#------------------------------------------------------------------------------
#$Date: 2016-02-20 00:18:51 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176760 $
#$URL: svn://www.crystallography.net/cod/cif/2/01/13/2011367.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2011367
loop_
_publ_author_name
'Filippou, Alexander, C.'
'Portius, Peter'
'Philippopoulos, Athanassios, I.'
'Kociok-Köhn, Gabriele'
'Ziemer, Burkhard'
_publ_section_title
;Pentane and tetrahydrofuran solvates of
 trans-dichlorobis[1,2-ethanediylbis(diphenylphosphine)-P,P']molybdenum(II)
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              e378
_journal_page_last               e379
_journal_paper_doi               10.1107/S010827010001060X
_journal_volume                  56
_journal_year                    2000
_chemical_formula_iupac          '[Mo Cl2 (C26 H24 P2)2], 2C4 H8 O'
_chemical_formula_moiety         'C52 H48 Cl2 Mo P4, 2C4 H8 O'
_chemical_formula_sum            'C60 H64 Cl2 Mo O2 P4'
_chemical_formula_weight         1107.83
_chemical_name_systematic
;
 trans-Dichlorobis[1,2-ethandiylbis[diphenylphosphane]-P,P']molybdenum
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_creation_method           SHELXL97
_cell_angle_alpha                90.00
_cell_angle_beta                 96.093(11)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   11.3197(11)
_cell_length_b                   13.4052(14)
_cell_length_c                   17.455(2)
_cell_measurement_reflns_used    26
_cell_measurement_temperature    180(2)
_cell_measurement_theta_max      16.4
_cell_measurement_theta_min      13.5
_cell_volume                     2633.7(5)
_computing_cell_refinement       STADI4-1.06
_computing_data_collection       'STADI4-1.06 (Stoe & Cie, 1997)'
_computing_data_reduction        'XRED-1.07 (Stoe & Cie, 1997)'
_computing_molecular_graphics    'XSTEP-2.18 (Stoe & Cie, 1997)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      180(2)
_diffrn_measured_fraction_theta_full .998
_diffrn_measured_fraction_theta_max .998
_diffrn_measurement_device       'Stoe Stadi-4'
_diffrn_measurement_method
'2θ/ω scans, ratio = 1.0, width (ω) = 1.2-1.68°'
_diffrn_radiation_monochromator  'planar graphite'
_diffrn_radiation_source         'fine-focus sealed X-ray tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_R_equivalents  .032
_diffrn_reflns_av_sigmaI/netI    .0254
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            6801
_diffrn_reflns_theta_full        24.97
_diffrn_reflns_theta_max         24.97
_diffrn_reflns_theta_min         1.81
_diffrn_standards_decay_%        8.6
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    .516
_exptl_absorpt_correction_T_max  .869
_exptl_absorpt_correction_T_min  .683
_exptl_absorpt_correction_type   '\y scan'
_exptl_absorpt_process_details   '(North et al., 1968)'
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.397
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    none
_exptl_crystal_description       block
_exptl_crystal_F_000             1152
_exptl_crystal_size_max          .80
_exptl_crystal_size_mid          .54
_exptl_crystal_size_min          .28
_refine_diff_density_max         .80
_refine_diff_density_min         -.85
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.068
