#------------------------------------------------------------------------------
#$Date: 2022-10-25 03:32:32 +0300 (Tue, 25 Oct 2022) $
#$Revision: 278760 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/78/1567837.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1567837
loop_
_publ_author_name
'Bao, Lipiao'
'Yu, Pengwei'
'Hu, Shuaifeng'
'Tian, Xinyue'
'Shen, Wangqiang'
'Yu, Pengyuan'
'Guo, Kun'
'Xie, Yun-Peng'
'Lu, Xing'
_publ_section_title
;
 Steering Lu3N cluster in C76-78 cages: Cluster configuration dominated by
 cage transformation
;
_journal_name_full               Nanoscale
_journal_paper_doi               10.1039/D2NR05049H
_journal_year                    2022
_chemical_formula_moiety
'C78, C36 H44 N4 Ni1.04, Lu3 N, 1.5(C6 H6), C S2'
_chemical_formula_sum            'C124 H53 Lu3 N5 Ni S2'
_chemical_formula_weight         2260.45
_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_Hall           '-C 2y'
_space_group_name_H-M_alt        'C 1 2/m 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2022-05-17 deposited with the CCDC.	2022-10-24 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 107.97(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   26.440(5)
_cell_length_b                   16.808(3)
_cell_length_c                   17.861(4)
_cell_measurement_reflns_used    9917
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      23.8205
_cell_measurement_theta_min      2.514
_cell_volume                     7550(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.7336
_diffrn_reflns_av_R_equivalents  0.0655
_diffrn_reflns_av_unetI/netI     0.0452
_diffrn_reflns_Laue_measured_fraction_full 0.993
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       31
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            44549
_diffrn_reflns_point_group_measured_fraction_full 0.993
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        26.114
_diffrn_reflns_theta_max         26.335
_diffrn_reflns_theta_min         1.504
_diffrn_source                   'SSRF, Beamline BL17B'
_exptl_absorpt_coefficient_mu    4.611
_exptl_absorpt_correction_T_max  0.602
_exptl_absorpt_correction_T_min  0.380
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.989
_exptl_crystal_description       block
_exptl_crystal_F_000             4420
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.11
_refine_diff_density_max         1.502
_refine_diff_density_min         -1.916
_refine_diff_density_rms         0.154
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.030
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1073
_refine_ls_number_reflns         7194
_refine_ls_number_restraints     1575
_refine_ls_restrained_S_all      1.058
_refine_ls_R_factor_all          0.0847
_refine_ls_R_factor_gt           0.0812
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1174P)²+111.3093P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2133
_refine_ls_wR_factor_ref         0.2168
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6688
_reflns_number_total             7194
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d2nr05049h2.cif
_cod_data_source_block           Lu3N@C78-II
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 
;
_cod_original_sg_symbol_H-M      'C 2/m'
_cod_database_code               1567837
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.4723
_shelx_estimated_absorpt_t_max   0.7450
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.1739(9) 0.6755(14) 0.0149(13) 0.086(7) Uani 0.5 1 d D U P A -1
C2 C 0.2000(9) 0.6224(14) -0.0284(14) 0.105(7) Uani 0.5 1 d D U P A -1
C3 C 0.1738(8) 0.5513(13) -0.0633(13) 0.074(6) Uani 0.5 1 d D U P A -1
C4 C 0.1222(7) 0.5275(13) -0.0619(13) 0.090(2) Uani 0.5 1 d D U P A -1
C5 C 0.0934(8) 0.5787(15) -0.0276(14) 0.089(3) Uani 0.5 1 d D U P A -1
C6 C 0.1214(7) 0.6516(16) 0.0024(15) 0.091(3) Uani 0.5 1 d D U P A -1
C7 C 0.1125(10) 0.686(2) 0.0840(14) 0.086(6) Uani 0.5 1 d D U P A -1
C8 C 0.2121(12) 0.712(2) 0.0830(17) 0.126(9) Uani 0.5 1 d D U P A -1
C9 C 0.2822(10) 0.5501(15) -0.0096(15) 0.097(6) Uani 0.5 1 d D U P A -1
C10 C 0.2146(7) 0.5171(15) 0.4205(9) 0.082(5) Uani 0.5 1 d D U P A -1
C11 C 0.3433(5) 0.4946(15) 0.3021(8) 0.075(3) Uani 0.5 1 d D U P A -1
C12 C 0.3253(6) 0.5574(13) 0.3438(10) 0.075(3) Uani 0.5 1 d D U P A -1
C13 C 0.3080(9) 0.6352(16) 0.3138(15) 0.088(6) Uani 0.5 1 d . U P A -1
C14 C 0.3365(9) 0.6389(18) 0.2555(17) 0.092(6) Uani 0.5 1 d . U P A -1
C15 C 0.3448(12) 0.594(2) 0.198(2) 0.090(6) Uani 0.5 1 d . U P A -1
C16 C 0.3563(5) 0.5232(14) 0.2313(12) 0.075(6) Uani 0.5 1 d . U P A -1
C17 C 0.2631(15) 0.674(2) 0.318(2) 0.090(8) Uani 0.5 1 d . U P A -1
C18 C 0.2962(11) 0.5342(17) 0.3957(15) 0.084(7) Uani 0.5 1 d D U P A -1
C19 C 0.2177(19) 0.648(2) 0.3495(19) 0.102(8) Uani 0.5 1 d . U P A -1
C20 C 0.2453(11) 0.720(2) 0.2527(19) 0.105(9) Uani 0.5 1 d D U P A -1
C21 C 0.1677(10) 0.714(2) 0.1181(16) 0.131(10) Uani 0.5 1 d D U P A -1
C22 C 0.0632(11) 0.5339(19) 0.0139(16) 0.088(2) Uani 0.5 1 d . U P A -1
C23 C 0.1891(10) 0.721(2) 0.2063(16) 0.129(10) Uani 0.5 1 d D U P A -1
C24 C 0.1504(10) 0.6905(17) 0.2446(13) 0.094(9) Uani 0.5 1 d D U P A -1
C25 C 0.1001(9) 0.6470(14) 0.2081(10) 0.064(6) Uani 0.5 1 d D U P A -1
C26 C 0.1770(11) 0.6576(17) 0.3236(14) 0.087(8) Uani 0.5 1 d D U P A -1
C27 C 0.0974(8) 0.5832(13) 0.2626(10) 0.073(6) Uani 0.5 1 d D U P A -1
C28 C 0.1581(6) 0.5140(16) 0.3733(8) 0.076(5) Uani 0.5 1 d D U P A -1
C29 C 0.0735(5) 0.5046(19) 0.2308(9) 0.082(4) Uani 0.5 1 d D U P A -1
C30 C 0.0548(9) 0.5670(15) 0.0857(12) 0.088(3) Uani 0.5 1 d D U P A -1
C31 C 0.0768(8) 0.6433(15) 0.1224(11) 0.090(4) Uani 0.5 1 d D U P A -1
C32 C 0.1428(8) 0.5910(16) 0.3341(11) 0.080(5) Uani 0.5 1 d D U P A -1
C33 C 0.0537(5) 0.502(2) 0.1436(9) 0.087(3) Uani 0.5 1 d D U P A -1
C34 C 0.1989(8) 0.4762(12) -0.0669(10) 0.086(7) Uani 0.5 1 d D U P A -1
C35 C 0.3268(11) 0.606(2) 0.113(2) 0.090(7) Uani 0.5 1 d . U P A -1
C36 C 0.2473(17) 0.578(2) 0.4047(18) 0.097(9) Uani 0.5 1 d . U P A -1
C37 C 0.2916(11) 0.708(2) 0.2186(18) 0.111(8) Uani 0.5 1 d D U P A -1
C38 C 0.2856(11) 0.6630(18) 0.0840(19) 0.091(7) Uani 0.5 1 d . U P A -1
C39 C 0.2807(11) 0.400(2) -0.0036(16) 0.096(7) Uani 0.5 1 d . U P A -1
C40 C 0.3268(13) 0.546(2) 0.0632(18) 0.087(7) Uani 0.5 1 d . U P A -1
C41 C 0.3646(6) 0.4647(15) 0.1788(11) 0.073(5) Uani 0.5 1 d . U P A -1
C42 C 0.2707(12) 0.702(2) 0.1321(17) 0.121(8) Uani 0.5 1 d D U P A -1
C43 C 0.2558(10) 0.6228(15) 0.0012(15) 0.098(6) Uani 0.5 1 d D U P A -1
C44 C 0.2559(8) 0.4769(13) -0.0346(12) 0.091(7) Uani 0.5 1 d D U P A -1
C45 C 0.3290(6) 0.4113(12) 0.3056(10) 0.075(3) Uani 0.5 1 d D U P A -1
C46 C 0.3175(7) 0.3517(15) 0.2395(11) 0.075(3) Uani 0.5 1 d D U P A -1
C47 C 0.2984(6) 0.3925(12) 0.3588(10) 0.075(3) Uani 0.5 1 d D U P A -1
C48 C 0.2891(12) 0.4517(16) 0.4096(16) 0.087(7) Uani 0.5 1 d D U P A -1
C49 C 0.3500(14) 0.377(2) 0.1889(19) 0.093(8) Uani 0.5 1 d . U P A -1
C50 C 0.3491(8) 0.4750(16) 0.0946(12) 0.076(6) Uani 0.5 1 d . U P A -1
C51 C 0.3275(11) 0.402(2) 0.0609(16) 0.091(7) Uani 0.5 1 d . U P A -1
C52 C 0.3310(11) 0.344(2) 0.1167(16) 0.090(7) Uani 0.5 1 d . U P A -1
C53 C 0.2455(10) 0.4440(16) 0.4243(13) 0.078(7) Uani 0.5 1 d D U P A -1
C54 C 0.2558(10) 0.3349(17) 0.3403(17) 0.090(9) Uani 0.5 1 d D U P A -1
C55 C 0.2259(11) 0.3707(18) 0.3777(17) 0.099(9) Uani 0.5 1 d D U P A -1
C56 C 0.1902(8) 0.2718(12) 0.1005(13) 0.083(6) Uani 0.5 1 d D U P A -1
C57 C 0.1881(8) 0.3427(13) -0.0174(14) 0.108(9) Uani 0.5 1 d D U P A -1
C58 C 0.1674(10) 0.4149(15) -0.0570(15) 0.096(8) Uani 0.5 1 d D U P A -1
C59 C 0.1612(8) 0.3050(14) 0.0292(13) 0.096(9) Uani 0.5 1 d D U P A -1
C60 C 0.0824(8) 0.3703(12) 0.1489(14) 0.104(7) Uani 0.5 1 d D U P A -1
C61 C 0.1107(8) 0.3171(14) 0.1108(13) 0.106(7) Uani 0.5 1 d D U P A -1
C62 C 0.1121(7) 0.3312(11) 0.0344(12) 0.099(8) Uani 0.5 1 d D U P A -1
C63 C 0.0590(10) 0.4349(17) 0.1067(12) 0.089(2) Uani 0.5 1 d D U P A -1
C64 C 0.0921(8) 0.4018(14) -0.0041(13) 0.090(2) Uani 0.5 1 d D U P A -1
C65 C 0.1200(8) 0.4396(15) -0.0502(14) 0.090(2) Uani 0.5 1 d D U P A -1
C66 C 0.0630(12) 0.4536(19) 0.0291(14) 0.089(2) Uani 0.5 1 d D U P A -1
C67 C 0.2717(10) 0.3014(16) 0.2124(17) 0.122(10) Uani 0.5 1 d D U P A -1
C68 C 0.1675(10) 0.3656(16) 0.3387(18) 0.081(7) Uani 0.5 1 d D U P A -1
C69 C 0.0965(10) 0.4391(18) 0.276(2) 0.083(4) Uani 0.5 1 d . U P A -1
C70 C 0.1570(9) 0.2770(15) 0.1484(13) 0.114(8) Uani 0.5 1 d D U P A -1
C71 C 0.0994(11) 0.3712(18) 0.2304(16) 0.080(7) Uani 0.5 1 d D U P A -1
C72 C 0.1767(13) 0.286(2) 0.2304(15) 0.103(8) Uani 0.5 1 d D U P A -1
C73 C 0.1461(13) 0.327(2) 0.2671(16) 0.082(7) Uani 0.5 1 d D U P A -1
C74 C 0.2440(10) 0.2813(15) 0.1361(17) 0.130(10) Uani 0.5 1 d D U P A -1
C75 C 0.1329(8) 0.4368(14) 0.3370(18) 0.083(4) Uani 0.5 1 d D U P A -1
C76 C 0.2359(11) 0.2961(19) 0.2622(19) 0.106(9) Uani 0.5 1 d D U P A -1
C77 C 0.2417(8) 0.3392(14) 0.0136(12) 0.078(6) Uani 0.5 1 d D U P A -1
