#------------------------------------------------------------------------------
#$Date: 2016-02-19 16:29:56 +0200 (Fri, 19 Feb 2016) $
#$Revision: 176759 $
#$URL: svn://www.crystallography.net/cod/cif/2/00/70/2007094.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2007094
loop_
_publ_author_name
'Baumeister, Ute'
'Hartung, Helmut'
'Schulz, Torsten'
'Weichmann, Horst'
_publ_section_title
;
 cis-Bis[(2-diphenylphosphinoethyl)dimethylstannyl]platinum(II)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              333
_journal_page_last               335
_journal_paper_doi               10.1107/S0108270197014029
_journal_volume                  54
_journal_year                    1998
_chemical_formula_iupac          '[Pt Sn2 (CH3)4 (C14 H14 P)2]'
_chemical_formula_moiety         'C32 H40 P2 Pt Sn2'
_chemical_formula_structural     'Pt ((C6 H5)2 P (C2 H4) SN (C H3)2)2'
_chemical_formula_sum            'C32 H40 P2 Pt Sn2'
_chemical_formula_weight         919.05
_chemical_melting_point          456.1(10)
_chemical_name_systematic
;
  cis-Bis[(2-Diphenylphosphinoethyl)dimethylstannyl]platinum(II)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_method           SHELXL
_cell_angle_alpha                90.00
_cell_angle_beta                 103.144(15)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.801(2)
_cell_length_b                   13.206(3)
_cell_length_c                   21.697(4)
_cell_measurement_reflns_used    76
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      17.1
_cell_measurement_theta_min      10.1
_cell_volume                     3292.8(11)
_computing_cell_refinement       DIF4
_computing_data_collection       'DIF4 (Stoe, 19??)'
_computing_data_reduction        'REDU4 (Stoe, 19??)'
_computing_molecular_graphics    'XP/PC (Siemens, 1990)'
_computing_publication_material  SHELXL93
_computing_structure_refinement  'SHELXL93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device       'Stoe Stadi-4'
_diffrn_measurement_method       ω/2θ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0209
_diffrn_reflns_av_sigmaI/netI    0.0256
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            17011
_diffrn_reflns_theta_max         28.0
_diffrn_reflns_theta_min         1.81
_diffrn_standards_decay_%        5.9
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    5.859
_exptl_absorpt_correction_T_max  0.136
_exptl_absorpt_correction_T_min  0.102
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.854
_exptl_crystal_density_meas      ?
_exptl_crystal_description       irregular
_exptl_crystal_F_000             1760
_exptl_crystal_size_max          0.53
_exptl_crystal_size_mid          0.36
_exptl_crystal_size_min          0.34
_refine_diff_density_max         1.239
_refine_diff_density_min         -1.022
_refine_ls_extinction_coef       0.00023(5)
_refine_ls_extinction_method     SHELXL93_(Sheldrick,_1993)
_refine_ls_goodness_of_fit_all   1.085
_refine_ls_goodness_of_fit_obs   1.138
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     335
_refine_ls_number_reflns         7945
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.085
_refine_ls_restrained_S_obs      1.138
_refine_ls_R_factor_all          0.0411
_refine_ls_R_factor_obs          .0285
_refine_ls_shift/esd_max         -0.001
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[σ²(Fo²)+(0.0369P)²+2.0278P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0712
_refine_ls_wR_factor_obs         .0673
_reflns_number_observed          6514
_reflns_number_total             7945
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            jz1255.cif
_cod_data_source_block           s261
_cod_depositor_comments
;
The following automatic conversions were performed:
'_geom_bond_publ_flag' value 'YES' changed to 'yes' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (4 times).

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_chemical_melting_point' value '182 - 184_C' was changed to
'456.1(10)' - it was converted from degrees Celsius(C) to Kelvins(K),
the average value was taken and precision was estimated.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_chemical_melting_point' value '182 - 184_C' was changed to
'456.1(10)' - it was converted from degrees Celsius(C) to Kelvins(K),
the average value was taken and precision was
estimated.

'_geom_bond_publ_flag' value 'YES' changed to 'yes'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29 (4
times).

