#------------------------------------------------------------------------------
#$Date: 2022-12-21 15:06:10 +0200 (Wed, 21 Dec 2022) $
#$Revision: 279967 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/81/1568141.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1568141
loop_
_publ_author_name
'Zhou, Xiuquan'
'Kolluru, Venkata Surya Chaitanya'
'Xu, Wenqian'
'Wang, Luqing'
'Chang, Tieyan'
'Chen, Yu-Sheng'
'Yu, Lei'
'Wen, Jianguo'
'Chan, Maria K. Y.'
'Chung, Duck Young'
'Kanatzidis, Mercouri G.'
_publ_section_title
;
 Discovery of chalcogenides structures and compositions using mixed fluxes
;
_journal_issue                   7938
_journal_name_full               Nature
_journal_page_first              72
_journal_page_last               77
_journal_paper_doi               10.1038/s41586-022-05307-7
_journal_volume                  612
_journal_year                    2022
_chemical_formula_moiety         'Cu11.4 Na9.74 O2 S10'
_chemical_formula_sum            'Cu11.4 Na9.74 O2 S10'
_chemical_formula_weight         1301.09
_space_group_crystal_system      monoclinic
_space_group_IT_number           13
_space_group_name_Hall           '-P 2yc'
_space_group_name_H-M_alt        'P 1 2/c 1'
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_audit_contact_author_name
;
;
_audit_creation_date             2022-08-15
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_cell_angle_alpha                90
_cell_angle_beta                 110.90(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   20.388(4)
_cell_length_b                   7.7841(16)
_cell_length_c                   15.311(3)
_cell_measurement_reflns_used    6099
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      58.332
_cell_measurement_theta_min      6.718
_cell_volume                     2270.0(9)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0753
_diffrn_reflns_av_unetI/netI     0.1836
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            6099
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.166
_diffrn_reflns_theta_min         3.359
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    11.556
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    3.807
_exptl_crystal_description       needle
_exptl_crystal_F_000             2455
_refine_diff_density_max         1.276
_refine_diff_density_min         -1.284
_refine_diff_density_rms         0.224
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.507
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     316
_refine_ls_number_reflns         6099
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.507
_refine_ls_R_factor_all          0.1450
_refine_ls_R_factor_gt           0.0317
_refine_ls_shift/su_max          1.655
_refine_ls_shift/su_mean         0.027
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0579P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0710
_refine_ls_wR_factor_ref         0.1091
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1332
_reflns_number_total             6099
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            V_Cu11.4Na9.74O2S10.cif
_cod_data_source_block           V
_cod_original_formula_sum        'Cu11.40 Na9.74 O2 S10'
_cod_database_code               1568141
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_olex2_refinement_description
;
1. Others
 Fixed Sof: Cu0X(0.125)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu01 Cu 0.50462(8) -0.1217(5) 0.34608(12) 0.0178(4) Uani 1 1 d . . . . .
Cu02 Cu 0.57608(8) 0.1229(4) 0.27877(12) 0.0176(4) Uani 1 1 d . . . . .
Cu03 Cu 0.49293(8) 0.3707(5) 0.15548(12) 0.0179(4) Uani 1 1 d . . . . .
Cu04 Cu 0.57386(9) -0.3698(4) 0.27459(12) 0.0185(4) Uani 1 1 d . . . . .
Cu05 Cu 0.82840(9) 1.1211(5) 0.90568(12) 0.0203(4) Uani 1 1 d . . . . .
Cu06 Cu 0.90239(9) 0.8718(5) 1.02894(12) 0.0224(4) Uani 1 1 d . . . . .
Cu07 Cu 0.82528(8) 0.6271(5) 0.91077(12) 0.0211(4) Uani 1 1 d . . . . .
Cu08 Cu 0.90776(8) 0.3709(5) 1.02636(12) 0.0208(4) Uani 1 1 d . . . . .
Cu09 Cu 0.90889(10) 0.8912(4) 0.83558(14) 0.0262(5) Uani 1 1 d . . . . .
Cu0A Cu 0.91077(10) 1.3587(5) 0.83882(14) 0.0276(5) Uani 1 1 d . . . . .
Cu0B Cu 1.04092(10) 1.3732(5) 1.05776(14) 0.0332(4) Uani 1 1 d . . . . .
S00C S 0.78968(15) 0.3711(8) 0.9584(2) 0.0132(6) Uani 1 1 d . . . . .
S00D S 0.61376(15) 0.3744(8) 0.2301(2) 0.0129(6) Uani 1 1 d . . . . .
S00E S 0.38331(15) -0.1239(8) 0.2734(2) 0.0129(6) Uani 1 1 d . . . . .
S00F S 0.55862(16) -0.3726(8) 0.4173(2) 0.0144(7) Uani 1 1 d . . . . .
S00G S 1.03260(16) 1.3746(9) 0.9035(2) 0.0142(6) Uani 1 1 d . . . . .
S00H S 0.56208(16) 0.1254(8) 0.4224(2) 0.0125(6) Uani 1 1 d . . . . .
S00I S 0.78471(15) 0.8760(8) 0.9596(2) 0.0144(6) Uani 1 1 d . . . . .
S00J S 0.96658(16) 0.1219(9) 1.1007(2) 0.0161(7) Uani 1 1 d . . . . .
S00K S 0.85977(16) 0.6249(9) 0.7821(2) 0.0173(6) Uani 1 1 d . . . . .
S00L S 0.84745(17) 1.1269(9) 0.7656(2) 0.0179(6) Uani 1 1 d . . . . .
Na0M Na 0.5801(3) -0.1380(13) 0.5714(4) 0.0190(13) Uani 1 1 d . . . . .
Na0N Na 0.5806(3) 0.3824(15) 0.5714(4) 0.0234(13) Uani 1 1 d . . . . .
Na0O Na 1.000000 0.376(2) 1.250000 0.0211(16) Uani 1 2 d S T P . .
Na0P Na 0.6747(3) 0.3861(15) 0.4316(4) 0.0210(13) Uani 1 1 d . . . . .
Na0Q Na 0.6750(3) -0.1344(14) 0.4301(4) 0.0214(13) Uani 1 1 d . . . . .
Na0R Na 0.7316(3) 0.3818(16) 0.7584(4) 0.0250(13) Uani 1 1 d . . . . .
Na0S Na 0.7306(3) -0.1392(14) 0.7592(4) 0.0220(14) Uani 1 1 d . . . . .
Na0T Na 1.000000 -0.125(2) 1.250000 0.0259(18) Uani 1 2 d S T P . .
Na0U Na 0.8232(3) -0.1339(16) 0.6171(4) 0.0267(14) Uani 1 1 d . . . . .
Cu0V Cu 0.9763(5) 0.0947(12) 0.9659(8) 0.039(4) Uani 0.277(7) 1 d . . . . .
Na0W Na 0.8243(3) 0.3912(14) 0.6183(4) 0.0243(15) Uani 1 1 d . . . . .
Cu0X Cu 1.000000 0.000000 1.000000 0.038(4) Uani 0.25 2 d S T P . .
Na00 Na 0.7011(2) 0.1248(10) 0.5933(4) 0.0153(15) Uani 0.744(16) 1 d . . . . .
O00Z O 0.7039(5) 0.394(2) 0.5971(7) 0.022(3) Uani 1 1 d . . . . .
O010 O 0.7035(5) -0.1513(15) 0.5971(7) 0.013(2) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Cu01 Cu01 Na0M 123.78(14) 2_655 3_656
Cu01 Cu01 Na0M 157.05(13) 2_655 .
Cu01 Cu01 Na0N 123.69(13) 2_655 3_656
Cu01 Cu01 Na0Q 94.35(12) 2_655 .
Cu02 Cu01 Cu01 58.56(7) . 2_655
Cu02 Cu01 Cu01 59.40(7) 2_655 2_655
Cu02 Cu01 Cu02 62.67(11) 2_655 .
Cu02 Cu01 Cu04 117.08(9) 2_655 .
Cu02 Cu01 Cu04 85.71(7) . .
Cu02 Cu01 Na0M 64.44(15) 2_655 3_656
Cu02 Cu01 Na0M 98.1(2) . 3_656
Cu02 Cu01 Na0M 107.83(17) . .
Cu02 Cu01 Na0M 134.3(2) 2_655 .
Cu02 Cu01 Na0N 115.63(15) 2_655 3_656
Cu02 Cu01 Na0N 176.5(2) . 3_656
Cu02 Cu01 Na0Q 125.5(2) 2_655 .
Cu02 Cu01 Na0Q 62.89(18) . .
Cu04 Cu01 Cu01 60.30(7) 2_655 2_655
Cu04 Cu01 Cu01 57.68(7) . 2_655
Cu04 Cu01 Cu02 87.67(7) 2_655 2_655
Cu04 Cu01 Cu02 118.85(9) 2_655 .
Cu04 Cu01 Cu04 60.87(11) 2_655 .
Cu04 Cu01 Na0M 176.1(2) . 3_656
Cu04 Cu01 Na0M 105.77(17) . .
Cu04 Cu01 Na0M 128.9(2) 2_655 .
Cu04 Cu01 Na0M 116.22(13) 2_655 3_656
Cu04 Cu01 Na0N 63.53(15) 2_655 3_656
Cu04 Cu01 Na0N 97.8(2) . 3_656
Cu04 Cu01 Na0Q 61.46(18) . .
Cu04 Cu01 Na0Q 121.8(2) 2_655 .
S00E Cu01 Cu01 80.82(11) . 2_655
S00E Cu01 Cu02 115.66(18) . .
S00E Cu01 Cu02 53.72(16) . 2_655
S00E Cu01 Cu04 113.73(18) . .
S00E Cu01 Cu04 53.79(16) . 2_655
S00E Cu01 S00H 120.3(2) . .
S00E Cu01 Na0M 63.95(17) . 3_656
S00E Cu01 Na0M 121.98(14) . .
S00E Cu01 Na0N 63.26(18) . 3_656
S00E Cu01 Na0Q 174.70(18) . .
S00F Cu01 Cu01 109.15(11) . 2_655
S00F Cu01 Cu02 121.55(12) . .
S00F Cu01 Cu02 165.05(17) . 2_655
S00F Cu01 Cu04 52.26(12) . .
S00F Cu01 Cu04 77.83(17) . 2_655
S00F Cu01 S00E 117.7(2) . .
S00F Cu01 S00H 112.93(12) . .
S00F Cu01 Na0M 60.0(2) . .
S00F Cu01 Na0M 125.48(17) . 3_656
S00F Cu01 Na0N 60.94(18) . 3_656
S00F Cu01 Na0Q 61.7(2) . .
S00H Cu01 Cu01 110.43(11) . 2_655
S00H Cu01 Cu02 52.56(12) . .
S00H Cu01 Cu02 81.29(16) . 2_655
S00H Cu01 Cu04 121.62(12) . .
S00H Cu01 Cu04 168.44(16) . 2_655
S00H Cu01 Na0M 62.4(2) . .
S00H Cu01 Na0M 61.78(17) . 3_656
S00H Cu01 Na0N 124.68(17) . 3_656
S00H Cu01 Na0Q 63.4(2) . .
Na0M Cu01 Na0M 73.9(2) 3_656 .
Na0M Cu01 Na0N 78.45(14) 3_656 3_656
Na0M Cu01 Na0Q 121.0(2) 3_656 .
Na0M Cu01 Na0Q 62.76(14) . .
Na0N Cu01 Na0M 70.98(18) 3_656 .
Na0N Cu01 Na0Q 118.5(2) 3_656 .
Cu01 Cu02 Cu01 62.04(11) 2_655 .
Cu01 Cu02 Cu02 58.24(7) . 2_655
Cu01 Cu02 Cu02 59.08(7) 2_655 2_655
Cu01 Cu02 Cu03 86.61(7) 2_655 .
Cu01 Cu02 Na0M 64.06(17) 2_655 4
Cu01 Cu02 Na0M 126.0(2) . 4
Cu01 Cu02 Na0P 115.86(14) . .
Cu01 Cu02 Na0P 176.4(2) 2_655 .
Cu01 Cu02 Na0Q 65.32(14) . .
Cu01 Cu02 Na0Q 97.8(2) 2_655 .
Cu01 Cu02 Na0S 108.43(18) 2_655 4
Cu01 Cu02 Na0S 134.7(2) . 4
Cu02 Cu02 Na0M 95.81(12) 2_655 4
Cu02 Cu02 Na0P 122.86(14) 2_655 .
Cu02 Cu02 Na0Q 123.47(14) 2_655 .
Cu02 Cu02 Na0S 158.52(14) 2_655 4
Cu03 Cu02 Cu01 118.17(9) 2_655 2_655
Cu03 Cu02 Cu01 86.65(7) 2_655 .
Cu03 Cu02 Cu01 116.42(8) . .
Cu03 Cu02 Cu02 58.19(7) . 2_655
Cu03 Cu02 Cu02 59.09(7) 2_655 2_655
Cu03 Cu02 Cu03 60.28(11) 2_655 .
Cu03 Cu02 Na0M 62.06(16) . 4
Cu03 Cu02 Na0M 121.9(2) 2_655 4
Cu03 Cu02 Na0P 63.92(15) 2_655 .
Cu03 Cu02 Na0P 97.0(2) . .
Cu03 Cu02 Na0Q 116.39(15) 2_655 .
Cu03 Cu02 Na0Q 175.5(2) . .
Cu03 Cu02 Na0S 129.4(2) 2_655 4
Cu03 Cu02 Na0S 106.38(18) . 4
S00D Cu02 Cu01 164.70(16) . .
S00D Cu02 Cu01 122.60(13) . 2_655
S00D Cu02 Cu02 110.03(10) . 2_655
S00D Cu02 Cu03 52.70(11) . .
S00D Cu02 Cu03 78.42(16) . 2_655
S00D Cu02 S00E 112.59(12) . 2_655
S00D Cu02 Na0M 61.5(2) . 4
S00D Cu02 Na0P 60.27(18) . .
S00D Cu02 Na0Q 124.67(17) . .
S00D Cu02 Na0S 59.9(2) . 4
S00E Cu02 Cu01 82.08(16) 2_655 .
S00E Cu02 Cu01 53.05(11) 2_655 2_655
S00E Cu02 Cu02 111.44(11) 2_655 2_655
S00E Cu02 Cu03 168.25(17) 2_655 2_655
S00E Cu02 Cu03 122.44(12) 2_655 .
S00E Cu02 Na0M 63.6(2) 2_655 4
S00E Cu02 Na0P 124.41(17) 2_655 .
S00E Cu02 Na0Q 61.50(18) 2_655 .
S00E Cu02 Na0S 62.0(2) 2_655 4
S00H Cu02 Cu01 114.52(18) . 2_655
S00H Cu02 Cu01 53.22(16) . .
S00H Cu02 Cu02 78.94(11) . 2_655
S00H Cu02 Cu03 112.54(18) . .
S00H Cu02 Cu03 53.17(16) . 2_655
S00H Cu02 S00D 117.7(2) . .
S00H Cu02 S00E 120.6(2) . 2_655
S00H Cu02 Na0M 174.15(18) . 4
S00H Cu02 Na0P 63.96(17) . .
S00H Cu02 Na0Q 64.80(18) . .
S00H Cu02 Na0S 122.39(14) . 4
Na0M Cu02 Na0P 117.8(2) 4 .
Na0M Cu02 Na0S 62.77(14) 4 4
Na0P Cu02 Na0S 70.73(19) . 4
Na0Q Cu02 Na0M 120.7(2) . 4
Na0Q Cu02 Na0P 78.59(14) . .
Na0Q Cu02 Na0S 73.17(19) . 4
Cu02 Cu03 Cu02 62.72(11) 2_655 .
Cu02 Cu03 Cu03 60.34(7) 2_655 2_655
Cu02 Cu03 Cu04 89.10(7) 2_655 2_665
Cu02 Cu03 Cu04 89.06(7) . 1_565
Cu02 Cu03 Cu04 119.30(9) . 2_665
Cu02 Cu03 Cu04 121.13(9) 2_655 1_565
Cu02 Cu03 Na0M 100.5(2) 2_655 4
Cu02 Cu03 Na0M 65.29(14) . 4
Cu02 Cu03 Na0N 173.1(2) 2_655 4_565
Cu02 Cu03 Na0N 132.4(2) . 2_655
Cu02 Cu03 Na0N 107.82(18) 2_655 2_655
Cu02 Cu03 Na0N 113.23(14) . 4_565
Cu02 Cu03 Na0P 127.3(2) . 2_655
Cu02 Cu03 Na0P 64.74(19) 2_655 2_655
Cu03 Cu03 Cu02 59.38(7) 2_655 .