C78 C 0.2719(11) 0.304(2) 0.0828(17) 0.114(9) Uani 0.5 1 d D U P A -1
N1 N 0.2133(2) 0.5000 0.1734(4) 0.0269(14) Uani 1 2 d S T P B 2
Lu1 Lu 0.15789(12) 0.5594(2) 0.09154(19) 0.0377(7) Uani 0.2189 1 d . U P B 2
Lu2 Lu 0.2140(3) 0.5000 0.2912(2) 0.0345(15) Uani 0.28 2 d S T P B 2
Lu3 Lu 0.26782(5) 0.45828(15) 0.11494(10) 0.0523(4) Uani 0.2721 1 d . . P B 2
Lu4 Lu 0.22224(16) 0.4705(3) 0.29028(13) 0.0253(5) Uani 0.2625 1 d . . P B 2
Lu5 Lu 0.26941(10) 0.5751(2) 0.14597(17) 0.0230(6) Uani 0.1513 1 d . U P B 2
Lu6 Lu 0.15227(19) 0.5698(3) 0.1119(2) 0.0227(8) Uani 0.1496 1 d . U P B 2
Lu7 Lu 0.1514(6) 0.5000 0.0798(10) 0.211(7) Uani 0.1162 2 d S TU P B 2
Lu8 Lu 0.1405(3) 0.5380(7) 0.1540(8) 0.090(3) Uani 0.0572 1 d . U P B 2
Lu9 Lu 0.2299(10) 0.4164(16) 0.2673(13) 0.188(15) Uani 0.048 1 d . . P B 2
Lu10 Lu 0.2638(8) 0.5537(13) 0.1798(15) 0.156(8) Uani 0.0463 1 d . U P B 2
Lu11 Lu 0.2654(7) 0.6012(7) 0.1569(12) 0.069(7) Uani 0.0427 1 d . U P B 2
Lu12 Lu 0.2455(3) 0.6163(4) 0.2180(4) 0.0253(13) Uani 0.0371 1 d . U P B 2
Lu13 Lu 0.1381(9) 0.5000 0.180(2) 0.076(4) Uani 0.0324 2 d S TU P B 2
Ni1P Ni 0.44911(4) 0.5000 0.41103(5) 0.0398(4) Uani 1 2 d S T P C 7
C1P C 0.4015(3) 0.5000 0.5660(5) 0.044(3) Uani 1 2 d S TU P C 7
H1P H 0.3893 0.5000 0.6108 0.052 Uiso 1 2 calc R U P C 7
N2P N 0.4292(2) 0.4178(5) 0.4742(3) 0.0466(11) Uani 1 1 d . U . C 7
C3P C 0.3978(2) 0.3526(6) 0.5662(3) 0.049(2) Uani 1 1 d . U . C 7
C4P C 0.3747(3) 0.3434(6) 0.6329(4) 0.053(2) Uani 1 1 d . U . C 7
H4PA H 0.3915 0.3825 0.6745 0.064 Uiso 1 1 calc R U . C 7
H4PB H 0.3830 0.2895 0.6558 0.064 Uiso 1 1 calc R U . C 7
C5P C 0.3143(3) 0.3555(6) 0.6066(4) 0.058(2) Uani 1 1 d . U . C 7
H5PA H 0.3013 0.3501 0.6520 0.087 Uiso 1 1 calc R U . C 7
H5PB H 0.2973 0.3154 0.5670 0.087 Uiso 1 1 calc R U . C 7
H5PC H 0.3058 0.4088 0.5838 0.087 Uiso 1 1 calc R U . C 7
C6P C 0.4098(3) 0.2945(6) 0.5217(4) 0.056(2) Uani 1 1 d . U . C 7
C7P C 0.4034(4) 0.2084(7) 0.5253(5) 0.073(3) Uani 1 1 d . U . C 7
H7PA H 0.4046 0.1935 0.5794 0.087 Uiso 1 1 calc R U . C 7
H7PB H 0.4337 0.1820 0.5139 0.087 Uiso 1 1 calc R U . C 7
C8P C 0.3518(5) 0.1776(7) 0.4678(6) 0.080(3) Uani 1 1 d . U . C 7
H8PA H 0.3504 0.1196 0.4720 0.120 Uiso 1 1 calc R U . C 7
H8PB H 0.3502 0.1922 0.4140 0.120 Uiso 1 1 calc R U . C 7
H8PC H 0.3215 0.2012 0.4804 0.120 Uiso 1 1 calc R U . C 7
C9P C 0.4294(2) 0.3361(6) 0.4646(3) 0.0482(12) Uani 1 1 d . U . C 7
C10P C 0.4459(3) 0.2981(6) 0.4084(4) 0.056(2) Uani 1 1 d . U . C 7
H10P H 0.4453 0.2416 0.4077 0.067 Uiso 1 1 calc R U . C 7
C11P C 0.4633(2) 0.3365(6) 0.3529(3) 0.050(2) Uani 1 1 d . U . C 7
C12P C 0.4791(3) 0.2945(6) 0.2929(4) 0.052(2) Uani 1 1 d . U . C 7
C13P C 0.4782(4) 0.2055(6) 0.2821(5) 0.066(3) Uani 1 1 d . U . C 7
H13A H 0.5021 0.1913 0.2510 0.079 Uiso 1 1 calc R U . C 7
H13B H 0.4924 0.1800 0.3344 0.079 Uiso 1 1 calc R U . C 7
C14P C 0.4238(5) 0.1723(7) 0.2415(6) 0.080(3) Uani 1 1 d . U . C 7
H14A H 0.4260 0.1143 0.2384 0.119 Uiso 1 1 calc R U . C 7
H14B H 0.4104 0.1944 0.1882 0.119 Uiso 1 1 calc R U . C 7
H14C H 0.3997 0.1867 0.2713 0.119 Uiso 1 1 calc R U . C 7
C15P C 0.4935(2) 0.3524(5) 0.2499(3) 0.0467(19) Uani 1 1 d . U . C 7
C16P C 0.5130(3) 0.3406(6) 0.1795(4) 0.056(2) Uani 1 1 d . U . C 7
H16A H 0.5357 0.3863 0.1756 0.067 Uiso 1 1 calc R U . C 7
H16B H 0.5352 0.2920 0.1876 0.067 Uiso 1 1 calc R U . C 7
C17P C 0.4683(4) 0.3328(9) 0.1031(4) 0.087(4) Uani 1 1 d . U . C 7
H17A H 0.4830 0.3188 0.0607 0.131 Uiso 1 1 calc R U . C 7
H17B H 0.4493 0.3835 0.0907 0.131 Uiso 1 1 calc R U . C 7
H17C H 0.4437 0.2911 0.1082 0.131 Uiso 1 1 calc R U . C 7
C18P C 0.4858(2) 0.4270(5) 0.2821(3) 0.0436(17) Uani 1 1 d . U . C 7
C19P C 0.4946(3) 0.5000 0.2539(5) 0.044(2) Uani 1 2 d S TU P C 7
H19P H 0.5081 0.5000 0.2104 0.053 Uiso 1 2 calc R U P C 7
C2P C 0.4093(2) 0.4284(5) 0.5371(3) 0.0463(11) Uani 1 1 d . U . C 7
N1P N 0.46688(18) 0.4176(4) 0.3458(3) 0.0411(15) Uani 1 1 d . . . C 7
C1D C 0.6554(4) 0.5000 0.2102(7) 0.052(3) Uani 1 2 d S TU P D 8
H1D H 0.6754 0.5000 0.2645 0.062 Uiso 1 2 calc R U P D 8
C2D C 0.6409(4) 0.4281(6) 0.1709(5) 0.067(2) Uani 1 1 d . U . D 8
H2D H 0.6530 0.3792 0.1972 0.081 Uiso 1 1 calc R U . D 8
C3D C 0.6087(4) 0.4281(6) 0.0931(5) 0.065(3) Uani 1 1 d . U . D 8
H3D H 0.5989 0.3792 0.0658 0.078 Uiso 1 1 calc R U . D 8
C4D C 0.5907(6) 0.5000 0.0550(7) 0.070(4) Uani 1 2 d S TU P D 8
H4D H 0.5663 0.5000 0.0032 0.084 Uiso 1 2 calc R U P D 8
C1E C 0.7920(5) 0.5000 0.2546(8) 0.067(3) Uani 1 2 d S T P E 9
S1E S 0.79104(16) 0.4091(3) 0.2544(3) 0.1112(12) Uani 1 1 d . . . E 9
C1F C 0.4941(8) 0.0000 0.4206(11) 0.081(4) Uani 1 2 d S TU P F 10
H1F H 0.4901 0.0000 0.3659 0.098 Uiso 1 2 calc R U P F 10
C2F C 0.4508(9) 0.0000 0.4466(15) 0.117(6) Uani 1 2 d S TU P F 10
H2F H 0.4160 0.0000 0.4102 0.140 Uiso 1 2 calc R U P F 10
C3F C 0.4582(8) 0.0000 0.5266(14) 0.103(6) Uani 1 2 d S TU P F 10
H3F H 0.4278 0.0000 0.5444 0.124 Uiso 1 2 calc R U P F 10
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0037 0.0018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0072 0.0037 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1331 0.1339 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3396 1.1864 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.4797 6.2410 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C6 C1 C8 131(2) . . ?
C6 C1 C2 110.0(18) . . ?
C8 C1 C2 112(2) . . ?
C6 C1 C21 83.1(14) . . ?
C8 C1 C21 47.9(12) . . ?
C2 C1 C21 148.7(18) . . ?
C43 C2 C3 118.7(17) . . ?
C43 C2 C1 113.8(19) . . ?
C3 C2 C1 119.4(17) . . ?
C2 C3 C4 124.4(16) . . ?
C2 C3 C34 125.9(17) . . ?
C4 C3 C34 102.3(18) . . ?
C5 C4 C3 119.0(16) . . ?
C5 C4 C65 120(2) . . ?
C3 C4 C65 110.9(17) . . ?
C4 C5 C6 113.2(17) . . ?
C4 C5 C22 111(2) . . ?
C6 C5 C22 123(2) . . ?
C1 C6 C5 132.4(19) . . ?
C1 C6 C7 99.4(16) . . ?
C5 C6 C7 115(2) . . ?
C21 C7 C31 129.8(18) . . ?
C21 C7 C6 94.7(18) . . ?
C31 C7 C6 121(2) . . ?
C1 C8 C21 86(2) . . ?
C1 C8 C42 138(3) . . ?
C21 C8 C42 123(2) . . ?
C44 C9 C43 124.3(18) . . ?
C44 C9 C40 115(2) . . ?
C43 C9 C40 102(2) . . ?
C36 C10 C53 104.3(16) . . ?
C36 C10 C28 119(2) . . ?
C53 C10 C28 116.7(17) . . ?
C12 C11 C45 123.1(15) . . ?
C12 C11 C16 114(2) . . ?
C45 C11 C16 118.5(16) . . ?
C18 C12 C13 108(2) . . ?
C18 C12 C11 117.5(17) . . ?
C13 C12 C11 126(2) . . ?
C17 C13 C12 126(3) . . ?
C17 C13 C14 131(3) . . ?
C12 C13 C14 97(2) . . ?
C17 C13 C37 78(2) . . ?
C12 C13 C37 145(2) . . ?
C14 C13 C37 53.3(17) . . ?
C15 C14 C13 140(3) . . ?
C15 C14 C37 111(3) . . ?
C13 C14 C37 81(2) . . ?
C16 C15 C14 103(3) . . ?
C16 C15 C35 123(4) . . ?
C14 C15 C35 130(4) . . ?
C15 C16 C41 113(3) . . ?
C15 C16 C11 126(3) . . ?
C41 C16 C11 117(2) . . ?
C20 C17 C13 108(3) . . ?
C20 C17 C19 112(3) . . ?
C13 C17 C19 132(3) . . ?
C12 C18 C48 120.1(19) . . ?
C12 C18 C36 125(2) . . ?
C48 C18 C36 107(3) . . ?
C26 C19 C17 127(4) . . ?
C26 C19 C36 130(4) . . ?
C17 C19 C36 99(3) . . ?
C17 C20 C23 121(3) . . ?
C17 C20 C37 99(3) . . ?
C23 C20 C37 125(2) . . ?
C7 C21 C8 129(2) . . ?
C7 C21 C23 117.7(19) . . ?
C8 C21 C23 110.5(18) . . ?
C7 C21 C1 82.6(16) . . ?
C8 C21 C1 46.4(16) . . ?
C23 C21 C1 151(2) . . ?
C66 C22 C5 130(3) . . ?
C66 C22 C30 101(3) . . ?
C5 C22 C30 120(2) . . ?
C20 C23 C24 117(2) . . ?
C20 C23 C21 126(2) . . ?
C24 C23 C21 111.3(18) . . ?
C26 C24 C25 109.5(12) . . ?
C26 C24 C23 112(2) . . ?
C25 C24 C23 128.3(19) . . ?
C31 C25 C27 125.0(16) . . ?
C31 C25 C24 120.8(16) . . ?
C27 C25 C24 106.8(11) . . ?
C19 C26 C24 127(3) . . ?
C19 C26 C32 114(3) . . ?
C24 C26 C32 105.9(12) . . ?
C32 C27 C25 108.6(11) . . ?
C32 C27 C29 123.2(15) . . ?
C25 C27 C29 119.7(15) . . ?
C32 C28 C10 108.9(19) . . ?
C32 C28 C75 122.2(15) . . ?
C10 C28 C75 120.7(15) . . ?
C69 C29 C33 122(3) . . ?
C69 C29 C27 114.8(18) . . ?
C33 C29 C27 113.2(18) . . ?
C31 C30 C22 125(2) . . ?
C31 C30 C33 114.4(17) . . ?
C22 C30 C33 111(2) . . ?
C25 C31 C30 118.8(16) . . ?
C25 C31 C7 109.6(15) . . ?
C30 C31 C7 115(2) . . ?
C27 C32 C28 111.6(18) . . ?
C27 C32 C26 109.0(12) . . ?
C28 C32 C26 129.4(18) . . ?
C63 C33 C29 119(2) . . ?
C63 C33 C30 104.2(15) . . ?
C29 C33 C30 129(2) . . ?
C58 C34 C3 110.3(18) . . ?
C58 C34 C44 123.9(19) . . ?
C3 C34 C44 114.6(16) . . ?
C40 C35 C38 115(3) . . ?
C40 C35 C15 122(3) . . ?
C38 C35 C15 116(3) . . ?
C10 C36 C18 105(2) . . ?
C10 C36 C19 116(3) . . ?
C18 C36 C19 124(3) . . ?
C42 C37 C20 109.7(19) . . ?
C42 C37 C14 111(3) . . ?
C20 C37 C14 120(2) . . ?
C42 C37 C13 139(3) . . ?
C20 C37 C13 74.8(19) . . ?
C14 C37 C13 45.4(15) . . ?
C42 C38 C35 118(3) . . ?
C42 C38 C43 134(3) . . ?
C35 C38 C43 99(3) . . ?
C51 C39 C44 117(3) . . ?
C51 C39 C77 109(3) . . ?
C44 C39 C77 114(2) . . ?
C35 C40 C50 118(3) . . ?
C35 C40 C9 113(3) . . ?
C50 C40 C9 122(3) . . ?
C16 C41 C50 124(2) . . ?
C16 C41 C49 119(2) . . ?
C50 C41 C49 104(2) . . ?
C38 C42 C37 132(3) . . ?
C38 C42 C8 98(3) . . ?
C37 C42 C8 125(2) . . ?
C2 C43 C9 116(2) . . ?
C2 C43 C38 120.9(19) . . ?
