#------------------------------------------------------------------------------
#$Date: 2016-02-19 16:29:56 +0200 (Fri, 19 Feb 2016) $
#$Revision: 176759 $
#$URL: svn://www.crystallography.net/cod/cif/2/00/04/2000467.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000467
loop_
_publ_author_name
'Khodadad, P.'
'Rodier, N.'
_publ_section_title
;
 Penta[bis(5-oxoprolinato)platinate(II) d'ammonium] monohydrate
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              2029
_journal_page_last               2031
_journal_paper_doi               10.1107/S0108270192003275
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         '5(C10 H15 N3 O6),H2 O1'
_chemical_formula_sum            'C50 H77 N15 O31 Pt5'
_chemical_formula_weight         2359.7
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.60(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.278(5)
_cell_length_b                   15.195(5)
_cell_length_c                   19.920(10)
_cell_volume                     3412(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    10.42
_exptl_crystal_density_diffrn    2.297
_exptl_crystal_density_meas      2.30(5)
_exptl_crystal_F_000             2240
_cod_data_source_file            du0338.cif
_cod_data_source_block           du0338a
_cod_original_cell_volume        3412(4)
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               2000467
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Pt(10) .39245(5) .250 .32736(3)
N(11) .4800(10) .3648(9) .3430(7)
C(12) .456(2) .4350(10) .3754(9)
C(13) .571(2) .4800(10) .3920(10)
C(14) .673(2) .4140(10) .3770(10)
C(15) .6100(10) .3520(10) .3278(9)
O(16) .3600(10) .4647(9) .3913(7)
C(17) .6430(10) .2610(10) .3311(8)
O(18) .7473(9) .2412(9) .3412(7)
O(19) .5597(8) .2026(8) .3217(6)
N'(11) .2240(10) .2766(9) .3371(6)
C'(12) .1530(10) .3490(10) .3319(8)
C'(13) .0230(10) .3180(10) .3323(9)
C'(14) .0250(10) .2200(10) .3280(10)
C'(15) .1560(10) .2030(10) .3517(7)
O'(16) .1850(10) .4244(9) .3223(7)
C'(17) .2130(10) .1220(10) .3212(9)
O'(18) .1630(10) .0497(9) .3121(7)
O'(19) .3250(10) .1282(8) .3111(6)
Pt(20) .64585(6) .15877(6) .96098(3)
N(21) .5340(10) .0630(10) .9849(7)
C(22) .526(2) .0090(10) 1.0320(10)
C(23) .408(2) -.0370(10) 1.0350(10)
C(24) .330(2) .0200(10) .9880(10)
C(25) .425(2) .072(2) .9463(8)
O(26) .6110(10) -.0190(10) 1.0734(8)
C(27) .3980(10) .1670(10) .9346(8)
O(28) .2970(10) .1960(10) .9249(7)
