#------------------------------------------------------------------------------
#$Date: 2016-02-20 00:18:51 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176760 $
#$URL: svn://www.crystallography.net/cod/cif/2/01/27/2012750.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2012750
loop_
_publ_author_name
'Parvez, Masood'
'Ali, Saqib'
'Ahmad, Sajjad'
'Bhatti, Moazzam Hussain'
'Mazhar, Muhammad'
_publ_section_title
catena-Poly[[tri-n-butyltin]-μ-N-(1-naphthyl)maleamato]
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m334
_journal_page_last               m335
_journal_paper_doi               10.1107/S0108270102007539
_journal_volume                  58
_journal_year                    2002
_chemical_formula_moiety         'C26 H37 N O3 Sn'
_chemical_formula_sum            'C26 H37 N O3 Sn'
_chemical_formula_weight         530.26
_chemical_name_common            Tri-n-butyltin-N-(1-naphthyl)-maleamate
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                97.011(3)
_cell_angle_beta                 107.571(4)
_cell_angle_gamma                102.297(6)
_cell_formula_units_Z            2
_cell_length_a                   9.5705(7)
_cell_length_b                   11.7377(9)
_cell_length_c                   12.4726(11)
_cell_measurement_reflns_used    8025
_cell_measurement_temperature    170(2)
_cell_measurement_theta_max      25.0
_cell_measurement_theta_min      1.0
_cell_volume                     1278.71(18)
_computing_cell_refinement       'HKL DENZO (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Hooft, 1998)'
_computing_data_reduction        'SCALEPACK (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SAPI91 (Fan, 1991)'
_diffrn_ambient_temperature      170(2)
_diffrn_measured_fraction_theta_full 0.969
_diffrn_measured_fraction_theta_max 0.969
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       'ω and φ'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.035
_diffrn_reflns_av_sigmaI/netI    0.059
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            8025
_diffrn_reflns_theta_full        25.0
_diffrn_reflns_theta_max         25.0
_diffrn_reflns_theta_min         3.3
_diffrn_standards_decay_%        <0.1
_exptl_absorpt_coefficient_mu    1.02
_exptl_absorpt_correction_T_max  0.922
_exptl_absorpt_correction_T_min  0.861
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SORTAV: Blessing, 1997)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.377
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             548
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.80
_refine_diff_density_min         -1.43
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.13
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     280
_refine_ls_number_reflns         4329
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.13
