 3 65.51(4) ?
Al7A Ni1 Al9 1_554 3 137.13(5) ?
Al9 Ni1 Al9 . 3 62.46(7) ?
Al7A Ni1 Al13 9_576 12_554 107.32(6) ?
Al10 Ni1 Al13 13_566 12_554 123.79(5) ?
Al10 Ni1 Al13 8_466 12_554 63.61(4) ?
Al11 Ni1 Al13 . 12_554 98.53(4) ?
Al11 Ni1 Al13 12 12_554 62.09(4) ?
Al7A Ni1 Al13 1_554 12_554 59.81(5) ?
Al9 Ni1 Al13 . 12_554 160.69(5) ?
Al9 Ni1 Al13 3 12_554 113.34(4) ?
Al7A Ni1 Al13 9_576 1_554 107.32(6) ?
Al10 Ni1 Al13 13_566 1_554 63.61(4) ?
Al10 Ni1 Al13 8_466 1_554 123.79(5) ?
Al11 Ni1 Al13 . 1_554 62.09(4) ?
Al11 Ni1 Al13 12 1_554 98.53(4) ?
Al7A Ni1 Al13 1_554 1_554 59.81(5) ?
Al9 Ni1 Al13 . 1_554 113.34(4) ?
Al9 Ni1 Al13 3 1_554 160.69(5) ?
Al13 Ni1 Al13 12_554 1_554 63.74(6) ?
Al8 Mn1 Al8 15_456 13_556 115.05(12) ?
Al8 Mn1 Al6 15_456 2_565 66.07(5) ?
Al8 Mn1 Al6 13_556 2_565 66.07(5) ?
Al8 Mn1 Al6 15_456 9_566 66.07(5) ?
Al8 Mn1 Al6 13_556 9_566 66.07(5) ?
Al6 Mn1 Al6 2_565 9_566 81.85(9) ?
Al8 Mn1 Al4 15_456 . 118.28(5) ?
Al8 Mn1 Al4 13_556 . 118.28(5) ?
Al6 Mn1 Al4 2_565 . 167.13(6) ?
Al6 Mn1 Al4 9_566 . 111.02(5) ?
Al8 Mn1 Al4 15_456 10_557 118.28(5) ?
Al8 Mn1 Al4 13_556 10_557 118.28(5) ?
Al6 Mn1 Al4 2_565 10_557 111.02(5) ?
Al6 Mn1 Al4 9_566 10_557 167.13(6) ?
Al4 Mn1 Al4 . 10_557 56.11(7) ?
Al8 Mn1 Al10 15_456 3_556 67.33(3) ?
Al8 Mn1 Al10 13_556 3_556 120.48(3) ?
Al6 Mn1 Al10 2_565 3_556 62.28(4) ?
Al6 Mn1 Al10 9_566 3_556 129.53(5) ?
Al4 Mn1 Al10 . 3_556 107.18(5) ?
Al4 Mn1 Al10 10_557 3_556 60.29(4) ?
Al8 Mn1 Al10 15_456 12 67.33(3) ?
Al8 Mn1 Al10 13_556 12 120.48(3) ?
Al6 Mn1 Al10 2_565 12 129.53(5) ?
Al6 Mn1 Al10 9_566 12 62.28(4) ?
Al4 Mn1 Al10 . 12 60.29(4) ?
Al4 Mn1 Al10 10_557 12 107.18(5) ?
Al10 Mn1 Al10 3_556 12 114.48(5) ?
Al8 Mn1 Al10 15_456 10_557 120.48(3) ?
Al8 Mn1 Al10 13_556 10_557 67.33(3) ?
Al6 Mn1 Al10 2_565 10_557 62.28(4) ?
Al6 Mn1 Al10 9_566 10_557 129.53(5) ?
Al4 Mn1 Al10 . 10_557 107.18(5) ?
Al4 Mn1 Al10 10_557 10_557 60.29(4) ?
Al10 Mn1 Al10 3_556 10_557 63.89(5) ?
Al10 Mn1 Al10 12 10_557 166.98(7) ?
Al8 Mn1 Al10 15_456 . 120.48(3) ?
Al8 Mn1 Al10 13_556 . 67.33(3) ?
Al6 Mn1 Al10 2_565 . 129.54(5) ?
Al6 Mn1 Al10 9_566 . 62.28(4) ?
Al4 Mn1 Al10 . . 60.29(4) ?
Al4 Mn1 Al10 10_557 . 107.18(5) ?
Al10 Mn1 Al10 3_556 . 166.98(7) ?
Al10 Mn1 Al10 12 . 63.89(5) ?
Al10 Mn1 Al10 10_557 . 114.48(5) ?
Al8 Mn1 Al9 15_456 13_566 179.56(8) ?
Al8 Mn1 Al9 13_556 13_566 64.51(6) ?
Al6 Mn1 Al9 2_565 13_566 113.63(3) ?
Al6 Mn1 Al9 9_566 13_566 113.63(3) ?
Al4 Mn1 Al9 . 13_566 62.08(4) ?
Al4 Mn1 Al9 10_557 13_566 62.09(4) ?
Al10 Mn1 Al9 3_556 13_566 112.85(4) ?
Al10 Mn1 Al9 12 13_566 112.85(4) ?
Al10 Mn1 Al9 10_557 13_566 59.42(3) ?
Al10 Mn1 Al9 . 13_566 59.42(3) ?
Al8 Mn1 Al9 15_456 15_466 64.51(6) ?
Al8 Mn1 Al9 13_556 15_466 179.56(8) ?
Al6 Mn1 Al9 2_565 15_466 113.63(3) ?
Al6 Mn1 Al9 9_566 15_466 113.63(3) ?
Al4 Mn1 Al9 . 15_466 62.09(4) ?
Al4 Mn1 Al9 10_557 15_466 62.09(4) ?
Al10 Mn1 Al9 3_556 15_466 59.42(3) ?
Al10 Mn1 Al9 12 15_466 59.42(3) ?
Al10 Mn1 Al9 10_557 15_466 112.85(4) ?
Al10 Mn1 Al9 . 15_466 112.85(4) ?
Al9 Mn1 Al9 13_566 15_466 115.92(8) ?
Al8 Mn2 Al8 11_566 9_566 95.71(13) ?
Al8 Mn2 Al13 11_566 3_556 131.32(5) ?
Al8 Mn2 Al13 9_566 3_556 75.18(5) ?
Al8 Mn2 Al13 11_566 10_557 75.18(5) ?
Al8 Mn2 Al13 9_566 10_557 131.32(5) ?
Al13 Mn2 Al13 3_556 10_557 76.30(7) ?
Al8 Mn2 Al13 11_566 12 131.32(5) ?
Al8 Mn2 Al13 9_566 12 75.18(5) ?
Al13 Mn2 Al13 3_556 12 93.17(7) ?
Al13 Mn2 Al13 10_557 12 144.92(10) ?
Al8 Mn2 Al13 11_566 . 75.18(5) ?
Al8 Mn2 Al13 9_566 . 131.32(5) ?
Al13 Mn2 Al13 3_556 . 144.91(10) ?
Al13 Mn2 Al13 10_557 . 93.16(7) ?
Al13 Mn2 Al13 12 . 76.30(7) ?
Al8 Mn2 Al7A 11_566 10_557 65.38(5) ?
Al8 Mn2 Al7A 9_566 10_557 65.38(5) ?
Al13 Mn2 Al7A 3_556 10_557 67.53(5) ?
Al13 Mn2 Al7A 10_557 10_557 67.53(5) ?
Al13 Mn2 Al7A 12 10_557 139.16(5) ?
Al13 Mn2 Al7A . 10_557 139.16(5) ?
Al8 Mn2 Al7A 11_566 . 65.38(6) ?
Al8 Mn2 Al7A 9_566 . 65.38(5) ?
Al13 Mn2 Al7A 3_556 . 139.16(5) ?
Al13 Mn2 Al7A 10_557 . 139.16(5) ?
Al13 Mn2 Al7A 12 . 67.53(5) ?
Al13 Mn2 Al7A . . 67.53(5) ?
Al7A Mn2 Al7A 10_557 . 103.23(13) ?
Al8 Mn2 Al1 11_566 . 132.14(7) ?
Al8 Mn2 Al1 9_566 . 132.14(7) ?
Al13 Mn2 Al1 3_556 . 72.46(5) ?
Al13 Mn2 Al1 10_557 . 72.46(5) ?
Al13 Mn2 Al1 12 . 72.46(5) ?
Al13 Mn2 Al1 . . 72.46(5) ?
Al7A Mn2 Al1 10_557 . 128.38(6) ?
Al7A Mn2 Al1 . . 128.38(6) ?
Al3 Mn3 Al12 . 12 71.11(6) ?
Al3 Mn3 Al12 . . 71.11(6) ?
Al12 Mn3 Al12 12 . 69.36(6) ?
Al3 Mn3 Al6 . . 69.22(7) ?
Al12 Mn3 Al6 12 . 126.30(5) ?
Al12 Mn3 Al6 . . 126.30(5) ?
Al3 Mn3 Al4 . 1_554 177.36(8) ?
Al12 Mn3 Al4 12 1_554 110.99(5) ?
Al12 Mn3 Al4 . 1_554 110.99(5) ?
Al6 Mn3 Al4 . 1_554 108.13(6) ?
Al3 Mn3 Al13 . 8_466 72.43(4) ?
Al12 Mn3 Al13 12 8_466 65.12(4) ?
Al12 Mn3 Al13 . 8_466 128.48(5) ?
Al6 Mn3 Al13 . 8_466 69.36(3) ?
Al4 Mn3 Al13 1_554 8_466 106.82(4) ?
Al3 Mn3 Al13 . 13_566 72.43(4) ?
Al12 Mn3 Al13 12 13_566 128.48(5) ?
Al12 Mn3 Al13 . 13_566 65.12(4) ?
Al6 Mn3 Al13 . 13_566 69.36(3) ?
Al4 Mn3 Al13 1_554 13_566 106.82(4) ?
Al13 Mn3 Al13 8_466 13_566 132.84(7) ?
Al3 Mn3 Al5 . 1_554 124.43(8) ?