O(29) .4906(9) .2168(9) .9336(6)
N'(21) .8110(10) .1150(10) .9845(7)
C'(22) .859(2) .0360(10) 1.0002(9)
C'(23) .992(2) .0430(10) .9940(10)
C'(24) 1.012(2) .131(2) .9560(10)
C'(25) .901(2) .178(2) .9740(10)
O'(26) .7990(10) -.0296(9) 1.0173(8)
C'(27) .8540(10) .250(2) .9271(9)
O'(28) .9230(10) .3040(10) .8988(7)
O'(29) .7413(9) .2604(8) .9248(6)
Pt(30) .34223(6) .23665(5) .74535(3)
N(31) .2260(10) .1370(10) .7467(8)
C(32) .218(2) .0630(10) .7738(9)
C(33) .095(2) .025(2) .7660(10)
C(34) .017(2) .104(2) .7450(10)
C(35) .1090(10) .1660(10) .7143(8)
O(36) .3050(10) .0148(8) .7954(7)
C(37) .090(2) .2640(10) .7268(9)
O(38) -.0050(10) .2988(9) .7258(7)
O(39) .1940(10) .3074(9) .7324(7)
N'(31) .5020(10) .1820(10) .7623(7)
C'(32) .550(2) .1030(10) .7611(8)
C'(33) .682(2) .1160(10) .7640(10)
C'(34) .7090(10) .2140(10) .7520(10)
C'(35) .5920(10) .2520(10) .7775(8)
O'(36) .4990(10) .0322(7) .7560(7)
C'(37) .553(2) .3380(10) .7500(10)
O'(38) .6210(10) .4019(9) .7434(6)
O'(39) .4420(10) .3473(8) .7367(7)
Pt(40) .13160(5) .27483(5) .54038(3)
N(41) .0230(10) .1745(9) .5295(6)
C(42) .023(2) .0900(10) .5407(9)
C(43) -.0940(10) .0480(10) .5468(9)
C(44) -.174(2) .1270(10) .5550(10)
C(45) -.1080(10) .2020(10) .5192(8)
O(46) .1230(10) .0456(8) .5449(7)
C(47) -.1210(10) .2950(10) .5478(9)
O(48) -.2188(9) .3199(9) .5614(8)
O(49) -.0250(10) .3376(9) .5526(7)
N'(41) .2930(10) .2308(9) .5337(6)
C'(42) .3450(10) .1610(10) .5029(7)
C'(43) .4800(10) .1760(10) .5002(9)
C'(44) .4920(10) .2710(10) .5200(9)
C'(45) .3860(10) .2850(10) .5635(8)
O'(46) .2910(10) .0942(8) .4784(6)
C'(47) .3370(10) .3810(10) .5642(9)
O'(48) .4020(10) .4454(9) .5732(7)
O'(49) .2231(9) .3845(7) .5560(6)
Pt(50) .07560(5) .18219(5) .14758(3)
N(51) .1910(10) .2800(10) .1299(6)
C(52) .192(2) .3640(10) .1370(10)
C(53) .319(2) .395(2) .1350(10)
C(54) .392(2) .3150(10) .1360(10)
C(55) .3050(10) .2500(10) .1102(9)
O(56) .1030(10) .4127(9) .1481(7)
C(57) .3230(10) .1560(10) .1367(9)
O(58) .4230(10) .1200(10) .1418(7)
O(59) .2252(9) .1117(8) .1477(6)
N'(51) -.0830(10) .2381(8) .1508(6)
C'(52) -.1360(10) .3040(10) .1227(9)
C'(53) -.2680(10) .3020(10) .1280(10)
C'(54) -.2920(10) .2070(10) .1501(9)
C'(55) -.168(2) .1780(10) .1848(7)
O'(56) -.0830(10) .3669(9) .0964(7)
C'(57) -.135(2) .0880(10) .1807(9)
O'(58) -.1960(10) .0243(9) .1929(7)
O'(59) -.0206(9) .0735(8) .1679(6)
N(60) .5670(10) .0395(9) .2395(7)
N(61) .3550(10) .9580(10) .3948(7)
N(62) 1.1670(10) .3420(10) .8839(8)