'_geom_angle_publ_flag' value 'YES' changed to 'yes'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29 (4
times).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc w =
1/[\s^2^(Fo^2^)+(0.0369P)^2^+2.0278P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(Fo^2^)+(0.0369P)^2^+2.0278P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2007094
_cod_database_fobs_code          2007094
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_group
_atom_site_type_symbol
Pt1 .051540(10) .179440(10) .155460(10) .03216(5) Uani d . 1 . Pt
Sn1 .25989(2) .18215(2) .133990(10) .03938(7) Uani d . 1 . Sn
Sn2 .13009(2) .05585(2) .248480(10) .03921(7) Uani d . 1 . Sn
P1 .01792(9) .29913(7) .07727(5) .0337(2) Uani d . 1 . P
P2 -.11826(9) .16265(8) .18815(5) .0362(2) Uani d . 1 . P
C1 .2562(4) .3314(3) .0878(2) .0501(10) Uani d . 1 . C
H1A .3210(4) .3720(3) .1104(2) .060 Uiso calc R 1 . H
H1B .2647(4) .3225(3) .0447(2) .060 Uiso calc R 1 . H
C2 .1424(3) .3865(3) .0871(2) .0418(9) Uani d . 1 . C
H2A .1277(3) .4353(3) .0528(2) .050 Uiso calc R 1 . H
H2B .1499(3) .4234(3) .1265(2) .050 Uiso calc R 1 . H
C3 -.0351(4) -.0019(4) .2675(2) .0527(11) Uani d . 1 . C
H3A -.0334(4) -.0754(4) .2686(2) .063 Uiso calc R 1 . H
H3B -.0434(4) .0220(4) .3086(2) .063 Uiso calc R 1 . H
C4 -.1383(4) .0335(3) .2168(2) .0482(10) Uani d . 1 . C
H4A -.2077(4) .0322(3) .2337(2) .058 Uiso calc R 1 . H
H4B -.1502(4) -.0132(3) .1813(2) .058 Uiso calc R 1 . H
C5 .4161(4) .1768(5) .2097(3) .0665(15) Uani d . 1 . C
H5A .4088(4) .2237(5) .2423(3) .100 Uiso calc R 1 . H
H5B .4823(4) .1948(5) .1932(3) .100 Uiso calc R 1 . H
H5C .4262(4) .1096(5) .2269(3) .100 Uiso calc R 1 . H
C6 .2913(5) .0730(4) .0653(3) .0688(15) Uani d . 1 . C
H6A .2254(5) .0709(4) .0300(3) .103 Uiso calc R 1 . H
H6B .3032(5) .0072(4) .0846(3) .103 Uiso calc R 1 . H
H6C .3593(5) .0924(4) .0509(3) .103 Uiso calc R 1 . H
C7 .2450(4) -.0672(3) .2375(2) .0556(12) Uani d . 1 . C
H7A .2131(4) -.1029(3) .1989(2) .083 Uiso calc R 1 . H
H7B .2529(4) -.1128(3) .2727(2) .083 Uiso calc R 1 . H
H7C .3200(4) -.0405(3) .2360(2) .083 Uiso calc R 1 . H
C8 .2142(5) .1270(4) .3365(2) .0633(13) Uani d . 1 . C
H8A .1679(5) .1830(4) .3448(2) .095 Uiso calc R 1 . H
H8B .2897(5) .1510(4) .3337(2) .095 Uiso calc R 1 . H
H8C .2226(5) .0787(4) .3703(2) .095 Uiso calc R 1 . H
C9 .0037(3) .2508(3) -.0026(2) .0355(8) Uani d . 1 . C
C10 .0254(4) .3111(3) -.0506(2) .0469(10) Uani d . 1 . C
H10 .0445(4) .3790(3) -.0427(2) .056 Uiso calc R 1 . H
C11 .0190(4) .2716(4) -.1101(2) .0541(11) Uani d . 1 . C
H11 .0329(4) .3130(4) -.1423(2) .065 Uiso calc R 1 . H
C12 -.0083(4) .1701(4) -.1222(2) .0581(13) Uani d . 1 . C
H12 -.0115(4) .1436(4) -.1622(2) .070 Uiso calc R 1 . H
C13 -.0305(5) .1089(4) -.0751(3) .0658(14) Uani d . 1 . C
H13 -.0489(5) .0409(4) -.0831(3) .079 Uiso calc R 1 . H
C14 -.0251(4) .1496(4) -.0157(2) .0511(11) Uani d . 1 . C