_refine_ls_R_factor_all          0.076
_refine_ls_R_factor_gt           0.061
_refine_ls_shift/su_max          0.00
_refine_ls_shift/su_mean         0.00
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0842P)²+3.9999P] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.160
_refine_ls_wR_factor_ref         0.169
_reflns_number_gt                3640
_reflns_number_total             4329
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            fg1647.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_database_code               2012750
_cod_database_fobs_code          2012750
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
Sn1 0.22096(5) 0.23271(4) 0.55844(4) 0.0376(2) Uani d . 1 . . Sn
O1 -0.0238(5) 0.1951(4) 0.4825(5) 0.0463(12) Uani d . 1 . . O
O2 -0.0329(5) 0.3347(5) 0.6164(5) 0.0498(13) Uani d . 1 . . O
O3 -0.5023(5) 0.2679(4) 0.6421(4) 0.0420(11) Uani d . 1 . . O
N1 -0.2518(6) 0.3604(5) 0.7011(5) 0.0387(13) Uani d . 1 . . N
H1 -0.1686 0.3661 0.6833 0.046 Uiso calc R 1 . . H
C1 0.2107(8) 0.0846(6) 0.4366(6) 0.0429(17) Uani d . 1 . . C
H1A 0.3064 0.0604 0.4634 0.051 Uiso calc R 1 . . H
H1B 0.1264 0.0171 0.4332 0.051 Uiso calc R 1 . . H
C2 0.1872(8) 0.1093(7) 0.3157(7) 0.0486(18) Uani d . 1 . . C
H2A 0.0917 0.1337 0.2891 0.058 Uiso calc R 1 . . H
H2B 0.2716 0.1769 0.3193 0.058 Uiso calc R 1 . . H
C3 0.1797(9) 0.0041(8) 0.2278(8) 0.062(2) Uani d . 1 . . C
H3A 0.1044 -0.0665 0.2311 0.075 Uiso calc R 1 . . H
H3B 0.1433 0.0220 0.1501 0.075 Uiso calc R 1 . . H
C4 0.3301(9) -0.0257(8) 0.2456(8) 0.056(2) Uani d . 1 . . C
H4A 0.3169 -0.0944 0.1868 0.084 Uiso calc R 1 . . H
H4B 0.3664 -0.0447 0.3218 0.084 Uiso calc R 1 . . H
H4C 0.4045 0.0428 0.2396 0.084 Uiso calc R 1 . . H
C5 0.2702(8) 0.4026(6) 0.5116(7) 0.0443(17) Uani d . 1 . . C
H5A 0.3051 0.3926 0.4449 0.053 Uiso calc R 1 . . H
H5B 0.1739 0.4261 0.4857 0.053 Uiso calc R 1 . . H
C6 0.3875(9) 0.5052(7) 0.6027(7) 0.0498(19) Uani d . 1 . . C
H6A 0.4801 0.4789 0.6362 0.060 Uiso calc R 1 . . H
H6B 0.4156 0.5717 0.5649 0.060 Uiso calc R 1 . . H
C7 0.3374(11) 0.5513(8) 0.6985(8) 0.063(2) Uani d . 1 . . C
H7A 0.3140 0.4864 0.7393 0.076 Uiso calc R 1 . . H
H7B 0.2428 0.5754 0.6656 0.076 Uiso calc R 1 . . H
C8 0.4563(12) 0.6566(8) 0.7840(8) 0.074(3) Uani d . 1 . . C
H8A 0.4167 0.6846 0.8432 0.111 Uiso calc R 1 . . H
H8B 0.4806 0.7210 0.7440 0.111 Uiso calc R 1 . . H
H8C 0.5484 0.6322 0.8199 0.111 Uiso calc R 1 . . H
C9 0.2300(8) 0.1950(7) 0.7226(7) 0.0462(18) Uani d . 1 . . C
H9A 0.3045 0.2616 0.7829 0.055 Uiso calc R 1 . . H
H9B 0.1292 0.1885 0.7311 0.055 Uiso calc R 1 . . H
C10 0.2756(9) 0.0788(7) 0.7390(7) 0.0523(19) Uani d . 1 . . C
H10A 0.2034 0.0142 0.6755 0.063 Uiso calc R 1 . . H
H10B 0.3774 0.0875 0.7319 0.063 Uiso calc R 1 . . H
C11 0.2802(12) 0.0409(9) 0.8495(9) 0.075(3) Uani d . 1 . . C