Al12 Mn3 Al5 12 1_554 63.87(4) ?
Al12 Mn3 Al5 . 1_554 63.87(4) ?
Al6 Mn3 Al5 . 1_554 166.34(6) ?
Al4 Mn3 Al5 1_554 1_554 58.21(5) ?
Al13 Mn3 Al5 8_466 1_554 112.78(3) ?
Al13 Mn3 Al5 13_566 1_554 112.78(3) ?
Al3 Mn3 Al11 . 8_465 121.85(3) ?
Al12 Mn3 Al11 12 8_465 61.18(4) ?
Al12 Mn3 Al11 . 8_465 116.13(5) ?
Al6 Mn3 Al11 . 8_465 115.10(3) ?
Al4 Mn3 Al11 1_554 8_465 58.97(3) ?
Al13 Mn3 Al11 8_466 8_465 58.86(4) ?
Al13 Mn3 Al11 13_566 8_465 165.67(5) ?
Al5 Mn3 Al11 1_554 8_465 59.51(3) ?
Al3 Mn3 Al11 . 13_565 121.85(3) ?
Al12 Mn3 Al11 12 13_565 116.14(5) ?
Al12 Mn3 Al11 . 13_565 61.18(4) ?
Al6 Mn3 Al11 . 13_565 115.10(3) ?
Al4 Mn3 Al11 1_554 13_565 58.97(3) ?
Al13 Mn3 Al11 8_466 13_565 165.67(5) ?
Al13 Mn3 Al11 13_566 13_565 58.86(4) ?
Al5 Mn3 Al11 1_554 13_565 59.51(3) ?
Al11 Mn3 Al11 8_465 13_565 108.34(5) ?
Al3 Mn3 Al10 . 12_554 119.02(6) ?
Al12 Mn3 Al10 12 12_554 114.67(4) ?
Al12 Mn3 Al10 . 12_554 169.66(5) ?
Al6 Mn3 Al10 . 12_554 59.98(4) ?
Al4 Mn3 Al10 1_554 12_554 58.82(4) ?
Al13 Mn3 Al10 8_466 12_554 60.10(4) ?
Al13 Mn3 Al10 13_566 12_554 114.44(5) ?
Al5 Mn3 Al10 1_554 12_554 108.59(4) ?
Al11 Mn3 Al10 8_465 12_554 61.50(3) ?
Al11 Mn3 Al10 13_565 12_554 109.26(4) ?
Al3 Mn3 Al10 . 1_554 119.02(6) ?
Al12 Mn3 Al10 12 1_554 169.66(5) ?
Al12 Mn3 Al10 . 1_554 114.67(4) ?
Al6 Mn3 Al10 . 1_554 59.98(4) ?
Al4 Mn3 Al10 1_554 1_554 58.82(4) ?
Al13 Mn3 Al10 8_466 1_554 114.44(5) ?
Al13 Mn3 Al10 13_566 1_554 60.10(4) ?
Al5 Mn3 Al10 1_554 1_554 108.59(4) ?
Al11 Mn3 Al10 8_465 1_554 109.26(4) ?
Al11 Mn3 Al10 13_565 1_554 61.50(3) ?
Al10 Mn3 Al10 12_554 1_554 59.69(5) ?
Al2 Mn4 Al12 13_566 13_566 70.30(6) ?
Al2 Mn4 Al12 13_566 6_565 70.30(6) ?
Al12 Mn4 Al12 13_566 6_565 77.24(6) ?
Al2 Mn4 Al4 13_566 . 119.16(6) ?
Al12 Mn4 Al4 13_566 . 112.57(5) ?
Al12 Mn4 Al4 6_565 . 167.76(5) ?
Al2 Mn4 Al4 13_566 10_557 119.16(6) ?
Al12 Mn4 Al4 13_566 10_557 167.76(5) ?
Al12 Mn4 Al4 6_565 10_557 112.57(5) ?
Al4 Mn4 Al4 . 10_557 56.78(7) ?
Al2 Mn4 Al11 13_566 6_565 67.93(4) ?
Al12 Mn4 Al11 13_566 6_565 130.89(5) ?
Al12 Mn4 Al11 6_565 6_565 65.30(4) ?
Al4 Mn4 Al11 . 6_565 109.69(5) ?
Al4 Mn4 Al11 10_557 6_565 61.32(4) ?
Al2 Mn4 Al11 13_566 13_566 67.93(4) ?
Al12 Mn4 Al11 13_566 13_566 65.30(4) ?
Al12 Mn4 Al11 6_565 13_566 130.89(5) ?
Al4 Mn4 Al11 . 13_566 61.32(4) ?
Al4 Mn4 Al11 10_557 13_566 109.69(5) ?
Al11 Mn4 Al11 6_565 13_566 118.44(6) ?
Al2 Mn4 Al1 13_566 . 125.73(7) ?
Al12 Mn4 Al1 13_566 . 67.95(4) ?
Al12 Mn4 Al1 6_565 . 67.95(4) ?
Al4 Mn4 Al1 . . 108.06(4) ?
Al4 Mn4 Al1 10_557 . 108.06(4) ?
Al11 Mn4 Al1 6_565 . 120.10(3) ?
Al11 Mn4 Al1 13_566 . 120.10(3) ?
Al2 Mn4 Al5 13_566 . 121.80(3) ?
Al12 Mn4 Al5 13_566 . 62.05(4) ?
Al12 Mn4 Al5 6_565 . 124.60(5) ?
Al4 Mn4 Al5 . . 58.77(5) ?
Al4 Mn4 Al5 10_557 . 105.73(4) ?
Al11 Mn4 Al5 6_565 . 167.00(5) ?
Al11 Mn4 Al5 13_566 . 63.11(4) ?
Al1 Mn4 Al5 . . 62.93(4) ?
Al2 Mn4 Al5 13_566 10_557 121.80(3) ?
Al12 Mn4 Al5 13_566 10_557 124.60(5) ?
Al12 Mn4 Al5 6_565 10_557 62.05(4) ?
Al4 Mn4 Al5 . 10_557 105.73(4) ?
Al4 Mn4 Al5 10_557 10_557 58.77(5) ?
Al11 Mn4 Al5 6_565 10_557 63.11(4) ?
Al11 Mn4 Al5 13_566 10_557 167.00(5) ?
Al1 Mn4 Al5 . 10_557 62.93(4) ?
Al5 Mn4 Al5 . 10_557 112.26(5) ?
Al2 Mn4 Al9 13_566 13_566 65.12(7) ?
Al12 Mn4 Al9 13_566 13_566 119.85(5) ?
Al12 Mn4 Al9 6_565 13_566 119.85(5) ?
Al4 Mn4 Al9 . 13_566 62.64(4) ?
Al4 Mn4 Al9 10_557 13_566 62.64(4) ?
Al11 Mn4 Al9 6_565 13_566 61.75(3) ?
Al11 Mn4 Al9 13_566 13_566 61.75(3) ?
Al1 Mn4 Al9 . 13_566 169.14(6) ?
Al5 Mn4 Al9 . 13_566 112.73(4) ?
Al5 Mn4 Al9 10_557 13_566 112.73(4) ?
Al2 Mn4 Mn4 13_566 3_556 175.64(6) ?
Al12 Mn4 Mn4 13_566 3_556 112.93(3) ?
Al12 Mn4 Mn4 6_565 3_556 112.93(3) ?
Al4 Mn4 Mn4 . 3_556 57.21(3) ?
Al4 Mn4 Mn4 10_557 3_556 57.21(3) ?
Al11 Mn4 Mn4 6_565 3_556 110.38(3) ?
Al11 Mn4 Mn4 13_566 3_556 110.38(3) ?
Al1 Mn4 Mn4 . 3_556 58.63(3) ?
Al5 Mn4 Mn4 . 3_556 59.23(2) ?
Al5 Mn4 Mn4 10_557 3_556 59.23(2) ?
Al9 Mn4 Mn4 13_566 3_556 110.52(4) ?
Mn2 Al1 Mn4 . . 148.62(3) ?
Mn2 Al1 Mn4 . 3_556 148.63(3) ?
Mn4 Al1 Mn4 . 3_556 62.75(6) ?
Mn2 Al1 Al5 . . 126.65(5) ?
Mn4 Al1 Al5 . . 59.36(5) ?
Mn4 Al1 Al5 3_556 . 59.36(5) ?
Mn2 Al1 Al5 . 10_557 126.65(5) ?
Mn4 Al1 Al5 . 10_557 59.36(5) ?
Mn4 Al1 Al5 3_556 10_557 59.36(5) ?
Al5 Al1 Al5 . 10_557 106.69(10) ?
Mn2 Al1 Al12 . 15_466 102.72(5) ?
Mn4 Al1 Al12 . 15_466 103.75(7) ?
Mn4 Al1 Al12 3_556 15_466 52.13(3) ?
Al5 Al1 Al12 . 15_466 107.16(6) ?
Al5 Al1 Al12 10_557 15_466 56.09(3) ?
Mn2 Al1 Al12 . 13_566 102.72(5) ?
Mn4 Al1 Al12 . 13_566 52.13(3) ?
Mn4 Al1 Al12 3_556 13_566 103.75(7) ?
Al5 Al1 Al12 . 13_566 56.09(3) ?
Al5 Al1 Al12 10_557 13_566 107.16(6) ?
Al12 Al1 Al12 15_466 13_566 154.55(10) ?
Mn2 Al1 Al12 . 8_466 102.72(5) ?
Mn4 Al1 Al12 . 8_466 103.75(7) ?
Mn4 Al1 Al12 3_556 8_466 52.13(3) ?
Al5 Al1 Al12 . 8_466 56.09(3) ?
Al5 Al1 Al12 10_557 8_466 107.16(6) ?
Al12 Al1 Al12 15_466 8_466 64.22(5) ?
Al12 Al1 Al12 13_566 8_466 109.74(6) ?
Mn2 Al1 Al12 . 6_565 102.72(5) ?
Mn4 Al1 Al12 . 6_565 52.13(3) ?
Mn4 Al1 Al12 3_556 6_565 103.75(7) ?