Cu03 Cu03 Cu04 60.82(7) 2_655 1_565
Cu03 Cu03 Cu04 59.95(7) 2_655 2_665
Cu03 Cu03 Na0M 124.20(13) 2_655 4
Cu03 Cu03 Na0N 159.98(13) 2_655 2_655
Cu03 Cu03 Na0N 123.36(15) 2_655 4_565
Cu03 Cu03 Na0P 97.55(13) 2_655 2_655
Cu04 Cu03 Cu04 59.87(11) 1_565 2_665
Cu04 Cu03 Na0M 170.3(2) 2_665 4
Cu04 Cu03 Na0M 113.21(15) 1_565 4
Cu04 Cu03 Na0N 63.10(16) 1_565 4_565
Cu04 Cu03 Na0N 97.8(2) 2_665 4_565
Cu04 Cu03 Na0N 106.33(19) 2_665 2_655
Cu04 Cu03 Na0N 127.5(2) 1_565 2_655
Cu04 Cu03 Na0P 63.06(18) 2_665 2_655
Cu04 Cu03 Na0P 122.2(2) 1_565 2_655
S00D Cu03 Cu02 52.84(16) . .
S00D Cu03 Cu02 114.63(18) . 2_655
S00D Cu03 Cu03 77.96(11) . 2_655
S00D Cu03 Cu04 53.09(17) . 1_565
S00D Cu03 Cu04 111.88(18) . 2_665
S00D Cu03 S00F 116.2(2) . 2_665
S00D Cu03 S00H 119.9(2) . 2_655
S00D Cu03 Na0M 63.16(18) . 4
S00D Cu03 Na0N 121.96(14) . 2_655
S00D Cu03 Na0N 62.70(17) . 4_565
S00D Cu03 Na0P 174.7(2) . 2_655
S00F Cu03 Cu02 124.36(12) 2_665 2_655
S00F Cu03 Cu02 164.97(16) 2_665 .
S00F Cu03 Cu03 110.73(11) 2_665 2_655
S00F Cu03 Cu04 75.95(15) 2_665 1_565
S00F Cu03 Cu04 51.81(12) 2_665 2_665
S00F Cu03 Na0M 121.54(17) 2_665 4
S00F Cu03 Na0N 61.04(18) 2_665 4_565
S00F Cu03 Na0N 60.8(2) 2_665 2_655
S00F Cu03 Na0P 62.5(2) 2_665 2_655
S00H Cu03 Cu02 81.08(17) 2_655 .
S00H Cu03 Cu02 53.12(12) 2_655 2_655
S00H Cu03 Cu03 112.55(12) 2_655 2_655
S00H Cu03 Cu04 124.67(12) 2_655 2_665
S00H Cu03 Cu04 170.11(17) 2_655 1_565
S00H Cu03 S00F 113.88(12) 2_655 2_665
S00H Cu03 Na0M 63.36(18) 2_655 4
S00H Cu03 Na0N 61.3(2) 2_655 2_655
S00H Cu03 Na0N 121.78(19) 2_655 4_565
S00H Cu03 Na0P 64.4(2) 2_655 2_655
Na0M Cu03 Na0N 72.53(15) 4 4_565
Na0M Cu03 Na0N 71.89(19) 4 2_655
Na0M Cu03 Na0P 122.1(2) 4 2_655
Na0N Cu03 Na0N 70.4(2) 4_565 2_655
Na0N Cu03 Na0P 118.6(2) 4_565 2_655
Na0P Cu03 Na0N 62.45(14) 2_655 2_655
Cu01 Cu04 Cu01 62.02(11) 2_655 .
Cu01 Cu04 Cu03 88.13(7) . 2_645
Cu01 Cu04 Cu03 120.51(8) 2_655 2_645
Cu01 Cu04 Cu03 90.15(7) 2_655 1_545
Cu01 Cu04 Cu04 60.90(7) 2_655 2_655
Cu01 Cu04 Na0N 127.1(2) . 4
Cu01 Cu04 Na0N 65.23(18) 2_655 4
Cu01 Cu04 Na0P 113.12(15) . 1_545
Cu01 Cu04 Na0P 172.2(2) 2_655 1_545
Cu01 Cu04 Na0Q 99.6(2) 2_655 .
Cu01 Cu04 Na0Q 65.80(15) . .
Cu01 Cu04 Na0R 108.45(19) 2_655 4
Cu01 Cu04 Na0R 132.7(2) . 4
Cu03 Cu04 Cu01 118.69(9) 1_545 .
Cu03 Cu04 Cu03 59.23(11) 1_545 2_645
Cu03 Cu04 Cu04 60.49(7) 1_545 2_655
Cu03 Cu04 Na0N 122.8(2) 2_645 4
Cu03 Cu04 Na0N 64.12(18) 1_545 4
Cu03 Cu04 Na0P 63.81(14) 2_645 1_545
Cu03 Cu04 Na0P 97.6(2) 1_545 1_545
Cu03 Cu04 Na0Q 170.1(2) 1_545 .
Cu03 Cu04 Na0Q 113.75(15) 2_645 .
Cu03 Cu04 Na0R 106.9(2) 1_545 4
Cu03 Cu04 Na0R 127.9(2) 2_645 4
Cu04 Cu04 Cu01 58.23(7) 2_655 .
Cu04 Cu04 Cu03 59.63(7) 2_655 2_645
Cu04 Cu04 Na0N 98.84(13) 2_655 4
Cu04 Cu04 Na0P 122.75(14) 2_655 1_545
Cu04 Cu04 Na0Q 123.52(14) 2_655 .
Cu04 Cu04 Na0R 161.55(14) 2_655 4
S00D Cu04 Cu01 125.43(12) 1_545 2_655
S00D Cu04 Cu01 164.75(17) 1_545 .
S00D Cu04 Cu03 52.26(11) 1_545 1_545
S00D Cu04 Cu03 76.64(15) 1_545 2_645
S00D Cu04 Cu04 111.68(10) 1_545 2_655
S00D Cu04 Na0N 63.0(2) 1_545 4
S00D Cu04 Na0P 60.90(18) 1_545 1_545
S00D Cu04 Na0Q 121.12(19) 1_545 .
S00D Cu04 Na0R 60.5(2) 1_545 4
S00E Cu04 Cu01 53.54(12) 2_655 2_655
S00E Cu04 Cu01 81.73(17) 2_655 .
S00E Cu04 Cu03 169.84(17) 2_655 2_645
S00E Cu04 Cu03 125.60(13) 2_655 1_545
S00E Cu04 Cu04 113.51(11) 2_655 2_655
S00E Cu04 S00D 113.48(12) 2_655 1_545
S00E Cu04 Na0N 64.0(2) 2_655 4
S00E Cu04 Na0P 121.08(17) 2_655 1_545
S00E Cu04 Na0Q 62.57(19) 2_655 .
S00E Cu04 Na0R 61.1(2) 2_655 4
S00F Cu04 Cu01 52.29(16) . .
S00F Cu04 Cu01 113.45(18) . 2_655
S00F Cu04 Cu03 111.01(18) . 1_545
S00F Cu04 Cu03 52.81(16) . 2_645
S00F Cu04 Cu04 76.28(11) . 2_655
S00F Cu04 S00D 116.4(2) . 1_545
S00F Cu04 S00E 119.8(2) . 2_655
S00F Cu04 Na0N 174.60(19) . 4
S00F Cu04 Na0P 63.15(18) . 1_545
S00F Cu04 Na0Q 63.93(18) . .
S00F Cu04 Na0R 122.07(14) . 4
Na0N Cu04 Na0P 118.8(2) 4 1_545
Na0N Cu04 Na0R 62.75(14) 4 4
Na0P Cu04 Na0R 69.90(18) 1_545 4
Na0Q Cu04 Na0N 121.3(2) . 4
Na0Q Cu04 Na0P 72.62(14) . 1_545
Na0Q Cu04 Na0R 71.3(2) . 4
Cu06 Cu05 Cu08 89.46(7) . 1_565
Cu06 Cu05 Cu09 64.64(10) . .
Cu06 Cu05 Cu0A 116.37(9) . .
Cu06 Cu05 Na0Q 104.82(18) . 4_566
Cu06 Cu05 Na0R 174.5(2) . 1_565
Cu06 Cu05 Na0S 95.0(2) . 1_565
Cu06 Cu05 Na0U 63.07(19) . 4_566
Cu06 Cu05 Cu0V 57.7(2) . 1_565
Cu08 Cu05 Cu09 114.17(9) 1_565 .
Cu08 Cu05 Cu0A 61.12(9) 1_565 .
Cu08 Cu05 Na0Q 104.79(18) 1_565 4_566
Cu08 Cu05 Na0R 95.3(2) 1_565 1_565
Cu08 Cu05 Na0S 175.4(2) 1_565 1_565
Cu08 Cu05 Na0U 62.42(19) 1_565 4_566
Cu08 Cu05 Cu0V 62.1(2) 1_565 1_565
Cu09 Cu05 Cu0A 77.73(7) . .
Cu09 Cu05 Na0Q 139.0(2) . 4_566
Cu09 Cu05 Na0R 115.36(14) . 1_565
Cu09 Cu05 Na0S 68.61(15) . 1_565
Cu09 Cu05 Na0U 127.6(2) . 4_566
Cu0A Cu05 Na0Q 135.3(2) . 4_566
Cu0A Cu05 Na0R 68.45(16) . 1_565
Cu0A Cu05 Na0S 117.07(15) . 1_565
Cu0A Cu05 Na0U 123.5(2) . 4_566
S00C Cu05 Cu06 121.19(13) 1_565 .
S00C Cu05 Cu08 51.49(12) 1_565 1_565
S00C Cu05 Cu09 161.51(17) 1_565 .
S00C Cu05 Cu0A 84.34(17) 1_565 .
S00C Cu05 S00I 109.43(11) 1_565 .
S00C Cu05 Na0Q 58.9(2) 1_565 4_566
S00C Cu05 Na0R 60.68(19) 1_565 1_565
S00C Cu05 Na0S 124.94(18) 1_565 1_565
S00C Cu05 Na0U 60.1(2) 1_565 4_566
S00C Cu05 Cu0V 113.5(2) 1_565 1_565
S00I Cu05 Cu06 51.46(11) . .
S00I Cu05 Cu08 122.29(12) . 1_565
S00I Cu05 Cu09 87.97(17) . .
S00I Cu05 Cu0A 164.86(17) . .
S00I Cu05 Na0Q 59.7(2) . 4_566
S00I Cu05 Na0R 123.33(18) . 1_565
S00I Cu05 Na0S 60.67(18) . 1_565
S00I Cu05 Na0U 62.2(2) . 4_566
S00I Cu05 Cu0V 108.5(2) . 1_565
S00L Cu05 Cu06 114.68(18) . .
S00L Cu05 Cu08 110.69(19) . 1_565
S00L Cu05 Cu09 50.23(16) . .
S00L Cu05 Cu0A 49.77(16) . .
S00L Cu05 S00C 119.4(2) . 1_565
S00L Cu05 S00I 123.1(2) . .
S00L Cu05 Na0Q 125.98(14) . 4_566
S00L Cu05 Na0R 66.00(18) . 1_565
S00L Cu05 Na0S 67.98(19) . 1_565
S00L Cu05 Na0U 172.15(18) . 4_566
S00L Cu05 Cu0V 78.0(2) . 1_565
Na0R Cu05 Na0Q 71.5(2) 1_565 4_566
Na0R Cu05 Na0S 80.15(15) 1_565 1_565
Na0R Cu05 Na0U 117.0(2) 1_565 4_566
Na0S Cu05 Na0Q 73.4(2) 1_565 4_566
Na0S Cu05 Na0U 119.2(2) 1_565 4_566
Na0U Cu05 Na0Q 61.22(14) 4_566 4_566
Cu0V Cu05 Cu09 52.7(2) 1_565 .
Cu0V Cu05 Cu0A 58.7(2) 1_565 .
Cu0V Cu05 Na0Q 156.0(3) 1_565 4_566
Cu0V Cu05 Na0R 127.1(3) 1_565 1_565
Cu0V Cu05 Na0S 121.1(2) 1_565 1_565
Cu0V Cu05 Na0U 95.0(2) 1_565 4_566
Cu05 Cu06 Cu09 59.77(8) . .
Cu05 Cu06 Cu0B 111.93(10) . 3_777
Cu05 Cu06 Na0U 66.56(16) . 4_566
Cu05 Cu06 Na0W 120.79(15) . 4_566
Cu07 Cu06 Cu05 89.56(7) . .
Cu07 Cu06 Cu09 66.28(9) . .
Cu07 Cu06 Cu0B 56.19(9) . 3_777
Cu07 Cu06 Na0U 118.18(15) . 4_566
Cu07 Cu06 Na0W 64.87(16) . 4_566
Cu09 Cu06 Na0U 126.22(18) . 4_566
Cu09 Cu06 Na0W 131.12(18) . 4_566
Cu0B Cu06 Cu09 52.97(9) 3_777 .
Cu0B Cu06 Na0U 174.37(17) 3_777 4_566
Cu0B Cu06 Na0W 96.9(2) 3_777 4_566
S00G Cu06 Cu05 164.19(14) 3_777 .
S00G Cu06 Cu07 79.75(17) 3_777 .
S00G Cu06 Cu09 104.92(13) 3_777 .
S00G Cu06 Cu0B 52.36(13) 3_777 3_777
S00G Cu06 S00J 109.43(11) 3_777 1_565
S00G Cu06 Na0U 128.86(18) 3_777 4_566
S00G Cu06 Cu0V 70.7(3) 3_777 3_767
S00G Cu06 Cu0V 112.6(2) 3_777 1_565
S00G Cu06 Na0W 64.95(18) 3_777 4_566
S00G Cu06 Cu0X 92.63(12) 3_777 1_565
S00I Cu06 Cu05 55.59(17) . .
S00I Cu06 Cu07 55.14(16) . .
S00I Cu06 Cu09 87.07(11) . .
S00I Cu06 Cu0B 109.70(17) . 3_777
S00I Cu06 S00G 123.9(2) . 3_777
S00I Cu06 S00J 121.5(2) . 1_565
S00I Cu06 Na0U 64.83(18) . 4_566
S00I Cu06 Cu0V 154.7(3) . 3_767
S00I Cu06 Cu0V 117.4(3) . 1_565
S00I Cu06 Na0W 66.42(19) . 4_566
S00I Cu06 Cu0X 136.05(17) . 1_565
S00J Cu06 Cu05 79.45(16) 1_565 .
S00J Cu06 Cu07 166.91(16) 1_565 .
S00J Cu06 Cu09 101.69(15) 1_565 .
S00J Cu06 Cu0B 121.57(13) 1_565 3_777
S00J Cu06 Na0U 63.87(19) 1_565 4_566
S00J Cu06 Cu0V 49.7(2) 1_565 1_565
S00J Cu06 Cu0V 61.2(2) 1_565 3_767
S00J Cu06 Na0W 127.08(18) 1_565 4_566
S00J Cu06 Cu0X 52.54(10) 1_565 1_565
Na0U Cu06 Na0W 79.81(15) 4_566 4_566
Cu0V Cu06 Cu05 62.6(3) 1_565 .
Cu0V Cu06 Cu05 104.3(3) 3_767 .
Cu0V Cu06 Cu07 115.7(2) 3_767 .
Cu0V Cu06 Cu07 118.6(2) 1_565 .
Cu0V Cu06 Cu09 68.3(3) 3_767 .
Cu0V Cu06 Cu09 52.4(2) 1_565 .
Cu0V Cu06 Cu0B 60.4(2) 3_767 3_777
Cu0V Cu06 Cu0B 83.72(19) 1_565 3_777
Cu0V Cu06 Na0U 125.1(3) 3_767 4_566
Cu0V Cu06 Na0U 99.9(3) 1_565 4_566
Cu0V Cu06 Cu0V 42.1(5) 3_767 1_565
Cu0V Cu06 Na0W 175.7(3) 1_565 4_566
Cu0V Cu06 Na0W 134.8(3) 3_767 4_566
Cu0X Cu06 Cu05 82.43(10) 1_565 .
Cu0X Cu06 Cu07 119.32(9) 1_565 .
Cu0X Cu06 Cu09 57.92(7) 1_565 .
Cu0X Cu06 Cu0B 71.72(8) 1_565 3_777
Cu0X Cu06 Na0U 113.0(2) 1_565 4_566
Cu0X Cu06 Cu0V 22.1(2) 1_565 3_767
Cu0X Cu06 Cu0V 20.1(2) 1_565 1_565
Cu0X Cu06 Na0W 156.78(16) 1_565 4_566
Cu06 Cu07 Cu08 90.24(7) . .
Cu06 Cu07 Na0P 107.75(18) . 4_566
Cu06 Cu07 Na0R 173.2(2) . .
Cu06 Cu07 Na0S 98.5(2) . 1_565
Cu06 Cu07 Na0W 64.81(18) . 4_566
Cu08 Cu07 Na0P 107.21(19) . 4_566
Cu08 Cu07 Na0R 96.2(2) . .