H14 -.0411(4) .1085(4) .0160(2) .061 Uiso calc R 1 . H
C15 -.1038(4) .3862(3) .0720(2) .0422(9) Uani d . 1 . C
C16 -.1958(4) .3937(4) .0191(2) .0532(11) Uani d . 1 . C
H16 -.1967(4) .3538(4) -.0163(2) .064 Uiso calc R 1 . H
C17 -.2864(5) .4608(5) .0193(3) .076(2) Uani d . 1 . C
H17 -.3468(5) .4663(5) -.0165(3) .091 Uiso calc R 1 . H
C18 -.2879(6) .5191(5) .0714(4) .087(2) Uani d . 1 . C
H18 -.3487(6) .5641(5) .0709(4) .104 Uiso calc R 1 . H
C19 -.1996(6) .5106(4) .1240(4) .080(2) Uani d . 1 . C
H19 -.2013(6) .5491(4) .1596(4) .096 Uiso calc R 1 . H
C20 -.1066(5) .4447(4) .1249(3) .0586(12) Uani d . 1 . C
H20 -.0465(5) .4401(4) .1609(3) .070 Uiso calc R 1 . H
C21 -.2548(3) .1875(3) .1315(2) .0426(9) Uani d . 1 . C
C22 -.3284(4) .2672(4) .1362(2) .0481(10) Uani d . 1 . C
H22 -.3109(4) .3098(4) .1713(2) .058 Uiso calc R 1 . H
C23 -.4272(4) .2842(4) .0896(3) .0616(13) Uani d . 1 . C
H23 -.4765(4) .3374(4) .0939(3) .074 Uiso calc R 1 . H
C24 -.4537(5) .2236(5) .0370(3) .074(2) Uani d . 1 . C
H24 -.5200(5) .2364(5) .0055(3) .088 Uiso calc R 1 . H
C25 -.3825(5) .1443(5) .0311(3) .075(2) Uani d . 1 . C
H25 -.4011(5) .1023(5) -.0041(3) .089 Uiso calc R 1 . H
C26 -.2827(5) .1264(4) .0776(3) .0634(13) Uani d . 1 . C
H26 -.2337(5) .0732(4) .0729(3) .076 Uiso calc R 1 . H
C27 -.1207(4) .2419(3) .2566(2) .0401(8) Uani d . 1 . C
C28 -.2087(4) .2359(4) .2900(2) .0523(11) Uani d . 1 . C
H28 -.2712(4) .1922(4) .2763(2) .063 Uiso calc R 1 . H
C29 -.2028(5) .2950(4) .3436(2) .0616(13) Uani d . 1 . C
H29 -.2611(5) .2901(4) .3660(2) .074 Uiso calc R 1 . H
C30 -.1116(5) .3604(5) .3637(3) .071(2) Uani d . 1 . C
H30 -.1085(5) .3996(5) .3997(3) .086 Uiso calc R 1 . H
C31 -.0254(5) .3686(5) .3314(3) .0694(15) Uani d . 1 . C
H31 .0355(5) .4139(5) .3449(3) .083 Uiso calc R 1 . H
C32 -.0291(4) .3089(4) .2783(2) .0539(11) Uani d . 1 . C
H32 .0306(4) .3137(4) .2568(2) .065 Uiso calc R 1 . H
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C .0033 .0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H .0000 .0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P .1023 .0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
P2 Pt1 P1 106.33(4) yes
P2 Pt1 Sn2 83.16(3) yes
P1 Pt1 Sn2 169.13(3) ?
P2 Pt1 Sn1 170.98(3) ?
P1 Pt1 Sn1 82.49(3) yes
Sn2 Pt1 Sn1 87.88(2) yes
C6 Sn1 C5 104.5(2) ?
C6 Sn1 C1 105.7(2) ?
C5 Sn1 C1 107.3(2) ?
C6 Sn1 Pt1 115.5(2) ?
C5 Sn1 Pt1 122.5(2) ?
C1 Sn1 Pt1 99.86(12) ?
C8 Sn2 C7 104.5(2) ?
C8 Sn2 C3 103.4(2) ?
C7 Sn2 C3 111.2(2) ?
C8 Sn2 Pt1 115.16(15) ?
C7 Sn2 Pt1 120.55(13) ?
C3 Sn2 Pt1 100.81(12) ?
C9 P1 C15 105.2(2) ?
C9 P1 C2 103.3(2) ?
C15 P1 C2 102.0(2) ?
C9 P1 Pt1 115.27(14) ?
C15 P1 Pt1 118.92(14) ?
C2 P1 Pt1 110.33(14) ?
C21 P2 C27 105.7(2) ?
C21 P2 C4 103.4(2) ?
C27 P2 C4 103.2(2) ?
C21 P2 Pt1 118.54(14) ?
C27 P2 Pt1 112.03(14) ?
C4 P2 Pt1 112.48(15) ?
C2 C1 Sn1 110.9(3) ?
C1 C2 P1 112.3(3) ?