C9 C43 C38 111(2) . . ?
C9 C44 C34 119.1(15) . . ?
C9 C44 C39 122(2) . . ?
C34 C44 C39 116(2) . . ?
C11 C45 C47 116.0(14) . . ?
C11 C45 C46 126.8(17) . . ?
C47 C45 C46 110.3(16) . . ?
C67 C46 C49 123(2) . . ?
C67 C46 C45 127.2(18) . . ?
C49 C46 C45 106(2) . . ?
C48 C47 C54 110(2) . . ?
C48 C47 C45 120.3(17) . . ?
C54 C47 C45 123.1(17) . . ?
C53 C48 C47 114(3) . . ?
C53 C48 C18 108(2) . . ?
C47 C48 C18 121(2) . . ?
C52 C49 C46 110(3) . . ?
C52 C49 C41 108(3) . . ?
C46 C49 C41 123(2) . . ?
C40 C50 C51 121(2) . . ?
C40 C50 C41 118(2) . . ?
C51 C50 C41 107(2) . . ?
C52 C51 C50 112(2) . . ?
C52 C51 C39 115(3) . . ?
C50 C51 C39 121(3) . . ?
C49 C52 C51 109(3) . . ?
C49 C52 C78 124(3) . . ?
C51 C52 C78 100(2) . . ?
C48 C53 C10 116(3) . . ?
C48 C53 C55 99(2) . . ?
C10 C53 C55 125.2(17) . . ?
C55 C54 C47 97(2) . . ?
C55 C54 C76 126(2) . . ?
C47 C54 C76 122(2) . . ?
C54 C55 C53 120(3) . . ?
C54 C55 C68 115(2) . . ?
C53 C55 C68 116(2) . . ?
C74 C56 C59 125.3(18) . . ?
C74 C56 C70 118(2) . . ?
C59 C56 C70 105.2(12) . . ?
C77 C57 C59 113.3(18) . . ?
C77 C57 C58 116(2) . . ?
C59 C57 C58 119.5(18) . . ?
C65 C58 C34 113(2) . . ?
C65 C58 C57 115.9(19) . . ?
C34 C58 C57 123(2) . . ?
C56 C59 C57 119.3(17) . . ?
C56 C59 C62 109.1(12) . . ?
C57 C59 C62 123.2(17) . . ?
C63 C60 C71 121.3(19) . . ?
C63 C60 C61 116.2(19) . . ?
C71 C60 C61 116.8(18) . . ?
C70 C61 C62 105.8(12) . . ?
C70 C61 C60 125.3(17) . . ?
C62 C61 C60 121.5(17) . . ?
C64 C62 C61 120.5(17) . . ?
C64 C62 C59 116.9(16) . . ?
C61 C62 C59 108.4(12) . . ?
C33 C63 C60 120.0(19) . . ?
C33 C63 C66 110(2) . . ?
C60 C63 C66 123(2) . . ?
C62 C64 C66 119.5(17) . . ?
C62 C64 C65 119.0(16) . . ?
C66 C64 C65 115(2) . . ?
C58 C65 C64 125.1(18) . . ?
C58 C65 C4 102.2(18) . . ?
C64 C65 C4 125(2) . . ?
C22 C66 C64 119(3) . . ?
C22 C66 C63 114(3) . . ?
C64 C66 C63 118.5(18) . . ?
C74 C67 C46 128(3) . . ?
C74 C67 C76 110(2) . . ?
C46 C67 C76 117(2) . . ?
C73 C68 C55 122(2) . . ?
C73 C68 C75 106(2) . . ?
C55 C68 C75 120.1(19) . . ?
C75 C69 C29 129(3) . . ?
C75 C69 C71 109(2) . . ?
C29 C69 C71 113(3) . . ?
C61 C70 C72 116.3(18) . . ?
C61 C70 C56 111.2(13) . . ?
C72 C70 C56 123(2) . . ?
C60 C71 C73 115.7(19) . . ?
C60 C71 C69 124(2) . . ?
C73 C71 C69 110(2) . . ?
C73 C72 C70 118(2) . . ?
C73 C72 C76 117(3) . . ?
C70 C72 C76 115(2) . . ?
C72 C73 C68 123(3) . . ?
C72 C73 C71 127(2) . . ?
C68 C73 C71 104(2) . . ?
C56 C74 C67 130(3) . . ?
C56 C74 C78 113(2) . . ?
C67 C74 C78 112(3) . . ?
C69 C75 C68 111(2) . . ?
C69 C75 C28 119(2) . . ?
C68 C75 C28 119.4(16) . . ?
C54 C76 C67 116(2) . . ?
C54 C76 C72 116(2) . . ?
C67 C76 C72 124(2) . . ?
C57 C77 C78 129(2) . . ?
C57 C77 C39 124.5(19) . . ?
C78 C77 C39 103(2) . . ?
C77 C78 C74 116(2) . . ?
C77 C78 C52 112(2) . . ?
C74 C78 C52 120(2) . . ?
Lu10 N1 Lu10 69(2) . 6_565 ?
Lu10 N1 Lu7 121.9(8) . . ?
Lu10 N1 Lu7 121.9(8) 6_565 . ?
Lu10 N1 Lu8 163.7(9) . 6_565 ?
Lu10 N1 Lu8 126.0(10) 6_565 6_565 ?
Lu7 N1 Lu8 47.7(7) . 6_565 ?
Lu10 N1 Lu8 126.0(10) . . ?
Lu10 N1 Lu8 163.7(9) 6_565 . ?
Lu7 N1 Lu8 47.7(7) . . ?
Lu8 N1 Lu8 38.1(8) 6_565 . ?
Lu10 N1 Lu1 138.7(11) . 6_565 ?
Lu10 N1 Lu1 100.4(6) 6_565 6_565 ?
Lu7 N1 Lu1 30.13(14) . 6_565 ?
Lu8 N1 Lu1 40.9(5) 6_565 6_565 ?
Lu8 N1 Lu1 64.7(4) . 6_565 ?
Lu10 N1 Lu1 100.4(6) . . ?
Lu10 N1 Lu1 138.7(11) 6_565 . ?
Lu7 N1 Lu1 30.13(14) . . ?
Lu8 N1 Lu1 64.7(4) 6_565 . ?
Lu8 N1 Lu1 40.9(5) . . ?
Lu1 N1 Lu1 60.2(3) 6_565 . ?
Lu10 N1 Lu6 151.8(12) . 6_565 ?
Lu10 N1 Lu6 102.8(7) 6_565 6_565 ?
Lu7 N1 Lu6 38.3(3) . 6_565 ?
Lu8 N1 Lu6 30.4(5) 6_565 6_565 ?
Lu8 N1 Lu6 61.1(4) . 6_565 ?
Lu1 N1 Lu6 13.33(11) 6_565 6_565 ?
Lu1 N1 Lu6 67.0(2) . 6_565 ?
Lu10 N1 Lu6 102.8(7) . . ?
Lu10 N1 Lu6 151.8(12) 6_565 . ?
Lu7 N1 Lu6 38.3(3) . . ?
Lu8 N1 Lu6 61.1(4) 6_565 . ?
Lu8 N1 Lu6 30.4(5) . . ?
Lu1 N1 Lu6 67.0(2) 6_565 . ?
Lu1 N1 Lu6 13.33(11) . . ?
Lu6 N1 Lu6 70.9(4) 6_565 . ?
Lu10 N1 Lu13 144.5(12) . . ?
Lu10 N1 Lu13 144.5(12) 6_565 . ?
Lu7 N1 Lu13 58.2(13) . . ?
Lu8 N1 Lu13 23.3(7) 6_565 . ?
Lu8 N1 Lu13 23.3(7) . . ?
Lu1 N1 Lu13 62.1(10) 6_565 . ?
Lu1 N1 Lu13 62.1(9) . . ?
Lu6 N1 Lu13 53.2(8) 6_565 . ?
Lu6 N1 Lu13 53.2(8) . . ?
Lu10 N1 Lu4 103.3(9) . . ?
Lu10 N1 Lu4 87.7(11) 6_565 . ?
Lu7 N1 Lu4 131.7(7) . . ?
Lu8 N1 Lu4 84.3(5) 6_565 . ?
Lu8 N1 Lu4 93.2(5) . . ?
Lu1 N1 Lu4 116.5(3) 6_565 . ?
Lu1 N1 Lu4 133.2(3) . . ?
Lu6 N1 Lu4 103.3(3) 6_565 . ?
Lu6 N1 Lu4 120.4(3) . . ?
Lu13 N1 Lu4 75.5(11) . . ?
Lu10 N1 Lu4 87.7(11) . 6_565 ?
Lu10 N1 Lu4 103.3(9) 6_565 6_565 ?
Lu7 N1 Lu4 131.7(7) . 6_565 ?
Lu8 N1 Lu4 93.2(5) 6_565 6_565 ?
Lu8 N1 Lu4 84.3(5) . 6_565 ?
Lu1 N1 Lu4 133.2(3) 6_565 6_565 ?
Lu1 N1 Lu4 116.5(3) . 6_565 ?
Lu6 N1 Lu4 120.4(3) 6_565 6_565 ?
Lu6 N1 Lu4 103.3(3) . 6_565 ?
Lu13 N1 Lu4 75.5(11) . 6_565 ?
Lu4 N1 Lu4 27.5(2) . 6_565 ?
Lu7 Lu1 Lu8 80.5(13) . . ?
Lu7 Lu1 N1 72.5(7) . . ?
Lu8 Lu1 N1 68.2(4) . . ?
Lu7 Lu1 Lu1 12.7(7) . 6_565 ?
Lu8 Lu1 Lu1 74.9(5) . 6_565 ?
N1 Lu1 Lu1 59.88(14) . 6_565 ?
Lu7 Lu1 Lu13 67.7(13) . . ?
Lu8 Lu1 Lu13 14.0(8) . . ?
N1 Lu1 Lu13 59.9(7) . . ?
Lu1 Lu1 Lu13 61.2(5) 6_565 . ?
Lu7 Lu1 Lu8 45.7(12) . 6_565 ?
Lu8 Lu1 Lu8 35.8(8) . 6_565 ?
N1 Lu1 Lu8 56.9(3) . 6_565 ?
Lu1 Lu1 Lu8 39.1(4) 6_565 6_565 ?
Lu13 Lu1 Lu8 22.2(7) . 6_565 ?
Lu7 Lu1 Lu6 20.2(10) . 6_565 ?
Lu8 Lu1 Lu6 63.6(5) . 6_565 ?
N1 Lu1 Lu6 57.2(2) . 6_565 ?
Lu1 Lu1 Lu6 11.26(12) 6_565 6_565 ?
Lu13 Lu1 Lu6 50.0(5) . 6_565 ?
Lu8 Lu1 Lu6 27.9(4) 6_565 6_565 ?
Lu7 Lu1 Lu10 99.1(9) . . ?
Lu8 Lu1 Lu10 93.6(7) . . ?
N1 Lu1 Lu10 34.5(4) . . ?
Lu1 Lu1 Lu10 88.0(5) 6_565 . ?
Lu13 Lu1 Lu10 89.9(9) . . ?
Lu8 Lu1 Lu10 91.1(4) 6_565 . ?
Lu6 Lu1 Lu10 88.9(4) 6_565 . ?
Lu7 Lu1 Lu11 114.4(9) . . ?
Lu8 Lu1 Lu11 106.0(6) . . ?
N1 Lu1 Lu11 53.0(4) . . ?
Lu1 Lu1 Lu11 104.5(3) 6_565 . ?
Lu13 Lu1 Lu11 105.3(9) . . ?
Lu8 Lu1 Lu11 109.4(4) 6_565 . ?
Lu6 Lu1 Lu11 106.7(4) 6_565 . ?
Lu10 Lu1 Lu11 18.6(4) . . ?
Lu7 Lu1 Lu5 104.6(9) . . ?
Lu8 Lu1 Lu5 108.7(4) . . ?
N1 Lu1 Lu5 48.60(17) . . ?
Lu1 Lu1 Lu5 95.38(11) 6_565 . ?
Lu13 Lu1 Lu5 105.4(8) . . ?
Lu8 Lu1 Lu5 105.4(3) 6_565 . ?
Lu6 Lu1 Lu5 98.7(2) 6_565 . ?
Lu10 Lu1 Lu5 15.5(5) . . ?
Lu11 Lu1 Lu5 10.3(3) . . ?
Lu7 Lu1 Lu3 91.5(10) . 6_565 ?
Lu8 Lu1 Lu3 116.0(4) . 6_565 ?
N1 Lu1 Lu3 49.23(18) . 6_565 ?
Lu1 Lu1 Lu3 83.96(9) 6_565 6_565 ?
Lu13 Lu1 Lu3 109.1(7) . 6_565 ?
Lu8 Lu1 Lu3 102.9(3) 6_565 6_565 ?
Lu6 Lu1 Lu3 89.46(19) 6_565 6_565 ?
Lu10 Lu1 Lu3 25.0(7) . 6_565 ?
Lu11 Lu1 Lu3 25.9(4) . 6_565 ?
Lu5 Lu1 Lu3 15.91(7) . 6_565 ?
Lu7 Lu1 Lu12 122.1(7) . . ?
Lu8 Lu1 Lu12 80.7(5) . . ?
N1 Lu1 Lu12 49.68(18) . . ?
Lu1 Lu1 Lu12 109.55(16) 6_565 . ?
Lu13 Lu1 Lu12 83.7(8) . . ?
Lu8 Lu1 Lu12 95.6(3) 6_565 . ?
Lu6 Lu1 Lu12 106.1(3) 6_565 . ?
Lu10 Lu1 Lu12 29.2(7) . . ?
Lu11 Lu1 Lu12 28.0(5) . . ?
Lu5 Lu1 Lu12 35.75(17) . . ?
Lu3 Lu1 Lu12 51.00(17) 6_565 . ?
Lu4 Lu2 Lu4 132(2) 6_565 . ?
Lu4 Lu2 Lu9 132.0(16) 6_565 . ?
Lu4 Lu2 Lu9 13.7(8) . . ?
Lu4 Lu2 Lu9 13.7(8) 6_565 6_565 ?
Lu4 Lu2 Lu9 132.0(16) . 6_565 ?