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     313
_refine_ls_number_reflns         4617
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.071
_refine_ls_R_factor_all          .039
_refine_ls_R_factor_gt           .033
_refine_ls_shift/su_max          .009
_refine_ls_shift/su_mean         .001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0565P)²+1.2270P] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         .094
_reflns_number_gt                4065
_reflns_number_total             4617
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            qd0007.cif
_cod_data_source_block           IIIb
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        2633.7(4)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2011367
_cod_database_fobs_code          2011367
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
C1 -.2744(2) -.09477(17) -.10487(14) .0253(5) Uani d . 1 . . C
C2 -.3390(2) -.05496(19) -.17043(15) .0316(6) Uani d . 1 . . C
H2 -.2998 -.0389 -.2143 .038 Uiso calc R 1 . . H
C3 -.4607(2) -.0387(2) -.17162(18) .0422(7) Uani d . 1 . . C
H3 -.5040 -.0109 -.2162 .051 Uiso calc R 1 . . H
C4 -.5185(2) -.0625(2) -.10882(19) .0436(7) Uani d . 1 . . C
H4 -.6013 -.0505 -.1097 .052 Uiso calc R 1 . . H
C5 -.4558(2) -.1042(2) -.04412(18) .0388(7) Uani d . 1 . . C
H5 -.4963 -.1229 -.0013 .047 Uiso calc R 1 . . H
C6 -.3340(2) -.11877(19) -.04172(15) .0303(5) Uani d . 1 . . C
H6 -.2911 -.1453 .0034 .036 Uiso calc R 1 . . H
C7 -.0943(2) -.24637(18) -.09879(13) .0255(5) Uani d . 1 . . C
C8 -.1893(2) -.31124(19) -.11594(16) .0337(6) Uani d . 1 . . C
H8 -.2671 -.2854 -.1285 .040 Uiso calc R 1 . . H
C9 -.1708(3) -.4140(2) -.11482(18) .0420(7) Uani d . 1 . . C
H9 -.2361 -.4579 -.1264 .050 Uiso calc R 1 . . H
C10 -.0582(3) -.4523(2) -.09695(17) .0398(7) Uani d . 1 . . C
H10 -.0460 -.5224 -.0959 .048 Uiso calc R 1 . . H
C11 .0361(3) -.3890(2) -.08070(17) .0403(7) Uani d . 1 . . C
H11 .1138 -.4155 -.0690 .048 Uiso calc R 1 . . H
C12 .0190(2) -.28608(19) -.08119(16) .0335(6) Uani d . 1 . . C
H12 .0849 -.2428 -.0695 .040 Uiso calc R 1 . . H
C13 -.0666(2) -.07568(18) -.19102(13) .0259(5) Uani d . 1 . . C
H13A .0133 -.1039 -.1953 .031 Uiso calc R 1 . . H
H13B -.1222 -.1062 -.2320 .031 Uiso calc R 1 . . H
C14 .1449(2) -.20764(18) .13228(14) .0281(5) Uani d . 1 . . C
C15 .2447(2) -.2041(2) .09352(17) .0395(6) Uani d . 1 . . C
H15 .2501 -.1559 .0542 .047 Uiso calc R 1 . . H
C16 .3383(3) -.2712(3) .11179(18) .0490(8) Uani d . 1 . . C
H16 .4069 -.2682 .0849 .059 Uiso calc R 1 . . H
C17 .3311(3) -.3417(2) .16882(19) .0458(7) Uani d . 1 . . C
H17 .3938 -.3881 .1803 .055 Uiso calc R 1 . . H
C18 .2332(3) -.3447(2) .20896(19) .0441(7) Uani d . 1 . . C
H18 .2289 -.3922 .2490 .053 Uiso calc R 1 . . H
C19 .1403(2) -.2781(2) .19089(17) .0382(6) Uani d . 1 . . C
H19 .0728 -.2806 .2188 .046 Uiso calc R 1 . . H
C20 -.1049(2) -.18610(18) .13252(14) .0259(5) Uani d . 1 . . C
C21 -.1917(2) -.1512(2) .17613(16) .0381(6) Uani d . 1 . . C
H21 -.1808 -.0892 .2022 .046 Uiso calc R 1 . . H
C22 -.2945(3) -.2062(3) .18209(19) .0514(8) Uani d . 1 . . C
H22 -.3538 -.1811 .2116 .062 Uiso calc R 1 . . H
C23 -.3107(3) -.2973(3) .14507(19) .0503(8) Uani d . 1 . . C
H23 -.3805 -.3350 .1498 .060 Uiso calc R 1 . . H
C24 -.2256(3) -.3330(2) .10151(18) .0432(7) Uani d . 1 . . C