Cu08 Cu07 Na0S 170.4(2) . 1_565
Cu08 Cu07 Na0W 63.48(17) . 4_566
Cu0B Cu07 Cu06 63.62(10) 3_777 .
Cu0B Cu07 Cu08 61.76(10) 3_777 .
Cu0B Cu07 Na0P 164.56(13) 3_777 4_566
Cu0B Cu07 Na0R 117.72(17) 3_777 .
Cu0B Cu07 Na0S 118.80(17) 3_777 1_565
Cu0B Cu07 Na0W 101.24(12) 3_777 4_566
S00C Cu07 Cu06 124.39(12) . .
S00C Cu07 Cu08 51.29(11) . .
S00C Cu07 Cu0B 111.47(17) . 3_777
S00C Cu07 S00I 115.18(12) . .
S00C Cu07 Na0P 61.5(2) . 4_566
S00C Cu07 Na0R 61.9(2) . .
S00C Cu07 Na0S 124.64(19) . 1_565
S00C Cu07 Na0W 62.3(2) . 4_566
S00I Cu07 Cu06 52.38(12) . .
S00I Cu07 Cu08 126.30(13) . .
S00I Cu07 Cu0B 114.25(17) . 3_777
S00I Cu07 Na0P 62.1(2) . 4_566
S00I Cu07 Na0R 124.11(19) . .
S00I Cu07 Na0S 62.99(19) . 1_565
S00I Cu07 Na0W 65.7(2) . 4_566
S00K Cu07 Cu06 107.04(18) . .
S00K Cu07 Cu08 103.69(17) . .
S00K Cu07 Cu0B 62.60(10) . 3_777
S00K Cu07 S00C 118.9(2) . .
S00K Cu07 S00I 121.9(3) . .
S00K Cu07 Na0P 132.68(14) . 4_566
S00K Cu07 Na0R 69.34(18) . .
S00K Cu07 Na0S 69.97(18) . 1_565
S00K Cu07 Na0W 163.59(15) . 4_566
Na0R Cu07 Na0P 72.47(19) . 4_566
Na0R Cu07 Na0W 120.2(2) . 4_566
Na0S Cu07 Na0P 74.0(2) 1_565 4_566
Na0S Cu07 Na0R 74.95(16) 1_565 .
Na0S Cu07 Na0W 124.1(2) 1_565 4_566
Na0W Cu07 Na0P 63.37(14) 4_566 4_566
Cu05 Cu08 Cu07 90.13(7) 1_545 .
Cu05 Cu08 Cu0A 61.94(9) 1_545 1_545
Cu05 Cu08 Cu0B 114.95(9) 1_545 3_777
Cu05 Cu08 Na0O 133.5(3) 1_545 .
Cu05 Cu08 Na0U 66.66(18) 1_545 4_556
Cu05 Cu08 Cu0V 59.9(2) 1_545 .
Cu05 Cu08 Na0W 115.37(15) 1_545 4_566
Cu07 Cu08 Cu0A 67.44(9) . 1_545
Cu07 Cu08 Na0O 130.3(3) . .
Cu07 Cu08 Na0U 113.26(16) . 4_556
Cu07 Cu08 Cu0V 125.3(2) . .
Cu07 Cu08 Na0W 64.31(15) . 4_566
Cu0A Cu08 Na0O 146.31(7) 1_545 .
Cu0A Cu08 Na0U 128.6(2) 1_545 4_556
Cu0A Cu08 Na0W 131.70(17) 1_545 4_566
Cu0B Cu08 Cu05 117.00(14) 1_545 1_545
Cu0B Cu08 Cu07 55.57(9) 3_777 .
Cu0B Cu08 Cu07 117.89(14) 1_545 .
Cu0B Cu08 Cu0A 78.00(8) 1_545 1_545
Cu0B Cu08 Cu0A 54.39(10) 3_777 1_545
Cu0B Cu08 Cu0B 62.32(13) 1_545 3_777
Cu0B Cu08 Na0O 107.9(2) 3_777 .
Cu0B Cu08 Na0O 68.34(6) 1_545 .
Cu0B Cu08 Na0U 128.57(19) 1_545 4_556
Cu0B Cu08 Na0U 168.0(2) 3_777 4_556
Cu0B Cu08 Cu0V 94.60(19) 3_777 .
Cu0B Cu08 Cu0V 57.9(2) 1_545 .
Cu0B Cu08 Na0W 97.9(2) 3_777 4_566
Cu0B Cu08 Na0W 127.55(19) 1_545 4_566
S00C Cu08 Cu05 54.54(16) . 1_545
S00C Cu08 Cu07 53.52(17) . .
S00C Cu08 Cu0A 86.51(11) . 1_545
S00C Cu08 Cu0B 164.48(12) . 1_545
S00C Cu08 Cu0B 107.61(17) . 3_777
S00C Cu08 S00G 119.9(2) . 3_777
S00C Cu08 S00J 120.0(2) . .
S00C Cu08 Na0O 127.16(11) . .
S00C Cu08 Na0U 62.89(18) . 4_556
S00C Cu08 Cu0V 114.3(3) . .
S00C Cu08 Na0W 63.27(17) . 4_566
S00G Cu08 Cu05 166.19(15) 3_777 1_545
S00G Cu08 Cu07 77.65(16) 3_777 .
S00G Cu08 Cu0A 106.72(15) 3_777 1_545
S00G Cu08 Cu0B 52.60(13) 3_777 3_777
S00G Cu08 Cu0B 64.84(14) 3_777 1_545
S00G Cu08 Na0O 60.3(3) 3_777 .
S00G Cu08 Na0U 124.0(2) 3_777 4_556
S00G Cu08 Cu0V 122.6(2) 3_777 .
S00G Cu08 Na0W 65.16(19) 3_777 4_566
S00J Cu08 Cu05 79.63(17) . 1_545
S00J Cu08 Cu07 169.56(17) . .
S00J Cu08 Cu0A 105.42(16) . 1_545
S00J Cu08 Cu0B 127.31(12) . 3_777
S00J Cu08 Cu0B 66.08(15) . 1_545
S00J Cu08 S00G 112.28(11) . 3_777
S00J Cu08 Na0O 59.9(3) . .
S00J Cu08 Na0U 64.54(19) . 4_556
S00J Cu08 Cu0V 47.1(3) . .
S00J Cu08 Na0W 122.00(18) . 4_566
Na0U Cu08 Na0O 75.4(2) 4_556 .
Na0U Cu08 Na0W 71.47(16) 4_556 4_566
Cu0V Cu08 Cu0A 58.3(2) . 1_545
Cu0V Cu08 Na0O 100.5(3) . .
Cu0V Cu08 Na0U 96.2(3) . 4_556
Cu0V Cu08 Na0W 167.4(3) . 4_566
Na0W Cu08 Na0O 74.1(2) 4_566 .
Cu05 Cu09 Cu06 55.58(9) . .
Cu05 Cu09 Na0O 178.89(8) . 3_767
Cu05 Cu09 Na0S 59.42(17) . 1_565
Cu05 Cu09 Na0T 106.8(3) . 3_767
Cu05 Cu09 Na0U 104.94(18) . 1_565
Cu06 Cu09 Na0O 125.30(19) . 3_767
Cu06 Cu09 Na0S 85.32(12) . 1_565
Cu06 Cu09 Na0T 131.79(18) . 3_767
Cu06 Cu09 Na0U 146.11(13) . 1_565
Cu0B Cu09 Cu05 113.99(10) 3_777 .
Cu0B Cu09 Cu06 59.26(10) 3_777 .
Cu0B Cu09 Na0O 66.75(19) 3_777 3_767
Cu0B Cu09 Na0S 107.1(2) 3_777 1_565
Cu0B Cu09 Na0T 123.6(2) 3_777 3_767
Cu0B Cu09 Na0U 123.9(3) 3_777 1_565
Cu0B Cu09 Cu0X 70.99(8) 3_777 1_565
S00J Cu09 Cu05 122.76(18) 3_767 .
S00J Cu09 Cu06 90.56(11) 3_767 .
S00J Cu09 Cu0B 65.45(18) 3_767 3_777
S00J Cu09 Na0O 58.23(17) 3_767 3_767
S00J Cu09 Na0S 172.5(3) 3_767 1_565
S00J Cu09 Na0T 60.04(19) 3_767 3_767
S00J Cu09 Na0U 122.34(15) 3_767 1_565
S00J Cu09 Cu0V 60.2(3) 3_767 1_565
S00J Cu09 Cu0X 49.16(11) 3_767 1_565
S00K Cu09 Cu05 117.04(13) . .
S00K Cu09 Cu06 97.89(14) . .
S00K Cu09 Cu0B 62.49(14) . 3_777
S00K Cu09 S00J 111.7(2) . 3_767
S00K Cu09 Na0O 62.4(2) . 3_767
S00K Cu09 Na0S 62.8(2) . 1_565
S00K Cu09 Na0T 127.2(2) . 3_767
S00K Cu09 Na0U 64.4(2) . 1_565
S00K Cu09 Cu0V 151.7(3) . 1_565
S00K Cu09 Cu0X 132.98(15) . 1_565
S00L Cu09 Cu05 51.71(12) . .
S00L Cu09 Cu06 107.11(14) . .
S00L Cu09 Cu0B 165.06(14) . 3_777
S00L Cu09 S00J 124.0(2) . 3_767
S00L Cu09 S00K 117.43(14) . .
S00L Cu09 Na0O 127.5(2) . 3_767
S00L Cu09 Na0S 63.3(2) . 1_565
S00L Cu09 Na0T 69.4(2) . 3_767
S00L Cu09 Na0U 63.2(2) . 1_565
S00L Cu09 Cu0V 85.3(3) . 1_565
S00L Cu09 Cu0X 105.63(17) . 1_565
Na0O Cu09 Na0S 119.7(2) 3_767 1_565
Na0T Cu09 Na0O 73.1(2) 3_767 3_767
Na0T Cu09 Na0S 127.1(2) 3_767 1_565
Na0U Cu09 Na0O 73.96(17) 1_565 3_767
Na0U Cu09 Na0S 61.05(14) 1_565 1_565
Na0U Cu09 Na0T 77.60(17) 1_565 3_767
Cu0V Cu09 Cu05 62.6(2) 1_565 .
Cu0V Cu09 Cu06 57.3(2) 1_565 .
Cu0V Cu09 Cu0B 91.1(3) 1_565 3_777
Cu0V Cu09 Na0O 118.4(3) 1_565 3_767
Cu0V Cu09 Na0S 121.7(3) 1_565 1_565
Cu0V Cu09 Na0T 74.7(3) 1_565 3_767
Cu0V Cu09 Na0U 143.8(4) 1_565 1_565
Cu0V Cu09 Cu0X 20.4(3) 1_565 1_565
Cu0X Cu09 Cu05 75.50(8) 1_565 .
Cu0X Cu09 Cu06 49.55(6) 1_565 .
Cu0X Cu09 Na0O 105.58(8) 1_565 3_767
Cu0X Cu09 Na0S 129.96(14) 1_565 1_565
Cu0X Cu09 Na0T 83.99(11) 1_565 3_767
Cu0X Cu09 Na0U 160.9(2) 1_565 1_565
Cu05 Cu0A Na0O 176.80(13) . 3_777
Cu05 Cu0A Na0R 58.99(19) . 1_565
Cu05 Cu0A Na0T 106.0(3) . 3_767
Cu05 Cu0A Na0W 104.46(17) . 1_565
Cu08 Cu0A Cu05 56.94(9) 1_565 .
Cu08 Cu0A Na0O 126.2(2) 1_565 3_777
Cu08 Cu0A Na0R 87.55(11) 1_565 1_565
Cu08 Cu0A Na0T 131.07(19) 1_565 3_767
Cu08 Cu0A Na0W 147.31(13) 1_565 1_565
Cu0B Cu0A Cu05 115.89(10) 3_787 .
Cu0B Cu0A Cu08 60.37(10) 3_787 1_565
Cu0B Cu0A Na0O 66.9(2) 3_787 3_777
Cu0B Cu0A Na0R 107.6(2) 3_787 1_565
Cu0B Cu0A Na0T 124.6(2) 3_787 3_767
Cu0B Cu0A Cu0V 100.5(2) 3_787 1_565
Cu0B Cu0A Na0W 121.7(2) 3_787 1_565
S00G Cu0A Cu05 123.04(19) . .
S00G Cu0A Cu08 88.47(11) . 1_565
S00G Cu0A Cu0B 65.29(18) . 3_787
S00G Cu0A S00K 112.1(2) . 1_565
S00G Cu0A Na0O 59.14(17) . 3_777
S00G Cu0A Na0R 172.8(3) . 1_565
S00G Cu0A Na0T 61.84(18) . 3_767
S00G Cu0A Cu0V 64.8(3) . 1_565
S00G Cu0A Na0W 123.06(15) . 1_565
S00K Cu0A Cu05 117.12(13) 1_565 .
S00K Cu0A Cu08 100.07(15) 1_565 1_565
S00K Cu0A Cu0B 62.33(15) 1_565 3_787
S00K Cu0A Na0O 62.4(2) 1_565 3_777
S00K Cu0A Na0R 62.9(2) 1_565 1_565
S00K Cu0A Na0T 126.1(2) 1_565 3_767
S00K Cu0A Cu0V 160.0(2) 1_565 1_565
S00K Cu0A Na0W 62.4(2) 1_565 1_565
S00L Cu0A Cu05 51.08(12) . .
S00L Cu0A Cu08 107.83(16) . 1_565
S00L Cu0A Cu0B 165.31(13) . 3_787
S00L Cu0A S00G 125.9(2) . .
S00L Cu0A S00K 114.94(14) . 1_565
S00L Cu0A Na0O 125.9(2) . 3_777
S00L Cu0A Na0R 61.1(2) . 1_565
S00L Cu0A Na0T 69.4(2) . 3_767
S00L Cu0A Cu0V 78.9(3) . 1_565
S00L Cu0A Na0W 62.7(2) . 1_565
Na0O Cu0A Na0R 119.2(2) 3_777 1_565
Na0T Cu0A Na0O 72.7(2) 3_767 3_777
Na0T Cu0A Na0R 125.0(2) 3_767 1_565
Na0T Cu0A Na0W 77.30(16) 3_767 1_565
Cu0V Cu0A Cu05 59.1(2) 1_565 .