Lu9 Lu2 Lu9 128.1(18) . 6_565 ?
Lu4 Lu2 N1 81.4(7) 6_565 . ?
Lu4 Lu2 N1 81.4(7) . . ?
Lu9 Lu2 N1 69.3(7) . . ?
Lu9 Lu2 N1 69.3(7) 6_565 . ?
Lu4 Lu2 Lu13 102.7(9) 6_565 . ?
Lu4 Lu2 Lu13 102.7(9) . . ?
Lu9 Lu2 Lu13 90.1(6) . . ?
Lu9 Lu2 Lu13 90.1(6) 6_565 . ?
N1 Lu2 Lu13 54.0(9) . . ?
Lu4 Lu2 Lu12 27.8(6) 6_565 . ?
Lu4 Lu2 Lu12 118.3(11) . . ?
Lu9 Lu2 Lu12 112.4(9) . . ?
Lu9 Lu2 Lu12 16.6(8) 6_565 . ?
N1 Lu2 Lu12 53.6(2) . . ?
Lu13 Lu2 Lu12 84.3(6) . . ?
Lu4 Lu2 Lu12 118.3(11) 6_565 6_565 ?
Lu4 Lu2 Lu12 27.8(6) . 6_565 ?
Lu9 Lu2 Lu12 16.6(8) . 6_565 ?
Lu9 Lu2 Lu12 112.4(9) 6_565 6_565 ?
N1 Lu2 Lu12 53.6(2) . 6_565 ?
Lu13 Lu2 Lu12 84.3(6) . 6_565 ?
Lu12 Lu2 Lu12 96.2(4) . 6_565 ?
Lu4 Lu2 Lu8 86.5(8) 6_565 . ?
Lu4 Lu2 Lu8 111.8(8) . . ?
Lu9 Lu2 Lu8 98.3(6) . . ?
Lu9 Lu2 Lu8 73.6(6) 6_565 . ?
N1 Lu2 Lu8 46.1(3) . . ?
Lu13 Lu2 Lu8 16.7(5) . . ?
Lu12 Lu2 Lu8 67.8(3) . . ?
Lu12 Lu2 Lu8 88.5(3) 6_565 . ?
Lu4 Lu2 Lu8 111.8(8) 6_565 6_565 ?
Lu4 Lu2 Lu8 86.5(8) . 6_565 ?
Lu9 Lu2 Lu8 73.6(6) . 6_565 ?
Lu9 Lu2 Lu8 98.3(6) 6_565 6_565 ?
N1 Lu2 Lu8 46.1(3) . 6_565 ?
Lu13 Lu2 Lu8 16.7(5) . 6_565 ?
Lu12 Lu2 Lu8 88.5(3) . 6_565 ?
Lu12 Lu2 Lu8 67.8(3) 6_565 6_565 ?
Lu8 Lu2 Lu8 27.4(5) . 6_565 ?
Lu4 Lu2 Lu10 54.3(10) 6_565 . ?
Lu4 Lu2 Lu10 89.7(12) . . ?
Lu9 Lu2 Lu10 82.7(11) . . ?
Lu9 Lu2 Lu10 45.9(10) 6_565 . ?
N1 Lu2 Lu10 33.2(4) . . ?
Lu13 Lu2 Lu10 82.5(9) . . ?
Lu12 Lu2 Lu10 29.6(6) . . ?
Lu12 Lu2 Lu10 66.6(6) 6_565 . ?
Lu8 Lu2 Lu10 69.5(4) . . ?
Lu8 Lu2 Lu10 78.4(4) 6_565 . ?
Lu4 Lu2 Lu10 89.7(11) 6_565 6_565 ?
Lu4 Lu2 Lu10 54.3(10) . 6_565 ?
Lu9 Lu2 Lu10 45.9(10) . 6_565 ?
Lu9 Lu2 Lu10 82.7(11) 6_565 6_565 ?
N1 Lu2 Lu10 33.2(4) . 6_565 ?
Lu13 Lu2 Lu10 82.5(9) . 6_565 ?
Lu12 Lu2 Lu10 66.6(6) . 6_565 ?
Lu12 Lu2 Lu10 29.6(6) 6_565 6_565 ?
Lu8 Lu2 Lu10 78.4(4) . 6_565 ?
Lu8 Lu2 Lu10 69.5(4) 6_565 6_565 ?
Lu10 Lu2 Lu10 36.9(11) . 6_565 ?
Lu5 Lu3 Lu10 37.2(9) 6_565 6_565 ?
Lu5 Lu3 Lu11 8.6(9) 6_565 6_565 ?
Lu10 Lu3 Lu11 42.8(11) 6_565 6_565 ?
Lu5 Lu3 Lu3 136.0(2) 6_565 6_565 ?
Lu10 Lu3 Lu3 99.6(9) 6_565 6_565 ?
Lu11 Lu3 Lu3 142.3(9) 6_565 6_565 ?
Lu5 Lu3 Lu10 99.6(6) 6_565 . ?
Lu10 Lu3 Lu10 62.9(11) 6_565 . ?
Lu11 Lu3 Lu10 105.7(12) 6_565 . ?
Lu3 Lu3 Lu10 36.7(6) 6_565 . ?
Lu5 Lu3 Lu5 120.5(3) 6_565 . ?
Lu10 Lu3 Lu5 84.3(9) 6_565 . ?
Lu11 Lu3 Lu5 127.0(9) 6_565 . ?
Lu3 Lu3 Lu5 15.44(7) 6_565 . ?
Lu10 Lu3 Lu5 21.5(6) . . ?
Lu5 Lu3 N1 77.7(2) 6_565 . ?
Lu10 Lu3 N1 47.1(8) 6_565 . ?
Lu11 Lu3 N1 78.7(9) 6_565 . ?
Lu3 Lu3 N1 70.89(9) 6_565 . ?
Lu10 Lu3 N1 44.9(7) . . ?
Lu5 Lu3 N1 60.82(11) . . ?
Lu5 Lu3 Lu12 21.5(2) 6_565 6_565 ?
Lu10 Lu3 Lu12 23.5(10) 6_565 6_565 ?
Lu11 Lu3 Lu12 22.9(9) 6_565 6_565 ?
Lu3 Lu3 Lu12 120.83(17) 6_565 6_565 ?
Lu10 Lu3 Lu12 84.7(6) . 6_565 ?
Lu5 Lu3 Lu12 106.19(18) . 6_565 ?
N1 Lu3 Lu12 56.36(19) . 6_565 ?
Lu5 Lu3 Lu11 118.3(5) 6_565 . ?
Lu10 Lu3 Lu11 81.8(12) 6_565 . ?
Lu11 Lu3 Lu11 124.5(14) 6_565 . ?
Lu3 Lu3 Lu11 17.8(5) 6_565 . ?
Lu10 Lu3 Lu11 18.9(7) . . ?
Lu5 Lu3 Lu11 3.5(5) . . ?
N1 Lu3 Lu11 57.4(5) . . ?
Lu12 Lu3 Lu11 103.3(5) 6_565 . ?
Lu5 Lu3 Lu1 81.8(2) 6_565 6_565 ?
Lu10 Lu3 Lu1 74.6(9) 6_565 6_565 ?
Lu11 Lu3 Lu1 76.4(9) 6_565 6_565 ?
Lu3 Lu3 Lu1 96.04(9) 6_565 6_565 ?
Lu10 Lu3 Lu1 86.2(6) . 6_565 ?
Lu5 Lu3 Lu1 94.34(12) . 6_565 ?
N1 Lu3 Lu1 44.69(17) . 6_565 ?
Lu12 Lu3 Lu1 65.24(17) 6_565 6_565 ?
Lu11 Lu3 Lu1 91.4(5) . 6_565 ?
Lu5 Lu3 Lu7 98.2(3) 6_565 . ?
Lu10 Lu3 Lu7 81.6(9) 6_565 . ?
Lu11 Lu3 Lu7 94.1(9) 6_565 . ?
Lu3 Lu3 Lu7 76.60(9) 6_565 . ?
Lu10 Lu3 Lu7 72.7(6) . . ?
Lu5 Lu3 Lu7 76.55(12) . . ?
N1 Lu3 Lu7 39.7(4) . . ?
Lu12 Lu3 Lu7 79.0(3) 6_565 . ?
Lu11 Lu3 Lu7 73.9(4) . . ?
Lu1 Lu3 Lu7 19.75(14) 6_565 . ?
Lu5 Lu3 Lu6 74.8(2) 6_565 6_565 ?
Lu10 Lu3 Lu6 67.2(9) 6_565 6_565 ?
Lu11 Lu3 Lu6 69.9(9) 6_565 6_565 ?
Lu3 Lu3 Lu6 98.84(11) 6_565 6_565 ?
Lu10 Lu3 Lu6 84.5(6) . 6_565 ?
Lu5 Lu3 Lu6 95.17(14) . 6_565 ?
N1 Lu3 Lu6 40.95(17) . 6_565 ?
Lu12 Lu3 Lu6 57.71(17) 6_565 6_565 ?
Lu11 Lu3 Lu6 92.0(5) . 6_565 ?
Lu1 Lu3 Lu6 7.63(11) 6_565 6_565 ?
Lu7 Lu3 Lu6 24.6(2) . 6_565 ?
Lu2 Lu4 Lu4 24.1(12) . 6_565 ?
Lu2 Lu4 Lu9 159.2(10) . . ?
Lu4 Lu4 Lu9 150.7(12) 6_565 . ?
Lu2 Lu4 Lu9 36.1(13) . 6_565 ?
Lu4 Lu4 Lu9 15.0(8) 6_565 6_565 ?
Lu9 Lu4 Lu9 136(2) . 6_565 ?
Lu2 Lu4 N1 83.7(7) . . ?
Lu4 Lu4 N1 76.25(12) 6_565 . ?
Lu9 Lu4 N1 77.8(9) . . ?
Lu9 Lu4 N1 63.2(6) 6_565 . ?
Lu2 Lu4 Lu12 145.5(8) . 6_565 ?
Lu4 Lu4 Lu12 132.5(2) 6_565 6_565 ?
Lu9 Lu4 Lu12 18.2(12) . 6_565 ?
Lu9 Lu4 Lu12 117.4(9) 6_565 6_565 ?
N1 Lu4 Lu12 61.8(2) . 6_565 ?
Lu2 Lu4 Lu13 65.1(9) . . ?
Lu4 Lu4 Lu13 78.64(18) 6_565 . ?
Lu9 Lu4 Lu13 95.6(9) . . ?
Lu9 Lu4 Lu13 76.7(5) 6_565 . ?
N1 Lu4 Lu13 51.2(8) . . ?
Lu12 Lu4 Lu13 90.8(7) 6_565 . ?
Lu2 Lu4 Lu10 115.8(11) . 6_565 ?
Lu4 Lu4 Lu10 99.1(6) 6_565 6_565 ?
Lu9 Lu4 Lu10 51.6(13) . 6_565 ?
Lu9 Lu4 Lu10 84.1(10) 6_565 6_565 ?
N1 Lu4 Lu10 38.1(4) . 6_565 ?
Lu12 Lu4 Lu10 33.5(6) 6_565 6_565 ?
Lu13 Lu4 Lu10 85.2(9) . 6_565 ?
Lu2 Lu4 Lu8 82.0(9) . 6_565 ?
Lu4 Lu4 Lu8 93.0(3) 6_565 6_565 ?
Lu9 Lu4 Lu8 78.4(8) . 6_565 ?
Lu9 Lu4 Lu8 88.2(4) 6_565 6_565 ?
N1 Lu4 Lu8 45.8(3) . 6_565 ?
Lu12 Lu4 Lu8 74.0(4) 6_565 6_565 ?
Lu13 Lu4 Lu8 17.2(5) . 6_565 ?
Lu10 Lu4 Lu8 73.4(4) 6_565 6_565 ?
Lu2 Lu4 Lu10 79.5(12) . . ?
Lu4 Lu4 Lu10 61.1(6) 6_565 . ?
Lu9 Lu4 Lu10 89.5(14) . . ?
Lu9 Lu4 Lu10 46.1(10) 6_565 . ?
N1 Lu4 Lu10 32.2(4) . . ?
Lu12 Lu4 Lu10 71.4(7) 6_565 . ?
Lu13 Lu4 Lu10 78.7(8) . . ?
Lu10 Lu4 Lu10 38.0(12) 6_565 . ?
Lu8 Lu4 Lu10 77.2(4) 6_565 . ?
Lu2 Lu4 Lu12 52.3(10) . . ?
Lu4 Lu4 Lu12 33.02(17) 6_565 . ?
Lu9 Lu4 Lu12 117.7(12) . . ?
Lu9 Lu4 Lu12 18.0(8) 6_565 . ?
N1 Lu4 Lu12 48.18(19) . . ?
Lu12 Lu4 Lu12 99.5(4) 6_565 . ?
Lu13 Lu4 Lu12 75.3(4) . . ?
Lu10 Lu4 Lu12 66.1(6) 6_565 . ?
Lu8 Lu4 Lu12 82.3(3) 6_565 . ?
Lu10 Lu4 Lu12 28.2(6) . . ?
Lu2 Lu4 Lu8 58.3(7) . . ?
Lu4 Lu4 Lu8 67.3(2) 6_565 . ?
Lu9 Lu4 Lu8 101.1(7) . . ?
Lu9 Lu4 Lu8 63.3(5) 6_565 . ?
N1 Lu4 Lu8 41.6(3) . . ?
Lu12 Lu4 Lu8 92.2(3) 6_565 . ?
Lu13 Lu4 Lu8 14.6(5) . . ?
Lu10 Lu4 Lu8 78.7(4) 6_565 . ?
Lu8 Lu4 Lu8 25.7(5) 6_565 . ?
Lu10 Lu4 Lu8 65.6(4) . . ?
Lu12 Lu4 Lu8 60.8(3) . . ?
Lu11 Lu5 Lu10 89(3) . . ?
Lu11 Lu5 Lu3 158(2) . 6_565 ?
Lu10 Lu5 Lu3 104(2) . 6_565 ?
Lu11 Lu5 Lu12 37(2) . . ?
Lu10 Lu5 Lu12 53(2) . . ?
Lu3 Lu5 Lu12 149.0(4) 6_565 . ?