H24 -.2369 -.3953 .0758 .052 Uiso calc R 1 . . H
C25 -.1231(2) -.27803(19) .09508(15) .0315(6) Uani d . 1 . . C
H25 -.0646 -.3031 .0649 .038 Uiso calc R 1 . . H
C26 .0625(2) -.03727(19) .20475(14) .0310(6) Uani d . 1 . . C
H26A .0021 -.0513 .2404 .037 Uiso calc R 1 . . H
H26B .1405 -.0590 .2304 .037 Uiso calc R 1 . . H
C27 .5564(3) .3270(3) .1901(2) .0569(9) Uani d . 1 . . C
H27A .5165 .2612 .1885 .068 Uiso calc R 1 . . H
H27B .5889 .3411 .2439 .068 Uiso calc R 1 . . H
C28 .6540(3) .3272(3) .1384(2) .0693(11) Uani d . 1 . . C
H28A .7291 .3518 .1662 .083 Uiso calc R 1 . . H
H28B .6672 .2593 .1187 .083 Uiso calc R 1 . . H
C29 .6129(4) .3936(5) .0761(3) .108(2) Uani d D 1 . . C
H29A .6649 .4531 .0769 .129 Uiso calc R 1 . . H
H29B .6151 .3593 .0260 .129 Uiso calc R 1 . . H
C30 .4928(4) .4234(4) .0856(2) .0745(12) Uani d D 1 . . C
H30A .4819 .4955 .0744 .089 Uiso calc R 1 . . H
H30B .4356 .3855 .0499 .089 Uiso calc R 1 . . H
P1 -.11330(5) -.11024(4) -.09633(3) .02144(15) Uani d . 1 . . P
P2 .02695(5) -.11315(4) .11497(3) .02242(15) Uani d . 1 . . P
Mo .0000 .0000 .0000 .01831(10) Uani d S 1 . . Mo
O .4741(2) .4033(2) .16214(13) .0627(7) Uani d . 1 . . O
Cl -.17261(5) .05089(4) .06254(3) .02631(15) Uani d . 1 . . Cl
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C .0033 .0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H .0000 .0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P .1023 .0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 .6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O .0106 .0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl .1484 .1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
C6 C1 C2 . . 118.8(2)
C6 C1 P1 . . 118.28(19)
C2 C1 P1 . . 122.83(19)
C3 C2 C1 . . 120.2(3)
C4 C3 C2 . . 120.4(3)
C3 C4 C5 . . 119.9(3)
C4 C5 C6 . . 120.1(3)
C5 C6 C1 . . 120.5(3)
C8 C7 C12 . . 118.8(2)
C8 C7 P1 . . 122.40(19)
C12 C7 P1 . . 118.80(19)
C7 C8 C9 . . 120.2(2)
C10 C9 C8 . . 120.4(3)
C11 C10 C9 . . 119.8(2)
C10 C11 C12 . . 120.5(3)
C7 C12 C11 . . 120.3(2)
C26 C13 P1 3 . 113.79(16)
C15 C14 C19 . . 118.6(2)
C15 C14 P2 . . 120.9(2)
C19 C14 P2 . . 120.2(2)
C14 C15 C16 . . 120.4(3)
C17 C16 C15 . . 120.2(3)
C18 C17 C16 . . 120.0(3)
C17 C18 C19 . . 119.8(3)
C18 C19 C14 . . 121.0(3)
C21 C20 C25 . . 118.4(2)
C21 C20 P2 . . 123.2(2)
C25 C20 P2 . . 118.23(19)
C20 C21 C22 . . 120.7(3)
C23 C22 C21 . . 120.2(3)
C24 C23 C22 . . 120.0(3)
C23 C24 C25 . . 120.0(3)
C24 C25 C20 . . 120.8(3)
C13 C26 P2 3 . 114.33(16)
O C27 C28 . . 106.7(3)
C29 C28 C27 . . 104.8(3)
C30 C29 C28 . . 108.5(4)
O C30 C29 . . 107.2(3)
C1 P1 C7 . . 103.25(11)
C1 P1 C13 . . 106.06(11)
C7 P1 C13 . . 100.53(11)
C1 P1 Mo . . 115.23(8)
C7 P1 Mo . . 123.49(8)
C13 P1 Mo . . 106.24(8)
C20 P2 C14 . . 101.18(11)
C20 P2 C26 . . 104.80(11)
C14 P2 C26 . . 98.54(12)
C20 P2 Mo . . 115.05(7)
C14 P2 Mo . . 124.87(8)
C26 P2 Mo . . 109.73(8)
Cl Mo Cl . 3 180.00(2)
Cl Mo P1 . . 95.093(19)
Cl Mo P1 3 . 84.907(19)
Cl Mo P1 . 3 84.907(19)
Cl Mo P1 3 3 95.093(19)
P1 Mo P1 . 3 180.00(3)
Cl Mo P2 . . 81.136(19)
Cl Mo P2 3 . 98.864(19)
P1 Mo P2 . . 101.048(19)
P1 Mo P2 3 . 78.952(19)
Cl Mo P2 . 3 98.864(19)
Cl Mo P2 3 3 81.136(19)
P1 Mo P2 . 3 78.952(19)
P1 Mo P2 3 3 101.048(19)
P2 Mo P2 . 3 180.00(3)
C30 O C27 . . 107.6(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
C1 C6 . 1.390(4) ?