Cu0V Cu0A Cu08 60.8(2) 1_565 1_565
Cu0V Cu0A Na0O 122.6(2) 1_565 3_777
Cu0V Cu0A Na0R 118.0(3) 1_565 1_565
Cu0V Cu0A Na0T 71.2(3) 1_565 3_767
Cu0V Cu0A Na0W 136.9(3) 1_565 1_565
Na0W Cu0A Na0O 72.44(16) 1_565 3_777
Na0W Cu0A Na0R 60.14(14) 1_565 1_565
Cu07 Cu0B Cu06 60.19(10) 3_777 3_777
Cu07 Cu0B Cu08 62.67(10) 3_777 3_777
Cu07 Cu0B Cu09 74.37(11) 3_777 3_777
Cu07 Cu0B Cu0B 118.17(18) 3_777 3_787
Cu07 Cu0B S00G 126.7(2) 3_777 3_787
Cu07 Cu0B S00J 126.8(2) 3_777 1_565
Cu07 Cu0B Cu0V 112.8(3) 3_777 1_565
Cu08 Cu0B Cu06 88.92(8) 3_777 3_777
Cu08 Cu0B Cu06 119.44(14) 1_565 3_777
Cu08 Cu0B Cu07 179.5(2) 1_565 3_777
Cu08 Cu0B Cu08 117.68(13) 1_565 3_777
Cu08 Cu0B Cu09 105.27(14) 1_565 3_777
Cu08 Cu0B Cu0A 105.33(14) 1_565 3_787
Cu08 Cu0B Cu0B 55.50(12) 3_777 3_787
Cu08 Cu0B Cu0B 62.18(10) 1_565 3_787
Cu08 Cu0B S00G 53.75(13) 1_565 3_787
Cu08 Cu0B S00J 52.78(13) 1_565 1_565
Cu08 Cu0B Cu0V 66.8(2) 1_565 1_565
Cu09 Cu0B Cu06 67.77(12) 3_777 3_777
Cu09 Cu0B Cu08 137.03(10) 3_777 3_777
Cu09 Cu0B Cu0B 167.38(15) 3_777 3_787
Cu09 Cu0B S00G 124.79(13) 3_777 3_787
Cu09 Cu0B S00J 53.26(13) 3_777 1_565
Cu09 Cu0B Cu0V 72.4(3) 3_777 1_565
Cu0A Cu0B Cu06 135.01(10) 3_787 3_777
Cu0A Cu0B Cu07 75.06(11) 3_787 3_777
Cu0A Cu0B Cu08 65.23(12) 3_787 3_777
Cu0A Cu0B Cu09 105.97(9) 3_787 3_777
Cu0A Cu0B Cu0B 80.08(19) 3_787 3_787
Cu0A Cu0B S00G 52.53(13) 3_787 3_787
Cu0A Cu0B S00J 124.01(13) 3_787 1_565
Cu0A Cu0B Cu0V 170.6(2) 3_787 1_565
Cu0B Cu0B Cu06 116.02(12) 3_787 3_777
S00G Cu0B Cu06 53.80(16) . 3_777
S00G Cu0B Cu06 165.70(12) 3_787 3_777
S00G Cu0B Cu07 83.03(11) . 3_777
S00G Cu0B Cu08 84.80(18) 3_787 3_777
S00G Cu0B Cu08 96.95(11) . 1_565
S00G Cu0B Cu08 54.76(17) . 3_777
S00G Cu0B Cu09 121.0(2) . 3_777
S00G Cu0B Cu0A 119.7(2) . 3_787
S00G Cu0B Cu0B 50.15(13) 3_787 3_787
S00G Cu0B Cu0B 62.38(16) . 3_787
S00G Cu0B S00G 112.53(16) . 3_787
S00G Cu0B S00J 114.25(18) . 1_565
S00G Cu0B S00J 94.04(11) 3_787 1_565
S00G Cu0B S00K 136.37(13) . 3_777
S00G Cu0B Cu0V 67.8(3) . 1_565
S00J Cu0B Cu06 89.11(18) 1_565 3_777
S00J Cu0B Cu08 166.68(12) 1_565 3_777
S00J Cu0B Cu0B 114.14(14) 1_565 3_787
S00K Cu0B Cu06 97.97(16) 3_777 3_777
S00K Cu0B Cu07 53.35(9) 3_777 3_777
S00K Cu0B Cu08 98.05(16) 3_777 3_777
S00K Cu0B Cu08 126.68(11) 3_777 1_565
S00K Cu0B Cu09 53.41(17) 3_777 3_777
S00K Cu0B Cu0A 54.05(17) 3_777 3_787
S00K Cu0B Cu0B 134.1(3) 3_777 3_787
S00K Cu0B S00G 95.63(17) 3_777 3_787
S00K Cu0B S00J 95.26(17) 3_777 1_565
S00K Cu0B Cu0V 125.7(4) 3_777 1_565
Cu0V Cu0B Cu06 53.5(2) 1_565 3_777
Cu0V Cu0B Cu08 122.5(2) 1_565 3_777
Cu0V Cu0B Cu0B 99.8(3) 1_565 3_787
Cu0V Cu0B S00G 120.4(2) 1_565 3_787
Cu0V Cu0B S00J 47.4(3) 1_565 1_565
Cu05 S00C Na0P 147.0(2) 1_545 4_566
Cu05 S00C Na0Q 76.9(2) 1_545 4_556
Cu05 S00C Na0R 73.6(3) 1_545 .
Cu05 S00C Na0U 75.8(3) 1_545 4_556
Cu05 S00C Na0W 142.7(2) 1_545 4_566
Cu07 S00C Cu05 114.94(14) . 1_545
Cu07 S00C Na0P 74.1(2) . 4_566
Cu07 S00C Na0Q 145.8(2) . 4_556
Cu07 S00C Na0R 72.3(3) . .
Cu07 S00C Na0U 142.5(2) . 4_556
Cu07 S00C Na0W 73.3(2) . 4_566
Cu08 S00C Cu05 73.96(16) . 1_545
Cu08 S00C Cu07 75.18(17) . .
Cu08 S00C Na0P 137.3(3) . 4_566
Cu08 S00C Na0Q 138.0(3) . 4_556
Cu08 S00C Na0R 117.36(17) . .
Cu08 S00C Na0U 73.87(17) . 4_556
Cu08 S00C Na0W 73.59(17) . 4_566
Na0P S00C Na0U 117.5(2) 4_566 4_556
Na0P S00C Na0W 69.7(2) 4_566 4_566
Na0Q S00C Na0P 79.93(16) 4_556 4_566
Na0Q S00C Na0U 70.1(2) 4_556 4_556
Na0Q S00C Na0W 117.8(2) 4_556 4_566
Na0R S00C Na0P 80.0(2) . 4_566
Na0R S00C Na0Q 81.6(2) . 4_556
Na0R S00C Na0U 142.2(4) . 4_556
Na0R S00C Na0W 139.1(4) . 4_566
Na0U S00C Na0W 77.92(18) 4_556 4_566
Cu02 S00D Cu04 115.74(14) . 1_565
Cu02 S00D Na0M 74.3(2) . 4
Cu02 S00D Na0N 142.9(2) . 4_565
Cu02 S00D Na0P 75.5(2) . .
Cu02 S00D Na0R 146.7(2) . 4_565
Cu02 S00D Na0S 76.5(2) . 4
Cu03 S00D Cu02 74.47(16) . .
Cu03 S00D Cu04 74.65(16) . 1_565
Cu03 S00D Na0M 71.92(17) . 4
Cu03 S00D Na0N 73.27(17) . 4_565
Cu03 S00D Na0P 120.23(16) . .
Cu03 S00D Na0R 138.0(3) . 4_565
Cu03 S00D Na0S 137.4(3) . 4
Cu04 S00D Na0M 140.6(2) 1_565 4
Cu04 S00D Na0N 72.2(2) 1_565 4_565
Cu04 S00D Na0P 74.0(2) 1_565 .
Cu04 S00D Na0R 76.2(3) 1_565 4_565
Cu04 S00D Na0S 147.2(2) 1_565 4
Na0M S00D Na0N 78.69(17) 4 4_565
Na0M S00D Na0R 117.5(2) 4 4_565
Na0N S00D Na0R 69.4(2) 4_565 4_565
Na0P S00D Na0M 142.3(4) . 4
Na0P S00D Na0N 137.9(4) . 4_565
Na0P S00D Na0R 78.8(2) . 4_565
Na0P S00D Na0S 80.8(2) . 4
Na0S S00D Na0M 70.6(2) 4 4
Na0S S00D Na0N 117.6(2) 4 4_565
Na0S S00D Na0R 78.72(16) 4 4_565
Cu01 S00E Cu02 73.23(16) . 2_655
Cu01 S00E Cu04 72.67(15) . 2_655
Cu01 S00E Na0M 72.27(17) . 3_656
Cu01 S00E Na0N 72.97(17) . 3_656
Cu01 S00E Na0Q 118.07(16) . 2_655
Cu01 S00E Na0R 136.2(3) . 3_656
Cu01 S00E Na0S 134.7(3) . 3_656
Cu01 S00E Na00 115.53(16) . 3_656
Cu02 S00E Na0M 72.3(2) 2_655 3_656
Cu02 S00E Na0N 143.53(19) 2_655 3_656
Cu02 S00E Na0Q 73.6(2) 2_655 2_655
Cu02 S00E Na0R 147.8(2) 2_655 3_656
Cu02 S00E Na0S 74.4(2) 2_655 3_656
Cu02 S00E Na00 124.9(3) 2_655 3_656
Cu04 S00E Cu02 110.38(13) 2_655 2_655
Cu04 S00E Na0M 142.10(19) 2_655 3_656
Cu04 S00E Na0N 71.6(2) 2_655 3_656
Cu04 S00E Na0Q 72.2(2) 2_655 2_655
Cu04 S00E Na0R 75.9(2) 2_655 3_656
Cu04 S00E Na0S 149.7(2) 2_655 3_656
Cu04 S00E Na00 124.3(3) 2_655 3_656
Na0M S00E Na00 61.52(19) 3_656 3_656
Na0N S00E Na0M 84.71(16) 3_656 3_656
Na0N S00E Na0S 123.1(2) 3_656 3_656
Na0N S00E Na00 60.95(19) 3_656 3_656
Na0Q S00E Na0M 138.9(4) 2_655 3_656
Na0Q S00E Na0N 136.0(4) 2_655 3_656
Na0Q S00E Na0R 79.0(2) 2_655 3_656
Na0Q S00E Na0S 81.1(2) 2_655 3_656
Na0Q S00E Na00 126.38(17) 2_655 3_656
Na0R S00E Na0M 122.8(2) 3_656 3_656
Na0R S00E Na0N 68.6(2) 3_656 3_656
Na0R S00E Na0S 85.20(16) 3_656 3_656
Na0R S00E Na00 61.3(2) 3_656 3_656
Na0S S00E Na0M 68.2(2) 3_656 3_656
Na0S S00E Na00 62.2(2) 3_656 3_656
Cu01 S00F Cu03 115.96(15) . 2_645
Cu01 S00F Na0M 76.1(3) . .
Cu01 S00F Na0N 74.9(2) . 3_656
Cu01 S00F Na0N 146.7(2) . 1_545
Cu01 S00F Na0P 143.3(2) . 1_545
Cu01 S00F Na0Q 74.8(2) . .
Cu03 S00F Na0M 146.9(2) 2_645 .
Cu03 S00F Na0N 74.0(2) 2_645 3_656
Cu03 S00F Na0N 75.1(2) 2_645 1_545
Cu03 S00F Na0P 72.9(2) 2_645 1_545
Cu03 S00F Na0Q 141.0(2) 2_645 .
Cu04 S00F Cu01 75.45(16) . .
Cu04 S00F Cu03 75.39(18) . 2_645
Cu04 S00F Na0M 137.1(3) . .
Cu04 S00F Na0N 136.9(3) . 1_545
Cu04 S00F Na0N 121.29(18) . 3_656
Cu04 S00F Na0P 72.74(18) . 1_545
Cu04 S00F Na0Q 71.49(17) . .
Na0M S00F Na0N 80.5(2) . 3_656
Na0M S00F Na0N 79.60(17) . 1_545
Na0M S00F Na0P 117.1(2) . 1_545
Na0M S00F Na0Q 70.5(2) . .
Na0N S00F Na0N 78.9(2) 3_656 1_545
Na0N S00F Na0P 69.0(2) 1_545 1_545
Na0N S00F Na0P 138.5(4) 3_656 1_545
Na0N S00F Na0Q 142.1(4) 3_656 .
Na0N S00F Na0Q 117.6(2) 1_545 .
Na0Q S00F Na0P 78.03(16) . 1_545
Cu06 S00G Cu08 111.39(13) 3_777 3_777
Cu06 S00G Cu0B 141.02(16) 3_777 3_787
Cu06 S00G Na0O 145.4(2) 3_777 3_777
Cu06 S00G Na0T 75.2(3) 3_777 3_767
Cu06 S00G Cu0V 56.5(3) 3_777 1_565
Cu06 S00G Na0W 70.9(2) 3_777 2_766
Cu08 S00G Cu0B 61.41(17) 3_777 3_787
Cu08 S00G Na0O 75.1(3) 3_777 3_777
Cu08 S00G Na0T 148.0(2) 3_777 3_767
Cu08 S00G Cu0V 134.9(3) 3_777 1_565
Cu08 S00G Na0W 70.1(2) 3_777 2_766
Cu0A S00G Cu06 119.5(3) . 3_777
Cu0A S00G Cu08 122.3(3) . 3_777
Cu0A S00G Cu0B 62.19(14) . 3_787
Cu0A S00G Na0O 77.99(16) . 3_777
Cu0A S00G Na0T 73.83(16) . 3_767
Cu0A S00G Cu0V 66.2(3) . 1_565
Cu0A S00G Na0W 150.70(18) . 2_766
Cu0B S00G Cu06 73.84(16) . 3_777
Cu0B S00G Cu08 72.64(16) . 3_777
Cu0B S00G Cu0A 96.48(14) . .
Cu0B S00G Cu0B 67.47(16) . 3_787
Cu0B S00G Na0O 72.9(2) 3_787 3_777
Cu0B S00G Na0O 137.4(4) . 3_777
Cu0B S00G Na0T 132.94(18) 3_787 3_767
Cu0B S00G Na0T 136.9(4) . 3_767
Cu0B S00G Cu0V 62.2(3) . 1_565
Cu0B S00G Cu0V 99.6(2) 3_787 1_565
Cu0B S00G Na0W 112.81(17) . 2_766
Cu0B S00G Na0W 128.9(3) 3_787 2_766
Na0O S00G Na0W 80.6(2) 3_777 2_766
Na0T S00G Na0O 82.8(2) 3_767 3_777
Na0T S00G Na0W 83.9(2) 3_767 2_766
Cu0V S00G Na0O 142.0(3) 1_565 3_777
Cu0V S00G Na0T 75.8(3) 1_565 3_767
Cu0V S00G Na0W 126.7(4) 1_565 2_766
Cu01 S00H Na0M 73.8(2) . .
Cu01 S00H Na0M 73.7(2) . 3_656
Cu01 S00H Na0N 147.8(2) . .
Cu01 S00H Na0P 144.2(2) . .
Cu01 S00H Na0Q 73.1(2) . .
Cu01 S00H Na00 124.5(3) . .
Cu02 S00H Cu01 74.22(17) . .
Cu02 S00H Cu03 73.71(16) . 2_655
Cu02 S00H Na0M 119.25(17) . 3_656
Cu02 S00H Na0M 134.1(3) . .
Cu02 S00H Na0N 135.5(3) . .
Cu02 S00H Na0P 72.66(17) . .
Cu02 S00H Na0Q 71.51(18) . .
Cu02 S00H Na00 114.61(15) . .
Cu03 S00H Cu01 110.90(13) 2_655 .
Cu03 S00H Na0M 71.8(2) 2_655 3_656
Cu03 S00H Na0M 149.6(2) 2_655 .
Cu03 S00H Na0N 75.2(3) 2_655 .
Cu03 S00H Na0P 72.0(2) 2_655 .
Cu03 S00H Na0Q 142.2(2) 2_655 .
Cu03 S00H Na00 124.4(3) 2_655 .
Na0M S00H Na0M 81.5(2) 3_656 .
Na0M S00H Na0N 78.9(2) 3_656 .
Na0M S00H Na0P 135.8(3) 3_656 .
Na0M S00H Na0P 122.6(2) . .
Na0M S00H Na0Q 139.9(3) 3_656 .
Na0M S00H Na0Q 68.2(2) . .
Na0M S00H Na00 126.11(17) 3_656 .
Na0M S00H Na00 61.86(19) . .
Na0N S00H Na0M 85.86(17) . .
Na0N S00H Na0P 68.0(2) . .
Na0N S00H Na0Q 122.3(2) . .
Na0N S00H Na00 61.5(2) . .
Na0P S00H Na0Q 83.87(16) . .
Na0P S00H Na00 60.8(2) . .
Na0Q S00H Na00 60.86(19) . .
Cu05 S00I Na0P 150.0(2) . 4_566
Cu05 S00I Na0Q 75.8(2) . 4_566
Cu05 S00I Na0S 73.2(2) . 1_565
Cu05 S00I Na0U 73.8(2) . 4_566
Cu05 S00I Na0W 142.35(19) . 4_566
Cu05 S00I Na00 126.5(3) . 4_566
Cu06 S00I Cu05 72.95(16) . .
Cu06 S00I Cu07 72.48(16) . .
Cu06 S00I Na0P 133.3(3) . 4_566
Cu06 S00I Na0Q 135.3(3) . 4_566
Cu06 S00I Na0S 116.26(17) . 1_565
Cu06 S00I Na0U 72.73(17) . 4_566
Cu06 S00I Na0W 71.51(18) . 4_566
Cu06 S00I Na00 115.69(16) . 4_566
Cu07 S00I Cu05 109.65(14) . .
Cu07 S00I Na0P 73.6(2) . 4_566
Cu07 S00I Na0Q 149.6(2) . 4_566
Cu07 S00I Na0S 70.6(2) . 1_565
Cu07 S00I Na0U 142.0(2) . 4_566
Cu07 S00I Na0W 70.7(2) . 4_566
Cu07 S00I Na00 123.5(3) . 4_566
Na0P S00I Na0U 122.9(2) 4_566 4_566
Na0P S00I Na0W 67.6(2) 4_566 4_566
Na0P S00I Na00 61.6(2) 4_566 4_566
Na0Q S00I Na0P 87.30(16) 4_566 4_566
Na0Q S00I Na0U 68.4(2) 4_566 4_566
Na0Q S00I Na0W 123.9(2) 4_566 4_566
Na0Q S00I Na00 62.1(2) 4_566 4_566
Na0S S00I Na0P 80.4(2) 1_565 4_566
Na0S S00I Na0Q 83.2(2) 1_565 4_566
Na0S S00I Na0U 140.6(4) 1_565 4_566
Na0S S00I Na0W 135.1(4) 1_565 4_566
Na0S S00I Na00 127.93(18) 1_565 4_566
Na0U S00I Na0W 84.17(16) 4_566 4_566
Na0U S00I Na00 61.36(19) 4_566 4_566
Na0W S00I Na00 61.8(2) 4_566 4_566
Cu06 S00J Cu0B 138.07(16) 1_545 1_545
Cu06 S00J Na0O 148.5(2) 1_545 .
Cu06 S00J Na0T 75.8(3) 1_545 .