Lu11 Lu5 Lu3 162(2) . . ?
Lu10 Lu5 Lu3 76(2) . . ?
Lu3 Lu5 Lu3 28.58(19) 6_565 . ?
Lu12 Lu5 Lu3 127.0(3) . . ?
Lu11 Lu5 N1 100(2) . . ?
Lu10 Lu5 N1 37.6(11) . . ?
Lu3 Lu5 N1 81.2(3) 6_565 . ?
Lu12 Lu5 N1 68.1(3) . . ?
Lu3 Lu5 N1 62.03(16) . . ?
Lu11 Lu5 Lu10 134(3) . 6_565 ?
Lu10 Lu5 Lu10 45(2) . 6_565 ?
Lu3 Lu5 Lu10 60.5(7) 6_565 6_565 ?
Lu12 Lu5 Lu10 96.6(7) . 6_565 ?
Lu3 Lu5 Lu10 32.2(7) . 6_565 ?
N1 Lu5 Lu10 42.3(6) . 6_565 ?
Lu11 Lu5 Lu5 150(2) . 6_565 ?
Lu10 Lu5 Lu5 62(2) . 6_565 ?
Lu3 Lu5 Lu5 44.0(2) 6_565 6_565 ?
Lu12 Lu5 Lu5 113.4(3) . 6_565 ?
Lu3 Lu5 Lu5 15.44(7) . 6_565 ?
N1 Lu5 Lu5 53.40(15) . 6_565 ?
Lu10 Lu5 Lu5 17.0(7) 6_565 6_565 ?
Lu11 Lu5 Lu9 57(3) . 6_565 ?
Lu10 Lu5 Lu9 33(3) . 6_565 ?
Lu3 Lu5 Lu9 131.4(7) 6_565 6_565 ?
Lu12 Lu5 Lu9 20.4(7) . 6_565 ?
Lu3 Lu5 Lu9 106.9(6) . 6_565 ?
N1 Lu5 Lu9 50.9(6) . 6_565 ?
Lu10 Lu5 Lu9 76.2(9) 6_565 6_565 ?
Lu5 Lu5 Lu9 93.0(6) 6_565 6_565 ?
Lu11 Lu5 Lu1 84(2) . . ?
Lu10 Lu5 Lu1 77.8(12) . . ?
Lu3 Lu5 Lu1 82.3(2) 6_565 . ?
Lu12 Lu5 Lu1 73.3(2) . . ?
Lu3 Lu5 Lu1 83.34(13) . . ?
N1 Lu5 Lu1 44.80(18) . . ?
Lu10 Lu5 Lu1 81.7(5) 6_565 . ?
Lu5 Lu5 Lu1 84.61(11) 6_565 . ?
Lu9 Lu5 Lu1 69.9(4) 6_565 . ?
Lu11 Lu5 Lu6 77(2) . . ?
Lu10 Lu5 Lu6 72.6(14) . . ?
Lu3 Lu5 Lu6 90.5(2) 6_565 . ?
Lu12 Lu5 Lu6 64.6(2) . . ?
Lu3 Lu5 Lu6 89.01(14) . . ?
N1 Lu5 Lu6 42.97(18) . . ?
Lu10 Lu5 Lu6 82.9(5) 6_565 . ?
Lu5 Lu5 Lu6 88.29(13) 6_565 . ?
Lu9 Lu5 Lu6 61.7(4) 6_565 . ?
Lu1 Lu5 Lu6 8.77(9) . . ?
Lu11 Lu5 Lu11 146(3) . 6_565 ?
Lu10 Lu5 Lu11 57(3) . 6_565 ?
Lu3 Lu5 Lu11 48.3(4) 6_565 6_565 ?
Lu12 Lu5 Lu11 108.6(6) . 6_565 ?
Lu3 Lu5 Lu11 19.8(4) . 6_565 ?
N1 Lu5 Lu11 49.4(5) . 6_565 ?
Lu10 Lu5 Lu11 12.4(8) 6_565 6_565 ?
Lu5 Lu5 Lu11 4.8(4) 6_565 6_565 ?
Lu9 Lu5 Lu11 88.2(8) 6_565 6_565 ?
Lu1 Lu5 Lu11 82.8(4) . 6_565 ?
Lu6 Lu5 Lu11 85.8(4) . 6_565 ?
Lu8 Lu6 Lu7 83.5(10) . . ?
Lu8 Lu6 Lu13 10.1(11) . . ?
Lu7 Lu6 Lu13 74.6(12) . . ?
Lu8 Lu6 Lu8 32.8(8) . 6_565 ?
Lu7 Lu6 Lu8 51.1(9) . 6_565 ?
Lu13 Lu6 Lu8 23.5(10) . 6_565 ?
Lu8 Lu6 N1 71.2(6) . . ?
Lu7 Lu6 N1 67.6(6) . . ?
Lu13 Lu6 N1 63.6(7) . . ?
Lu8 Lu6 N1 57.8(3) 6_565 . ?
Lu8 Lu6 Lu1 70.5(7) . 6_565 ?
Lu7 Lu6 Lu1 15.7(7) . 6_565 ?
Lu13 Lu6 Lu1 61.0(8) . 6_565 ?
Lu8 Lu6 Lu1 37.6(4) 6_565 6_565 ?
N1 Lu6 Lu1 55.8(2) . 6_565 ?
Lu8 Lu6 Lu6 59.2(6) . 6_565 ?
Lu7 Lu6 Lu6 25.7(8) . 6_565 ?
Lu13 Lu6 Lu6 49.7(8) . 6_565 ?
Lu8 Lu6 Lu6 26.4(4) 6_565 6_565 ?
N1 Lu6 Lu6 54.53(19) . 6_565 ?
Lu1 Lu6 Lu6 11.26(12) 6_565 6_565 ?
Lu8 Lu6 Lu12 93.0(6) . . ?
Lu7 Lu6 Lu12 116.9(7) . . ?
Lu13 Lu6 Lu12 92.7(9) . . ?
Lu8 Lu6 Lu12 102.0(4) 6_565 . ?
N1 Lu6 Lu12 52.3(2) . . ?
Lu1 Lu6 Lu12 107.6(3) 6_565 . ?
Lu6 Lu6 Lu12 106.66(19) 6_565 . ?
Lu8 Lu6 Lu10 98.3(7) . . ?
Lu7 Lu6 Lu10 88.6(9) . . ?
Lu13 Lu6 Lu10 93.1(9) . . ?
Lu8 Lu6 Lu10 90.8(4) 6_565 . ?
N1 Lu6 Lu10 33.1(4) . . ?
Lu1 Lu6 Lu10 82.1(5) 6_565 . ?
Lu6 Lu6 Lu10 84.5(4) 6_565 . ?
Lu12 Lu6 Lu10 29.5(6) . . ?
Lu8 Lu6 Lu11 113.8(7) . . ?
Lu7 Lu6 Lu11 99.3(9) . . ?
Lu13 Lu6 Lu11 109.9(9) . . ?
Lu8 Lu6 Lu11 108.9(4) 6_565 . ?
N1 Lu6 Lu11 51.1(3) . . ?
Lu1 Lu6 Lu11 96.2(3) 6_565 . ?
Lu6 Lu6 Lu11 100.5(3) 6_565 . ?
Lu12 Lu6 Lu11 28.1(5) . . ?
Lu10 Lu6 Lu11 18.1(3) . . ?
Lu8 Lu6 Lu9 68.4(10) . 6_565 ?
Lu7 Lu6 Lu9 113.7(7) . 6_565 ?
Lu13 Lu6 Lu9 68.9(12) . 6_565 ?
Lu8 Lu6 Lu9 82.0(8) 6_565 6_565 ?
N1 Lu6 Lu9 47.0(4) . 6_565 ?
Lu1 Lu6 Lu9 99.8(5) 6_565 6_565 ?
Lu6 Lu6 Lu9 94.5(6) 6_565 6_565 ?
Lu12 Lu6 Lu9 24.6(8) . 6_565 ?
Lu10 Lu6 Lu9 42.7(9) . 6_565 ?
Lu11 Lu6 Lu9 49.9(9) . 6_565 ?
Lu8 Lu6 Lu5 113.0(6) . . ?
Lu7 Lu6 Lu5 89.6(8) . . ?
Lu13 Lu6 Lu5 107.5(8) . . ?
Lu8 Lu6 Lu5 102.8(3) 6_565 . ?
N1 Lu6 Lu5 45.50(18) . . ?
Lu1 Lu6 Lu5 86.8(2) 6_565 . ?
Lu6 Lu6 Lu5 91.71(13) 6_565 . ?
Lu12 Lu6 Lu5 35.33(18) . . ?
Lu10 Lu6 Lu5 14.7(5) . . ?
Lu11 Lu6 Lu5 9.8(3) . . ?
Lu9 Lu6 Lu5 54.4(7) 6_565 . ?
Lu1 Lu7 Lu1 154.5(14) 6_565 . ?
Lu1 Lu7 Lu6 18.6(5) 6_565 6_565 ?
Lu1 Lu7 Lu6 144.1(16) . 6_565 ?
Lu1 Lu7 Lu6 144.1(16) 6_565 . ?
Lu1 Lu7 Lu6 18.6(5) . . ?
Lu6 Lu7 Lu6 128.6(15) 6_565 . ?
Lu1 Lu7 Lu8 59.7(10) 6_565 6_565 ?
Lu1 Lu7 Lu8 106.6(15) . 6_565 ?
Lu6 Lu7 Lu8 41.3(7) 6_565 6_565 ?
Lu6 Lu7 Lu8 88.8(12) . 6_565 ?
Lu1 Lu7 Lu8 106.6(15) 6_565 . ?
Lu1 Lu7 Lu8 59.7(10) . . ?
Lu6 Lu7 Lu8 88.8(12) 6_565 . ?
Lu6 Lu7 Lu8 41.3(7) . . ?
Lu8 Lu7 Lu8 47.8(12) 6_565 . ?
Lu1 Lu7 Lu13 82.9(12) 6_565 . ?
Lu1 Lu7 Lu13 82.9(12) . . ?
Lu6 Lu7 Lu13 64.9(8) 6_565 . ?
Lu6 Lu7 Lu13 64.9(8) . . ?
Lu8 Lu7 Lu13 23.9(6) 6_565 . ?
Lu8 Lu7 Lu13 23.9(6) . . ?
Lu1 Lu7 N1 77.4(7) 6_565 . ?
Lu1 Lu7 N1 77.4(7) . . ?
Lu6 Lu7 N1 74.2(6) 6_565 . ?
Lu6 Lu7 N1 74.2(6) . . ?
Lu8 Lu7 N1 66.5(6) 6_565 . ?
Lu8 Lu7 N1 66.5(6) . . ?
Lu13 Lu7 N1 63.1(9) . . ?
Lu1 Lu7 Lu3 95.1(10) 6_565 6_565 ?
Lu1 Lu7 Lu3 68.7(9) . 6_565 ?
Lu6 Lu7 Lu3 103.8(8) 6_565 6_565 ?
Lu6 Lu7 Lu3 79.7(7) . 6_565 ?
Lu8 Lu7 Lu3 111.0(7) 6_565 6_565 ?
Lu8 Lu7 Lu3 99.8(6) . 6_565 ?
Lu13 Lu7 Lu3 105.8(9) . 6_565 ?
N1 Lu7 Lu3 44.8(4) . 6_565 ?
Lu1 Lu7 Lu3 68.7(9) 6_565 . ?
Lu1 Lu7 Lu3 95.1(10) . . ?
Lu6 Lu7 Lu3 79.7(7) 6_565 . ?
Lu6 Lu7 Lu3 103.8(8) . . ?
Lu8 Lu7 Lu3 99.8(6) 6_565 . ?
Lu8 Lu7 Lu3 111.0(7) . . ?
Lu13 Lu7 Lu3 105.8(9) . . ?
N1 Lu7 Lu3 44.8(4) . . ?
Lu3 Lu7 Lu3 26.79(18) 6_565 . ?
Lu1 Lu7 Lu10 95.6(9) 6_565 . ?
Lu1 Lu7 Lu10 61.8(8) . . ?
Lu6 Lu7 Lu10 97.3(7) 6_565 . ?
Lu6 Lu7 Lu10 66.5(8) . . ?
Lu8 Lu7 Lu10 91.5(8) 6_565 . ?
Lu8 Lu7 Lu10 77.8(9) . . ?
Lu13 Lu7 Lu10 83.2(10) . . ?
N1 Lu7 Lu10 25.8(5) . . ?
Lu3 Lu7 Lu10 22.8(6) 6_565 . ?
Lu3 Lu7 Lu10 38.1(7) . . ?
Lu1 Lu7 Lu10 61.8(8) 6_565 6_565 ?
Lu1 Lu7 Lu10 95.6(9) . 6_565 ?
Lu6 Lu7 Lu10 66.5(8) 6_565 6_565 ?
Lu6 Lu7 Lu10 97.3(7) . 6_565 ?
Lu8 Lu7 Lu10 77.8(9) 6_565 6_565 ?
Lu8 Lu7 Lu10 91.5(8) . 6_565 ?
Lu13 Lu7 Lu10 83.2(10) . 6_565 ?
N1 Lu7 Lu10 25.8(5) . 6_565 ?
Lu3 Lu7 Lu10 38.1(7) 6_565 6_565 ?
Lu3 Lu7 Lu10 22.8(6) . 6_565 ?
Lu10 Lu7 Lu10 34.0(8) . 6_565 ?
Lu13 Lu8 Lu6 157(3) . . ?
Lu13 Lu8 Lu8 38(3) . 6_565 ?
Lu6 Lu8 Lu8 120.8(6) . 6_565 ?
Lu13 Lu8 Lu1 142(3) . . ?
Lu6 Lu8 Lu1 15.7(4) . . ?
Lu8 Lu8 Lu1 105.1(5) 6_565 . ?
Lu13 Lu8 Lu7 104(3) . . ?
Lu6 Lu8 Lu7 55.2(7) . . ?
Lu8 Lu8 Lu7 66.1(6) 6_565 . ?
Lu1 Lu8 Lu7 39.8(5) . . ?
Lu13 Lu8 N1 84(2) . . ?
Lu6 Lu8 N1 78.4(6) . . ?
