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#$Date: 2023-11-10 21:21:08 +0200 (Fri, 10 Nov 2023) $
#$Revision: 287519 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/00/07/2000734.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000734
loop_
_publ_author_name
'Averbuch-Pouchot, M.-T.'
'Durif, A.'
_publ_section_title
;
 Structure of nonasilver sodium cyclo-octaphosphate dinitrate
 tetrahydrate: Ag₉NaP₈O₂₄(NO₃)₂.4H₂O
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1173
_journal_page_last               1176
_journal_paper_doi               10.1107/S0108270191014543
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'Ag9 Na1 O24 P8,2(N1 O3),4(H2 O1)'
_chemical_formula_sum            'Ag9 H8 N2 Na O34 P8'
_chemical_formula_weight         1821.638
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.254(5)
_cell_length_b                   7.5430(10)
_cell_length_c                   23.465(5)
_cell_volume                     3054(2)
_diffrn_radiation_type           Ag
_diffrn_radiation_wavelength     0.5608
_exptl_absorpt_coefficient_mu    3.086
_exptl_crystal_density_diffrn    3.961
_exptl_crystal_F_000             3392
_cod_data_source_file            pa0262.cif
_cod_data_source_block           pa0262a
_cod_original_formula_sum        'Ag9 H8 N2 Na1 O34 P8'
_cod_database_code               2000734
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Ag(1) .0 .33850(10) .03390(4)
Ag(2) .21658(5) .37180(10) .14692(3)
Ag(3) .38723(8) .2476(2) .25
Ag(4) .31600(10) .0 .0
Na(4) .3160 .0 .0
P(1) .13760(10) .0385(3) .43819(8)
P(2) .41600(10) .2084(2) .38980(7)
O(E11) .1192(4) .2272(8) .0765(2)
O(L11) .1012(4) .0 .0
O(L12) .4166(3) .4188(7) .3990(2)
O(E12) .2816(3) .4734(9) .0650(2)
O(E21) .4128(4) .1185(8) .0533(2)
O(E22) .3582(4) .1593(8) .1541(2)
O(L22) .5 .1843(9) .3612(3)
N .1828(6) .1520(10) .25
O(1) .2096(8) .305(2) .25
O(2) .1701(5) .0770(10) .2043(3)
O(W1) .0 .2390(10) .1692(4)
O(W2) .0 .958(2) .25
O(W3) .0 .522(2) .25
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
P(1) O(E11) 1.499(6)
P(1) O(L11) 1.607(3)
P(1) O(L12) 1.593(5)
P(1) O(E12) 1.479(6)
P(1) P(1) 2.958(2)
P(1) P(2) 2.889(3)
P(2) P(2) 2.900(3)
Ag(1) O(E11) 2.436(6)
Ag(1) O(E21) 2.633(6)
Ag(1) O(E21) 2.561(5)
Ag(4) O(E11) 2.950(6)
Ag(4) O(E12) 2.281(6)
Ag(4) O(E21) 2.270(6)
Ag(2) O(E11) 2.597(6)
Ag(2) O(E12) 2.354(6)
Ag(2) O(E22) 2.528(6)
Ag(2) O(E22) 2.927(6)
Ag(2) O(1) 2.474(2)
Ag(2) O(2) 2.719(8)
Ag(2) O(2) 2.834(8)
Ag(3) O(E22) 2.401(5)
Ag(3) O(2) 2.883(8)
Ag(3) O(W2) 2.512(10)
Ag(3) O(W3) 2.584(11)
N O(1) 1.24(2)
N O(2) 1.231(9)
_cod_duplicate_entry 1007200