C4 C3 Sn2 110.6(3) ?
C3 C4 P2 112.7(3) ?
C10 C9 C14 118.5(4) ?
C10 C9 P1 121.5(3) ?
C14 C9 P1 119.9(3) ?
C11 C10 C9 120.5(4) ?
C10 C11 C12 120.1(5) ?
C13 C12 C11 120.2(4) ?
C12 C13 C14 119.1(5) ?
C13 C14 C9 121.5(4) ?
C20 C15 C16 118.7(4) ?
C20 C15 P1 117.8(4) ?
C16 C15 P1 123.5(4) ?
C17 C16 C15 120.0(5) ?
C18 C17 C16 121.0(6) ?
C19 C18 C17 119.5(5) ?
C18 C19 C20 120.8(6) ?
C15 C20 C19 120.0(6) ?
C22 C21 C26 118.0(4) ?
C22 C21 P2 124.1(4) ?
C26 C21 P2 117.7(3) ?
C23 C22 C21 120.7(5) ?
C24 C23 C22 120.7(5) ?
C25 C24 C23 119.8(5) ?
C24 C25 C26 120.1(6) ?
C25 C26 C21 120.7(5) ?
C32 C27 C28 118.2(4) ?
C32 C27 P2 119.0(3) ?
C28 C27 P2 122.8(3) ?
C29 C28 C27 120.0(5) ?
C30 C29 C28 120.4(5) ?
C31 C30 C29 120.5(5) ?
C30 C31 C32 119.8(5) ?
C31 C32 C27 121.0(5) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Pt1 P2 . 2.2833(10) yes
Pt1 P1 . 2.2865(10) yes
Pt1 Sn2 . 2.5973(5) yes
Pt1 Sn1 . 2.6047(5) yes
Sn1 C6 . 2.165(5) ?
Sn1 C5 . 2.174(5) ?
Sn1 C1 . 2.207(4) ?
Sn2 C8 . 2.158(5) ?
Sn2 C7 . 2.164(4) ?
Sn2 C3 . 2.219(5) ?
P1 C9 . 1.818(4) ?
P1 C15 . 1.823(4) ?
P1 C2 . 1.842(4) ?
P2 C21 . 1.821(4) ?
P2 C27 . 1.823(4) ?
P2 C4 . 1.849(4) ?
C1 C2 . 1.524(6) ?
C3 C4 . 1.518(6) ?
C9 C10 . 1.382(6) ?
C9 C14 . 1.392(6) ?
C10 C11 . 1.379(6) ?
C11 C12 . 1.389(7) ?
C12 C13 . 1.374(7) ?
C13 C14 . 1.384(7) ?
C15 C20 . 1.390(7) ?
C15 C16 . 1.393(6) ?
C16 C17 . 1.388(7) ?
C17 C18 . 1.372(9) ?
C18 C19 . 1.363(10) ?
C19 C20 . 1.397(8) ?
C21 C22 . 1.383(6) ?
C21 C26 . 1.397(7) ?
C22 C23 . 1.378(7) ?
C23 C24 . 1.370(8) ?
C24 C25 . 1.367(9) ?
C25 C26 . 1.386(7) ?
C27 C32 . 1.394(6) ?
C27 C28 . 1.397(6) ?
C28 C29 . 1.390(7) ?
C29 C30 . 1.372(9) ?
C30 C31 . 1.365(8) ?