Lu8 Lu8 N1 70.9(4) 6_565 . ?
Lu1 Lu8 N1 70.9(5) . . ?
Lu7 Lu8 N1 65.8(6) . . ?
Lu13 Lu8 Lu6 64(3) . 6_565 ?
Lu6 Lu8 Lu6 94.4(8) . 6_565 ?
Lu8 Lu8 Lu6 26.4(4) 6_565 6_565 ?
Lu1 Lu8 Lu6 78.7(6) . 6_565 ?
Lu7 Lu8 Lu6 40.1(4) . 6_565 ?
N1 Lu8 Lu6 61.1(3) . 6_565 ?
Lu13 Lu8 Lu1 76(3) . 6_565 ?
Lu6 Lu8 Lu1 81.6(7) . 6_565 ?
Lu8 Lu8 Lu1 39.1(4) 6_565 6_565 ?
Lu1 Lu8 Lu1 66.0(5) . 6_565 ?
Lu7 Lu8 Lu1 27.7(4) . 6_565 ?
N1 Lu8 Lu1 58.4(3) . 6_565 ?
Lu6 Lu8 Lu1 12.75(13) 6_565 6_565 ?
Lu13 Lu8 Lu2 56(2) . . ?
Lu6 Lu8 Lu2 119.0(7) . . ?
Lu8 Lu8 Lu2 76.3(3) 6_565 . ?
Lu1 Lu8 Lu2 118.1(5) . . ?
Lu7 Lu8 Lu2 113.6(6) . . ?
N1 Lu8 Lu2 50.7(3) . . ?
Lu6 Lu8 Lu2 88.6(4) 6_565 . ?
Lu1 Lu8 Lu2 94.8(4) 6_565 . ?
Lu13 Lu8 Lu9 90(3) . 6_565 ?
Lu6 Lu8 Lu9 90.5(11) . 6_565 ?
Lu8 Lu8 Lu9 106.5(6) 6_565 6_565 ?
Lu1 Lu8 Lu9 95.7(10) . 6_565 ?
Lu7 Lu8 Lu9 113.5(9) . 6_565 ?
N1 Lu8 Lu9 51.3(5) . 6_565 ?
Lu6 Lu8 Lu9 109.4(5) 6_565 6_565 ?
Lu1 Lu8 Lu9 109.4(5) 6_565 6_565 ?
Lu2 Lu8 Lu9 33.6(8) . 6_565 ?
Lu13 Lu8 Lu4 68(2) . 6_565 ?
Lu6 Lu8 Lu4 109.9(7) . 6_565 ?
Lu8 Lu8 Lu4 87.0(3) 6_565 6_565 ?
Lu1 Lu8 Lu4 111.5(5) . 6_565 ?
Lu7 Lu8 Lu4 115.5(6) . 6_565 ?
N1 Lu8 Lu4 49.9(3) . 6_565 ?
Lu6 Lu8 Lu4 96.6(4) 6_565 6_565 ?
Lu1 Lu8 Lu4 101.0(4) 6_565 6_565 ?
Lu2 Lu8 Lu4 11.54(6) . 6_565 ?
Lu9 Lu8 Lu4 22.2(8) 6_565 6_565 ?
Lu13 Lu8 Lu4 52(2) . . ?
Lu6 Lu8 Lu4 119.2(6) . . ?
Lu8 Lu8 Lu4 67.3(2) 6_565 . ?
Lu1 Lu8 Lu4 115.3(5) . . ?
Lu7 Lu8 Lu4 105.1(6) . . ?
N1 Lu8 Lu4 45.2(3) . . ?
Lu6 Lu8 Lu4 78.7(4) 6_565 . ?
Lu1 Lu8 Lu4 85.1(3) 6_565 . ?
Lu2 Lu8 Lu4 9.89(8) . . ?
Lu9 Lu8 Lu4 40.6(7) 6_565 . ?
Lu4 Lu8 Lu4 19.7(2) 6_565 . ?
Lu4 Lu9 Lu12 146.2(15) . 6_565 ?
Lu4 Lu9 Lu2 7.1(3) . . ?
Lu12 Lu9 Lu2 141.7(12) 6_565 . ?
Lu4 Lu9 Lu4 14.3(5) . 6_565 ?
Lu12 Lu9 Lu4 131.9(11) 6_565 6_565 ?
Lu2 Lu9 Lu4 11.8(3) . 6_565 ?
Lu4 Lu9 Lu10 105.4(11) . 6_565 ?
Lu12 Lu9 Lu10 41.0(9) 6_565 6_565 ?
Lu2 Lu9 Lu10 101.6(9) . 6_565 ?
Lu4 Lu9 Lu10 91.1(8) 6_565 6_565 ?
Lu4 Lu9 N1 73.6(8) . . ?
Lu12 Lu9 N1 76.1(9) 6_565 . ?
Lu2 Lu9 N1 67.3(7) . . ?
Lu4 Lu9 N1 61.1(6) 6_565 . ?
Lu10 Lu9 N1 44.2(6) 6_565 . ?
Lu4 Lu9 Lu11 126.3(12) . 6_565 ?
Lu12 Lu9 Lu11 20.0(6) 6_565 6_565 ?
Lu2 Lu9 Lu11 122.0(8) . 6_565 ?
Lu4 Lu9 Lu11 112.0(7) 6_565 6_565 ?
Lu10 Lu9 Lu11 21.1(7) 6_565 6_565 ?
N1 Lu9 Lu11 58.8(7) . 6_565 ?
Lu4 Lu9 Lu5 116.3(10) . 6_565 ?
Lu12 Lu9 Lu5 30.0(6) 6_565 6_565 ?
Lu2 Lu9 Lu5 112.1(7) . 6_565 ?
Lu4 Lu9 Lu5 102.0(6) 6_565 6_565 ?
Lu10 Lu9 Lu5 11.3(6) 6_565 6_565 ?
N1 Lu9 Lu5 50.6(6) . 6_565 ?
Lu11 Lu9 Lu5 10.0(3) 6_565 6_565 ?
Lu4 Lu9 Lu8 79.4(12) . 6_565 ?
Lu12 Lu9 Lu8 90.0(8) 6_565 6_565 ?
Lu2 Lu9 Lu8 72.7(10) . 6_565 ?
Lu4 Lu9 Lu8 76.1(9) 6_565 6_565 ?
Lu10 Lu9 Lu8 81.4(6) 6_565 6_565 ?
N1 Lu9 Lu8 45.8(4) . 6_565 ?
Lu11 Lu9 Lu8 84.0(8) 6_565 6_565 ?
Lu5 Lu9 Lu8 81.3(6) 6_565 6_565 ?
Lu4 Lu9 Lu9 29.3(12) . 6_565 ?
Lu12 Lu9 Lu9 116.9(9) 6_565 6_565 ?
Lu2 Lu9 Lu9 26.0(9) . 6_565 ?
Lu4 Lu9 Lu9 15.0(8) 6_565 6_565 ?
Lu10 Lu9 Lu9 76.1(11) 6_565 6_565 ?
N1 Lu9 Lu9 48.7(9) . 6_565 ?
Lu11 Lu9 Lu9 96.9(6) 6_565 6_565 ?
Lu5 Lu9 Lu9 87.0(6) 6_565 6_565 ?
Lu8 Lu9 Lu9 73.6(6) 6_565 6_565 ?
Lu4 Lu9 Lu13 62.9(12) . . ?
Lu12 Lu9 Lu13 104.7(11) 6_565 . ?
Lu2 Lu9 Lu13 56.3(10) . . ?
Lu4 Lu9 Lu13 60.5(8) 6_565 . ?
Lu10 Lu9 Lu13 87.9(9) 6_565 . ?
N1 Lu9 Lu13 45.9(8) . . ?
Lu11 Lu9 Lu13 95.5(10) 6_565 . ?
Lu5 Lu9 Lu13 90.7(9) 6_565 . ?
Lu8 Lu9 Lu13 16.6(6) 6_565 . ?
Lu9 Lu9 Lu13 60.1(5) 6_565 . ?
Lu4 Lu9 Lu6 98.1(10) . 6_565 ?
Lu12 Lu9 Lu6 69.0(7) 6_565 6_565 ?
Lu2 Lu9 Lu6 91.1(8) . 6_565 ?
Lu4 Lu9 Lu6 92.0(7) 6_565 6_565 ?
Lu10 Lu9 Lu6 66.8(6) 6_565 6_565 ?
N1 Lu9 Lu6 44.1(3) . 6_565 ?
Lu11 Lu9 Lu6 64.8(7) 6_565 6_565 ?
Lu5 Lu9 Lu6 63.9(5) 6_565 6_565 ?
Lu8 Lu9 Lu6 21.1(4) 6_565 6_565 ?
Lu9 Lu9 Lu6 85.5(6) 6_565 6_565 ?
Lu13 Lu9 Lu6 36.9(7) . 6_565 ?
Lu5 Lu10 Lu11 34.0(13) . . ?
Lu5 Lu10 Lu3 38.7(18) . 6_565 ?
Lu11 Lu10 Lu3 72(2) . 6_565 ?
Lu5 Lu10 Lu12 102(2) . . ?
Lu11 Lu10 Lu12 68(3) . . ?
Lu3 Lu10 Lu12 136.7(13) 6_565 . ?
Lu5 Lu10 N1 125.5(17) . . ?
Lu11 Lu10 N1 129(2) . . ?
Lu3 Lu10 N1 99.0(13) 6_565 . ?
Lu12 Lu10 N1 93.0(18) . . ?
Lu5 Lu10 Lu10 118(2) . 6_565 ?
Lu11 Lu10 Lu10 152(3) . 6_565 ?
Lu3 Lu10 Lu10 80.4(9) 6_565 6_565 ?
Lu12 Lu10 Lu10 137.9(9) . 6_565 ?
N1 Lu10 Lu10 55.3(10) . 6_565 ?
Lu5 Lu10 Lu3 82(3) . . ?
Lu11 Lu10 Lu3 115(3) . . ?
Lu3 Lu10 Lu3 43.8(10) 6_565 . ?
Lu12 Lu10 Lu3 163.8(12) . . ?
N1 Lu10 Lu3 72.3(9) . . ?
Lu10 Lu10 Lu3 36.7(6) 6_565 . ?
Lu5 Lu10 Lu9 136(3) . 6_565 ?
Lu11 Lu10 Lu9 102(3) . 6_565 ?
Lu3 Lu10 Lu9 159.9(13) 6_565 6_565 ?
Lu12 Lu10 Lu9 34.1(12) . 6_565 ?
N1 Lu10 Lu9 69.2(14) . 6_565 ?
Lu10 Lu10 Lu9 103.9(11) 6_565 6_565 ?
Lu3 Lu10 Lu9 137.5(13) . 6_565 ?
Lu5 Lu10 Lu5 101(3) . 6_565 ?
Lu11 Lu10 Lu5 135(3) . 6_565 ?
Lu3 Lu10 Lu5 63.5(13) 6_565 6_565 ?
Lu12 Lu10 Lu5 153.8(16) . 6_565 ?
N1 Lu10 Lu5 63.9(8) . 6_565 ?
Lu10 Lu10 Lu5 17.0(7) 6_565 6_565 ?
Lu3 Lu10 Lu5 19.9(3) . 6_565 ?
Lu9 Lu10 Lu5 120.5(13) 6_565 6_565 ?
Lu5 Lu10 Lu4 158(3) . 6_565 ?
Lu11 Lu10 Lu4 125(3) . 6_565 ?
Lu3 Lu10 Lu4 153.0(11) 6_565 6_565 ?
Lu12 Lu10 Lu4 57.1(11) . 6_565 ?
N1 Lu10 Lu4 54.2(9) . 6_565 ?
Lu10 Lu10 Lu4 80.9(6) 6_565 6_565 ?
Lu3 Lu10 Lu4 115.4(7) . 6_565 ?
Lu9 Lu10 Lu4 23.0(10) 6_565 6_565 ?
Lu5 Lu10 Lu4 97.6(6) 6_565 6_565 ?
Lu5 Lu10 Lu11 109(3) . 6_565 ?
Lu11 Lu10 Lu11 143(4) . 6_565 ?
Lu3 Lu10 Lu11 71.2(15) 6_565 6_565 ?
Lu12 Lu10 Lu11 146.1(16) . 6_565 ?
N1 Lu10 Lu11 58.7(8) . 6_565 ?
Lu10 Lu10 Lu11 9.2(8) 6_565 6_565 ?
Lu3 Lu10 Lu11 27.5(6) . 6_565 ?
Lu9 Lu10 Lu11 112.5(13) 6_565 6_565 ?
Lu5 Lu10 Lu11 8.0(5) 6_565 6_565 ?
Lu4 Lu10 Lu11 89.6(7) 6_565 6_565 ?
Lu5 Lu10 Lu1 86.6(11) . . ?
Lu11 Lu10 Lu1 83.7(16) . . ?
Lu3 Lu10 Lu1 80.3(7) 6_565 . ?
Lu12 Lu10 Lu1 79.2(10) . . ?
N1 Lu10 Lu1 45.2(4) . . ?
Lu10 Lu10 Lu1 92.0(5) 6_565 . ?
Lu3 Lu10 Lu1 85.6(6) . . ?
Lu9 Lu10 Lu1 79.9(9) 6_565 . ?
Lu5 Lu10 Lu1 91.1(6) 6_565 . ?
Lu4 Lu10 Lu1 81.1(7) 6_565 . ?
Lu11 Lu10 Lu1 90.4(7) 6_565 . ?
Lu5 Lu11 Lu10 57(3) . . ?
Lu5 Lu11 Lu3 13.3(15) . 6_565 ?
Lu10 Lu11 Lu3 66(3) . 6_565 ?
Lu5 Lu11 Lu12 130(3) . . ?
Lu10 Lu11 Lu12 74(3) . . ?
Lu3 Lu11 Lu12 136.0(14) 6_565 . ?
Lu5 Lu11 N1 67(2) . . ?
Lu10 Lu11 N1 33.2(15) . . ?
Lu3 Lu11 N1 68.1(7) 6_565 . ?
Lu12 Lu11 N1 68.8(8) . . ?
Lu5 Lu11 Lu9 113(3) . 6_565 ?
Lu10 Lu11 Lu9 56(3) . 6_565 ?