Cu06 S00J Na0U 71.1(2) 1_545 4_556
Cu06 S00J Cu0V 60.9(3) 1_545 3_757
Cu08 S00J Cu06 110.42(14) . 1_545
Cu08 S00J Cu09 121.4(3) . 3_767
Cu08 S00J Cu0B 61.14(17) . 1_545
Cu08 S00J Na0O 75.9(3) . .
Cu08 S00J Na0T 150.7(2) . .
Cu08 S00J Na0U 70.9(2) . 4_556
Cu08 S00J Cu0V 126.7(3) . 3_757
Cu09 S00J Cu06 119.0(3) 3_767 1_545
Cu09 S00J Cu0B 61.28(14) 3_767 1_545
Cu09 S00J Na0O 77.90(16) 3_767 .
Cu09 S00J Na0T 74.32(15) 3_767 .
Cu09 S00J Na0U 152.98(18) 3_767 4_556
Cu09 S00J Cu0V 63.1(3) 3_767 3_757
Cu0B S00J Na0O 72.8(2) 1_545 .
Cu0B S00J Na0T 133.20(18) 1_545 .
Cu0B S00J Na0U 130.0(3) 1_545 4_556
Na0O S00J Na0U 82.9(2) . 4_556
Na0T S00J Na0O 84.7(2) . .
Na0T S00J Na0U 85.2(2) . 4_556
Cu0V S00J Cu06 72.6(3) . 1_545
Cu0V S00J Cu08 79.8(3) . .
Cu0V S00J Cu09 86.5(3) . 3_767
Cu0V S00J Cu0B 65.5(3) . 1_545
Cu0V S00J Cu0B 90.3(2) 3_757 1_545
Cu0V S00J Na0O 138.0(4) . .
Cu0V S00J Na0O 140.8(3) 3_757 .
Cu0V S00J Na0T 128.2(4) . .
Cu0V S00J Na0T 81.9(4) 3_757 .
Cu0V S00J Na0U 132.0(4) 3_757 4_556
Cu0V S00J Na0U 120.3(3) . 4_556
Cu0V S00J Cu0V 47.0(5) . 3_757
Cu0X S00J Cu06 64.22(16) . 1_545
Cu0X S00J Cu08 104.94(17) . .
Cu0X S00J Cu09 72.88(13) . 3_767
Cu0X S00J Cu0B 78.04(13) . 1_545
Cu0X S00J Na0O 146.0(2) . .
Cu0X S00J Na0T 103.4(3) . .
Cu0X S00J Na0U 130.2(3) . 4_556
Cu0X S00J Cu0V 21.8(3) . 3_757
Cu0X S00J Cu0V 25.2(3) . .
Cu07 S00K Cu09 85.3(2) . .
Cu07 S00K Cu0A 85.44(19) . 1_545
Cu07 S00K Cu0B 64.04(10) . 3_777
Cu07 S00K Na0O 135.99(14) . 3_767
Cu07 S00K Na0R 67.04(17) . .
Cu07 S00K Na0S 65.92(17) . 1_565
Cu07 S00K Na0U 130.4(3) . 1_565
Cu07 S00K Na0W 131.8(3) . .
Cu09 S00K Cu0A 125.52(15) . 1_545
Cu09 S00K Cu0B 64.10(15) . 3_777
Cu09 S00K Na0O 75.5(3) . 3_767
Cu09 S00K Na0R 144.6(2) . .
Cu09 S00K Na0S 75.8(2) . 1_565
Cu09 S00K Na0U 71.7(2) . 1_565
Cu09 S00K Na0W 142.1(2) . .
Cu0A S00K Cu0B 63.62(16) 1_545 3_777
Cu0A S00K Na0O 75.0(3) 1_545 3_767
Cu0A S00K Na0R 75.6(3) 1_545 .
Cu0A S00K Na0S 143.7(2) 1_545 1_565
Cu0A S00K Na0U 143.6(2) 1_545 1_565
Cu0A S00K Na0W 73.3(2) 1_545 .
Cu0B S00K Na0O 71.95(9) 3_777 3_767
Cu0B S00K Na0R 117.0(2) 3_777 .
Cu0B S00K Na0S 116.8(2) 3_777 1_565
Cu0B S00K Na0U 132.2(3) 3_777 1_565
Cu0B S00K Na0W 133.0(3) 3_777 .
Na0O S00K Na0R 139.8(4) 3_767 .
Na0O S00K Na0S 141.2(4) 3_767 1_565
Na0S S00K Na0R 73.03(16) 1_565 .
Na0U S00K Na0O 80.4(2) 1_565 3_767
Na0U S00K Na0R 109.3(2) 1_565 .
Na0U S00K Na0S 66.1(2) 1_565 1_565
Na0W S00K Na0O 79.8(2) . 3_767
Na0W S00K Na0R 65.9(2) . .
Na0W S00K Na0S 108.8(2) . 1_565
Na0W S00K Na0U 76.19(17) . 1_565
Cu05 S00L Na0R 70.29(18) . 1_565
Cu05 S00L Na0S 68.83(18) . 1_565
Cu05 S00L Na0T 123.93(13) . 3_767
Cu05 S00L Na0U 131.5(3) . 1_565
Cu05 S00L Na0W 133.3(3) . 1_565
Cu05 S00L Na00 110.42(15) . 1_565
Cu09 S00L Cu05 78.07(18) . .
Cu09 S00L Cu0A 106.84(14) . .
Cu09 S00L Na0R 146.4(2) . 1_565
Cu09 S00L Na0S 76.4(2) . 1_565
Cu09 S00L Na0T 69.2(3) . 3_767
Cu09 S00L Na0U 73.7(3) . 1_565
Cu09 S00L Na0W 146.5(2) . 1_565
Cu09 S00L Na00 125.6(3) . 1_565
Cu0A S00L Cu05 79.15(17) . .
Cu0A S00L Na0R 78.3(3) . 1_565
Cu0A S00L Na0S 146.5(2) . 1_565
Cu0A S00L Na0T 69.1(3) . 3_767
Cu0A S00L Na0U 146.7(2) . 1_565
Cu0A S00L Na0W 74.4(2) . 1_565
Cu0A S00L Na00 127.6(3) . 1_565
Na0R S00L Na0S 81.88(16) 1_565 1_565
Na0R S00L Na0T 139.3(4) 1_565 3_767
Na0R S00L Na00 59.5(2) 1_565 1_565
Na0S S00L Na0T 138.0(4) 1_565 3_767
Na0S S00L Na00 59.72(19) 1_565 1_565
Na0U S00L Na0R 120.2(2) 1_565 1_565
Na0U S00L Na0S 66.7(2) 1_565 1_565
Na0U S00L Na0T 80.8(3) 1_565 3_767
Na0U S00L Na0W 87.34(17) 1_565 1_565
Na0U S00L Na00 60.8(2) 1_565 1_565
Na0W S00L Na0R 67.1(2) 1_565 1_565
Na0W S00L Na0S 121.5(2) 1_565 1_565
Na0W S00L Na0T 80.9(3) 1_565 3_767
Na0W S00L Na00 61.8(2) 1_565 1_565
Na00 S00L Na0T 125.63(14) 1_565 3_767
Cu01 Na0M Cu01 106.1(2) 3_656 .
Cu01 Na0M Cu02 51.50(12) 3_656 4_556
Cu01 Na0M Na0S 148.1(2) . .
Cu01 Na0M Na0S 96.9(2) 3_656 .
Cu02 Na0M Cu01 151.96(19) 4_556 .
Cu02 Na0M Na0S 59.56(14) 4_556 .
Cu03 Na0M Cu01 74.72(13) 4_556 3_656
Cu03 Na0M Cu01 109.8(2) 4_556 .
Cu03 Na0M Cu02 52.65(12) 4_556 4_556
Cu03 Na0M Na0S 97.2(2) 4_556 .
Cu03 Na0M Na00 151.5(2) 4_556 .
S00D Na0M Cu01 93.98(18) 4_556 3_656
S00D Na0M Cu01 142.2(3) 4_556 .
S00D Na0M Cu02 44.17(14) 4_556 4_556
S00D Na0M Cu03 44.93(14) 4_556 4_556
S00D Na0M S00E 81.51(16) 4_556 3_656
S00D Na0M S00H 173.0(3) 4_556 .
S00D Na0M S00H 86.3(2) 4_556 3_656
S00D Na0M Na0S 54.4(2) 4_556 .
S00D Na0M Na00 112.3(2) 4_556 .
S00E Na0M Cu01 43.78(13) 3_656 3_656
S00E Na0M Cu01 134.6(4) 3_656 .
S00E Na0M Cu02 44.10(14) 3_656 4_556
S00E Na0M Cu03 94.87(17) 3_656 4_556
S00E Na0M Na0S 55.7(2) 3_656 .
S00E Na0M Na00 60.6(2) 3_656 .
S00F Na0M Cu01 43.92(14) . .
S00F Na0M Cu01 140.9(2) . 3_656
S00F Na0M Cu02 141.4(4) . 4_556
S00F Na0M Cu03 91.6(3) . 4_556
S00F Na0M S00D 101.7(3) . 4_556
S00F Na0M S00E 173.2(3) . 3_656
S00F Na0M S00H 100.6(2) . 3_656
S00F Na0M S00H 82.46(17) . .
S00F Na0M Na0S 121.4(3) . .
S00F Na0M Na00 112.6(2) . .
S00H Na0M Cu01 43.81(14) . .
S00H Na0M Cu01 44.54(15) 3_656 3_656
S00H Na0M Cu01 86.1(3) . 3_656
S00H Na0M Cu01 86.22(15) 3_656 .
S00H Na0M Cu02 65.96(13) 3_656 4_556
S00H Na0M Cu02 133.7(4) . 4_556
S00H Na0M Cu03 141.3(2) . 4_556
S00H Na0M Cu03 44.89(15) 3_656 4_556
S00H Na0M S00E 85.5(2) 3_656 3_656
S00H Na0M S00E 93.8(3) . 3_656
S00H Na0M S00H 98.5(2) 3_656 .
S00H Na0M Na0S 125.5(2) 3_656 .
S00H Na0M Na0S 118.6(3) . .
S00H Na0M Na00 136.4(4) 3_656 .
S00H Na0M Na00 60.7(2) . .
Na00 Na0M Cu01 93.5(3) . 3_656
Na00 Na0M Cu01 98.3(2) . .
Na00 Na0M Cu02 99.6(2) . 4_556
Na00 Na0M Na0S 57.9(2) . .
O010 Na0M Cu01 104.3(3) . .
O010 Na0M Cu01 130.0(4) . 3_656
O010 Na0M Cu02 103.5(3) . 4_556
O010 Na0M Cu03 128.6(4) . 4_556
O010 Na0M S00D 85.1(3) . 4_556
O010 Na0M S00E 87.1(3) . 3_656
O010 Na0M S00F 87.2(3) . .
O010 Na0M S00H 169.5(3) . 3_656
O010 Na0M S00H 89.5(3) . .
O010 Na0M Na0S 44.0(3) . .
O010 Na0M Na00 43.3(3) . .
Cu01 Na0N Cu03 107.1(2) 3_656 2_655
Cu01 Na0N Na0P 140.5(4) 3_656 .
Cu03 Na0N Cu01 76.26(13) 4_566 3_656
Cu03 Na0N Cu03 109.6(2) 4_566 2_655
Cu03 Na0N Na0P 141.6(4) 4_566 .
Cu03 Na0N Na0P 57.89(13) 2_655 .
Cu04 Na0N Cu01 51.25(13) 4_556 3_656
Cu04 Na0N Cu03 52.78(12) 4_556 4_566
Cu04 Na0N Cu03 152.00(19) 4_556 2_655
Cu04 Na0N Na0P 149.9(2) 4_556 .
S00D Na0N Cu01 94.52(18) 4_566 3_656
S00D Na0N Cu03 140.9(4) 4_566 2_655
S00D Na0N Cu03 44.04(13) 4_566 4_566
S00D Na0N Cu04 44.81(14) 4_566 4_556
S00D Na0N S00E 81.93(16) 4_566 3_656
S00D Na0N Na0P 120.3(3) 4_566 .
S00D Na0N Na00 112.7(2) 4_566 .
S00E Na0N Cu01 43.78(15) 3_656 3_656
S00E Na0N Cu03 135.7(4) 3_656 2_655
S00E Na0N Cu03 95.70(18) 3_656 4_566
S00E Na0N Cu04 44.33(15) 3_656 4_556
S00E Na0N Na0P 118.6(3) 3_656 .
S00E Na0N Na00 61.2(2) 3_656 .
S00F Na0N Cu01 44.16(16) 3_656 3_656
S00F Na0N Cu01 141.0(2) 1_565 3_656
S00F Na0N Cu03 89.2(3) 1_565 4_566
S00F Na0N Cu03 44.11(15) 1_565 2_655
S00F Na0N Cu03 88.57(16) 3_656 2_655
S00F Na0N Cu03 44.95(16) 3_656 4_566
S00F Na0N Cu04 139.6(4) 1_565 4_556
S00F Na0N Cu04 63.57(13) 3_656 4_556
S00F Na0N S00D 99.7(4) 1_565 4_566
S00F Na0N S00D 84.8(2) 3_656 4_566
S00F Na0N S00E 174.3(2) 1_565 3_656
S00F Na0N S00E 84.5(2) 3_656 3_656
S00F Na0N S00F 101.1(2) 3_656 1_565
S00F Na0N S00H 83.02(17) 1_565 .
S00F Na0N S00H 99.8(3) 3_656 .
S00F Na0N Na0P 55.9(2) 1_565 .
S00F Na0N Na0P 146.5(2) 3_656 .
S00F Na0N Na00 113.2(2) 1_565 .
S00F Na0N Na00 137.0(4) 3_656 .
S00H Na0N Cu01 86.4(3) . 3_656
S00H Na0N Cu03 141.6(2) . 4_566
S00H Na0N Cu03 43.46(14) . 2_655
S00H Na0N Cu04 134.4(4) . 4_556
S00H Na0N S00D 174.2(3) . 4_566
S00H Na0N S00E 94.9(4) . 3_656
S00H Na0N Na0P 57.1(2) . .
S00H Na0N Na00 61.5(2) . .
Na00 Na0N Cu01 93.9(3) . 3_656
Na00 Na0N Cu03 98.2(2) . 2_655
Na00 Na0N Cu03 152.1(2) . 4_566
Na00 Na0N Cu04 100.7(3) . 4_556
Na00 Na0N Na0P 57.4(2) . .
O00Z Na0N Cu01 129.9(5) . 3_656
O00Z Na0N Cu03 127.9(5) . 4_566
O00Z Na0N Cu03 103.4(3) . 2_655
O00Z Na0N Cu04 104.5(3) . 4_556
O00Z Na0N S00D 85.5(4) . 4_566
O00Z Na0N S00E 87.1(4) . 3_656
O00Z Na0N S00F 87.6(4) . 1_565
O00Z Na0N S00F 168.0(3) . 3_656
O00Z Na0N S00H 89.5(4) . .
O00Z Na0N Na0P 45.5(3) . .
O00Z Na0N Na00 42.6(5) . .
Cu08 Na0O Cu08 178.6(6) . 2_757
Cu08 Na0O Cu0A 76.98(15) 2_757 4_576
Cu08 Na0O Cu0A 76.98(15) . 3_777
Cu08 Na0O Cu0A 103.9(2) . 4_576
Cu08 Na0O Cu0A 103.9(2) 2_757 3_777
Cu08 Na0O Cu0B 46.07(5) . 1_545
Cu08 Na0O Cu0B 133.92(5) 2_757 1_545
Cu08 Na0O Cu0B 133.92(5) . 2_747
Cu08 Na0O Cu0B 46.07(5) 2_757 2_747
Cu0A Na0O Cu0A 103.8(5) 3_777 4_576
Cu0B Na0O Cu0A 45.68(11) 1_545 3_777
Cu0B Na0O Cu0A 45.68(11) 2_747 4_576
Cu0B Na0O Cu0A 135.0(4) 1_545 4_576
Cu0B Na0O Cu0A 135.0(4) 2_747 3_777
Cu0B Na0O Cu0B 179.2(6) 2_747 1_545
S00G Na0O Cu08 44.58(14) 3_777 .
S00G Na0O Cu08 136.8(5) 4_576 .