Al5 Al1 Al12 . 6_565 107.16(6) ?
Al5 Al1 Al12 10_557 6_565 56.09(3) ?
Al12 Al1 Al12 15_466 6_565 109.74(6) ?
Al12 Al1 Al12 13_566 6_565 64.22(5) ?
Al12 Al1 Al12 8_466 6_565 154.55(10) ?
Mn2 Al1 Al13 . . 49.10(4) ?
Mn4 Al1 Al13 . . 107.71(3) ?
Mn4 Al1 Al13 3_556 . 144.48(4) ?
Al5 Al1 Al13 . . 85.93(4) ?
Al5 Al1 Al13 10_557 . 148.52(3) ?
Al12 Al1 Al13 15_466 . 148.29(8) ?
Al12 Al1 Al13 13_566 . 55.78(3) ?
Al12 Al1 Al13 8_466 . 103.80(4) ?
Al12 Al1 Al13 6_565 . 92.86(4) ?
Mn2 Al1 Al13 . 12 49.10(4) ?
Mn4 Al1 Al13 . 12 144.49(4) ?
Mn4 Al1 Al13 3_556 12 107.71(3) ?
Al5 Al1 Al13 . 12 85.93(4) ?
Al5 Al1 Al13 10_557 12 148.52(3) ?
Al12 Al1 Al13 15_466 12 92.86(4) ?
Al12 Al1 Al13 13_566 12 103.80(4) ?
Al12 Al1 Al13 8_466 12 55.79(3) ?
Al12 Al1 Al13 6_565 12 148.29(8) ?
Al13 Al1 Al13 . 12 58.63(6) ?
Mn2 Al1 Al13 . 10_557 49.10(4) ?
Mn4 Al1 Al13 . 10_557 107.71(3) ?
Mn4 Al1 Al13 3_556 10_557 144.49(4) ?
Al5 Al1 Al13 . 10_557 148.52(3) ?
Al5 Al1 Al13 10_557 10_557 85.93(4) ?
Al12 Al1 Al13 15_466 10_557 103.80(4) ?
Al12 Al1 Al13 13_566 10_557 92.86(4) ?
Al12 Al1 Al13 8_466 10_557 148.29(8) ?
Al12 Al1 Al13 6_565 10_557 55.79(3) ?
Al13 Al1 Al13 . 10_557 70.31(7) ?
Al13 Al1 Al13 12 10_557 98.19(9) ?
Mn4 Al2 Mn4 15_465 13_566 171.29(12) ?
Mn4 Al2 Al12 15_465 . 117.15(7) ?
Mn4 Al2 Al12 13_566 . 56.15(4) ?
Mn4 Al2 Al12 15_465 12 56.15(4) ?
Mn4 Al2 Al12 13_566 12 117.15(7) ?
Al12 Al2 Al12 . 12 61.08(6) ?
Mn4 Al2 Al12 15_465 3 56.15(4) ?
Mn4 Al2 Al12 13_566 3 117.15(7) ?
Al12 Al2 Al12 . 3 97.05(9) ?
Al12 Al2 Al12 12 3 66.82(7) ?
Mn4 Al2 Al12 15_465 10_556 117.15(7) ?
Mn4 Al2 Al12 13_566 10_556 56.15(4) ?
Al12 Al2 Al12 . 10_556 66.82(7) ?
Al12 Al2 Al12 12 10_556 97.05(9) ?
Al12 Al2 Al12 3 10_556 61.08(6) ?
Mn4 Al2 Al9 15_465 3 64.57(5) ?
Mn4 Al2 Al9 13_566 3 124.14(9) ?
Al12 Al2 Al9 . 3 145.81(4) ?
Al12 Al2 Al9 12 3 108.81(4) ?
Al12 Al2 Al9 3 3 108.81(4) ?
Al12 Al2 Al9 10_556 3 145.82(4) ?
Mn4 Al2 Al9 15_465 . 124.14(9) ?
Mn4 Al2 Al9 13_566 . 64.57(5) ?
Al12 Al2 Al9 . . 108.81(4) ?
Al12 Al2 Al9 12 . 145.81(4) ?
Al12 Al2 Al9 3 . 145.81(4) ?
Al12 Al2 Al9 10_556 . 108.81(4) ?
Al9 Al2 Al9 3 . 59.57(9) ?
Mn4 Al2 Al11 15_465 10_556 122.17(3) ?
Mn4 Al2 Al11 13_566 10_556 60.75(3) ?
Al12 Al2 Al11 . 10_556 112.13(4) ?
Al12 Al2 Al11 12 10_556 153.77(8) ?
Al12 Al2 Al11 3 10_556 90.36(4) ?
Al12 Al2 Al11 10_556 10_556 59.07(3) ?
Al9 Al2 Al11 3 10_556 90.20(6) ?
Al9 Al2 Al11 . 10_556 59.65(4) ?
Mn4 Al2 Al11 15_465 12 60.75(3) ?
Mn4 Al2 Al11 13_566 12 122.17(3) ?
Al12 Al2 Al11 . 12 90.36(4) ?
Al12 Al2 Al11 12 12 59.07(3) ?
Al12 Al2 Al11 3 12 112.13(4) ?
Al12 Al2 Al11 10_556 12 153.77(8) ?
Al9 Al2 Al11 3 12 59.65(4) ?
Al9 Al2 Al11 . 12 90.19(6) ?
Al11 Al2 Al11 10_556 12 146.39(10) ?
Mn4 Al2 Al11 15_465 3 60.75(3) ?
Mn4 Al2 Al11 13_566 3 122.17(3) ?
Al12 Al2 Al11 . 3 153.77(8) ?
Al12 Al2 Al11 12 3 112.13(4) ?
Al12 Al2 Al11 3 3 59.07(3) ?
Al12 Al2 Al11 10_556 3 90.36(4) ?
Al9 Al2 Al11 3 3 59.65(4) ?
Al9 Al2 Al11 . 3 90.19(6) ?
Al11 Al2 Al11 10_556 3 61.59(5) ?
Al11 Al2 Al11 12 3 107.97(6) ?
Mn4 Al2 Al11 15_465 . 122.17(3) ?
Mn4 Al2 Al11 13_566 . 60.75(3) ?
Al12 Al2 Al11 . . 59.07(3) ?
Al12 Al2 Al11 12 . 90.36(4) ?
Al12 Al2 Al11 3 . 153.77(8) ?
Al12 Al2 Al11 10_556 . 112.13(4) ?
Al9 Al2 Al11 3 . 90.19(6) ?
Al9 Al2 Al11 . . 59.65(4) ?
Al11 Al2 Al11 10_556 . 107.97(6) ?
Al11 Al2 Al11 12 . 61.59(5) ?
Al11 Al2 Al11 3 . 146.39(10) ?
Mn3 Al3 Mn3 . 10_556 174.83(12) ?
Mn3 Al3 Al6 . 10_556 128.61(10) ?
Mn3 Al3 Al6 10_556 10_556 56.56(5) ?
Mn3 Al3 Al6 . . 56.56(5) ?
Mn3 Al3 Al6 10_556 . 128.61(10) ?
Al6 Al3 Al6 10_556 . 72.05(9) ?
Mn3 Al3 Al12 . 10_556 120.36(8) ?
Mn3 Al3 Al12 10_556 10_556 55.46(4) ?
Al6 Al3 Al12 10_556 10_556 103.70(4) ?
Al6 Al3 Al12 . 10_556 150.24(3) ?
Mn3 Al3 Al12 . 3 120.36(8) ?
Mn3 Al3 Al12 10_556 3 55.46(4) ?
Al6 Al3 Al12 10_556 3 103.70(4) ?
Al6 Al3 Al12 . 3 150.24(3) ?
Al12 Al3 Al12 10_556 3 59.39(6) ?
Mn3 Al3 Al12 . 12 55.46(4) ?
Mn3 Al3 Al12 10_556 12 120.35(8) ?
Al6 Al3 Al12 10_556 12 150.24(3) ?
Al6 Al3 Al12 . 12 103.70(4) ?
Al12 Al3 Al12 10_556 12 93.84(8) ?
Al12 Al3 Al12 3 12 64.92(6) ?
Mn3 Al3 Al12 . . 55.46(4) ?
Mn3 Al3 Al12 10_556 . 120.35(8) ?
Al6 Al3 Al12 10_556 . 150.24(3) ?
Al6 Al3 Al12 . . 103.70(4) ?
Al12 Al3 Al12 10_556 . 64.92(6) ?
Al12 Al3 Al12 3 . 93.84(8) ?
Al12 Al3 Al12 12 . 59.38(6) ?
Mn3 Al3 Al13 . 8_466 55.87(3) ?
Mn3 Al3 Al13 10_556 8_466 125.40(3) ?
Al6 Al3 Al13 10_556 8_466 99.90(7) ?
Al6 Al3 Al13 . 8_466 60.04(4) ?
Al12 Al3 Al13 10_556 8_466 147.01(8) ?
Al12 Al3 Al13 3 8_466 92.89(4) ?
Al12 Al3 Al13 12 8_466 55.79(3) ?
Al12 Al3 Al13 . 8_466 103.07(5) ?
Mn3 Al3 Al13 . 6_564 125.40(3) ?
Mn3 Al3 Al13 10_556 6_564 55.87(3) ?
Al6 Al3 Al13 10_556 6_564 60.04(4) ?
Al6 Al3 Al13 . 6_564 99.90(7) ?
Al12 Al3 Al13 10_556 6_564 55.79(3) ?
Al12 Al3 Al13 3 6_564 103.07(5) ?
Al12 Al3 Al13 12 6_564 147.01(8) ?
Al12 Al3 Al13 . 6_564 92.89(4) ?
Al13 Al3 Al13 8_466 6_564 156.64(10) ?
Mn3 Al3 Al13 . 15_465 125.40(3) ?
Mn3 Al3 Al13 10_556 15_465 55.87(3) ?
Al6 Al3 Al13 10_556 15_465 60.04(4) ?
Al6 Al3 Al13 . 15_465 99.90(7) ?
Al12 Al3 Al13 10_556 15_465 103.07(5) ?
Al12 Al3 Al13 3 15_465 55.79(3) ?