Lu3 Lu11 Lu9 119.0(12) 6_565 6_565 ?
Lu12 Lu11 Lu9 17.6(7) . 6_565 ?
N1 Lu11 Lu9 53.5(8) . 6_565 ?
Lu5 Lu11 Lu3 14.1(19) . . ?
Lu10 Lu11 Lu3 46(3) . . ?
Lu3 Lu11 Lu3 19.9(4) 6_565 . ?
Lu12 Lu11 Lu3 117.6(9) . . ?
N1 Lu11 Lu3 52.8(3) . . ?
Lu9 Lu11 Lu3 100.1(8) 6_565 . ?
Lu5 Lu11 Lu10 39(2) . 6_565 ?
Lu10 Lu11 Lu10 19(2) . 6_565 ?
Lu3 Lu11 Lu10 46.9(9) 6_565 6_565 ?
Lu12 Lu11 Lu10 91.8(10) . 6_565 ?
N1 Lu11 Lu10 36.8(6) . 6_565 ?
Lu9 Lu11 Lu10 74.2(10) 6_565 6_565 ?
Lu3 Lu11 Lu10 27.0(7) . 6_565 ?
Lu5 Lu11 Lu1 86(2) . . ?
Lu10 Lu11 Lu1 77.6(16) . . ?
Lu3 Lu11 Lu1 77.6(8) 6_565 . ?
Lu12 Lu11 Lu1 77.9(8) . . ?
N1 Lu11 Lu1 44.6(4) . . ?
Lu9 Lu11 Lu1 73.4(7) 6_565 . ?
Lu3 Lu11 Lu1 75.7(4) . . ?
Lu10 Lu11 Lu1 75.8(6) 6_565 . ?
Lu5 Lu11 Lu6 93(2) . . ?
Lu10 Lu11 Lu6 77.2(18) . . ?
Lu3 Lu11 Lu6 85.9(8) 6_565 . ?
Lu12 Lu11 Lu6 68.9(8) . . ?
N1 Lu11 Lu6 44.1(4) . . ?
Lu9 Lu11 Lu6 65.3(7) 6_565 . ?
Lu3 Lu11 Lu6 82.1(4) . . ?
Lu10 Lu11 Lu6 78.4(6) 6_565 . ?
Lu1 Lu11 Lu6 9.23(10) . . ?
Lu5 Lu11 Lu5 25(2) . 6_565 ?
Lu10 Lu11 Lu5 32(3) . 6_565 ?
Lu3 Lu11 Lu5 33.2(5) 6_565 6_565 ?
Lu12 Lu11 Lu5 105.4(9) . 6_565 ?
N1 Lu11 Lu5 45.2(3) . 6_565 ?
Lu9 Lu11 Lu5 87.9(8) 6_565 6_565 ?
Lu3 Lu11 Lu5 13.36(9) . 6_565 ?
Lu10 Lu11 Lu5 13.9(7) 6_565 6_565 ?
Lu1 Lu11 Lu5 77.0(4) . 6_565 ?
Lu6 Lu11 Lu5 81.7(4) . 6_565 ?
Lu5 Lu11 Lu4 97(2) . 6_565 ?
Lu10 Lu11 Lu4 41(3) . 6_565 ?
Lu3 Lu11 Lu4 103.9(9) 6_565 6_565 ?
Lu12 Lu11 Lu4 32.9(5) . 6_565 ?
N1 Lu11 Lu4 40.9(4) . 6_565 ?
Lu9 Lu11 Lu4 15.3(6) 6_565 6_565 ?
Lu3 Lu11 Lu4 84.8(5) . 6_565 ?
Lu10 Lu11 Lu4 58.9(7) 6_565 6_565 ?
Lu1 Lu11 Lu4 70.5(5) . 6_565 ?
Lu6 Lu11 Lu4 63.9(4) . 6_565 ?
Lu5 Lu11 Lu4 72.5(4) 6_565 6_565 ?
Lu9 Lu12 Lu11 142.5(11) 6_565 . ?
Lu9 Lu12 Lu10 104.9(12) 6_565 . ?
Lu11 Lu12 Lu10 37.7(8) . . ?
Lu9 Lu12 Lu5 129.7(10) 6_565 . ?
Lu11 Lu12 Lu5 12.8(5) . . ?
Lu10 Lu12 Lu5 25.1(8) . . ?
Lu9 Lu12 Lu4 15.6(8) 6_565 6_565 ?
Lu11 Lu12 Lu4 126.9(7) . 6_565 ?
Lu10 Lu12 Lu4 89.4(9) . 6_565 ?
Lu5 Lu12 Lu4 114.1(4) . 6_565 ?
Lu9 Lu12 N1 71.2(9) 6_565 . ?
Lu11 Lu12 N1 75.3(6) . . ?
Lu10 Lu12 N1 46.6(8) . . ?
Lu5 Lu12 N1 64.2(3) . . ?
Lu4 Lu12 N1 57.5(2) 6_565 . ?
Lu9 Lu12 Lu3 122.0(9) 6_565 6_565 ?
Lu11 Lu12 Lu3 21.0(6) . 6_565 ?
Lu10 Lu12 Lu3 19.9(7) . 6_565 ?
Lu5 Lu12 Lu3 9.46(12) . 6_565 ?
Lu4 Lu12 Lu3 106.5(3) 6_565 6_565 ?
N1 Lu12 Lu3 54.8(2) . 6_565 ?
Lu9 Lu12 Lu2 21.6(8) 6_565 . ?
Lu11 Lu12 Lu2 121.1(7) . . ?
Lu10 Lu12 Lu2 84.0(9) . . ?
Lu5 Lu12 Lu2 108.4(4) . . ?
Lu4 Lu12 Lu2 6.75(14) 6_565 . ?
N1 Lu12 Lu2 50.7(2) . . ?
Lu3 Lu12 Lu2 100.4(3) 6_565 . ?
Lu9 Lu12 Lu6 86.4(9) 6_565 . ?
Lu11 Lu12 Lu6 83.1(7) . . ?
Lu10 Lu12 Lu6 79.7(7) . . ?
Lu5 Lu12 Lu6 80.1(3) . . ?
Lu4 Lu12 Lu6 81.9(2) 6_565 . ?
N1 Lu12 Lu6 47.2(2) . . ?
Lu3 Lu12 Lu6 72.9(2) 6_565 . ?
Lu2 Lu12 Lu6 77.0(2) . . ?
Lu9 Lu12 Lu1 92.7(9) 6_565 . ?
Lu11 Lu12 Lu1 74.0(7) . . ?
Lu10 Lu12 Lu1 71.6(6) . . ?
Lu5 Lu12 Lu1 70.9(2) . . ?
Lu4 Lu12 Lu1 86.3(2) 6_565 . ?
N1 Lu12 Lu1 44.0(2) . . ?
Lu3 Lu12 Lu1 63.77(18) 6_565 . ?
Lu2 Lu12 Lu1 80.8(2) . . ?
Lu6 Lu12 Lu1 9.19(8) . . ?
Lu9 Lu12 Lu4 30.1(8) 6_565 . ?
Lu11 Lu12 Lu4 112.4(6) . . ?
Lu10 Lu12 Lu4 75.0(9) . . ?
Lu5 Lu12 Lu4 99.6(3) . . ?
Lu4 Lu12 Lu4 14.52(15) 6_565 . ?
N1 Lu12 Lu4 45.5(2) . . ?
Lu3 Lu12 Lu4 92.0(2) 6_565 . ?
Lu2 Lu12 Lu4 9.43(13) . . ?
Lu6 Lu12 Lu4 78.4(2) . . ?
Lu1 Lu12 Lu4 80.7(2) . . ?
Lu9 Lu12 Lu8 65.8(9) 6_565 . ?
Lu11 Lu12 Lu8 98.8(8) . . ?
Lu10 Lu12 Lu8 84.5(7) . . ?
Lu5 Lu12 Lu8 92.8(4) . . ?
Lu4 Lu12 Lu8 61.6(3) 6_565 . ?
N1 Lu12 Lu8 41.2(3) . . ?
Lu3 Lu12 Lu8 84.1(3) 6_565 . ?
Lu2 Lu12 Lu8 57.2(3) . . ?
Lu6 Lu12 Lu8 20.6(3) . . ?
Lu1 Lu12 Lu8 27.3(3) . . ?
Lu4 Lu12 Lu8 59.9(3) . . ?
Lu8 Lu13 Lu8 105(6) . 6_565 ?
Lu8 Lu13 Lu6 93(4) . 6_565 ?
Lu8 Lu13 Lu6 13.2(18) 6_565 6_565 ?
Lu8 Lu13 Lu6 13.2(18) . . ?
Lu8 Lu13 Lu6 93(4) 6_565 . ?
Lu6 Lu13 Lu6 80.5(16) 6_565 . ?
Lu8 Lu13 Lu7 52(3) . . ?
Lu8 Lu13 Lu7 52(3) 6_565 . ?
Lu6 Lu13 Lu7 40.5(8) 6_565 . ?
Lu6 Lu13 Lu7 40.5(8) . . ?
Lu8 Lu13 N1 73(2) . . ?
Lu8 Lu13 N1 73(2) 6_565 . ?
Lu6 Lu13 N1 63.2(9) 6_565 . ?
Lu6 Lu13 N1 63.2(9) . . ?
Lu7 Lu13 N1 58.7(11) . . ?
Lu8 Lu13 Lu1 24(2) . . ?
Lu8 Lu13 Lu1 81(3) 6_565 . ?
Lu6 Lu13 Lu1 69.1(13) 6_565 . ?
Lu6 Lu13 Lu1 11.5(3) . . ?
Lu7 Lu13 Lu1 29.3(5) . . ?
N1 Lu13 Lu1 58.0(9) . . ?
Lu8 Lu13 Lu1 81(3) . 6_565 ?
Lu8 Lu13 Lu1 24(2) 6_565 6_565 ?
Lu6 Lu13 Lu1 11.5(3) 6_565 6_565 ?
Lu6 Lu13 Lu1 69.1(13) . 6_565 ?
Lu7 Lu13 Lu1 29.3(5) . 6_565 ?
N1 Lu13 Lu1 58.0(9) . 6_565 ?
Lu1 Lu13 Lu1 57.6(10) . 6_565 ?
Lu8 Lu13 Lu2 107(2) . . ?
Lu8 Lu13 Lu2 107(2) 6_565 . ?
Lu6 Lu13 Lu2 105.5(9) 6_565 . ?
Lu6 Lu13 Lu2 105.5(9) . . ?
Lu7 Lu13 Lu2 115.4(12) . . ?
N1 Lu13 Lu2 56.8(7) . . ?
Lu1 Lu13 Lu2 107.1(9) . . ?
Lu1 Lu13 Lu2 107.1(9) 6_565 . ?
Lu8 Lu13 Lu4 95(2) . 6_565 ?
Lu8 Lu13 Lu4 114(2) 6_565 6_565 ?
Lu6 Lu13 Lu4 109.6(10) 6_565 6_565 ?
Lu6 Lu13 Lu4 94.7(8) . 6_565 ?
Lu7 Lu13 Lu4 110.7(12) . 6_565 ?
N1 Lu13 Lu4 53.3(7) . 6_565 ?
Lu1 Lu13 Lu4 97.5(8) . 6_565 ?
Lu1 Lu13 Lu4 108.7(10) 6_565 6_565 ?
Lu2 Lu13 Lu4 12.15(15) . 6_565 ?
Lu8 Lu13 Lu4 114(2) . . ?
Lu8 Lu13 Lu4 95(2) 6_565 . ?
Lu6 Lu13 Lu4 94.7(8) 6_565 . ?
Lu6 Lu13 Lu4 109.6(10) . . ?
Lu7 Lu13 Lu4 110.7(12) . . ?
N1 Lu13 Lu4 53.3(7) . . ?
Lu1 Lu13 Lu4 108.7(10) . . ?
Lu1 Lu13 Lu4 97.5(8) 6_565 . ?
Lu2 Lu13 Lu4 12.15(15) . . ?
Lu4 Lu13 Lu4 22.7(4) 6_565 . ?
Lu8 Lu13 Lu9 120(2) . . ?
Lu8 Lu13 Lu9 74(2) 6_565 . ?
Lu6 Lu13 Lu9 74.2(10) 6_565 . ?
Lu6 Lu13 Lu9 111.8(12) . . ?
Lu7 Lu13 Lu9 98.0(12) . . ?
N1 Lu13 Lu9 48.8(7) . . ?
Lu1 Lu13 Lu9 106.5(11) . . ?
Lu1 Lu13 Lu9 78.7(10) 6_565 . ?
Lu2 Lu13 Lu9 33.6(7) . . ?
Lu4 Lu13 Lu9 42.8(7) 6_565 . ?
Lu4 Lu13 Lu9 21.6(7) . . ?
N2P Ni1P N2P 89.9(4) . 6_565 ?
N2P Ni1P N1P 90.0(3) . . ?
N2P Ni1P N1P 178.3(2) 6_565 . ?
N2P Ni1P N1P 178.3(2) . 6_565 ?
N2P Ni1P N1P 90.0(3) 6_565 6_565 ?
N1P Ni1P N1P 90.0(4) . 6_565 ?
C2P C1P C2P 125.9(8) 6_565 . ?
C9P N2P C2P 104.1(6) . . ?
C9P N2P Ni1P 128.2(4) . . ?
C2P N2P Ni1P 127.7(6) . . ?
C6P C3P C2P 108.2(6) . . ?
C6P C3P C4P 128.0(8) . . ?
C2P C3P C4P 123.8(8) . . ?
C3P C4P C5P 112.5(5) . . ?
C3P C6P C9P 105.2(8) . . ?
C3P C6P C7P 129.5(7) . . ?
C9P C6P C7P 125.2(8) . . ?
C6P C7P C8P 113.5(7) . . ?
C10P C9P N2P 124.5(7) . . ?
C10P C9P C6P 123.5(9) . . ?
N2P C9P C6P 112.0(7) . . ?
C9P C10P C11P 124.2(10) . . ?
N1P C11P C10P 125.5(7) . . ?
N1P C11P C12P 111.7(6) . . ?
C10P C11P C12P 122.8(9) . . ?