C1 C2 . 1.397(4) ?
C1 P1 . 1.825(2) ?
C2 C3 . 1.393(4) ?
C3 C4 . 1.372(4) ?
C4 C5 . 1.386(4) ?
C5 C6 . 1.389(4) ?
C7 C8 . 1.391(3) ?
C7 C12 . 1.392(4) ?
C7 P1 . 1.838(2) ?
C8 C9 . 1.393(4) ?
C9 C10 . 1.379(4) ?
C10 C11 . 1.369(4) ?
C11 C12 . 1.393(4) ?
C13 C26 3 1.534(3) ?
C13 P1 . 1.847(2) ?
C14 C15 . 1.379(4) ?
C14 C19 . 1.398(4) ?
C14 P2 . 1.842(2) ?
C15 C16 . 1.400(4) ?
C16 C17 . 1.381(4) ?
C17 C18 . 1.373(5) ?
C18 C19 . 1.389(4) ?
C20 C21 . 1.387(4) ?
C20 C25 . 1.400(4) ?
C20 P2 . 1.837(2) ?
C21 C22 . 1.390(4) ?
C22 C23 . 1.385(5) ?
C23 C24 . 1.375(5) ?
C24 C25 . 1.389(4) ?
C26 C13 3 1.534(3) ?
C26 P2 . 1.876(3) ?
C27 O . 1.435(4) ?
C27 C28 . 1.499(5) ?
C28 C29 . 1.444(6) ?
C29 C30 . 1.443(6) ?
C30 O . 1.402(4) ?
P1 Mo . 2.4896(6) ?
P2 Mo . 2.5082(6) ?
Mo Cl . 2.4346(5) ?
Mo Cl 3 2.4346(5) ?
Mo P1 3 2.4896(6) ?
Mo P2 3 2.5082(6) ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
_geom_torsion
C6 C1 C2 C3 . . .8(4)
P1 C1 C2 C3 . . -175.6(2)
C1 C2 C3 C4 . . -.7(4)
C2 C3 C4 C5 . . -.8(4)
C3 C4 C5 C6 . . 2.2(4)
C4 C5 C6 C1 . . -2.1(4)
C2 C1 C6 C5 . . .6(4)
P1 C1 C6 C5 . . 177.2(2)
C12 C7 C8 C9 . . .5(4)
P1 C7 C8 C9 . . -178.1(2)
C7 C8 C9 C10 . . -.2(4)
C8 C9 C10 C11 . . -.4(5)
C9 C10 C11 C12 . . .8(5)
C8 C7 C12 C11 . . -.2(4)
P1 C7 C12 C11 . . 178.5(2)
C10 C11 C12 C7 . . -.5(4)
C19 C14 C15 C16 . . 1.2(4)
P2 C14 C15 C16 . . 174.6(2)
C14 C15 C16 C17 . . .1(5)
C15 C16 C17 C18 . . -1.5(5)
C16 C17 C18 C19 . . 1.4(5)
C17 C18 C19 C14 . . -.1(4)
C15 C14 C19 C18 . . -1.2(4)
P2 C14 C19 C18 . . -174.7(2)
C25 C20 C21 C22 . . -.3(4)
P2 C20 C21 C22 . . 174.5(2)
C20 C21 C22 C23 . . .8(4)
C21 C22 C23 C24 . . -.8(5)
C22 C23 C24 C25 . . .4(4)
C23 C24 C25 C20 . . .0(4)
C21 C20 C25 C24 . . -.1(4)
P2 C20 C25 C24 . . -175.1(2)