Al12 Al3 Al13 12 15_465 92.89(4) ?
Al12 Al3 Al13 . 15_465 147.01(8) ?
Al13 Al3 Al13 8_466 15_465 69.61(5) ?
Al13 Al3 Al13 6_564 15_465 105.46(6) ?
Mn3 Al3 Al13 . 13_566 55.87(3) ?
Mn3 Al3 Al13 10_556 13_566 125.40(3) ?
Al6 Al3 Al13 10_556 13_566 99.90(7) ?
Al6 Al3 Al13 . 13_566 60.04(4) ?
Al12 Al3 Al13 10_556 13_566 92.89(4) ?
Al12 Al3 Al13 3 13_566 147.01(8) ?
Al12 Al3 Al13 12 13_566 103.07(5) ?
Al12 Al3 Al13 . 13_566 55.79(3) ?
Al13 Al3 Al13 8_466 13_566 105.46(6) ?
Al13 Al3 Al13 6_564 13_566 69.61(5) ?
Al13 Al3 Al13 15_465 13_566 156.64(10) ?
Al4 Al4 Mn3 10_557 1_556 179.94(4) ?
Al4 Al4 Mn4 10_557 3_556 61.61(4) ?
Mn3 Al4 Mn4 1_556 3_556 118.34(5) ?
Al4 Al4 Mn4 10_557 . 61.61(4) ?
Mn3 Al4 Mn4 1_556 . 118.34(5) ?
Mn4 Al4 Mn4 3_556 . 65.57(5) ?
Al4 Al4 Mn1 10_557 . 61.94(4) ?
Mn3 Al4 Mn1 1_556 . 118.11(6) ?
Mn4 Al4 Mn1 3_556 . 112.85(5) ?
Mn4 Al4 Mn1 . . 112.85(5) ?
Al4 Al4 Al5 10_557 . 113.51(5) ?
Mn3 Al4 Al5 1_556 . 66.43(6) ?
Mn4 Al4 Al5 3_556 . 63.50(5) ?
Mn4 Al4 Al5 . . 63.50(5) ?
Mn1 Al4 Al5 . . 175.45(8) ?
Al4 Al4 Al10 10_557 . 113.02(4) ?
Mn3 Al4 Al10 1_556 . 67.03(5) ?
Mn4 Al4 Al10 3_556 . 174.21(8) ?
Mn4 Al4 Al10 . . 114.51(3) ?
Mn1 Al4 Al10 . . 61.53(4) ?
Al5 Al4 Al10 . . 122.04(7) ?
Al4 Al4 Al10 10_557 12 113.02(4) ?
Mn3 Al4 Al10 1_556 12 67.03(5) ?
Mn4 Al4 Al10 3_556 12 114.51(3) ?
Mn4 Al4 Al10 . 12 174.21(8) ?
Mn1 Al4 Al10 . 12 61.53(4) ?
Al5 Al4 Al10 . 12 122.04(7) ?
Al10 Al4 Al10 . 12 64.76(6) ?
Al4 Al4 Al11 10_557 13_566 113.18(4) ?
Mn3 Al4 Al11 1_556 13_566 66.80(4) ?
Mn4 Al4 Al11 3_556 13_566 116.83(6) ?
Mn4 Al4 Al11 . 13_566 60.63(3) ?
Mn1 Al4 Al11 . 13_566 116.63(4) ?
Al5 Al4 Al11 . 13_566 64.51(4) ?
Al10 Al4 Al11 . 13_566 66.64(4) ?
Al10 Al4 Al11 12 13_566 122.34(7) ?
Al4 Al4 Al11 10_557 8_466 113.18(4) ?
Mn3 Al4 Al11 1_556 8_466 66.80(4) ?
Mn4 Al4 Al11 3_556 8_466 60.63(3) ?
Mn4 Al4 Al11 . 8_466 116.83(6) ?
Mn1 Al4 Al11 . 8_466 116.63(4) ?
Al5 Al4 Al11 . 8_466 64.51(4) ?
Al10 Al4 Al11 . 8_466 122.34(7) ?
Al10 Al4 Al11 12 8_466 66.64(4) ?
Al11 Al4 Al11 13_566 8_466 120.83(8) ?
Al4 Al4 Al9 10_557 15_466 63.95(3) ?
Mn3 Al4 Al9 1_556 15_466 116.07(4) ?
Mn4 Al4 Al9 3_556 15_466 62.23(4) ?
Mn4 Al4 Al9 . 15_466 117.00(6) ?
Mn1 Al4 Al9 . 15_466 62.31(4) ?
Al5 Al4 Al9 . 15_466 116.32(5) ?
Al10 Al4 Al9 . 15_466 114.06(7) ?
Al10 Al4 Al9 12 15_466 59.86(4) ?
Al11 Al4 Al9 13_566 15_466 177.12(7) ?
Al11 Al4 Al9 8_466 15_466 61.41(4) ?
Al4 Al4 Al9 10_557 13_566 63.95(3) ?
Mn3 Al4 Al9 1_556 13_566 116.07(4) ?
Mn4 Al4 Al9 3_556 13_566 117.00(6) ?
Mn4 Al4 Al9 . 13_566 62.23(4) ?
Mn1 Al4 Al9 . 13_566 62.31(4) ?
Al5 Al4 Al9 . 13_566 116.32(5) ?
Al10 Al4 Al9 . 13_566 59.86(4) ?
Al10 Al4 Al9 12 13_566 114.06(7) ?
Al11 Al4 Al9 13_566 13_566 61.41(4) ?
Al11 Al4 Al9 8_466 13_566 177.12(7) ?
Al9 Al4 Al9 15_466 13_566 116.30(7) ?
Al4 Al5 Al12 . 13_566 104.51(5) ?
Al4 Al5 Al12 . 8_466 104.51(5) ?
Al12 Al5 Al12 13_566 8_466 122.57(8) ?
Al4 Al5 Mn4 . . 57.73(5) ?
Al12 Al5 Mn4 13_566 . 53.78(4) ?
Al12 Al5 Mn4 8_466 . 107.85(6) ?
Al4 Al5 Mn4 . 3_556 57.73(5) ?
Al12 Al5 Mn4 13_566 3_556 107.85(6) ?
Al12 Al5 Mn4 8_466 3_556 53.78(4) ?
Mn4 Al5 Mn4 . 3_556 61.54(5) ?
Al4 Al5 Al12 . 1_556 98.93(6) ?
Al12 Al5 Al12 13_566 1_556 82.56(4) ?
Al12 Al5 Al12 8_466 1_556 138.55(6) ?
Mn4 Al5 Al12 . 1_556 113.56(4) ?
Mn4 Al5 Al12 3_556 1_556 155.84(7) ?
Al4 Al5 Al12 . 12_556 98.93(6) ?
Al12 Al5 Al12 13_566 12_556 138.55(6) ?
Al12 Al5 Al12 8_466 12_556 82.56(4) ?
Mn4 Al5 Al12 . 12_556 155.84(7) ?
Mn4 Al5 Al12 3_556 12_556 113.56(4) ?
Al12 Al5 Al12 1_556 12_556 60.15(6) ?
Al4 Al5 Mn3 . 1_556 55.36(5) ?
Al12 Al5 Mn3 13_566 1_556 118.66(4) ?
Al12 Al5 Mn3 8_466 1_556 118.66(4) ?
Mn4 Al5 Mn3 . 1_556 104.50(5) ?
Mn4 Al5 Mn3 3_556 1_556 104.50(5) ?
Al12 Al5 Mn3 1_556 1_556 52.26(4) ?
Al12 Al5 Mn3 12_556 1_556 52.26(4) ?
Al4 Al5 Al11 . 8_466 58.75(4) ?
Al12 Al5 Al11 13_566 8_466 161.14(7) ?
Al12 Al5 Al11 8_466 8_466 60.11(4) ?
Mn4 Al5 Al11 . 8_466 107.38(6) ?
Mn4 Al5 Al11 3_556 8_466 57.04(3) ?
Al12 Al5 Al11 1_556 8_466 107.35(6) ?
Al12 Al5 Al11 12_556 8_466 58.17(4) ?
Mn3 Al5 Al11 1_556 8_466 61.09(4) ?
Al4 Al5 Al11 . 13_566 58.75(4) ?
Al12 Al5 Al11 13_566 13_566 60.11(4) ?
Al12 Al5 Al11 8_466 13_566 161.14(7) ?
Mn4 Al5 Al11 . 13_566 57.04(3) ?
Mn4 Al5 Al11 3_556 13_566 107.38(6) ?
Al12 Al5 Al11 1_556 13_566 58.17(4) ?
Al12 Al5 Al11 12_556 13_566 107.35(6) ?
Mn3 Al5 Al11 1_556 13_566 61.09(4) ?
Al11 Al5 Al11 8_466 13_566 110.89(7) ?
Al4 Al5 Al1 . . 103.14(8) ?
Al12 Al5 Al1 13_566 . 62.86(4) ?
Al12 Al5 Al1 8_466 . 62.86(4) ?
Mn4 Al5 Al1 . . 57.71(5) ?
Mn4 Al5 Al1 3_556 . 57.71(5) ?
Al12 Al5 Al1 1_556 . 142.53(5) ?
Al12 Al5 Al1 12_556 . 142.53(5) ?
Mn3 Al5 Al1 1_556 . 158.50(8) ?
Al11 Al5 Al1 8_466 . 109.95(5) ?
Al11 Al5 Al1 13_566 . 109.95(5) ?
Mn3 Al6 Mn1 . 9_566 157.26(8) ?
Mn3 Al6 Al8 . 7 113.33(6) ?
Mn1 Al6 Al8 9_566 7 55.75(5) ?
Mn3 Al6 Al8 . 5_455 113.33(6) ?
Mn1 Al6 Al8 9_566 5_455 55.75(5) ?
Al8 Al6 Al8 7 5_455 99.45(9) ?
Mn3 Al6 Al10 . 9_566 134.52(6) ?
Mn1 Al6 Al10 9_566 9_566 62.46(4) ?
Al8 Al6 Al10 7 9_566 111.74(7) ?