N(63) .1590(10) .9330(10) .1911(9)
N(64) -.0520(10) -.0370(10) .3446(9)
O(65) .2340(10) .5690(10) .6198(9)
H(131) .577 .493 .440
H(132) .581 .531 .368
H(141) .701 .382 .415
H(142) .739 .443 .358
H(15) .630 .369 .282
H'(131) -.018 .345 .294
H'(132) -.014 .338 .372
H'(141) .014 .197 .282
H'(142) -.029 .190 .355
H'(15) .160 .193 .398
H(231) .379 -.038 1.081
H(232) .412 -.097 1.021
H(241) .282 .059 1.014
H(242) .280 -.015 .960
H(25) .421 .050 .901
H'(231) 1.018 -.008 .968
H'(232) 1.032 .039 1.037
H'(241) 1.016 .120 .911
H'(242) 1.079 .158 .975
H'(25) .923 .215 1.011
H(331) .070 .000 .809
H(332) .092 -.022 .734
H(341) -.021 .132 .782
H(342) -.044 .089 .712
H(35) .104 .157 .667
H'(331) .719 .081 .731
H'(332) .711 .100 .808
H'(341) .716 .225 .705
H'(342) .779 .232 .775
H'(35) .604 .267 .826
H(431) -.095 .010 .588
H(432) -.116 .012 .510
H(441) -.184 .142 .601
H(442) -.250 .117 .534
H(45) -.139 .204 .472
H'(431) .507 .166 .456
H'(432) .521 .138 .531
H'(441) .490 .308 .481
H'(442) .568 .280 .543
H'(45) .414 .277 .610
H(531) .341 .431 .174
H(532) .339 .428 .096
H(541) .420 .305 .183
H(542) .463 .325 .111
H(55) .314 .250 .061
H'(531) -.310 .314 .087
H'(532) -.297 .343 .161
H'(541) -.312 .167 .114
H'(542) -.355 .201 .183
H'(55) -.168 .182 .232
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N(11) Pt(10) O(19) 82.1(5)
N(11) Pt(10) N'(11) 106.1(5)
N(11) Pt(10) O'(19) 172.8(5)
O(19) Pt(10) N'(11) 170.8(6)
O(19) Pt(10) O'(19) 90.6(5)
N'(11) Pt(10) O'(19) 81.1(5)
Pt(10) N(11) C(12) 133.0(10)
Pt(10) N(11) C(15) 109.0(10)
C(12) N(11) C(15) 115.0(10)
N(11) C(12) C(13) 107(2)
N(11) C(12) O(16) 130(2)
C(13) C(12) O(16) 123(2)
C(12) C(13) C(14) 107(2)
C(13) C(14) C(15) 101.0(10)
N(11) C(15) C(14) 103.0(10)
N(11) C(15) C(17) 111.0(10)
C(14) C(15) C(17) 117.0(10)
C(15) C(17) O(18) 119.0(10)
C(15) C(17) O(19) 118.0(10)
O(18) C(17) O(19) 123(2)
Pt(10) O(19) C(17) 115.0(10)
Pt(10) N'(11) C'(12) 137.0(10)
Pt(10) N'(11) C'(15) 113.3(9)
C'(12) N'(11) C'(15) 110.0(10)
N'(11) C'(12) C'(13) 108.0(10)
N'(11) C'(12) O'(16) 126.0(10)
C'(13) C'(12) O'(16) 125(2)
C'(12) C'(13) C'(14) 107.0(10)
C'(13) C'(14) C'(15) 100.0(10)
N'(11) C'(15) C'(14) 109.0(10)
N'(11) C'(15) C'(17) 109.0(10)
C'(14) C'(15) C'(17) 115.0(10)
C'(15) C'(17) O'(18) 125.0(10)
C'(15) C'(17) O'(19) 115.0(10)
O'(18) C'(17) O'(19) 119(2)
Pt(10) O'(19) C'(17) 114.0(10)
N(21) Pt(20) O(29) 80.3(5)
N(21) Pt(20) N'(21) 107.0(6)
N(21) Pt(20) O'(29) 171.0(5)