S00G Na0O Cu08 136.8(5) 3_777 2_757
S00G Na0O Cu08 44.58(13) 4_576 2_757
S00G Na0O Cu0A 85.2(4) 4_576 3_777
S00G Na0O Cu0A 85.2(4) 3_777 4_576
S00G Na0O Cu0A 42.86(17) 4_576 4_576
S00G Na0O Cu0A 42.86(17) 3_777 3_777
S00G Na0O Cu0B 49.77(13) 3_777 1_545
S00G Na0O Cu0B 130.9(4) 4_576 1_545
S00G Na0O Cu0B 49.77(14) 4_576 2_747
S00G Na0O Cu0B 130.9(4) 3_777 2_747
S00G Na0O S00G 97.2(5) 4_576 3_777
S00G Na0O S00K 80.3(2) 4_576 4_566
S00G Na0O S00K 99.9(3) 4_576 3_767
S00G Na0O S00K 80.3(2) 3_777 3_767
S00G Na0O S00K 99.9(3) 3_777 4_566
S00J Na0O Cu08 44.21(14) 2_757 2_757
S00J Na0O Cu08 134.4(5) . 2_757
S00J Na0O Cu08 44.21(14) . .
S00J Na0O Cu08 134.4(5) 2_757 .
S00J Na0O Cu0A 136.81(9) . 4_576
S00J Na0O Cu0A 136.81(9) 2_757 3_777
S00J Na0O Cu0A 96.26(11) 2_757 4_576
S00J Na0O Cu0A 96.26(11) . 3_777
S00J Na0O Cu0B 128.7(4) . 2_747
S00J Na0O Cu0B 128.7(4) 2_757 1_545
S00J Na0O Cu0B 50.58(14) 2_757 2_747
S00J Na0O Cu0B 50.58(14) . 1_545
S00J Na0O S00G 178.5(5) 2_757 3_777
S00J Na0O S00G 84.16(9) . 3_777
S00J Na0O S00G 84.16(9) 2_757 4_576
S00J Na0O S00G 178.5(5) . 4_576
S00J Na0O S00J 94.5(5) 2_757 .
S00J Na0O S00K 81.0(2) . 3_767
S00J Na0O S00K 81.0(2) 2_757 4_566
S00J Na0O S00K 98.8(3) . 4_566
S00J Na0O S00K 98.8(3) 2_757 3_767
S00K Na0O Cu08 86.97(7) 3_767 2_757
S00K Na0O Cu08 93.03(7) 4_566 2_757
S00K Na0O Cu08 86.97(7) 4_566 .
S00K Na0O Cu08 93.03(7) 3_767 .
S00K Na0O Cu0A 42.57(16) 4_566 4_576
S00K Na0O Cu0A 42.57(15) 3_767 3_777
S00K Na0O Cu0A 137.7(5) 3_767 4_576
S00K Na0O Cu0A 137.7(5) 4_566 3_777
S00K Na0O Cu0B 46.97(7) 3_767 1_545
S00K Na0O Cu0B 133.03(7) 3_767 2_747
S00K Na0O Cu0B 133.03(7) 4_566 1_545
S00K Na0O Cu0B 46.97(7) 4_566 2_747
S00K Na0O S00K 179.7(7) 4_566 3_767
Cu02 Na0P Na0N 96.2(2) . .
Cu03 Na0P Cu02 51.35(12) 2_655 .
Cu03 Na0P Cu07 151.4(2) 2_655 4_565
Cu03 Na0P Na0N 59.67(13) 2_655 .
Cu04 Na0P Cu02 76.29(12) 1_565 .
Cu04 Na0P Cu03 53.13(12) 1_565 2_655
Cu04 Na0P Cu07 109.2(2) 1_565 4_565
Cu04 Na0P Na0N 97.2(2) 1_565 .
Cu07 Na0P Cu02 106.2(2) 4_565 .
Cu07 Na0P Na0N 148.5(2) 4_565 .
S00C Na0P Cu02 140.8(2) 4_565 .
S00C Na0P Cu03 140.1(4) 4_565 2_655
S00C Na0P Cu04 89.4(3) 4_565 1_565
S00C Na0P Cu07 44.34(14) 4_565 4_565
S00C Na0P S00F 100.4(4) 4_565 1_565
S00C Na0P S00H 174.8(2) 4_565 .
S00C Na0P S00I 84.05(15) 4_565 4_565
S00C Na0P Na0N 122.0(3) 4_565 .
S00C Na0P Na00 114.2(2) 4_565 .
S00D Na0P Cu02 44.27(16) . .
S00D Na0P Cu03 64.21(12) . 2_655
S00D Na0P Cu04 45.14(16) . 1_565
S00D Na0P Cu07 87.40(16) . 4_565
S00D Na0P S00C 100.8(2) . 4_565
S00D Na0P S00F 85.1(2) . 1_565
S00D Na0P S00H 84.2(2) . .
S00D Na0P S00I 98.5(3) . 4_565
S00D Na0P Na0N 123.88(19) . .
S00D Na0P Na00 135.9(4) . .
S00F Na0P Cu02 94.28(17) 1_565 .
S00F Na0P Cu03 44.55(14) 1_565 2_655
S00F Na0P Cu04 44.11(14) 1_565 1_565
S00F Na0P Cu07 141.4(4) 1_565 4_565
S00F Na0P S00H 81.35(15) 1_565 .
S00F Na0P Na0N 55.1(2) 1_565 .
S00F Na0P Na00 112.4(2) 1_565 .
S00H Na0P Cu02 43.38(14) . .
S00H Na0P Cu03 43.60(14) . 2_655
S00H Na0P Cu04 95.19(17) . 1_565
S00H Na0P Cu07 135.4(4) . 4_565
S00H Na0P Na0N 55.0(2) . .
S00H Na0P Na00 60.7(2) . .
S00I Na0P Cu02 84.9(3) 4_565 .
S00I Na0P Cu03 132.8(4) 4_565 2_655
S00I Na0P Cu04 141.0(2) 4_565 1_565
S00I Na0P Cu07 44.34(14) 4_565 4_565
S00I Na0P S00F 173.8(3) 4_565 1_565
S00I Na0P S00H 93.9(3) 4_565 .
S00I Na0P Na0N 118.8(3) 4_565 .
S00I Na0P Na00 61.5(2) 4_565 .
Na00 Na0P Cu02 92.8(3) . .
Na00 Na0P Cu03 99.4(2) . 2_655
Na00 Na0P Cu04 151.4(2) . 1_565
Na00 Na0P Cu07 99.1(2) . 4_565
Na00 Na0P Na0N 57.3(2) . .
O00Z Na0P Cu02 130.0(5) . .
O00Z Na0P Cu03 105.6(3) . 2_655
O00Z Na0P Cu04 129.5(5) . 1_565
O00Z Na0P Cu07 102.8(3) . 4_565
O00Z Na0P S00C 87.1(4) . 4_565
O00Z Na0P S00D 169.8(3) . .
O00Z Na0P S00F 87.2(4) . 1_565
O00Z Na0P S00H 88.0(4) . .
O00Z Na0P S00I 88.6(4) . 4_565
O00Z Na0P Na0N 45.9(3) . .
O00Z Na0P Na00 42.6(5) . .
Cu01 Na0Q Cu05 151.91(19) . 4_565
Cu01 Na0Q Na0U 148.5(2) . .
Cu02 Na0Q Cu01 51.78(12) . .
Cu02 Na0Q Cu05 106.2(2) . 4_565
Cu02 Na0Q Na0U 140.2(4) . .
Cu04 Na0Q Cu01 52.74(12) . .
Cu04 Na0Q Cu02 74.92(13) . .
Cu04 Na0Q Cu05 109.1(2) . 4_565
Cu04 Na0Q Na0U 143.4(4) . .
Cu05 Na0Q Na0U 59.33(14) 4_565 .
S00C Na0Q Cu01 140.7(4) 4 .
S00C Na0Q Cu02 141.3(2) 4 .
S00C Na0Q Cu04 91.1(3) 4 .
S00C Na0Q Cu05 44.19(14) 4 4_565
S00C Na0Q S00E 100.2(2) 4 2_655
S00C Na0Q S00F 101.4(4) 4 .
S00C Na0Q S00H 173.8(3) 4 .
S00C Na0Q S00I 83.19(16) 4 4_565
S00C Na0Q Na0U 55.6(2) 4 .
S00C Na0Q Na00 113.4(2) 4 .
S00E Na0Q Cu01 66.72(13) 2_655 .
S00E Na0Q Cu02 44.95(16) 2_655 .
S00E Na0Q Cu04 45.20(15) 2_655 .
S00E Na0Q Cu05 85.32(15) 2_655 4_565
S00E Na0Q S00F 86.3(2) 2_655 .
S00E Na0Q S00H 85.7(2) 2_655 .
S00E Na0Q S00I 98.2(3) 2_655 4_565
S00E Na0Q Na0U 144.7(2) 2_655 .
S00E Na0Q Na00 136.8(4) 2_655 .
S00F Na0Q Cu01 43.50(14) . .
S00F Na0Q Cu02 93.52(17) . .
S00F Na0Q Cu04 44.58(14) . .
S00F Na0Q Cu05 141.8(4) . 4_565
S00F Na0Q S00H 80.58(15) . .
S00F Na0Q Na0U 121.1(3) . .
S00F Na0Q Na00 111.3(2) . .
S00H Na0Q Cu01 43.51(14) . .
S00H Na0Q Cu02 43.68(14) . .
S00H Na0Q Cu04 94.36(17) . .
S00H Na0Q Cu05 135.6(4) . 4_565
S00H Na0Q Na0U 118.3(3) . .
S00H Na0Q Na00 60.6(2) . .
S00I Na0Q Cu01 133.8(4) 4_565 .
S00I Na0Q Cu02 86.0(3) 4_565 .
S00I Na0Q Cu04 141.4(2) 4_565 .
S00I Na0Q Cu05 44.54(14) 4_565 4_565
S00I Na0Q S00F 173.0(3) 4_565 .
S00I Na0Q S00H 94.3(3) 4_565 .
S00I Na0Q Na0U 57.2(2) 4_565 .
S00I Na0Q Na00 61.7(2) 4_565 .
Na00 Na0Q Cu01 98.7(2) . .
Na00 Na0Q Cu02 93.4(3) . .
Na00 Na0Q Cu04 150.5(2) . .
Na00 Na0Q Cu05 100.0(2) . 4_565
Na00 Na0Q Na0U 57.8(2) . .
O010 Na0Q Cu01 104.0(3) . .
O010 Na0Q Cu02 131.0(4) . .
O010 Na0Q Cu04 128.2(4) . .
O010 Na0Q Cu05 104.1(3) . 4_565
O010 Na0Q S00C 86.0(3) . 4
O010 Na0Q S00E 170.5(3) . 2_655
O010 Na0Q S00F 85.5(3) . .
O010 Na0Q S00H 88.3(3) . .
O010 Na0Q S00I 89.5(3) . 4_565
O010 Na0Q Na0U 44.8(3) . .
O010 Na0Q Na00 43.7(3) . .
Cu04 Na0R Na0N 56.45(13) 4_556 .
Cu04 Na0R Na0W 147.0(2) 4_556 .
Cu05 Na0R Cu04 107.8(3) 1_545 4_556
Cu05 Na0R Na0N 139.2(4) 1_545 .
Cu05 Na0R Na0W 96.9(2) 1_545 .
Cu07 Na0R Cu04 108.4(2) . 4_556
Cu07 Na0R Cu05 78.31(13) . 1_545
Cu07 Na0R S00K 43.62(15) . .
Cu07 Na0R Na0N 140.4(4) . .
Cu07 Na0R Na0W 97.6(2) . .
Cu07 Na0R Na00 154.4(2) . .
S00C Na0R Cu04 87.80(16) . 4_556
S00C Na0R Cu05 45.68(17) . 1_545
S00C Na0R Cu07 45.78(17) . .
S00C Na0R S00D 100.3(3) . 4_566
S00C Na0R S00E 99.0(3) . 3_656
S00C Na0R S00K 83.4(2) . .
S00C Na0R S00L 85.6(2) . 1_545
S00C Na0R Na0N 144.2(2) . .
S00C Na0R Na0W 125.2(2) . .
S00C Na0R Na00 137.5(5) . .
S00D Na0R Cu04 43.34(14) 4_566 4_556
S00D Na0R Cu05 141.6(2) 4_566 1_545
S00D Na0R Cu07 88.0(3) 4_566 .
S00D Na0R S00E 81.91(16) 4_566 3_656
S00D Na0R S00K 103.2(4) 4_566 .
S00D Na0R S00L 174.1(2) 4_566 1_545
S00D Na0R Na0N 55.2(2) 4_566 .
S00D Na0R Na0W 120.5(3) 4_566 .
S00D Na0R Na00 112.1(2) 4_566 .
S00E Na0R Cu04 43.00(14) 3_656 4_556
S00E Na0R Cu05 86.5(3) 3_656 1_545
S00E Na0R Cu07 140.8(2) 3_656 .
S00E Na0R S00K 174.0(4) 3_656 .
S00E Na0R S00L 96.9(4) 3_656 1_545
S00E Na0R Na0N 55.8(2) 3_656 .
S00E Na0R Na0W 120.1(3) 3_656 .
S00E Na0R Na00 61.1(2) 3_656 .
S00K Na0R Cu04 142.9(4) . 4_556
S00K Na0R Cu05 91.30(17) . 1_545
S00K Na0R Na0N 124.5(3) . .
S00K Na0R Na0W 54.6(2) . .
S00L Na0R Cu04 137.5(4) 1_545 4_556
S00L Na0R Cu05 43.71(15) 1_545 1_545
S00L Na0R Cu07 96.45(18) 1_545 .
S00L Na0R S00K 77.68(16) 1_545 .
S00L Na0R Na0N 119.4(3) 1_545 .
S00L Na0R Na0W 55.1(2) 1_545 .
S00L Na0R Na00 62.6(2) 1_545 .
Na0W Na0R Na0N 90.51(19) . .
Na00 Na0R Cu04 97.2(2) . 4_556
Na00 Na0R Cu05 93.4(3) . 1_545
Na00 Na0R S00K 113.5(2) . .
Na00 Na0R Na0N 56.9(2) . .
Na00 Na0R Na0W 59.0(2) . .
O00Z Na0R Cu04 101.9(3) . 4_556
O00Z Na0R Cu05 129.7(6) . 1_545
O00Z Na0R Cu07 128.7(6) . .
O00Z Na0R S00C 170.3(3) . .
O00Z Na0R S00D 86.6(4) . 4_566
O00Z Na0R S00E 88.6(4) . 3_656
O00Z Na0R S00K 88.5(4) . .
O00Z Na0R S00L 87.5(4) . 1_545
O00Z Na0R Na0N 45.4(3) . .
O00Z Na0R Na0W 45.1(3) . .
O00Z Na0R Na00 42.5(5) . .
Cu02 Na0S Na0M 57.68(13) 4_556 .
Cu02 Na0S Na0U 147.5(2) 4_556 .
Cu05 Na0S Cu02 107.2(2) 1_545 4_556
Cu05 Na0S Na0M 139.2(4) 1_545 .
Cu05 Na0S Na0U 95.4(2) 1_545 .
Cu05 Na0S Na00 92.6(3) 1_545 .
Cu07 Na0S Cu02 108.9(2) 1_545 4_556
Cu07 Na0S Cu05 76.86(13) 1_545 1_545
Cu07 Na0S S00K 44.11(13) 1_545 1_545
Cu07 Na0S S00L 95.91(18) 1_545 1_545
Cu07 Na0S Na0M 142.1(4) 1_545 .
Cu07 Na0S Na0U 98.7(2) 1_545 .
Cu07 Na0S Na00 153.2(2) 1_545 .
S00D Na0S Cu02 43.62(14) 4_556 4_556
S00D Na0S Cu05 142.1(2) 4_556 1_545
S00D Na0S Cu07 90.1(3) 4_556 1_545
S00D Na0S S00E 82.03(16) 4_556 3_656
S00D Na0S S00K 105.0(4) 4_556 1_545
S00D Na0S S00L 173.2(3) 4_556 1_545
S00D Na0S Na0M 54.9(2) 4_556 .
S00D Na0S Na0U 121.9(3) 4_556 .
S00D Na0S Na00 112.1(2) 4_556 .
S00E Na0S Cu02 43.59(14) 3_656 4_556
S00E Na0S Cu05 86.3(3) 3_656 1_545
S00E Na0S Cu07 141.2(2) 3_656 1_545
S00E Na0S S00K 172.0(4) 3_656 1_545
S00E Na0S S00L 95.1(3) 3_656 1_545
S00E Na0S Na0M 56.1(2) 3_656 .
S00E Na0S Na0U 117.7(3) 3_656 .
S00E Na0S Na00 60.5(2) 3_656 .
S00I Na0S Cu02 85.17(16) 1_545 4_556
S00I Na0S Cu05 46.18(17) 1_545 1_545
S00I Na0S Cu07 46.40(16) 1_545 1_545
S00I Na0S S00D 99.8(2) 1_545 4_556
S00I Na0S S00E 97.4(3) 1_545 3_656
S00I Na0S S00K 85.2(2) 1_545 1_545
S00I Na0S S00L 86.6(2) 1_545 1_545
S00I Na0S Na0M 142.8(2) 1_545 .
S00I Na0S Na0U 127.1(2) 1_545 .
S00I Na0S Na00 136.4(4) 1_545 .