Al8 Al6 Al10 5_455 9_566 64.00(5) ?
Mn3 Al6 Al10 . 4_566 134.52(6) ?
Mn1 Al6 Al10 9_566 4_566 62.46(4) ?
Al8 Al6 Al10 7 4_566 64.00(5) ?
Al8 Al6 Al10 5_455 4_566 111.74(7) ?
Al10 Al6 Al10 9_566 4_566 64.01(6) ?
Mn3 Al6 Al10 . 12_554 67.07(5) ?
Mn1 Al6 Al10 9_566 12_554 130.58(6) ?
Al8 Al6 Al10 7 12_554 160.60(7) ?
Al8 Al6 Al10 5_455 12_554 97.78(4) ?
Al10 Al6 Al10 9_566 12_554 68.47(6) ?
Al10 Al6 Al10 4_566 12_554 101.20(7) ?
Mn3 Al6 Al10 . 1_554 67.07(5) ?
Mn1 Al6 Al10 9_566 1_554 130.58(6) ?
Al8 Al6 Al10 7 1_554 97.78(4) ?
Al8 Al6 Al10 5_455 1_554 160.60(7) ?
Al10 Al6 Al10 9_566 1_554 101.20(7) ?
Al10 Al6 Al10 4_566 1_554 68.47(6) ?
Al10 Al6 Al10 12_554 1_554 63.92(6) ?
Mn3 Al6 Al3 . . 54.21(5) ?
Mn1 Al6 Al3 9_566 . 103.05(7) ?
Al8 Al6 Al3 7 . 79.47(6) ?
Al8 Al6 Al3 5_455 . 79.47(6) ?
Al10 Al6 Al3 9_566 . 142.84(5) ?
Al10 Al6 Al3 4_566 . 142.84(5) ?
Al10 Al6 Al3 12_554 . 112.56(6) ?
Al10 Al6 Al3 1_554 . 112.56(6) ?
Mn3 Al6 Al13 . 13_566 56.36(4) ?
Mn1 Al6 Al13 9_566 13_566 116.48(5) ?
Al8 Al6 Al13 7 13_566 60.75(5) ?
Al8 Al6 Al13 5_455 13_566 139.08(8) ?
Al10 Al6 Al13 9_566 13_566 154.26(6) ?
Al10 Al6 Al13 4_566 13_566 92.09(4) ?
Al10 Al6 Al13 12_554 13_566 110.04(7) ?
Al10 Al6 Al13 1_554 13_566 58.63(4) ?
Al3 Al6 Al13 . 13_566 62.59(4) ?
Mn3 Al6 Al13 . 8_466 56.36(4) ?
Mn1 Al6 Al13 9_566 8_466 116.48(5) ?
Al8 Al6 Al13 7 8_466 139.08(8) ?
Al8 Al6 Al13 5_455 8_466 60.75(5) ?
Al10 Al6 Al13 9_566 8_466 92.09(4) ?
Al10 Al6 Al13 4_566 8_466 154.26(6) ?
Al10 Al6 Al13 12_554 8_466 58.63(4) ?
Al10 Al6 Al13 1_554 8_466 110.04(7) ?
Al3 Al6 Al13 . 8_466 62.59(4) ?
Al13 Al6 Al13 13_566 8_466 109.24(7) ?
Al7A Al7A Ni1 9_577 9_576 65.38(9) ?
Al7A Al7A Mn2 9_577 . 158.53(16) ?
Ni1 Al7A Mn2 9_576 . 136.09(12) ?
Al7A Al7A Al8 9_577 9_566 135.57(7) ?
Ni1 Al7A Al8 9_576 9_566 95.36(8) ?
Mn2 Al7A Al8 . 9_566 54.39(7) ?
Al7A Al7A Al8 9_577 11_566 135.57(7) ?
Ni1 Al7A Al8 9_576 11_566 95.36(8) ?
Mn2 Al7A Al8 . 11_566 54.39(7) ?
Al8 Al7A Al8 9_566 11_566 83.07(11) ?
Al7A Al7A Ni1 9_577 1_556 57.79(10) ?
Ni1 Al7A Ni1 9_576 1_556 123.17(10) ?
Mn2 Al7A Ni1 . 1_556 100.74(8) ?
Al8 Al7A Ni1 9_566 1_556 124.80(8) ?
Al8 Al7A Ni1 11_566 1_556 124.80(8) ?
Al7A Al7A Al13 9_577 12 109.59(12) ?
Ni1 Al7A Al13 9_576 12 147.49(4) ?
Mn2 Al7A Al13 . 12 53.47(6) ?
Al8 Al7A Al13 9_566 12 65.06(7) ?
Al8 Al7A Al13 11_566 12 106.89(10) ?
Ni1 Al7A Al13 1_556 12 61.56(6) ?
Al7A Al7A Al13 9_577 . 109.59(12) ?
Ni1 Al7A Al13 9_576 . 147.49(4) ?
Mn2 Al7A Al13 . . 53.47(6) ?
Al8 Al7A Al13 9_566 . 106.89(10) ?
Al8 Al7A Al13 11_566 . 65.06(7) ?
Ni1 Al7A Al13 1_556 . 61.56(6) ?
Al13 Al7A Al13 12 . 64.98(7) ?
Al7A Al7A Al10 9_577 16 73.80(7) ?
Ni1 Al7A Al10 9_576 16 54.58(4) ?
Mn2 Al7A Al10 . 16 116.50(6) ?
Al8 Al7A Al10 9_566 16 128.64(11) ?
Al8 Al7A Al10 11_566 16 62.94(5) ?
Ni1 Al7A Al10 1_556 16 106.41(7) ?
Al13 Al7A Al10 12 16 157.69(7) ?
Al13 Al7A Al10 . 16 92.91(4) ?
Al7A Al7A Al10 9_577 5_455 73.80(7) ?
Ni1 Al7A Al10 9_576 5_455 54.58(4) ?
Mn2 Al7A Al10 . 5_455 116.50(6) ?
Al8 Al7A Al10 9_566 5_455 62.94(5) ?
Al8 Al7A Al10 11_566 5_455 128.64(11) ?
Ni1 Al7A Al10 1_556 5_455 106.41(7) ?
Al13 Al7A Al10 12 5_455 92.91(4) ?
Al13 Al7A Al10 . 5_455 157.69(7) ?
Al10 Al7A Al10 16 5_455 108.96(8) ?
Ni1 Al7B Ni1 9_565 1_545 180.00(4) ?
Ni1 Al7B Al10 9_565 16_544 57.62(2) ?
Ni1 Al7B Al10 1_545 16_544 122.38(2) ?
Ni1 Al7B Al10 9_565 8_456 122.38(2) ?
Ni1 Al7B Al10 1_545 8_456 57.62(2) ?
Al10 Al7B Al10 16_544 8_456 180.00(6) ?
Ni1 Al7B Al10 9_565 5_444 57.62(2) ?
Ni1 Al7B Al10 1_545 5_444 122.38(2) ?
Al10 Al7B Al10 16_544 5_444 113.96(5) ?
Al10 Al7B Al10 8_456 5_444 66.04(5) ?
Ni1 Al7B Al10 9_565 13_556 122.38(2) ?
Ni1 Al7B Al10 1_545 13_556 57.62(2) ?
Al10 Al7B Al10 16_544 13_556 66.04(5) ?
Al10 Al7B Al10 8_456 13_556 113.96(5) ?
Al10 Al7B Al10 5_444 13_556 180.00(6) ?
Mn2 Al8 Mn1 9_566 13_556 170.33(12) ?
Mn2 Al8 Al7A 9_566 9_566 60.24(7) ?
Mn1 Al8 Al7A 13_556 9_566 124.28(6) ?
Mn2 Al8 Al7A 9_566 2_564 60.24(7) ?
Mn1 Al8 Al7A 13_556 2_564 124.28(6) ?
Al7A Al8 Al7A 9_566 2_564 96.93(11) ?
Mn2 Al8 Al6 9_566 14_546 114.85(7) ?
Mn1 Al8 Al6 13_556 14_546 58.18(6) ?
Al7A Al8 Al6 9_566 14_546 163.78(10) ?
Al7A Al8 Al6 2_564 14_546 92.78(5) ?
Mn2 Al8 Al6 9_566 5_545 114.85(7) ?
Mn1 Al8 Al6 13_556 5_545 58.18(6) ?
Al7A Al8 Al6 9_566 5_545 92.78(5) ?
Al7A Al8 Al6 2_564 5_545 163.78(10) ?
Al6 Al8 Al6 14_546 5_545 75.03(9) ?
Mn2 Al8 Al9 9_566 1_545 125.60(11) ?
Mn1 Al8 Al9 13_556 1_545 64.07(6) ?
Al7A Al8 Al9 9_566 1_545 86.07(8) ?
Al7A Al8 Al9 2_564 1_545 86.07(8) ?
Al6 Al8 Al9 14_546 1_545 107.60(7) ?
Al6 Al8 Al9 5_545 1_545 107.60(7) ?
Mn2 Al8 Al13 9_566 11_565 52.45(5) ?
Mn1 Al8 Al13 13_556 11_565 120.86(8) ?
Al7A Al8 Al13 9_566 11_565 111.92(9) ?
Al7A Al8 Al13 2_564 11_565 58.77(6) ?
Al6 Al8 Al13 14_546 11_565 62.71(5) ?
Al6 Al8 Al13 5_545 11_565 105.48(9) ?
Al9 Al8 Al13 1_545 11_565 141.28(5) ?
Mn2 Al8 Al13 9_566 4_566 52.45(5) ?
Mn1 Al8 Al13 13_556 4_566 120.86(8) ?
Al7A Al8 Al13 9_566 4_566 58.77(6) ?
Al7A Al8 Al13 2_564 4_566 111.92(9) ?
Al6 Al8 Al13 14_546 4_566 105.48(9) ?
Al6 Al8 Al13 5_545 4_566 62.71(5) ?
Al9 Al8 Al13 1_545 4_566 141.28(5) ?
Al13 Al8 Al13 11_565 4_566 73.12(7) ?
Mn2 Al8 Al10 9_566 13_556 122.79(6) ?