O(29) Pt(20) N'(21) 172.7(5)
O(29) Pt(20) O'(29) 92.1(4)
N'(21) Pt(20) O'(29) 80.7(5)
Pt(20) N(21) C(22) 136.0(10)
Pt(20) N(21) C(25) 110.0(10)
C(22) N(21) C(25) 113(2)
N(21) C(22) C(23) 114(2)
N(21) C(22) O(26) 128(2)
C(23) C(22) O(26) 117(2)
C(22) C(23) C(24) 102(2)
C(23) C(24) C(25) 103.0(10)
N(21) C(25) C(24) 105.0(10)
N(21) C(25) C(27) 110(2)
C(24) C(25) C(27) 115.0(10)
C(25) C(27) O(28) 124(2)
C(25) C(27) O(29) 114.0(10)
O(28) C(27) O(29) 122(2)
Pt(20) O(29) C(27) 116.0(10)
Pt(20) N'(21) C'(22) 135.0(10)
Pt(20) N'(21) C'(25) 114.0(10)
C'(22) N'(21) C'(25) 111.0(10)
N'(21) C'(22) C'(23) 108(2)
N'(21) C'(22) O'(26) 124(2)
C'(23) C'(22) O'(26) 128(2)
C'(22) C'(23) C'(24) 105(2)
C'(23) C'(24) C'(25) 100(2)
N'(21) C'(25) C'(24) 109(2)
N'(21) C'(25) C'(27) 110.0(10)
C'(24) C'(25) C'(27) 119(2)
C'(25) C'(27) O'(28) 121.0(10)
C'(25) C'(27) O'(29) 116(2)
O'(28) C'(27) O'(29) 122(2)
Pt(20) O'(29) C'(27) 116.0(10)
N(31) Pt(30) O(39) 82.0(6)
N(31) Pt(30) N'(31) 105.5(6)
N(31) Pt(30) O'(39) 171.8(5)
O(39) Pt(30) N'(31) 172.0(6)
O(39) Pt(30) O'(39) 90.4(4)
N'(31) Pt(30) O'(39) 82.2(6)
Pt(30) N(31) C(32) 138.0(10)
Pt(30) N(31) C(35) 110.0(10)
C(32) N(31) C(35) 112(2)
N(31) C(32) C(33) 112(2)
C(33) C(32) O(36) 121(2)
C(32) C(33) C(34) 104(2)
C(33) C(34) C(35) 101(2)
N(31) C(35) C(34) 104(2)
N(31) C(35) C(37) 110.0(10)
C(34) C(35) C(37) 116(2)
C(35) C(37) O(38) 124(2)
C(35) C(37) O(39) 111(2)
O(38) C(37) O(39) 124(2)
Pt(30) O(39) C(37) 118.0(10)
Pt(30) N'(31) C'(32) 138.0(10)
Pt(30) N'(31) C'(35) 110.0(10)
C'(32) N'(31) C'(35) 112.0(10)
N'(31) C'(32) C'(33) 107(2)
N'(31) C'(32) O'(36) 127(2)
C')33) C'(32) O'(36) 126(2)
C'(32) C'(33) C'(34) 109(2)
C'(33) C'(34) C'(35) 98.0(10)
N'(31) C'(35) C'(34) 105.0(10)
N'(31) C'(35) C'(37) 111.0(10)
C'(34) C'(35) C'(37) 117(2)
C'(35) C'(37) O'(38) 123(2)
C'(35) C'(37) O'(39) 117(2)
O'(38) C'(37) O'(39) 120(2)
Pt(30) O'(39) C'(37) 116.0(10)
N(41) Pt(40) O(49) 80.4(6)
N(41) Pt(40) N'(41) 107.9(6)
N(41) Pt(40) O'(49) 172.4(4)
O(49) Pt(40) N'(41) 171.4(5)
O(49) Pt(40) O'(49) 92.1(4)
N'(41) Pt(40) O'(49) 79.4(5)
Pt(40) N(41) C(42) 138.0(10)
Pt(40) N(41) C(45) 113.0(10)
C(42) N(41) C(45) 107.0(10)
N(41) C(42) C(43) 116.0(10)
N(41) C(42) O(46) 121(2)
C(43) C(42) O(46) 123(2)
C(42) C(43) C(44) 101.0(10)
C(43) C(45) C(45) 104.0(10)
N(41) C(45) C(44) 102.0(10)
N(41) C(45) C(47) 108.0(10)
C(44) C(45) C(47) 117.0(10)
C(45) C(47) O(48) 118.0(10)
C(45) C(47) O(49) 114.0(10)