S00K Na0S Cu02 144.4(4) 1_545 4_556
S00K Na0S Cu05 90.21(17) 1_545 1_545
S00K Na0S S00L 77.52(16) 1_545 1_545
S00K Na0S Na0M 124.8(3) 1_545 .
S00K Na0S Na0U 55.4(2) 1_545 .
S00K Na0S Na00 112.6(2) 1_545 .
S00L Na0S Cu02 135.9(4) 1_545 4_556
S00L Na0S Cu05 43.19(14) 1_545 1_545
S00L Na0S Na0M 118.4(3) 1_545 .
S00L Na0S Na0U 54.1(2) 1_545 .
S00L Na0S Na00 61.2(2) 1_545 .
Na0U Na0S Na0M 89.94(19) . .
Na00 Na0S Cu02 97.8(2) . 4_556
Na00 Na0S Na0M 57.2(2) . .
Na00 Na0S Na0U 57.2(2) . .
O010 Na0S Cu02 103.2(3) . 4_556
O010 Na0S Cu05 129.1(4) . 1_545
O010 Na0S Cu07 129.1(4) . 1_545
O010 Na0S S00D 86.7(3) . 4_556
O010 Na0S S00E 88.6(3) . 3_656
O010 Na0S S00I 171.6(3) . 1_545
O010 Na0S S00K 88.1(3) . 1_545
O010 Na0S S00L 87.1(3) . 1_545
O010 Na0S Na0M 45.5(3) . .
O010 Na0S Na0U 44.6(3) . .
O010 Na0S Na00 43.0(3) . .
Cu06 Na0T Cu06 179.2(6) 1_545 2_747
Cu09 Na0T Cu06 78.87(15) 3_767 1_545
Cu09 Na0T Cu06 101.6(2) 3_767 2_747
Cu09 Na0T Cu06 101.6(2) 4_566 1_545
Cu09 Na0T Cu06 78.87(15) 4_566 2_747
Cu09 Na0T Cu09 110.5(5) 3_767 4_566
Cu09 Na0T S00L 139.0(5) 4_566 3_767
Cu09 Na0T S00L 41.42(13) 3_767 3_767
Cu09 Na0T S00L 139.0(5) 3_767 4_566
Cu09 Na0T S00L 41.42(13) 4_566 4_566
Cu0A Na0T Cu06 77.50(15) 3_767 1_545
Cu0A Na0T Cu06 102.0(2) 4_566 1_545
Cu0A Na0T Cu06 77.50(15) 4_566 2_747
Cu0A Na0T Cu06 102.0(2) 3_767 2_747
Cu0A Na0T Cu09 179.09(11) 4_566 3_767
Cu0A Na0T Cu09 69.37(5) 3_767 3_767
Cu0A Na0T Cu09 179.09(11) 3_767 4_566
Cu0A Na0T Cu09 69.37(5) 4_566 4_566
Cu0A Na0T Cu0A 110.8(5) 4_566 3_767
Cu0A Na0T S00L 41.51(13) 4_566 4_566
Cu0A Na0T S00L 138.1(5) 3_767 4_566
Cu0A Na0T S00L 41.51(13) 3_767 3_767
Cu0A Na0T S00L 138.1(5) 4_566 3_767
S00G Na0T Cu06 44.25(13) 4_566 2_747
S00G Na0T Cu06 44.25(13) 3_767 1_545
S00G Na0T Cu06 135.0(5) 3_767 2_747
S00G Na0T Cu06 135.0(5) 4_566 1_545
S00G Na0T Cu09 92.72(11) 4_566 4_566
S00G Na0T Cu09 134.92(10) 4_566 3_767
S00G Na0T Cu09 134.92(10) 3_767 4_566
S00G Na0T Cu09 92.72(11) 3_767 3_767
S00G Na0T Cu0A 44.33(17) 3_767 3_767
S00G Na0T Cu0A 88.0(4) 4_566 3_767
S00G Na0T Cu0A 88.0(4) 3_767 4_566
S00G Na0T Cu0A 44.33(17) 4_566 4_566
S00G Na0T S00G 97.2(5) 3_767 4_566
S00G Na0T S00L 96.2(3) 3_767 4_566
S00G Na0T S00L 83.5(2) 3_767 3_767
S00G Na0T S00L 83.5(2) 4_566 4_566
S00G Na0T S00L 96.2(2) 4_566 3_767
S00J Na0T Cu06 135.5(5) . 2_747
S00J Na0T Cu06 45.21(14) . 1_545
S00J Na0T Cu06 45.21(14) 2_757 2_747
S00J Na0T Cu06 135.5(5) 2_757 1_545
S00J Na0T Cu09 86.4(4) . 4_566
S00J Na0T Cu09 45.64(18) 2_757 4_566
S00J Na0T Cu09 86.4(4) 2_757 3_767
S00J Na0T Cu09 45.65(18) . 3_767
S00J Na0T Cu0A 92.95(11) 2_757 4_566
S00J Na0T Cu0A 92.95(11) . 3_767
S00J Na0T Cu0A 135.10(11) . 4_566
S00J Na0T Cu0A 135.10(11) 2_757 3_767
S00J Na0T S00G 83.36(9) . 3_767
S00J Na0T S00G 179.1(4) . 4_566
S00J Na0T S00G 83.36(9) 2_757 4_566
S00J Na0T S00G 179.1(4) 2_757 3_767
S00J Na0T S00J 96.1(5) 2_757 .
S00J Na0T S00L 95.8(2) 2_757 3_767
S00J Na0T S00L 95.8(2) . 4_566
S00J Na0T S00L 84.5(2) 2_757 4_566
S00J Na0T S00L 84.5(2) . 3_767
S00L Na0T Cu06 80.10(7) 3_767 2_747
S00L Na0T Cu06 99.90(7) 4_566 2_747
S00L Na0T Cu06 80.10(7) 4_566 1_545
S00L Na0T Cu06 99.90(7) 3_767 1_545
S00L Na0T S00L 179.6(6) 4_566 3_767
Cu05 Na0U Na0Q 59.46(14) 4_565 .
Cu06 Na0U Cu05 50.37(13) 4_565 4_565
Cu06 Na0U Na0Q 94.5(3) 4_565 .
Cu08 Na0U Cu05 50.92(12) 4 4_565
Cu08 Na0U Cu06 75.49(14) 4 4_565
Cu08 Na0U Cu09 108.5(2) 4 1_545
Cu08 Na0U Na0Q 95.2(2) 4 .
Cu09 Na0U Cu05 146.92(19) 1_545 4_565
Cu09 Na0U Cu06 103.6(2) 1_545 4_565
Cu09 Na0U Na0Q 153.0(2) 1_545 .
S00C Na0U Cu05 44.01(14) 4 4_565
S00C Na0U Cu06 93.19(19) 4 4_565
S00C Na0U Cu08 43.24(14) 4 4
S00C Na0U Cu09 142.1(4) 4 1_545
S00C Na0U S00I 80.75(17) 4 4_565
S00C Na0U S00J 84.1(2) 4 4
S00C Na0U S00K 102.5(4) 4 1_545
S00C Na0U S00L 174.8(4) 4 1_545
S00C Na0U Na0Q 54.3(2) 4 .
S00C Na0U Na00 111.7(2) 4 .
S00I Na0U Cu05 44.07(15) 4_565 4_565
S00I Na0U Cu06 42.44(15) 4_565 4_565
S00I Na0U Cu08 93.67(19) 4_565 4
S00I Na0U Cu09 133.5(4) 4_565 1_545
S00I Na0U S00J 84.1(2) 4_565 4
S00I Na0U S00K 176.5(4) 4_565 1_545
S00I Na0U Na0Q 54.4(2) 4_565 .
S00I Na0U Na00 60.5(2) 4_565 .
S00J Na0U Cu05 62.89(13) 4 4_565
S00J Na0U Cu06 45.07(16) 4 4_565
S00J Na0U Cu08 44.54(16) 4 4
S00J Na0U Cu09 84.31(15) 4 1_545
S00J Na0U Na0Q 122.3(2) 4 .
S00J Na0U Na00 136.5(4) 4 .
S00K Na0U Cu05 139.5(4) 1_545 4_565
S00K Na0U Cu06 137.86(19) 1_545 4_565
S00K Na0U Cu08 89.7(3) 1_545 4
S00K Na0U Cu09 43.86(15) 1_545 1_545
S00K Na0U S00J 97.5(2) 1_545 4
S00K Na0U Na0Q 126.5(3) 1_545 .
S00K Na0U Na00 116.6(2) 1_545 .
S00L Na0U Cu05 133.1(4) 1_545 4_565
S00L Na0U Cu06 85.1(3) 1_545 4_565
S00L Na0U Cu08 140.4(2) 1_545 4
S00L Na0U Cu09 43.12(14) 1_545 1_545
S00L Na0U S00I 94.7(4) 1_545 4_565
S00L Na0U S00J 98.1(3) 1_545 4
S00L Na0U S00K 81.93(18) 1_545 1_545
S00L Na0U Na0Q 120.8(3) 1_545 .
S00L Na0U Na00 63.5(2) 1_545 .
Na00 Na0U Cu05 99.8(3) . 4_565
Na00 Na0U Cu06 92.3(3) . 4_565
Na00 Na0U Cu08 149.5(2) . 4
Na00 Na0U Cu09 101.5(3) . 1_545
Na00 Na0U Na0Q 57.3(2) . .
O010 Na0U Cu05 105.7(3) . 4_565
O010 Na0U Cu06 129.9(5) . 4_565
O010 Na0U Cu08 127.7(4) . 4
O010 Na0U Cu09 107.2(3) . 1_545
O010 Na0U S00C 86.1(3) . 4
O010 Na0U S00I 88.4(3) . 4_565
O010 Na0U S00J 168.5(4) . 4
O010 Na0U S00K 90.5(4) . 1_545
O010 Na0U S00L 91.2(4) . 1_545
O010 Na0U Na0Q 46.3(3) . .
O010 Na0U Na00 43.5(3) . .
Cu05 Cu0V Cu08 58.0(2) 1_545 .
Cu06 Cu0V Cu05 161.0(5) 3_767 1_545
Cu06 Cu0V Cu05 59.7(2) 1_545 1_545
Cu06 Cu0V Cu06 137.9(5) 3_767 1_545
Cu06 Cu0V Cu08 120.4(3) 3_767 .
Cu06 Cu0V Cu08 88.2(3) 1_545 .
Cu06 Cu0V Cu09 110.3(4) 3_767 1_545
Cu06 Cu0V Cu0A 99.7(3) 3_767 1_545
Cu06 Cu0V Cu0A 122.0(4) 1_545 1_545
Cu06 Cu0V Cu0B 66.1(2) 3_767 1_545
Cu06 Cu0V S00G 168.2(4) 1_545 1_545
Cu06 Cu0V S00G 52.8(2) 3_767 1_545
Cu06 Cu0V S00J 57.9(2) 3_767 3_757
Cu09 Cu0V Cu05 64.7(3) 1_545 1_545
Cu09 Cu0V Cu06 70.4(2) 1_545 1_545
Cu09 Cu0V Cu08 121.9(4) 1_545 .
Cu09 Cu0V Cu0A 85.5(4) 1_545 1_545
Cu09 Cu0V Cu0B 162.1(5) 1_545 1_545
Cu09 Cu0V S00G 113.1(4) 1_545 1_545
Cu0A Cu0V Cu05 62.2(2) 1_545 1_545
Cu0A Cu0V Cu08 61.0(2) 1_545 .
Cu0B Cu0V Cu05 112.5(3) 1_545 1_545
Cu0B Cu0V Cu06 124.8(4) 1_545 1_545
Cu0B Cu0V Cu08 55.3(2) 1_545 .
Cu0B Cu0V Cu0A 78.1(3) 1_545 1_545
Cu0B Cu0V S00G 50.0(2) 1_545 1_545
S00G Cu0V Cu05 110.7(4) 1_545 1_545
S00G Cu0V Cu08 80.4(3) 1_545 .
S00G Cu0V Cu0A 49.0(2) 1_545 1_545
S00J Cu0V Cu05 81.6(3) . 1_545
S00J Cu0V Cu05 121.4(4) 3_757 1_545
S00J Cu0V Cu06 96.6(3) 3_757 1_545
S00J Cu0V Cu06 57.7(3) . 1_545
S00J Cu0V Cu06 113.2(5) . 3_767
S00J Cu0V Cu08 53.1(3) . .
S00J Cu0V Cu08 173.8(5) 3_757 .
S00J Cu0V Cu09 127.4(4) . 1_545
S00J Cu0V Cu09 56.7(2) 3_757 1_545
S00J Cu0V Cu0A 114.0(4) . 1_545
S00J Cu0V Cu0A 113.0(4) 3_757 1_545
S00J Cu0V Cu0B 123.8(4) 3_757 1_545
S00J Cu0V Cu0B 67.1(3) . 1_545
S00J Cu0V S00G 94.5(3) 3_757 1_545
S00J Cu0V S00G 116.2(4) . 1_545
S00J Cu0V S00J 133.0(5) . 3_757
Cu0V Cu0V Cu05 121.3(7) 3_757 1_545
Cu0V Cu0V Cu06 75.6(6) 3_757 3_767
Cu0V Cu0V Cu06 62.3(5) 3_757 1_545
Cu0V Cu0V Cu08 128.5(8) 3_757 .
Cu0V Cu0V Cu09 88.5(6) 3_757 1_545
Cu0V Cu0V Cu0A 170.5(8) 3_757 1_545
Cu0V Cu0V Cu0B 106.7(8) 3_757 1_545
Cu0V Cu0V S00G 127.9(7) 3_757 1_545
Cu0V Cu0V S00J 57.6(5) 3_757 3_757
Cu0V Cu0V S00J 75.4(7) 3_757 .
Cu0X Cu0V Cu05 121.3(7) . 1_545
Cu0X Cu0V Cu06 75.6(6) . 3_767
Cu0X Cu0V Cu06 62.3(5) . 1_545
Cu0X Cu0V Cu08 128.5(8) . .
Cu0X Cu0V Cu09 88.5(6) . 1_545
Cu0X Cu0V Cu0A 170.5(8) . 1_545
Cu0X Cu0V Cu0B 106.7(8) . 1_545
Cu0X Cu0V S00G 127.9(7) . 1_545
Cu0X Cu0V S00J 75.4(7) . .
Cu0X Cu0V S00J 57.6(5) . 3_757
Cu0X Cu0V Cu0V 0.002(4) . 3_757
Cu06 Na0W Cu07 50.32(13) 4_565 4_565
Cu06 Na0W Cu0A 103.3(2) 4_565 1_545
Cu06 Na0W Na0R 138.5(4) 4_565 .
Cu07 Na0W Cu0A 147.9(2) 4_565 1_545
Cu07 Na0W Na0R 148.1(2) 4_565 .
Cu08 Na0W Cu06 75.80(14) 4_565 4_565
Cu08 Na0W Cu07 52.21(12) 4_565 4_565
Cu08 Na0W Cu0A 109.4(2) 4_565 1_545
Cu08 Na0W Na0R 145.0(4) 4_565 .
Cu08 Na0W Na00 149.0(2) 4_565 .
Cu0A Na0W Na0R 62.98(15) 1_545 .
S00C Na0W Cu06 93.14(19) 4_565 4_565
S00C Na0W Cu07 44.33(15) 4_565 4_565
S00C Na0W Cu08 43.15(14) 4_565 4_565
S00C Na0W Cu0A 143.3(4) 4_565 1_545
S00C Na0W S00G 83.7(2) 4_565 2_746
S00C Na0W S00I 81.41(17) 4_565 4_565
S00C Na0W S00K 103.3(4) 4_565 .
S00C Na0W S00L 173.8(3) 4_565 1_545
S00C Na0W Na0R 121.8(3) 4_565 .
S00C Na0W Na00 111.4(2) 4_565 .
S00G Na0W Cu06 44.19(16) 2_746 4_565
S00G Na0W Cu07 62.83(13) 2_746 4_565
S00G Na0W Cu08 44.79(15) 2_746 4_565
S00G Na0W Cu0A 85.64(16) 2_746 1_545
S00G Na0W S00I 82.9(2) 2_746 4_565
S00G Na0W Na0R 148.6(2) 2_746 .
S00G Na0W Na00 134.8(4) 2_746 .
S00I Na0W Cu06 42.06(14) 4_565 4_565
S00I Na0W Cu07 43.64(14) 4_565 4_565
S00I Na0W Cu08 94.32(18) 4_565 4_565
S00I Na0W Cu0A 131.8(4) 4_565 1_545
S00I Na0W Na0R 116.4(3) 4_565 .
S00I Na0W Na00 59.3(2) 4_565 .