Mn1 Al8 Al10 13_556 13_556 60.78(5) ?
Al7A Al8 Al10 9_566 13_556 63.50(5) ?
Al7A Al8 Al10 2_564 13_556 138.12(11) ?
Al6 Al8 Al10 14_546 13_556 116.10(9) ?
Al6 Al8 Al10 5_545 13_556 58.07(5) ?
Al9 Al8 Al10 1_545 13_556 57.55(4) ?
Al13 Al8 Al10 11_565 13_556 161.13(8) ?
Al13 Al8 Al10 4_566 13_556 89.92(4) ?
Mn2 Al8 Al10 9_566 6_554 122.79(6) ?
Mn1 Al8 Al10 13_556 6_554 60.78(5) ?
Al7A Al8 Al10 9_566 6_554 138.12(11) ?
Al7A Al8 Al10 2_564 6_554 63.50(5) ?
Al6 Al8 Al10 14_546 6_554 58.07(5) ?
Al6 Al8 Al10 5_545 6_554 116.10(9) ?
Al9 Al8 Al10 1_545 6_554 57.55(4) ?
Al13 Al8 Al10 11_565 6_554 89.92(4) ?
Al13 Al8 Al10 4_566 6_554 161.13(8) ?
Al10 Al8 Al10 13_556 6_554 105.39(8) ?
Ni1 Al9 Ni1 . 10_556 114.80(7) ?
Ni1 Al9 Al10 . 6_564 144.85(7) ?
Ni1 Al9 Al10 10_556 6_564 54.20(3) ?
Ni1 Al9 Al10 . 13_566 54.20(3) ?
Ni1 Al9 Al10 10_556 13_566 144.85(7) ?
Al10 Al9 Al10 6_564 13_566 112.70(8) ?
Ni1 Al9 Al9 . 3 58.77(3) ?
Ni1 Al9 Al9 10_556 3 58.77(3) ?
Al10 Al9 Al9 6_564 3 110.28(4) ?
Al10 Al9 Al9 13_566 3 110.28(4) ?
Ni1 Al9 Mn4 . 13_566 108.60(4) ?
Ni1 Al9 Mn4 10_556 13_566 108.60(4) ?
Al10 Al9 Mn4 6_564 13_566 106.47(5) ?
Al10 Al9 Mn4 13_566 13_566 106.47(5) ?
Al9 Al9 Mn4 3 13_566 110.52(4) ?
Ni1 Al9 Al11 . . 53.63(3) ?
Ni1 Al9 Al11 10_556 . 141.43(7) ?
Al10 Al9 Al11 6_564 . 157.30(8) ?
Al10 Al9 Al11 13_566 . 64.15(3) ?
Al9 Al9 Al11 3 . 91.08(4) ?
Mn4 Al9 Al11 13_566 . 56.79(4) ?
Ni1 Al9 Al11 . 10_556 141.43(7) ?
Ni1 Al9 Al11 10_556 10_556 53.63(3) ?
Al10 Al9 Al11 6_564 10_556 64.16(3) ?
Al10 Al9 Al11 13_566 10_556 157.30(8) ?
Al9 Al9 Al11 3 10_556 91.08(4) ?
Mn4 Al9 Al11 13_566 10_556 56.79(4) ?
Al11 Al9 Al11 . 10_556 109.37(7) ?
Ni1 Al9 Al4 . 6_564 148.57(6) ?
Ni1 Al9 Al4 10_556 6_564 96.50(4) ?
Al10 Al9 Al4 6_564 6_564 57.76(5) ?
Al10 Al9 Al4 13_566 6_564 101.40(7) ?
Al9 Al9 Al4 3 6_564 148.15(4) ?
Mn4 Al9 Al4 13_566 6_564 55.13(5) ?
Al11 Al9 Al4 . 6_564 99.98(7) ?
Al11 Al9 Al4 10_556 6_564 57.08(4) ?
Ni1 Al9 Al4 . 13_566 96.50(4) ?
Ni1 Al9 Al4 10_556 13_566 148.57(6) ?
Al10 Al9 Al4 6_564 13_566 101.40(7) ?
Al10 Al9 Al4 13_566 13_566 57.76(5) ?
Al9 Al9 Al4 3 13_566 148.15(4) ?
Mn4 Al9 Al4 13_566 13_566 55.13(5) ?
Al11 Al9 Al4 . 13_566 57.08(4) ?
Al11 Al9 Al4 10_556 13_566 99.98(7) ?
Al4 Al9 Al4 6_564 13_566 52.11(7) ?
Ni1 Al9 Al2 . . 82.51(4) ?
Ni1 Al9 Al2 10_556 . 82.51(4) ?
Al10 Al9 Al2 6_564 . 123.19(4) ?
Al10 Al9 Al2 13_566 . 123.19(4) ?
Al9 Al9 Al2 3 . 60.21(4) ?
Mn4 Al9 Al2 13_566 . 50.30(4) ?
Al11 Al9 Al2 . . 60.52(4) ?
Al11 Al9 Al2 10_556 . 60.52(4) ?
Al4 Al9 Al2 6_564 . 99.67(6) ?
Al4 Al9 Al2 13_566 . 99.67(6) ?
Ni1 Al9 Mn1 . 13_566 111.21(4) ?
Ni1 Al9 Mn1 10_556 13_566 111.21(4) ?
Al10 Al9 Mn1 6_564 13_566 58.46(4) ?
Al10 Al9 Mn1 13_566 13_566 58.46(4) ?
Al9 Al9 Mn1 3 13_566 147.96(4) ?
Mn4 Al9 Mn1 13_566 13_566 101.52(6) ?
Al11 Al9 Mn1 . 13_566 106.89(5) ?
Al11 Al9 Mn1 10_556 13_566 106.89(5) ?
Al4 Al9 Mn1 6_564 13_566 55.61(5) ?
Al4 Al9 Mn1 13_566 13_566 55.61(5) ?
Al2 Al9 Mn1 . 13_566 151.82(8) ?
Ni1 Al10 Al4 13_566 . 105.45(5) ?
Ni1 Al10 Al6 13_566 9_566 139.58(5) ?
Al4 Al10 Al6 . 9_566 103.57(5) ?
Ni1 Al10 Al6 13_566 1_556 123.31(5) ?
Al4 Al10 Al6 . 1_556 98.33(5) ?
Al6 Al10 Al6 9_566 1_556 78.80(7) ?
Ni1 Al10 Mn1 13_566 . 122.22(5) ?
Al4 Al10 Mn1 . . 58.18(5) ?
Al6 Al10 Mn1 9_566 . 55.26(5) ?
Al6 Al10 Mn1 1_556 . 114.14(5) ?
Ni1 Al10 Al9 13_566 13_566 61.91(5) ?
Al4 Al10 Al9 . 13_566 62.38(5) ?
Al6 Al10 Al9 9_566 13_566 109.94(6) ?
Al6 Al10 Al9 1_556 13_566 159.88(7) ?
Mn1 Al10 Al9 . 13_566 62.12(4) ?
Ni1 Al10 Al13 13_566 13_567 62.42(4) ?
Al4 Al10 Al13 . 13_567 98.14(6) ?
Al6 Al10 Al13 9_566 13_567 138.97(6) ?
Al6 Al10 Al13 1_556 13_567 63.76(5) ?
Mn1 Al10 Al13 . 13_567 156.23(6) ?
Al9 Al10 Al13 13_566 13_567 110.94(6) ?
Ni1 Al10 Al7B 13_566 5_556 49.75(3) ?
Al4 Al10 Al7B . 5_556 155.17(5) ?
Al6 Al10 Al7B 9_566 5_556 97.94(4) ?
Al6 Al10 Al7B 1_556 5_556 97.86(4) ?
Mn1 Al10 Al7B . 5_556 129.61(5) ?
Al9 Al10 Al7B 13_566 5_556 98.73(5) ?
Al13 Al10 Al7B 13_567 5_556 72.59(4) ?
Ni1 Al10 Al8 13_566 13_556 88.21(6) ?
Al4 Al10 Al8 . 13_556 103.25(6) ?
Al6 Al10 Al8 9_566 13_556 57.93(6) ?
Al6 Al10 Al8 1_556 13_556 134.91(7) ?
Mn1 Al10 Al8 . 13_556 51.89(5) ?
Al9 Al10 Al8 13_566 13_556 60.42(5) ?
Al13 Al10 Al8 13_567 13_556 147.50(8) ?
Ni1 Al10 Al10 13_566 12 161.38(3) ?
Al4 Al10 Al10 . 12 57.62(3) ?
Al6 Al10 Al10 9_566 12 57.99(3) ?
Al6 Al10 Al10 1_556 12 58.04(3) ?
Mn1 Al10 Al10 . 12 58.05(3) ?
Al9 Al10 Al10 13_566 12 110.28(4) ?
Al13 Al10 Al10 13_567 12 109.46(4) ?
Al8 Al10 Al10 13_556 12 102.64(6) ?
Ni1 Al10 Al7A 13_566 5_545 53.82(5) ?
Al4 Al10 Al7A . 5_545 144.61(7) ?
Al6 Al10 Al7A 9_566 5_545 86.56(5) ?
Al6 Al10 Al7A 1_556 5_545 116.97(7) ?
Mn1 Al10 Al7A . 5_545 105.45(6) ?
Al9 Al10 Al7A 13_566 5_545 82.25(7) ?
Al13 Al10 Al7A 13_567 5_545 95.49(6) ?
Al8 Al10 Al7A 13_556 5_545 53.56(7) ?
Al10 Al10 Al7A 12 5_545 144.48(4) ?
Ni1 Al10 Mn3 13_566 1_556 104.59(4) ?
Al4 Al10 Mn3 . 1_556 54.15(4) ?
Al6 Al10 Mn3 9_566 1_556 115.15(5) ?
Al6 Al10 Mn3 1_556 1_556 52.94(4) ?
Mn1 Al10 Mn3 . 1_556 104.50(4) ?
Al9 Al10 Mn3 13_566 1_556 107.56(5) ?
Al13 Al10 Mn3 13_567 1_556 54.12(4) ?
Al8 Al10 Mn3 13_556 1_556 156.03(6) ?