O(48) C(47) O(49) 127(2)
Pt(40) O(49) C(47) 120.0(10)
Pt(40) N'(41) C'(42) 136.0(10)
Pt(40) N'(41) C'(45) 116.0(10)
C'(42) N'(41) C'(45) 108.0(10)
N'(41) C'(42) C'(48) 110.0(10)
N'(41) C'(42) O'(46) 125.0(10)
C'(43) C'(42) O'(46) 124.0(10)
C'(42) C'(43) C'(44) 102.0(10)
C'(43) C'(44) C'(45) 103.0(10)
N'(41) C'(45) C'(44) 105.0(10)
N'(41) C'(45) C'(47) 106.0(10)
C'(44) C'(45) C'(47) 115.0(10)
C'(45) C'(47) O'(48) 122.0(10)
C'(45) C'(47) O'(49) 113.0(10)
O'(48) C'(47) O'(49) 125(2)
Pt(40) O'(49) C'(47) 120.0(10)
N(51) Pt(50) O(59) 81.2(5)
N(51) Pt(50) N'(51) 106.2(6)
N(51) Pt(50) O'(59) 172.2(5)
O(59) Pt(50) N'(51) 172.6(5)
O(59) Pt(50) O'(59) 91.1(5)
N'(51) Pt(50) O'(59) 81.1(5)
Pt(50) N(51) C(52) 136.0(10)
Pt(50) N(51) C(55) 114.0(10)
C(52) N(51) C(55) 110.0(10)
N(51) C(52) C(53) 108(2)
N(51) C(52) O(56) 126(2)
C(53) C(52) O(56) 125(2)
C(52) C(53) C(54) 106(2)
C(53) C(54) C(55) 101(2)
N(51) C(55) C(54) 107(2)
N(51) C(55) C(57) 108.0(10)
C(54) C(55) C(57) 115.0(10)
C(55) C(57) O(58) 123(2)
C(55) C(57) O(59) 115.0(10)
O(58) C(57) O(59) 121(2)
Pt(50) O(59) C(57) 116.0(10)
Pt(50) N'(51) C'(52) 136.0(10)
Pt(50) N'(51) C'(55) 110.1(9)
C'(52) N'(51) C'(55) 112.0(10)
N'(51) C'(52) C'(53) 114.0(10)
N'(51) C'(52) O'(56) 124.0(10)
C'(53) C'(52) O'(56) 122.0(10)
C'(52) C'(53) C'(54) 103.0(10)
C'(53) C'(54) C'(55) 103.0(10)
N'(51) C'(55) C'(54) 101.0(10)
N'(51) C'(55) C'(57) 113.0(10)
C'(54) C'(55) C'(57) 118.0(10)
C'(55) C'(57) O'(58) 127(2)
C'(55) C'(57) O'(59) 115(2)
O'(58) C'(57) O'(59) 118(2)
Pt(50) O'(59) C'(57) 116.0(10)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Pt(10) N(11) 2.030(10)
Pt(10) O(19) 2.030(10)
Pt(10) N'(11) 1.960(10)
Pt(10) O'(19) 2.020(10)
N(11) C(12) 1.28(2)
N(11) C(15) 1.52(2)
C(12) C(13) 1.50(3)
C(12) O(16) 1.22(2)
C(13) C(14) 1.56(3)
C(14) C(15) 1.51(3)
C(15) C(17) 1.44(2)
C(17) O(18) 1.23(2)
C(17) O(19) 1.29(2)
N'(11) C'(12) 1.37(2)
N'(11) C'(15) 1.40(2)
C'(12) C'(13) 1.54(2)
C'(12) O'(16) 1.21(2)
C'(13) C'(14) 1.50(3)
C'(14) C'(15) 1.56(2)
C'(15) C'(17) 1.53(2)
C'(17) O'(18) 1.24(2)
C'(17) O'(19) 1.29(2)
C(13) H(131) .97
C(13) H(132) .93
C(14) H(141) .95
C(14) H(142) .97
C(15) H(15) .97
C'(13) H'(131) .96
C'(13) H'(132) .95
C'(14) H'(141) .99
C'(14) H'(142) .94
C'(15) H'(15) .93
Pt(20) N(21) 1.99(2)
Pt(20) O(29) 2.020(10)
Pt(20) N'(21) 2.020(10)
Pt(20) O'(29) 2.030(10)
N(21) C(22) 1.26(3)
N(21) C(25) 1.43(2)
C(22) C(23) 1.51(3)
C(22) O(26) 1.31(2)