C15P C12P C11P 105.3(8) . . ?
C15P C12P C13P 129.2(6) . . ?
C11P C12P C13P 125.5(7) . . ?
C14P C13P C12P 113.9(7) . . ?
C12P C15P C18P 107.5(6) . . ?
C12P C15P C16P 126.9(8) . . ?
C18P C15P C16P 125.6(7) . . ?
C17P C16P C15P 113.0(6) . . ?
C19P C18P N1P 123.3(7) . . ?
C19P C18P C15P 125.2(5) . . ?
N1P C18P C15P 111.5(7) . . ?
C18P C19P C18P 126.6(8) . 6_565 ?
C1P C2P N2P 124.4(7) . . ?
C1P C2P C3P 125.1(5) . . ?
N2P C2P C3P 110.6(7) . . ?
C11P N1P C18P 104.0(6) . . ?
C11P N1P Ni1P 127.6(4) . . ?
C18P N1P Ni1P 128.4(6) . . ?
C2D C1D C2D 120.7(11) 6_565 . ?
C3D C2D C1D 119.6(9) . . ?
C2D C3D C4D 120.0(9) . . ?
C3D C4D C3D 119.8(11) 6_565 . ?
S1E C1E S1E 178.1(10) 6_565 . ?
C3F C1F C2F 118.2(18) 5_656 . ?
C1F C2F C3F 119(2) . . ?
C1F C3F C2F 122.5(16) 5_656 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C6 1.39(2) . ?
C1 C8 1.46(4) . ?
C1 C2 1.48(2) . ?
C1 C21 2.01(4) . ?
C2 C43 1.40(2) . ?
C2 C3 1.426(19) . ?
C3 C4 1.429(19) . ?
C3 C34 1.437(19) . ?
C4 C5 1.41(2) . ?
C4 C65 1.50(3) . ?
C5 C6 1.45(2) . ?
C5 C22 1.46(4) . ?
C6 C7 1.65(4) . ?
C7 C21 1.47(2) . ?
C7 C31 1.508(18) . ?
C8 C21 1.49(2) . ?
C8 C42 1.54(2) . ?
C9 C44 1.42(2) . ?
C9 C43 1.45(2) . ?
C9 C40 1.46(4) . ?
C10 C36 1.42(5) . ?
C10 C53 1.46(2) . ?
C10 C28 1.472(18) . ?
C11 C12 1.452(18) . ?
C11 C45 1.46(2) . ?
C11 C16 1.49(3) . ?
C12 C18 1.43(2) . ?
C12 C13 1.43(3) . ?
C13 C17 1.37(4) . ?
C13 C14 1.46(4) . ?
C13 C37 2.03(4) . ?
C14 C15 1.35(5) . ?
C14 C37 1.65(4) . ?
C15 C16 1.33(4) . ?
C15 C35 1.45(5) . ?
C16 C41 1.42(3) . ?
C17 C20 1.35(5) . ?
C17 C19 1.54(6) . ?
C18 C48 1.43(2) . ?
C18 C36 1.54(4) . ?
C19 C26 1.04(5) . ?
C19 C36 1.58(4) . ?
C20 C23 1.46(2) . ?
C20 C37 1.54(2) . ?
C21 C23 1.51(2) . ?
C22 C66 1.38(3) . ?
C22 C30 1.48(3) . ?
C23 C24 1.49(2) . ?
C24 C26 1.476(18) . ?
C24 C25 1.482(14) . ?
C25 C31 1.464(17) . ?
C25 C27 1.465(14) . ?
C26 C32 1.487(18) . ?
C27 C32 1.463(17) . ?
C27 C29 1.50(2) . ?
C28 C32 1.47(3) . ?
C28 C75 1.51(2) . ?
C29 C69 1.39(3) . ?
C29 C33 1.483(17) . ?
C30 C31 1.48(2) . ?
C30 C33 1.51(2) . ?
C33 C63 1.34(4) . ?
C34 C58 1.37(3) . ?
C34 C44 1.438(19) . ?
C35 C40 1.34(5) . ?
C35 C38 1.42(4) . ?
C37 C42 1.47(2) . ?
C38 C42 1.24(4) . ?
C38 C43 1.59(4) . ?
C39 C51 1.41(4) . ?
C39 C44 1.48(4) . ?
C39 C77 1.55(4) . ?
C40 C50 1.38(4) . ?
C41 C50 1.44(3) . ?
C41 C49 1.55(5) . ?
C45 C47 1.459(18) . ?
C45 C46 1.506(19) . ?
C46 C67 1.43(2) . ?
C46 C49 1.49(5) . ?
C47 C48 1.42(2) . ?
C47 C54 1.45(2) . ?
C48 C53 1.27(4) . ?
C49 C52 1.35(4) . ?
C50 C51 1.40(4) . ?
C51 C52 1.38(5) . ?
C52 C78 1.63(4) . ?
C53 C55 1.49(2) . ?
C54 C55 1.33(4) . ?
C54 C76 1.48(2) . ?
C55 C68 1.49(2) . ?
C56 C74 1.38(2) . ?
C56 C59 1.386(14) . ?
C56 C70 1.405(16) . ?
C57 C77 1.354(19) . ?
C57 C59 1.401(19) . ?
C57 C58 1.426(19) . ?
C58 C65 1.36(2) . ?
C59 C62 1.402(14) . ?
C60 C63 1.358(19) . ?
C60 C71 1.38(2) . ?
C60 C61 1.462(19) . ?
C61 C70 1.377(14) . ?
C61 C62 1.397(14) . ?
C62 C64 1.392(18) . ?
C63 C66 1.46(2) . ?
C64 C66 1.41(2) . ?
C64 C65 1.413(19) . ?
C67 C74 1.37(4) . ?
C67 C76 1.49(2) . ?
C68 C73 1.39(4) . ?
C68 C75 1.50(2) . ?
C69 C75 1.21(4) . ?
C69 C71 1.42(4) . ?
C70 C72 1.40(2) . ?
C71 C73 1.414(19) . ?
C72 C73 1.38(2) . ?
C72 C76 1.50(4) . ?
C74 C78 1.42(2) . ?
C77 C78 1.38(2) . ?
N1 Lu10 1.588(18) . ?
N1 Lu10 1.588(18) 6_565 ?
N1 Lu7 1.944(14) . ?
N1 Lu8 1.955(10) 6_565 ?
N1 Lu8 1.955(10) . ?
N1 Lu1 1.989(6) 6_565 ?
N1 Lu1 1.989(6) . ?
N1 Lu6 2.023(7) 6_565 ?
N1 Lu6 2.023(7) . ?
N1 Lu13 2.03(3) . ?
N1 Lu4 2.088(7) . ?
N1 Lu4 2.088(7) 6_565 ?
Lu1 Lu7 1.023(4) . ?
Lu1 Lu8 1.379(15) . ?
Lu1 Lu1 1.996(7) 6_565 ?
Lu1 Lu13 2.07(3) . ?
Lu1 Lu8 2.110(12) 6_565 ?
Lu1 Lu6 2.215(3) 6_565 ?
Lu1 Lu10 2.760(16) . ?
Lu1 Lu11 2.808(18) . ?
Lu1 Lu5 2.818(4) . ?
Lu1 Lu3 2.821(3) 6_565 ?
Lu1 Lu12 2.856(7) . ?
Lu2 Lu4 0.5440(18) 6_565 ?
Lu2 Lu4 0.5440(18) . ?
Lu2 Lu9 1.56(4) . ?
Lu2 Lu9 1.56(4) 6_565 ?
Lu2 Lu13 2.35(3) . ?
Lu2 Lu12 2.625(8) . ?
Lu2 Lu12 2.625(8) 6_565 ?
Lu2 Lu8 2.693(13) . ?
Lu2 Lu8 2.693(13) 6_565 ?
Lu2 Lu10 2.85(3) . ?
Lu2 Lu10 2.85(3) 6_565 ?
Lu3 Lu5 0.781(3) 6_565 ?
Lu3 Lu10 1.21(3) 6_565 ?
Lu3 Lu11 1.263(16) 6_565 ?
Lu3 Lu3 1.402(5) 6_565 ?
Lu3 Lu10 2.00(3) . ?
Lu3 Lu5 2.037(6) . ?
Lu3 Lu12 2.444(8) 6_565 ?
Lu3 Lu11 2.523(14) . ?
Lu3 Lu1 2.821(3) 6_565 ?
Lu3 Lu7 3.027(17) . ?
Lu3 Lu6 3.075(4) 6_565 ?
Lu4 Lu4 0.993(9) 6_565 ?
Lu4 Lu9 1.04(4) . ?
Lu4 Lu9 1.97(3) 6_565 ?
Lu4 Lu12 2.159(8) 6_565 ?
Lu4 Lu13 2.52(3) . ?
Lu4 Lu10 2.57(3) 6_565 ?
Lu4 Lu8 2.715(12) 6_565 ?
Lu4 Lu10 2.90(2) . ?
Lu4 Lu12 2.922(9) . ?
Lu4 Lu8 2.939(12) . ?
Lu5 Lu11 0.504(14) . ?
Lu5 Lu10 0.76(2) . ?
Lu5 Lu3 0.781(3) 6_565 ?
Lu5 Lu12 1.742(8) . ?
Lu5 Lu10 2.26(3) 6_565 ?
Lu5 Lu5 2.525(8) 6_565 ?
Lu5 Lu9 2.68(3) 6_565 ?
Lu5 Lu6 2.968(5) . ?
Lu5 Lu11 2.974(15) 6_565 ?
Lu6 Lu8 1.047(17) . ?
Lu6 Lu7 1.303(10) . ?
Lu6 Lu13 1.82(3) . ?
Lu6 Lu8 2.023(13) 6_565 ?
Lu6 Lu1 2.215(3) 6_565 ?
Lu6 Lu6 2.348(11) 6_565 ?
Lu6 Lu12 2.720(8) . ?
Lu6 Lu10 2.84(2) . ?
Lu6 Lu11 2.895(19) . ?
Lu6 Lu9 2.909(14) 6_565 ?
Lu7 Lu1 1.023(4) 6_565 ?
Lu7 Lu6 1.303(10) 6_565 ?
Lu7 Lu8 1.58(2) 6_565 ?
Lu7 Lu8 1.58(2) . ?
Lu7 Lu13 1.93(4) . ?
Lu7 Lu3 3.027(17) 6_565 ?
Lu7 Lu10 3.092(19) . ?
Lu7 Lu10 3.092(19) 6_565 ?
Lu8 Lu13 0.81(3) . ?
Lu8 Lu8 1.28(2) 6_565 ?
Lu8 Lu6 2.023(13) 6_565 ?
Lu8 Lu1 2.110(12) 6_565 ?
Lu8 Lu9 2.705(19) 6_565 ?
Lu8 Lu4 2.715(12) 6_565 ?
Lu9 Lu12 1.21(4) 6_565 ?
Lu9 Lu4 1.97(3) 6_565 ?
Lu9 Lu10 2.09(4) 6_565 ?
Lu9 Lu11 2.45(4) 6_565 ?
Lu9 Lu5 2.68(3) 6_565 ?
Lu9 Lu8 2.705(19) 6_565 ?
Lu9 Lu9 2.81(6) 6_565 ?
Lu9 Lu13 2.82(3) . ?
Lu9 Lu6 2.908(14) 6_565 ?
Lu10 Lu11 0.903(18) . ?
Lu10 Lu3 1.21(3) 6_565 ?
Lu10 Lu12 1.42(3) . ?
Lu10 Lu10 1.81(4) 6_565 ?
Lu10 Lu9 2.09(4) 6_565 ?
Lu10 Lu5 2.26(3) 6_565 ?
Lu10 Lu4 2.57(3) 6_565 ?
Lu10 Lu11 2.64(3) 6_565 ?
Lu11 Lu3 1.263(16) 6_565 ?
Lu11 Lu12 1.37(2) . ?
Lu11 Lu9 2.45(4) 6_565 ?
Lu11 Lu10 2.64(3) 6_565 ?
Lu11 Lu5 2.974(15) 6_565 ?
Lu11 Lu4 3.18(2) 6_565 ?
Lu12 Lu9 1.21(4) 6_565 ?
Lu12 Lu4 2.159(8) 6_565 ?
Lu12 Lu3 2.444(8) 6_565 ?
Lu13 Lu8 0.81(3) 6_565 ?
Lu13 Lu6 1.82(3) 6_565 ?
Lu13 Lu1 2.07(3) 6_565 ?
Lu13 Lu4 2.52(3) 6_565 ?
Ni1P N2P 1.956(6) . ?
Ni1P N2P 1.956(6) 6_565 ?
Ni1P N1P 1.959(6) . ?
Ni1P N1P 1.959(6) 6_565 ?
C1P C2P 1.351(9) 6_565 ?
C1P C2P 1.351(9) . ?
N2P C9P 1.385(12) . ?
N2P C2P 1.391(7) . ?
C3P C6P 1.356(12) . ?
C3P C2P 1.444(12) . ?
C3P C4P 1.506(8) . ?
C4P C5P 1.531(9) . ?
C6P C9P 1.456(10) . ?
C6P C7P 1.461(15) . ?
C7P C8P 1.523(16) . ?
C9P C10P 1.371(10) . ?
C10P C11P 1.376(10) . ?
C11P N1P 1.374(11) . ?
C11P C12P 1.449(10) . ?
C12P C15P 1.364(12) . ?
C12P C13P 1.508(14) . ?
C13P C14P 1.503(15) . ?
C15P C18P 1.422(12) . ?
C15P C16P 1.511(8) . ?
C16P C17P 1.510(11) . ?
C18P C19P 1.374(9) . ?
C18P N1P 1.385(7) . ?
C19P C18P 1.374(9) 6_565 ?
C1D C2D 1.391(11) 6_565 ?
C1D C2D 1.391(11) . ?
C2D C3D 1.388(12) . ?
C3D C4D 1.397(12) . ?
C4D C3D 1.397(12) 6_565 ?
C1E S1E 1.527(4) 6_565 ?
C1E S1E 1.527(4) . ?
C1F C3F 1.32(3) 5_656 ?
C1F C2F 1.36(3) . ?
C2F C3F 1.38(3) . ?
C3F C1F 1.32(3) 5_656 ?