Al10 Al10 Mn3 12 1_556 60.16(2) ?
Al7A Al10 Mn3 5_545 1_556 149.60(6) ?
Ni1 Al11 Mn4 . 13_566 120.04(5) ?
Ni1 Al11 Al4 . 13_566 105.21(5) ?
Mn4 Al11 Al4 13_566 13_566 58.05(5) ?
Ni1 Al11 Al13 . 1_554 63.18(4) ?
Mn4 Al11 Al13 13_566 1_554 157.51(6) ?
Al4 Al11 Al13 13_566 1_554 99.47(6) ?
Ni1 Al11 Al12 . 13_565 120.70(5) ?
Mn4 Al11 Al12 13_566 13_565 118.86(5) ?
Al4 Al11 Al12 13_566 13_565 99.45(6) ?
Al13 Al11 Al12 1_554 13_565 60.03(4) ?
Ni1 Al11 Al12 . . 140.58(6) ?
Mn4 Al11 Al12 13_566 . 53.81(4) ?
Al4 Al11 Al12 13_566 . 100.93(6) ?
Al13 Al11 Al12 1_554 . 139.80(6) ?
Al12 Al11 Al12 13_565 . 82.62(5) ?
Ni1 Al11 Al9 . . 60.86(4) ?
Mn4 Al11 Al9 13_566 . 61.46(4) ?
Al4 Al11 Al9 13_566 . 61.51(5) ?
Al13 Al11 Al9 1_554 . 110.64(6) ?
Al12 Al11 Al9 13_565 . 158.50(6) ?
Al12 Al11 Al9 . . 109.52(5) ?
Ni1 Al11 Al2 . . 85.94(6) ?
Mn4 Al11 Al2 13_566 . 51.31(3) ?
Al4 Al11 Al2 13_566 . 102.30(5) ?
Al13 Al11 Al2 1_554 . 145.99(6) ?
Al12 Al11 Al2 13_565 . 139.28(7) ?
Al12 Al11 Al2 . . 59.75(6) ?
Al9 Al11 Al2 . . 59.83(6) ?
Ni1 Al11 Al5 . 13_566 160.26(6) ?
Mn4 Al11 Al5 13_566 13_566 59.85(4) ?
Al4 Al11 Al5 13_566 13_566 56.74(5) ?
Al13 Al11 Al5 1_554 13_566 108.98(6) ?
Al12 Al11 Al5 13_565 13_566 60.86(5) ?
Al12 Al11 Al5 . 13_566 57.49(4) ?
Al9 Al11 Al5 . 13_566 109.91(6) ?
Al2 Al11 Al5 . 13_566 104.78(6) ?
Ni1 Al11 Mn3 . 13_565 104.64(4) ?
Mn4 Al11 Mn3 13_566 13_565 105.35(5) ?
Al4 Al11 Mn3 13_566 13_565 54.22(4) ?
Al13 Al11 Mn3 1_554 13_565 54.73(4) ?
Al12 Al11 Mn3 13_565 13_565 52.49(4) ?
Al12 Al11 Mn3 . 13_565 114.57(5) ?
Al9 Al11 Mn3 . 13_565 106.02(5) ?
Al2 Al11 Mn3 . 13_565 155.83(5) ?
Al5 Al11 Mn3 13_566 13_565 59.41(4) ?
Ni1 Al11 Al11 . 12 54.29(3) ?
Mn4 Al11 Al11 13_566 12 110.38(3) ?
Al4 Al11 Al11 13_566 12 150.42(4) ?
Al13 Al11 Al11 1_554 12 89.65(4) ?
Al12 Al11 Al11 13_565 12 109.41(4) ?
Al12 Al11 Al11 . 12 89.35(4) ?
Al9 Al11 Al11 . 12 88.92(4) ?
Al2 Al11 Al11 . 12 59.20(3) ?
Al5 Al11 Al11 13_566 12 145.45(4) ?
Mn3 Al11 Al11 13_565 12 144.17(3) ?
Ni1 Al11 Al10 . 13_566 53.44(3) ?
Mn4 Al11 Al10 13_566 13_566 104.42(5) ?
Al4 Al11 Al10 13_566 13_566 56.65(5) ?
Al13 Al11 Al10 1_554 13_566 58.05(4) ?
Al12 Al11 Al10 13_565 13_566 105.30(5) ?
Al12 Al11 Al10 . 13_566 156.83(6) ?
Al9 Al11 Al10 . 13_566 56.86(4) ?
Al2 Al11 Al10 . 13_566 115.42(6) ?
Al5 Al11 Al10 13_566 13_566 106.83(5) ?
Mn3 Al11 Al10 13_565 13_566 59.38(4) ?
Al11 Al11 Al10 12 13_566 107.73(3) ?
Mn4 Al12 Mn3 13_566 . 161.15(6) ?
Mn4 Al12 Al5 13_566 13_566 64.16(5) ?
Mn3 Al12 Al5 . 13_566 133.76(6) ?
Mn4 Al12 Al13 13_566 13_566 122.41(6) ?
Mn3 Al12 Al13 . 13_566 58.70(4) ?
Al5 Al12 Al13 13_566 13_566 93.09(6) ?
Mn4 Al12 Al11 13_566 13_565 131.84(6) ?
Mn3 Al12 Al11 . 13_565 66.33(4) ?
Al5 Al12 Al11 13_566 13_565 67.68(5) ?
Al13 Al12 Al11 13_566 13_565 58.79(4) ?
Mn4 Al12 Al11 13_566 . 60.89(4) ?
Mn3 Al12 Al11 . . 128.46(6) ?
Al5 Al12 Al11 13_566 . 62.40(5) ?
Al13 Al12 Al11 13_566 . 152.13(6) ?
Al11 Al12 Al11 13_565 . 97.38(5) ?
Mn4 Al12 Al2 13_566 . 53.54(3) ?
Mn3 Al12 Al2 . . 113.47(5) ?
Al5 Al12 Al2 13_566 . 109.70(6) ?
Al13 Al12 Al2 13_566 . 145.60(6) ?
Al11 Al12 Al2 13_565 . 153.67(6) ?
Al11 Al12 Al2 . . 61.18(5) ?
Mn4 Al12 Al5 13_566 1_554 125.99(6) ?
Mn3 Al12 Al5 . 1_554 63.87(4) ?
Al5 Al12 Al5 13_566 1_554 97.44(4) ?
Al13 Al12 Al5 13_566 1_554 108.09(6) ?
Al11 Al12 Al5 13_565 1_554 60.97(4) ?
Al11 Al12 Al5 . 1_554 65.61(5) ?
Al2 Al12 Al5 . 1_554 94.51(5) ?
Mn4 Al12 Al12 13_566 12 112.93(3) ?
Mn3 Al12 Al12 . 12 55.32(3) ?
Al5 Al12 Al12 13_566 12 151.29(4) ?
Al13 Al12 Al12 13_566 12 110.01(4) ?
Al11 Al12 Al12 13_565 12 109.41(4) ?
Al11 Al12 Al12 . 12 90.65(4) ?
Al2 Al12 Al12 . 12 59.46(3) ?
Al5 Al12 Al12 1_554 12 59.92(3) ?
Mn4 Al12 Al3 13_566 . 108.70(5) ?
Mn3 Al12 Al3 . . 53.43(4) ?
Al5 Al12 Al3 13_566 . 148.34(6) ?
Al13 Al12 Al3 13_566 . 63.77(5) ?
Al11 Al12 Al3 13_565 . 111.56(5) ?
Al11 Al12 Al3 . . 143.97(6) ?
Al2 Al12 Al3 . . 84.56(6) ?
Al5 Al12 Al3 1_554 . 109.80(5) ?
Al12 Al12 Al3 12 . 60.31(3) ?
Mn4 Al12 Al1 13_566 13_566 59.92(5) ?
Mn3 Al12 Al1 . 13_566 119.49(6) ?
Al5 Al12 Al1 13_566 13_566 61.05(5) ?
Al13 Al12 Al1 13_566 13_566 62.78(6) ?
Al11 Al12 Al1 13_565 13_566 95.91(5) ?
Al11 Al12 Al1 . 13_566 110.32(6) ?
Al2 Al12 Al1 . 13_566 105.59(5) ?
Al5 Al12 Al1 1_554 13_566 154.32(5) ?
Al12 Al12 Al1 12 13_566 144.87(3) ?
Al3 Al12 Al1 . 13_566 88.24(5) ?
Mn2 Al13 Mn3 . 13_566 149.28(6) ?
Mn2 Al13 Al7A . . 59.00(7) ?
Mn3 Al13 Al7A 13_566 . 134.09(6) ?
Mn2 Al13 Al11 . 1_556 140.75(7) ?
Mn3 Al13 Al11 13_566 1_556 66.42(4) ?
Al7A Al13 Al11 . 1_556 113.16(8) ?
Mn2 Al13 Ni1 . 1_556 102.62(5) ?
Mn3 Al13 Ni1 13_566 1_556 107.22(5) ?
Al7A Al13 Ni1 . 1_556 58.62(6) ?
Al11 Al13 Ni1 1_556 1_556 54.73(4) ?
Mn2 Al13 Al12 . 13_566 117.03(7) ?
Mn3 Al13 Al12 13_566 13_566 56.18(4) ?
Al7A Al13 Al12 . 13_566 167.20(7) ?
Al11 Al13 Al12 1_556 13_566 61.18(4) ?
Ni1 Al13 Al12 1_556 13_566 113.74(5) ?
Mn2 Al13 Al10 . 13_567 130.87(7) ?
Mn3 Al13 Al10 13_566 13_567 65.78(4) ?
Al7A Al13 Al10 . 13_567 72.73(6) ?
Al11 Al13 Al10 1_556 13_567 65.72(4) ?
Ni1 Al13 Al10 1_556 13_567 53.97(4) ?
Al12 Al13 Al10 13_566 13_567 112.08(6) ?
Mn2 Al13 Al8 . 11_566 52.37(6) ?
Mn3 Al13 Al8 13_566 11_566 107.45(7) ?
Al7A Al13 Al8 . 11_566 56.17(7) ?
