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#$Date: 2016-02-14 16:26:36 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176435 $
#$URL: svn://www.crystallography.net/cod/cif/2/00/19/2001941.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2001941
loop_
_publ_author_name
'Loris, R.'
'Maes, D.'
'Lisgarten, J. N.'
'Bettinelli, M.'
'Flint, C.'
_publ_section_title
;
 Structure of bis(tetramethylammonium) hexachlororhenate(IV)
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              231
_journal_page_last               233
_journal_paper_doi               10.1107/S0108270192005444
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         '2(C4 H12 N1),Cl6 Re1'
_chemical_formula_sum            'C8 H24 Cl6 N2 Re'
_chemical_formula_weight         547.2
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-F 4 2 3'
_symmetry_space_group_name_H-M   'F m -3 m'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   12.760(2)
_cell_length_b                   12.760(2)
_cell_length_c                   12.760(2)
_cell_volume                     2077.6(6)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    7.5
_exptl_crystal_density_diffrn    1.7505(6)
_exptl_crystal_F_000             1052
_cod_data_source_file            li1000.cif
_cod_data_source_block           li1000a
_cod_original_cell_volume        2077.5(6)
_cod_original_formula_sum        'C8 H24 Cl6 N2 Re1'
_cod_database_code               2001941
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Re .0 .0 .0 .0410(10)
Cl .1850(10) .0 .0 .09(2)
N .25 .25 .25 .044(19)
C .314(3) .314(3) .314(3) .15(3)
H .265(3) .363(3) .363(3) .19(17)
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
Cl Re Cl 90
C N C 109.5
H C H 109.5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Re Cl 2.360(2)
N C 1.42(6)
C H 1.03(6)