O C27 C28 C29 . . -8.6(5)
C27 C28 C29 C30 . . -5.5(6)
C28 C29 C30 O . . 18.1(7)
C6 C1 P1 C7 . . 72.9(2)
C2 C1 P1 C7 . . -110.6(2)
C6 C1 P1 C13 . . 178.16(19)
C2 C1 P1 C13 . . -5.4(2)
C6 C1 P1 Mo . . -64.6(2)
C2 C1 P1 Mo . . 111.85(19)
C8 C7 P1 C1 . . 8.7(2)
C12 C7 P1 C1 . . -169.8(2)
C8 C7 P1 C13 . . -100.7(2)
C12 C7 P1 C13 . . 80.7(2)
C8 C7 P1 Mo . . 141.62(19)
C12 C7 P1 Mo . . -36.9(2)
C26 C13 P1 C1 3 . 77.51(19)
C26 C13 P1 C7 3 . -175.26(18)
C26 C13 P1 Mo 3 . -45.57(18)
C21 C20 P2 C14 . . 134.9(2)
C25 C20 P2 C14 . . -50.3(2)
C21 C20 P2 C26 . . 32.8(2)
C25 C20 P2 C26 . . -152.34(19)
C21 C20 P2 Mo . . -87.8(2)
C25 C20 P2 Mo . . 87.07(19)
C15 C14 P2 C20 . . 149.3(2)
C19 C14 P2 C20 . . -37.5(2)
C15 C14 P2 C26 . . -103.7(2)
C19 C14 P2 C26 . . 69.6(2)
C15 C14 P2 Mo . . 17.7(3)
C19 C14 P2 Mo . . -169.04(18)
C13 C26 P2 C20 3 . -123.38(18)
C13 C26 P2 C14 3 . 132.59(19)
C13 C26 P2 Mo 3 . .7(2)
C1 P1 Mo Cl . . 13.75(9)
C7 P1 Mo Cl . . -114.24(10)
C13 P1 Mo Cl . . 130.87(8)
C1 P1 Mo Cl . 3 -166.25(9)
C7 P1 Mo Cl . 3 65.76(10)
C13 P1 Mo Cl . 3 -49.13(8)
C1 P1 Mo P1 . 3 -87.11(9)
C7 P1 Mo P1 . 3 144.89(10)
C13 P1 Mo P1 . 3 30.00(8)
C1 P1 Mo P2 . . 95.69(9)
C7 P1 Mo P2 . . -32.30(10)
C13 P1 Mo P2 . . -147.19(8)
C1 P1 Mo P2 . 3 -84.31(9)
C7 P1 Mo P2 . 3 147.70(10)
C13 P1 Mo P2 . 3 32.81(8)
C20 P2 Mo Cl . . 50.85(9)
C14 P2 Mo Cl . . 176.75(10)
C26 P2 Mo Cl . . -67.00(9)
C20 P2 Mo Cl . 3 -129.15(9)
C14 P2 Mo Cl . 3 -3.25(10)
C26 P2 Mo Cl . 3 113.00(9)
C20 P2 Mo P1 . . -42.65(9)
C14 P2 Mo P1 . . 83.25(10)
C26 P2 Mo P1 . . -160.50(9)
C20 P2 Mo P1 . 3 137.35(9)
C14 P2 Mo P1 . 3 -96.75(10)
C26 P2 Mo P1 . 3 19.50(9)
C20 P2 Mo P2 . 3 179.12(9)
C14 P2 Mo P2 . 3 -54.98(10)
C26 P2 Mo P2 . 3 61.27(9)
C29 C30 O C27 . . -23.6(5)
C28 C27 O C30 . . 20.0(4)