S00K Na0W Cu06 138.4(2) . 4_565
S00K Na0W Cu07 141.5(4) . 4_565
S00K Na0W Cu08 90.5(3) . 4_565
S00K Na0W Cu0A 44.30(15) . 1_545
S00K Na0W S00G 99.4(2) . 2_746
S00K Na0W S00I 174.9(4) . 4_565
S00K Na0W Na0R 59.5(2) . .
S00K Na0W Na00 116.5(2) . .
S00L Na0W Cu06 85.0(3) 1_545 4_565
S00L Na0W Cu07 132.2(4) 1_545 4_565
S00L Na0W Cu08 141.2(2) 1_545 4_565
S00L Na0W Cu0A 42.85(15) 1_545 1_545
S00L Na0W S00G 98.9(3) 1_545 2_746
S00L Na0W S00I 93.3(3) 1_545 4_565
S00L Na0W S00K 81.83(18) 1_545 .
S00L Na0W Na0R 57.8(2) 1_545 .
S00L Na0W Na00 62.8(2) 1_545 .
Na00 Na0W Cu06 91.3(3) . 4_565
Na00 Na0W Cu07 97.9(2) . 4_565
Na00 Na0W Cu0A 100.9(2) . 1_545
Na00 Na0W Na0R 57.1(2) . .
O00Z Na0W Cu06 127.0(5) . 4_565
O00Z Na0W Cu07 103.9(3) . 4_565
O00Z Na0W Cu08 129.1(5) . 4_565
O00Z Na0W Cu0A 107.4(3) . 1_545
O00Z Na0W S00C 87.2(4) . 4_565
O00Z Na0W S00G 166.6(4) . 2_746
O00Z Na0W S00I 86.1(4) . 4_565
O00Z Na0W S00K 92.2(4) . .
O00Z Na0W S00L 89.3(4) . 1_545
O00Z Na0W Na0R 44.5(3) . .
O00Z Na0W Na00 41.4(5) . .
Cu06 Cu0X Cu06 180.0 3_767 1_545
Cu06 Cu0X Cu09 107.47(7) 1_545 3_767
Cu06 Cu0X Cu09 72.53(7) 3_767 3_767
Cu06 Cu0X Cu09 107.47(7) 3_767 1_545
Cu06 Cu0X Cu09 72.53(7) 1_545 1_545
Cu09 Cu0X Cu09 180.0 1_545 3_767
S00J Cu0X Cu06 63.24(16) 3_757 3_767
S00J Cu0X Cu06 63.24(16) . 1_545
S00J Cu0X Cu06 116.76(16) 3_757 1_545
S00J Cu0X Cu06 116.76(16) . 3_767
S00J Cu0X Cu09 122.04(10) . 1_545
S00J Cu0X Cu09 57.96(10) 3_757 1_545
S00J Cu0X Cu09 122.04(10) 3_757 3_767
S00J Cu0X Cu09 57.96(10) . 3_767
S00J Cu0X S00J 180.0 3_757 .
Cu0V Cu0X Cu06 82.4(6) . 3_767
Cu0V Cu0X Cu06 82.4(6) 3_757 1_545
Cu0V Cu0X Cu06 97.6(6) 3_757 3_767
Cu0V Cu0X Cu06 97.6(6) . 1_545
Cu0V Cu0X Cu09 108.9(6) . 3_767
Cu0V Cu0X Cu09 71.1(6) . 1_545
Cu0V Cu0X Cu09 71.1(6) 3_757 3_767
Cu0V Cu0X Cu09 108.9(6) 3_757 1_545
Cu0V Cu0X S00J 100.6(6) 3_757 .
Cu0V Cu0X S00J 100.6(6) . 3_757
Cu0V Cu0X S00J 79.4(6) 3_757 3_757
Cu0V Cu0X S00J 79.4(6) . .
Cu0V Cu0X Cu0V 180.0 3_757 .
S00E Na00 Na0M 57.85(18) 3_656 .
S00E Na00 Na0Q 123.4(3) 3_656 .
S00E Na00 Na0R 57.6(2) 3_656 .
S00E Na00 Na0S 57.32(19) 3_656 .
S00E Na00 Na0U 121.9(3) 3_656 .
S00H Na00 S00E 90.02(15) . 3_656
S00H Na00 Na0M 57.42(19) . .
S00H Na00 Na0P 58.54(19) . .
S00H Na00 Na0Q 58.58(19) . .
S00H Na00 Na0R 122.9(3) . .
S00H Na00 Na0S 122.4(3) . .
S00H Na00 Na0U 123.5(3) . .
S00I Na00 S00E 179.6(3) 4_565 3_656
S00I Na00 S00H 89.73(16) 4_565 .
S00I Na00 Na0M 121.8(3) 4_565 .
S00I Na00 Na0P 56.85(19) 4_565 .
S00I Na00 Na0Q 56.21(19) 4_565 .
S00I Na00 Na0R 122.8(3) 4_565 .
S00I Na00 Na0S 122.6(3) 4_565 .
S00I Na00 Na0U 58.1(2) 4_565 .
Na0M Na00 Na0S 65.0(2) . .
Na0N Na00 S00E 57.83(19) . 3_656
Na0N Na00 S00H 57.03(19) . .
Na0N Na00 S00I 122.2(3) . 4_565
Na0N Na00 Na0M 81.18(18) . .
Na0N Na00 Na0P 65.4(2) . .
Na0N Na00 Na0Q 115.6(2) . .
Na0N Na00 Na0R 65.9(2) . .
Na0N Na00 Na0S 115.1(2) . .
Na0N Na00 Na0U 179.5(3) . .
Na0P Na00 S00E 123.2(3) . 3_656
Na0P Na00 Na0M 116.0(2) . .
Na0P Na00 Na0Q 81.55(19) . .
Na0P Na00 Na0R 98.9(3) . .
Na0P Na00 Na0S 179.1(2) . .
Na0P Na00 Na0U 114.9(2) . .
Na0Q Na00 Na0M 65.6(2) . .
Na0Q Na00 Na0R 178.4(2) . .
Na0Q Na00 Na0S 98.8(3) . .
Na0Q Na00 Na0U 64.9(2) . .
Na0R Na00 Na0M 115.4(2) . .
Na0R Na00 Na0S 80.73(19) . .
Na0R Na00 Na0U 113.6(2) . .
Na0U Na00 Na0M 99.0(3) . .
Na0U Na00 Na0S 64.6(2) . .
O00Z Na00 S00E 90.0(4) . 3_656
O00Z Na00 S00H 91.7(4) . .
O00Z Na00 S00I 90.3(4) . 4_565
O00Z Na00 Na0M 132.0(4) . .
O00Z Na00 Na0N 50.8(4) . .
O00Z Na00 Na0P 50.3(4) . .
O00Z Na00 Na0Q 131.8(4) . .
O00Z Na00 Na0R 48.6(4) . .
O00Z Na00 Na0S 129.3(4) . .
O00Z Na00 Na0U 129.0(4) . .
O00Z Na00 O010 176.6(4) . .
O010 Na00 S00E 89.6(4) . 3_656
O010 Na00 S00H 91.7(4) . .
O010 Na00 S00I 90.2(4) . 4_565
O010 Na00 Na0M 50.1(3) . .
O010 Na00 Na0N 131.3(4) . .
O010 Na00 Na0P 132.3(4) . .
O010 Na00 Na0Q 50.8(4) . .
O010 Na00 Na0R 128.7(4) . .
O010 Na00 Na0S 48.0(3) . .
O010 Na00 Na0U 48.9(3) . .
Na0P O00Z Na0N 88.6(4) . .
Na0R O00Z Na0N 90.9(4) . .
Na0R O00Z Na0P 176.1(10) . .
Na0R O00Z Na0W 90.4(4) . .
Na0W O00Z Na0N 176.9(9) . .
Na0W O00Z Na0P 90.0(4) . .
Na00 O00Z Na0N 86.6(6) . .
Na00 O00Z Na0P 87.1(6) . .
Na00 O00Z Na0R 89.0(6) . .
Na00 O00Z Na0W 90.6(6) . .
Na0M O010 Na0Q 88.9(4) . .
Na0S O010 Na0M 90.5(4) . .
Na0S O010 Na0Q 174.5(7) . .
Na0S O010 Na0U 91.0(4) . .
Na0U O010 Na0M 174.0(6) . .
Na0U O010 Na0Q 89.0(4) . .
Na00 O010 Na0M 86.6(5) . .
Na00 O010 Na0Q 85.5(5) . .
Na00 O010 Na0S 89.0(5) . .
Na00 O010 Na0U 87.6(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu01 Cu01 2.880(3) 2_655
Cu01 Cu02 2.782(4) 2_655
Cu01 Cu02 2.807(4) .
Cu01 Cu04 2.756(4) 2_655
Cu01 Cu04 2.833(4) .
Cu01 S00E 2.322(3) .
Cu01 S00F 2.315(7) .
Cu01 S00H 2.336(6) .
Cu01 Na0M 3.197(8) 3_656
Cu01 Na0M 3.240(6) .
Cu01 Na0N 3.209(9) 3_656
Cu01 Na0Q 3.246(5) .
Cu02 Cu02 2.907(3) 2_655
Cu02 Cu03 2.779(4) 2_655
Cu02 Cu03 2.806(4) .
Cu02 S00D 2.321(6) .
Cu02 S00E 2.342(6) 2_655
Cu02 S00H 2.316(4) .
Cu02 Na0M 3.207(6) 4
Cu02 Na0P 3.218(9) .
Cu02 Na0Q 3.180(9) .
Cu02 Na0S 3.272(6) 4
Cu03 Cu03 2.804(3) 2_655
Cu03 Cu04 2.825(4) 1_565
Cu03 Cu04 2.850(4) 2_665
Cu03 S00D 2.317(3) .
Cu03 S00F 2.346(7) 2_665
Cu03 S00H 2.317(6) 2_655
Cu03 Na0M 3.118(8) 4
Cu03 Na0N 3.192(8) 4_565
Cu03 Na0N 3.257(6) 2_655
Cu03 Na0P 3.196(5) 2_655
Cu04 Cu04 2.832(3) 2_655
Cu04 S00D 2.342(7) 1_545
Cu04 S00E 2.330(6) 2_655
Cu04 S00F 2.314(4) .
Cu04 Na0N 3.164(6) 4
Cu04 Na0P 3.176(8) 1_545
Cu04 Na0Q 3.127(8) .
Cu04 Na0R 3.314(6) 4
Cu05 Cu06 2.751(4) .
Cu05 Cu08 2.771(4) 1_565
Cu05 Cu09 2.882(4) .
Cu05 Cu0A 2.918(4) .
Cu05 S00C 2.349(6) 1_565
Cu05 S00I 2.374(6) .
Cu05 S00L 2.312(4) .
Cu05 Na0Q 3.282(5) 4_566
Cu05 Na0R 3.150(10) 1_565
Cu05 Na0S 3.150(9) 1_565
Cu05 Na0U 3.278(6) 4_566
Cu05 Cu0V 2.828(10) 1_565
Cu06 Cu07 2.710(4) .
Cu06 Cu09 3.014(3) .
Cu06 Cu0B 2.798(4) 3_777
Cu06 S00G 2.351(7) 3_777
Cu06 S00I 2.251(3) .
Cu06 S00J 2.384(7) 1_565
Cu06 Na0U 3.185(10) 4_566
Cu06 Cu0V 2.692(10) 1_565
Cu06 Cu0V 2.461(10) 3_767
Cu06 Na0W 3.186(9) 4_566
Cu06 Cu0X 2.405(2) 1_565
Cu07 Cu08 2.795(4) .
Cu07 Cu0B 2.595(3) 3_777
Cu07 S00C 2.325(7) .
Cu07 S00I 2.332(6) .
Cu07 S00K 2.316(4) .
Cu07 Na0P 3.200(5) 4_566
Cu07 Na0R 3.091(9) .
Cu07 Na0S 3.038(8) 1_565
Cu07 Na0W 3.188(6) 4_566
Cu08 Cu0A 2.895(3) 1_545
Cu08 Cu0B 2.583(3) 1_545
Cu08 Cu0B 2.772(4) 3_777
Cu08 S00C 2.256(3) .
Cu08 S00G 2.372(7) 3_777
Cu08 S00J 2.348(7) .
Cu08 Na0O 3.266(2) .
Cu08 Na0U 3.164(9) 4_556
Cu08 Cu0V 2.890(10) .
Cu08 Na0W 3.165(8) 4_566
Cu09 Cu0B 2.599(5) 3_777
Cu09 S00J 2.375(4) 3_767
Cu09 S00K 2.320(7) .
Cu09 S00L 2.264(6) .
Cu09 Na0O 3.351(11) 3_767
Cu09 Na0S 3.407(6) 1_565
Cu09 Na0T 3.198(10) 3_767
Cu09 Na0U 3.180(6) 1_565
Cu09 Cu0V 2.534(10) 1_565
Cu09 Cu0X 2.677(2) 1_565
Cu0A Cu0B 2.592(5) 3_787
Cu0A S00G 2.326(4) .
Cu0A S00K 2.342(7) 1_565
Cu0A S00L 2.268(6) .
Cu0A Na0O 3.345(11) 3_777
Cu0A Na0R 3.418(6) 1_565
Cu0A Na0T 3.197(10) 3_767
Cu0A Cu0V 2.817(12) 1_565
Cu0A Na0W 3.213(6) 1_565
Cu0B Cu0B 2.776(7) 3_787
Cu0B S00G 2.662(7) 3_787
Cu0B S00G 2.307(4) .
Cu0B S00J 2.696(7) 1_565
Cu0B S00K 2.563(4) 3_777
Cu0B Cu0V 2.663(11) 1_565
S00C Na0P 2.924(9) 4_566
S00C Na0Q 2.886(10) 4_556
S00C Na0R 2.862(6) .
S00C Na0U 2.932(10) 4_556
S00C Na0W 2.947(9) 4_566
S00D Na0M 2.927(9) 4
S00D Na0N 2.962(9) 4_565
S00D Na0P 2.887(6) .
S00D Na0R 2.970(10) 4_565
S00D Na0S 2.910(9) 4
S00E Na0M 3.015(9) 3_656
S00E Na0N 2.997(10) 3_656
S00E Na0Q 2.914(6) 2_655
S00E Na0R 2.990(10) 3_656
S00E Na0S 3.001(10) 3_656
S00E Na00 3.104(6) 3_656
S00F Na0M 2.891(9) .
S00F Na0N 2.941(10) 1_545
S00F Na0N 2.905(6) 3_656
S00F Na0P 2.967(10) 1_545
S00F Na0Q 2.962(9) .
S00G Na0O 2.935(12) 3_777
S00G Na0T 2.935(12) 3_767
S00G Cu0V 2.786(11) 1_565
S00G Na0W 3.056(6) 2_766
S00H Na0M 2.991(10) .
S00H Na0M 2.935(6) 3_656
S00H Na0N 2.956(10) .
S00H Na0P 3.029(10) .
S00H Na0Q 3.034(10) .
S00H Na00 3.097(6) .
S00I Na0P 2.949(10) 4_566
S00I Na0Q 2.922(10) 4_566
S00I Na0S 2.869(6) 1_565
S00I Na0U 3.019(11) 4_566
S00I Na0W 3.079(10) 4_566
S00I Na00 3.096(6) 4_566
S00J Na0O 2.914(13) .
S00J Na0T 2.878(13) .
S00J Na0U 3.023(6) 4_556
S00J Cu0V 2.468(11) 3_757
S00J Cu0V 2.153(11) .
S00J Cu0X 2.120(4) .
S00K Na0O 3.069(3) 3_767
S00K Na0R 3.141(10) .
S00K Na0S 3.126(9) 1_565
S00K Na0U 3.020(11) 1_565
S00K Na0W 2.972(9) .
S00L Na0R 3.056(10) 1_565
S00L Na0S 3.132(10) 1_565
S00L Na0T 3.204(3) 3_767
S00L Na0U 2.956(10) 1_565
S00L Na0W 2.964(10) 1_565
S00L Na00 3.201(6) 1_565
Na0M Na0S 3.374(7) .
Na0M Na00 3.130(10) .
Na0M O010 2.407(11) .
Na0N Na0P 3.346(7) .
Na0N Na00 3.096(10) .
Na0N O00Z 2.404(11) .
Na0P Na00 3.099(11) .
Na0P O00Z 2.388(12) .
Na0Q Na0U 3.340(8) .
Na0Q Na00 3.106(11) .
Na0Q O010 2.414(11) .
Na0R Na0W 3.327(8) .
Na0R Na00 3.108(11) .
Na0R O00Z 2.331(12) .
Na0S Na0U 3.351(8) .
Na0S Na00 3.153(11) .
Na0S O010 2.344(12) .
Na0U Na00 3.121(11) .
Na0U O010 2.352(11) .
Cu0V Cu0V 1.87(2) 3_757
Cu0V Cu0X 0.933(11) .
Na0W Na00 3.173(10) .
Na0W O00Z 2.358(11) .
Na00 O00Z 2.10(2) .
Na00 O010 2.151(14) .
