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#$Date: 2017-08-08 16:56:54 +0300 (Tue, 08 Aug 2017) $
#$Revision: 199646 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/00/02/2000213.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000213
loop_
_publ_author_name
'Boström, D.'
'Strandberg, R.'
'Norén, B.'
'Oskarsson, Å.'
_publ_section_title
;
 cis/trans influences on square-planar platinum(II)
 complexes. Structure of cis-bis(dimethyl
 sulfoxide)dinitratoplatinum(II)
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              2101
_journal_page_last               2104
_journal_paper_doi               10.1107/S010827019100567X
_journal_volume                  47
_journal_year                    1991
_chemical_formula_sum            'C4 H12 N2 O8 Pt S2'
_chemical_formula_weight         475.36
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 117.880(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.0060(10)
_cell_length_b                   14.209(2)
_cell_length_c                   10.908(2)
_cell_volume                     1233.8(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    11.84
_exptl_crystal_density_diffrn    2.559
_exptl_crystal_F_000             896
_cod_data_source_file            ab0214.cif
_cod_data_source_block           ab0214a
_cod_depositor_comments
;
 Marking attached hydrogen atoms.

 Antanas Vaitkus,
 2017-08-08
;
_cod_original_cell_volume        1233.9(2)
_cod_original_formula_sum        'C4 H12 N2 O8 Pt1 S2'
_cod_database_code               2000213
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_attached_hydrogens
Pt .68507(6) .01137(3) .19513(5) .0217(2) 0
S1 .8090(4) .1469(2) .2886(4) .0292(12) 0
O1 .7110(13) .2118(7) .3269(11) .041(2) 0
C11 .867(2) .2040(12) .1689(18) .050(4) 3
C12 1.006(2) .1300(11) .4408(18) .047(4) 3
S2 .5517(4) .0110(2) .3218(3) .0243(11) 0
O2 .6649(12) .0220(7) .4707(10) .040(2) 0
C21 .3889(19) .0963(10) .2595(16) .039(3) 3
C22 .4365(17) -.0959(9) .2908(15) .033(3) 3
N1 .9449(15) -.0477(9) .1259(14) .038(5) 0
O11 .7940(11) -.0036(7) .0690(10) .037(4) 0
O12 1.0416(14) -.0391(10) .2474(13) .062(6) 0
O13 .9761(16) -.0954(9) .0462(14) .059(6) 0
N2 .6365(16) -.1813(8) .1037(14) .039(6) 0
O21 .5507(11) -.1036(6) .0834(10) .032(4) 0
O22 .7667(15) -.1908(8) .2092(14) .064(6) 0
O23 .5751(18) -.2407(8) .0154(14) .070(6) 0
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Pt S1 2.220(3)
Pt S2 2.214(3)
Pt O11 2.040(9)
Pt O21 2.059(9)
S1 O1 1.470(10)
S1 C11 1.81(2)
S1 C12 1.79(2)
S2 O2 1.470(10)
S2 C21 1.77(2)
S2 C22 1.780(10)
N1 O11 1.35(2)
N1 O12 1.20(2)
N1 O13 1.23(2)
N2 O21 1.310(10)
N2 O22 1.21(2)
N2 O23 1.20(2)