C(23) C(24) 1.54(3)
C(24) C(25) 1.58(3)
C(25) C(27) 1.49(3)
C(27) O(28) 1.24(2)
C(27) O(29) 1.29(2)
N'(21) C'(22) 1.35(3)
N'(21) C'(25) 1.42(3)
C'(22) C'(23) 1.52(3)
C'(22) O'(26) 1.25(3)
C'(23) C'(24) 1.54(3)
C'(24) C'(25) 1.49(3)
C'(25) C'(27) 1.53(3)
C'(27) O'(28) 1.26(2)
C'(27) O'(29) 1.28(2)
C(23) H(231) .98
C(23) H(232) .95
C(24) H(241) .97
C(24) H(242) .94
C(25) H(25) .96
C'(23) H'(231) .98
C'(23) H'(232) .96
C'(24) H'(241) .92
C'(24) H'(242) .93
C'(25) H'(25) .97
Pt(30) N(31) 2.00(2)
Pt(30) O(39) 2.000(10)
Pt(30) N'(31) 2.000(10)
Pt(30) O'(39) 2.030(10)
N(31) C(32) 1.26(3)
N(31) C(35) 1.52(2)
C(32) C(33) 1.50(3)
C(32) O(36) 1.29(2)
C(33) C(34) 1.55(3)
C(34) C(35) 1.54(3)
C(35) C(37) 1.52(3)
C(37) O(38) 1.19(2)
C(37) O(39) 1.35(2)
N'(31) C'(32) 1.32(3)
N'(31) C'(35) 1.50(2)
C'(32) C'(33) 1.50(3)
C'(32) O'(36) 1.22(2)
C'(33) C'(34) 1.54(3)
C'(34) C'(35) 1.53(2)
C'(35) C'(37) 1.48(3)
C'(37) O'(38) 1.25(2)
C'(37) O'(39) 1.29(2)
C(33) H(331) .98
C(33) H(332) .95
C(34) H(341) .97
C(34) H(342) .96
C(35) H(35) .96
C'(33) H'(331) .94
C'(33) H'(332) .96
C'(34) H'(341) .96
C'(34) H'(342) .95
C'(35) H'(35) 1.00
Pt(40) N(41) 1.970(10)
Pt(40) O(49) 2.030(10)
Pt(40) N'(41) 1.940(10)
Pt(40) O'(49) 1.980(10)
N(41) C(42) 1.31(2)
N(41) C(45) 1.54(2)
C(42) C(43) 1.48(2)
C(42) O(46) 1.32(2)
C(43) C(44) 1.51(2)
C(44) C(45) 1.54(3)
C(45) C(47) 1.53(3)
C(47) O(48) 1.21(2)
C(47) O(49) 1.26(2)
N'(41) C'(42) 1.37(2)
N'(41) C'(45) 1.45(2)
C'(42) C'(43) 1.54(2)
C'(42) O'(46) 1.28(2)
C'(43) C'(44) 1.50(3)
C'(44) C'(45) 1.51(2)
C'(45) C'(47) 1.55(2)
C'(47) O'(48) 1.24(2)
C'(47) O'(49) 1.29(2)
C(43) H(431) .99
C(43) H(432) .94
C(44) H(441) .95
C(44) H(442) .96
C(45) H(45) 1.00
C'(43) H'(431) .95
C'(43) H'(432) .94
C'(44) H'(441) .95
C'(44) H'(442) .97
C'(45) H'(45) .98
Pt(50) N(51) 2.010(10)
Pt(50) O(59) 2.000(10)
Pt(50) N'(51) 1.990(10)
Pt(50) O'(59) 2.020(10)
N(51) C(52) 1.29(2)
N(51) C(55) 1.43(2)
C(52) C(53) 1.51(3)
C(52) O(56) 1.28(2)
C(53) C(54) 1.47(3)
C(54) C(55) 1.48(3)
C(55) C(57) 1.53(3)
C(57) O(58) 1.26(2)
C(57) O(59) 1.32(2)
N'(51) C'(52) 1.28(2)
N'(51) C'(55) 1.50(2)
C'(52) C'(53) 1.50(2)
C'(52) O'(56) 1.25(2)
C'(53) C'(54) 1.53(2)
C'(54) C'(55) 1.60(2)
C'(55) C'(57) 1.43(3)
C'(57) O'(58) 1.21(2)
C'(57) O'(59) 1.33(2)
C(53) H(531) .97
C(53) H(532) .95
C(54) H(541) .98
C(54) H(542) .97
C(55) H(55) .98
C'(53) H'(531) .96
C'(53) H'(532) .98
C'(54) H'(541) .95
C'(54) H'(542) .99
C'(55) H'(55) .95