C31 C32 . 1.389(7) ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
P2 Pt1 Sn1 C6 99.7(3)
P1 Pt1 Sn1 C6 -92.2(2)
Sn2 Pt1 Sn1 C6 92.9(2)
P2 Pt1 Sn1 C5 -29.5(3)
P1 Pt1 Sn1 C5 138.6(2)
Sn2 Pt1 Sn1 C5 -36.3(2)
P2 Pt1 Sn1 C1 -147.5(2)
P1 Pt1 Sn1 C1 20.66(14)
Sn2 Pt1 Sn1 C1 -154.28(13)
P2 Pt1 Sn2 C8 -95.0(2)
P1 Pt1 Sn2 C8 56.3(2)
Sn1 Pt1 Sn2 C8 84.0(2)
P2 Pt1 Sn2 C7 138.3(2)
P1 Pt1 Sn2 C7 -70.4(2)
Sn1 Pt1 Sn2 C7 -42.8(2)
P2 Pt1 Sn2 C3 15.56(14)
P1 Pt1 Sn2 C3 166.9(2)
Sn1 Pt1 Sn2 C3 -165.51(14)
P2 Pt1 P1 C9 -106.35(14)
Sn2 Pt1 P1 C9 103.4(2)
Sn1 Pt1 P1 C9 75.58(14)
P2 Pt1 P1 C15 19.9(2)
Sn2 Pt1 P1 C15 -130.3(2)
Sn1 Pt1 P1 C15 -158.2(2)
P2 Pt1 P1 C2 137.2(2)
Sn2 Pt1 P1 C2 -13.0(2)
Sn1 Pt1 P1 C2 -40.89(15)
P1 Pt1 P2 C21 29.0(2)
Sn2 Pt1 P2 C21 -156.4(2)
Sn1 Pt1 P2 C21 -163.2(2)
P1 Pt1 P2 C27 -94.51(15)
Sn2 Pt1 P2 C27 80.07(14)
Sn1 Pt1 P2 C27 73.2(2)
P1 Pt1 P2 C4 149.7(2)
Sn2 Pt1 P2 C4 -35.7(2)
Sn1 Pt1 P2 C4 -42.6(3)
C6 Sn1 C1 C2 124.0(3)
C5 Sn1 C1 C2 -124.9(3)
Pt1 Sn1 C1 C2 3.8(3)
Sn1 C1 C2 P1 -34.8(4)
C9 P1 C2 C1 -66.8(3)
C15 P1 C2 C1 -175.7(3)
Pt1 P1 C2 C1 57.0(3)
C8 Sn2 C3 C4 127.8(3)
C7 Sn2 C3 C4 -120.5(3)
Pt1 Sn2 C3 C4 8.4(3)
Sn2 C3 C4 P2 -35.8(4)
C21 P2 C4 C3 -177.5(3)
C27 P2 C4 C3 -67.5(4)
Pt1 P2 C4 C3 53.5(4)
C15 P1 C9 C10 70.9(4)
C2 P1 C9 C10 -35.7(4)
Pt1 P1 C9 C10 -156.1(3)
C15 P1 C9 C14 -111.8(4)
C2 P1 C9 C14 141.6(4)
Pt1 P1 C9 C14 21.2(4)
C14 C9 C10 C11 -0.2(7)
P1 C9 C10 C11 177.1(4)
C9 C10 C11 C12 -0.7(7)
C10 C11 C12 C13 0.9(8)
C11 C12 C13 C14 -0.1(8)
C12 C13 C14 C9 -0.8(8)
C10 C9 C14 C13 1.0(7)
P1 C9 C14 C13 -176.5(4)
C9 P1 C15 C20 -171.9(3)
C2 P1 C15 C20 -64.4(4)
Pt1 P1 C15 C20 57.1(4)
C9 P1 C15 C16 10.9(4)
C2 P1 C15 C16 118.4(4)
Pt1 P1 C15 C16 -120.0(3)
C20 C15 C16 C17 1.8(7)
P1 C15 C16 C17 178.9(4)
C15 C16 C17 C18 -1.2(8)
C16 C17 C18 C19 -0.4(9)
C17 C18 C19 C20 1.2(9)
C16 C15 C20 C19 -0.9(7)
P1 C15 C20 C19 -178.2(4)
C18 C19 C20 C15 -0.6(8)
C27 P2 C21 C22 13.1(4)
C4 P2 C21 C22 121.2(4)
Pt1 P2 C21 C22 -113.6(4)
C27 P2 C21 C26 -171.8(4)
C4 P2 C21 C26 -63.6(4)
Pt1 P2 C21 C26 61.6(4)
C26 C21 C22 C23 1.3(7)
P2 C21 C22 C23 176.5(4)
C21 C22 C23 C24 -1.2(8)
C22 C23 C24 C25 1.1(9)
C23 C24 C25 C26 -1.2(10)
C24 C25 C26 C21 1.4(10)
C22 C21 C26 C25 -1.4(8)
P2 C21 C26 C25 -176.9(5)
C21 P2 C27 C32 -125.0(4)
C4 P2 C27 C32 126.8(4)
Pt1 P2 C27 C32 5.5(4)
C21 P2 C27 C28 57.5(4)
C4 P2 C27 C28 -50.7(4)
Pt1 P2 C27 C28 -172.0(3)
C32 C27 C28 C29 -0.6(7)
P2 C27 C28 C29 177.0(4)
C27 C28 C29 C30 0.8(8)
C28 C29 C30 C31 0.1(9)
C29 C30 C31 C32 -1.1(10)
C30 C31 C32 C27 1.2(9)
C28 C27 C32 C31 -0.4(7)
P2 C27 C32 C31 -178.0(4)