Al11 Al13 Al8 1_556 11_566 159.89(6) ?
Ni1 Al13 Al8 1_556 11_566 113.35(6) ?
Al12 Al13 Al8 13_566 11_566 132.88(7) ?
Al10 Al13 Al8 13_567 11_566 94.20(5) ?
Mn2 Al13 Al13 . 12 51.85(3) ?
Mn3 Al13 Al13 13_566 12 156.42(3) ?
Al7A Al13 Al13 . 12 57.51(4) ?
Al11 Al13 Al13 1_556 12 90.35(4) ?
Ni1 Al13 Al13 1_556 12 58.13(3) ?
Al12 Al13 Al13 13_566 12 110.01(4) ?
Al10 Al13 Al13 13_567 12 109.45(4) ?
Al8 Al13 Al13 11_566 12 95.79(6) ?
Mn2 Al13 Al6 . 13_566 108.64(6) ?
Mn3 Al13 Al6 13_566 13_566 54.29(4) ?
Al7A Al13 Al6 . 13_566 87.37(5) ?
Al11 Al13 Al6 1_556 13_566 109.27(6) ?
Ni1 Al13 Al6 1_556 13_566 109.41(5) ?
Al12 Al13 Al6 13_566 13_566 105.27(6) ?
Al10 Al13 Al6 13_567 13_566 57.61(5) ?
Al8 Al13 Al6 11_566 13_566 56.54(6) ?
Al13 Al13 Al6 12 13_566 144.62(4) ?
Mn2 Al13 Al1 . . 58.45(6) ?
Mn3 Al13 Al1 13_566 . 115.78(6) ?
Al7A Al13 Al1 . . 109.92(7) ?
Al11 Al13 Al1 1_556 . 96.52(5) ?
Ni1 Al13 Al1 1_556 . 109.98(4) ?
Al12 Al13 Al1 13_566 . 61.44(5) ?
Al10 Al13 Al1 13_567 . 160.56(6) ?
Al8 Al13 Al1 11_566 . 103.19(6) ?
Al13 Al13 Al1 12 . 60.68(3) ?
Al6 Al13 Al1 13_566 . 140.42(6) ?
Mn2 Al13 Al3 . 13_566 97.93(5) ?
Mn3 Al13 Al3 13_566 13_566 51.70(3) ?
Al7A Al13 Al3 . 13_566 130.66(8) ?
Al11 Al13 Al3 1_556 13_566 110.78(6) ?
Ni1 Al13 Al3 1_556 13_566 158.58(5) ?
Al12 Al13 Al3 13_566 13_566 60.44(6) ?
Al10 Al13 Al3 13_567 13_566 107.22(5) ?
Al8 Al13 Al3 11_566 13_566 74.99(7) ?
Al13 Al13 Al3 12 13_566 142.73(3) ?
Al6 Al13 Al3 13_566 13_566 57.38(6) ?
Al1 Al13 Al3 . 13_566 85.90(5) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ni1 Al7B 1_565 2.2523(7) ?
Ni1 Al7A 9_576 2.468(2) ?
Ni1 Al10 13_566 2.4921(12) ?
Ni1 Al10 8_466 2.4921(12) ?
Ni1 Al11 . 2.4989(13) ?
Ni1 Al11 12 2.4989(13) ?
Ni1 Al7A 1_554 2.652(3) ?
Ni1 Al9 . 2.7106(12) ?
Ni1 Al9 3 2.7107(12) ?
Ni1 Al13 12_554 2.7315(15) ?
Ni1 Al13 1_554 2.7315(15) ?
Mn1 Al8 15_456 2.462(2) ?
Mn1 Al8 13_556 2.462(2) ?
Mn1 Al6 2_565 2.5310(19) ?
Mn1 Al6 9_566 2.5310(19) ?
Mn1 Al4 . 2.6399(19) ?
Mn1 Al4 10_557 2.6400(19) ?
Mn1 Al10 3_556 2.7312(12) ?
Mn1 Al10 12 2.7312(12) ?
Mn1 Al10 10_557 2.7312(12) ?
Mn1 Al10 . 2.7312(12) ?
Mn1 Al9 13_566 2.8328(18) ?
Mn1 Al9 15_466 2.8328(18) ?
Mn2 Al8 11_566 2.333(2) ?
Mn2 Al8 9_566 2.333(2) ?
Mn2 Al13 3_556 2.3349(14) ?
Mn2 Al13 10_557 2.3349(14) ?
Mn2 Al13 12 2.3349(14) ?
Mn2 Al13 . 2.3349(14) ?
Mn2 Al7A 10_557 2.491(3) ?
Mn2 Al7A . 2.491(3) ?
Mn2 Al1 . 2.633(3) ?
Mn3 Al3 . 2.4459(8) ?
Mn3 Al12 12 2.5085(13) ?
Mn3 Al12 . 2.5086(13) ?
Mn3 Al6 . 2.5162(19) ?
Mn3 Al4 1_554 2.5563(18) ?
Mn3 Al13 8_466 2.5800(14) ?
Mn3 Al13 13_566 2.5800(14) ?
Mn3 Al5 1_554 2.8481(18) ?
Mn3 Al11 8_465 2.8962(13) ?
Mn3 Al11 13_565 2.8962(13) ?
Mn3 Al10 12_554 2.9039(13) ?
Mn3 Al10 1_554 2.9039(13) ?
Mn4 Al2 13_566 2.3996(9) ?
Mn4 Al12 13_566 2.4779(13) ?
Mn4 Al12 6_565 2.4779(13) ?
Mn4 Al4 . 2.6116(15) ?
Mn4 Al4 10_557 2.6116(15) ?
Mn4 Al11 6_565 2.6823(12) ?
Mn4 Al11 13_566 2.6823(12) ?
Mn4 Al1 . 2.716(2) ?
Mn4 Al5 . 2.7642(15) ?
Mn4 Al5 10_557 2.7642(15) ?
Mn4 Al9 13_566 2.8163(19) ?
Mn4 Mn4 3_556 2.8282(17) ?
Al1 Al5 . 2.861(2) ?
Al1 Al5 10_557 2.861(2) ?
Al1 Al12 15_466 2.9093(14) ?
Al1 Al12 13_566 2.9093(14) ?
Al1 Al12 8_466 2.9093(14) ?
Al1 Al12 6_565 2.9093(14) ?
Al1 Al13 . 2.946(2) ?
Al1 Al13 12 2.946(2) ?
Al1 Al13 10_557 2.946(2) ?
Al2 Al12 . 2.809(2) ?
Al2 Al12 12 2.809(2) ?
Al2 Al12 3 2.809(2) ?
Al2 Al12 10_556 2.809(2) ?
Al2 Al9 3 2.829(3) ?
Al2 Al9 . 2.829(3) ?
Al2 Al11 10_556 2.8490(13) ?
Al2 Al11 12 2.8490(13) ?
Al2 Al11 3 2.8490(13) ?
Al2 Al11 . 2.8490(13) ?
Al3 Al6 10_556 2.819(3) ?
Al3 Al6 . 2.819(3) ?
Al3 Al12 10_556 2.881(2) ?
Al3 Al12 3 2.881(2) ?
Al3 Al12 12 2.881(2) ?
Al3 Al12 . 2.881(2) ?
Al3 Al13 8_466 2.9714(14) ?
Al3 Al13 6_564 2.9714(14) ?
Al3 Al13 15_465 2.9714(14) ?
Al3 Al13 13_566 2.9714(14) ?
Al4 Al4 10_557 2.483(3) ?
Al4 Al5 . 2.641(2) ?
Al4 Al10 . 2.6985(18) ?
Al4 Al10 12 2.6985(18) ?
Al4 Al11 13_566 2.7001(15) ?
Al4 Al11 8_466 2.7001(14) ?
Al4 Al9 15_466 2.8270(18) ?
Al4 Al9 13_566 2.8270(18) ?
Al5 Al12 13_566 2.7131(15) ?
Al5 Al12 8_466 2.7131(15) ?
Al5 Al12 1_556 2.8480(18) ?
Al5 Al12 12_556 2.8480(18) ?
Al5 Al11 8_466 2.8510(15) ?
Al5 Al11 13_566 2.8510(15) ?
Al6 Al8 7 2.722(2) ?
Al6 Al8 5_455 2.722(2) ?
Al6 Al10 9_566 2.7266(19) ?
Al6 Al10 4_566 2.7266(19) ?
Al6 Al10 12_554 2.7300(19) ?
Al6 Al10 1_554 2.7300(19) ?
Al6 Al13 13_566 2.9000(16) ?
Al6 Al13 8_466 2.9000(16) ?
Al7A Al7A 9_577 2.442(5) ?
Al7A Al8 9_566 2.608(3) ?
Al7A Al8 11_566 2.608(3) ?
Al7A Al13 12 2.685(2) ?
Al7A Al13 . 2.685(2) ?
Al7A Al10 16 2.9016(17) ?
Al7A Al10 5_455 2.9016(17) ?
Al7B Al10 16_544 2.8166(12) ?
Al7B Al10 8_456 2.8166(12) ?
Al7B Al10 5_444 2.8166(12) ?
Al7B Al10 13_556 2.8166(12) ?
Al8 Al9 1_545 2.843(3) ?
Al8 Al13 11_565 2.847(2) ?
Al8 Al13 4_566 2.847(2) ?
Al8 Al10 13_556 2.8874(16) ?
Al8 Al10 6_554 2.8874(16) ?
Al9 Al10 6_564 2.7591(15) ?
Al9 Al10 13_566 2.7591(15) ?
Al9 Al9 3 2.811(4) ?
Al9 Al11 . 2.8242(15) ?
Al9 Al11 10_556 2.8242(15) ?
Al10 Al13 13_567 2.7603(17) ?
Al10 Al10 12 2.890(2) ?
Al11 Al13 1_554 2.7046(17) ?
Al11 Al12 13_565 2.7705(16) ?
Al11 Al12 . 2.7891(16) ?
Al11 Al11 12 2.917(2) ?
Al12 Al13 13_566 2.7393(17) ?
Al12 Al12 12 2.855(3) ?
Al13 Al13 12 2.884(3) ?