H11A 0.1773 0.0285 0.8553 0.091 Uiso calc R 1 . . H
H11B 0.3054 -0.0367 0.8476 0.091 Uiso calc R 1 . . H
C12 0.3876(17) 0.1233(11) 0.9519(10) 0.102(4) Uani d . 1 . . C
H12A 0.3820 0.0913 1.0199 0.153 Uiso calc R 1 . . H
H12B 0.3626 0.2002 0.9560 0.153 Uiso calc R 1 . . H
H12C 0.4906 0.1342 0.9489 0.153 Uiso calc R 1 . . H
C13 -0.0952(7) 0.2523(6) 0.5332(7) 0.0416(16) Uani d . 1 . . C
C14 -0.2644(7) 0.2095(6) 0.4770(6) 0.0417(16) Uani d . 1 . . C
H14 -0.2976 0.1644 0.4011 0.050 Uiso calc R 1 . . H
C15 -0.3749(7) 0.2241(6) 0.5157(6) 0.0403(16) Uani d . 1 . . C
H15 -0.4731 0.1864 0.4614 0.048 Uiso calc R 1 . . H
C16 -0.3797(7) 0.2864(6) 0.6255(6) 0.0362(15) Uani d . 1 . . C
C17 -0.2369(8) 0.4304(6) 0.8064(6) 0.0397(16) Uani d . 1 . . C
C18 -0.3221(9) 0.3905(7) 0.8721(7) 0.0490(18) Uani d . 1 . . C
H18 -0.3943 0.3149 0.8459 0.059 Uiso calc R 1 . . H
C19 -0.3030(10) 0.4605(8) 0.9775(7) 0.058(2) Uani d . 1 . . C
H19 -0.3652 0.4329 1.0207 0.069 Uiso calc R 1 . . H
C20 -0.1983(11) 0.5661(8) 1.0186(7) 0.059(2) Uani d . 1 . . C
H20 -0.1847 0.6104 1.0917 0.070 Uiso calc R 1 . . H
C21 -0.1082(9) 0.6121(7) 0.9542(7) 0.0482(18) Uani d . 1 . . C
C22 -0.0005(10) 0.7234(8) 0.9929(8) 0.061(2) Uani d . 1 . . C
H22 0.0131 0.7698 1.0650 0.073 Uiso calc R 1 . . H
C23 0.0842(11) 0.7662(8) 0.9303(8) 0.063(2) Uani d . 1 . . C
H23 0.1562 0.8418 0.9586 0.076 Uiso calc R 1 . . H
C24 0.0662(10) 0.6995(7) 0.8240(7) 0.053(2) Uani d . 1 . . C
H24 0.1254 0.7300 0.7799 0.064 Uiso calc R 1 . . H
C25 -0.0363(8) 0.5905(7) 0.7835(7) 0.0453(17) Uani d . 1 . . C
H25 -0.0471 0.5459 0.7112 0.054 Uiso calc R 1 . . H
C26 -0.1263(8) 0.5430(6) 0.8461(6) 0.0407(16) Uani d . 1 . . C
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C1 Sn1 C9 . 114.5(3) y
C1 Sn1 C5 . 115.5(3) y
C9 Sn1 C5 . 128.5(3) y
C1 Sn1 O1 . 87.8(2) y
C9 Sn1 O1 . 97.8(2) y
C5 Sn1 O1 . 95.8(2) y
C1 Sn1 O3 1_655 90.3(2) y
C9 Sn1 O3 1_655 82.1(2) y
C5 Sn1 O3 1_655 85.8(2) y
O1 Sn1 O3 1_655 177.97(17) y
C13 O1 Sn1 . 118.6(4) y
C16 O3 Sn1 1_455 147.0(5) y
C16 N1 C17 . 126.6(6) y
C16 N1 H1 . 116.7 n
C17 N1 H1 . 116.7 n
C2 C1 Sn1 . 113.9(5) n
C2 C1 H1A . 108.8 n
Sn1 C1 H1A . 108.8 n
C2 C1 H1B . 108.8 n
Sn1 C1 H1B . 108.8 n
H1A C1 H1B . 107.7 n
C3 C2 C1 . 114.4(7) n
C3 C2 H2A . 108.7 n
C1 C2 H2A . 108.7 n
C3 C2 H2B . 108.7 n
C1 C2 H2B . 108.7 n
H2A C2 H2B . 107.6 n
C4 C3 C2 . 113.7(7) n
C4 C3 H3A . 108.8 n
C2 C3 H3A . 108.8 n
C4 C3 H3B . 108.8 n
C2 C3 H3B . 108.8 n
H3A C3 H3B . 107.7 n
C3 C4 H4A . 109.5 n
C3 C4 H4B . 109.5 n
H4A C4 H4B . 109.5 n
C3 C4 H4C . 109.5 n
H4A C4 H4C . 109.5 n
H4B C4 H4C . 109.5 n
C6 C5 Sn1 . 117.7(5) n
C6 C5 H5A . 107.9 n
Sn1 C5 H5A . 107.9 n
C6 C5 H5B . 107.9 n
Sn1 C5 H5B . 107.9 n
H5A C5 H5B . 107.2 n
C7 C6 C5 . 115.2(7) n
C7 C6 H6A . 108.5 n
C5 C6 H6A . 108.5 n
C7 C6 H6B . 108.5 n
C5 C6 H6B . 108.5 n
H6A C6 H6B . 107.5 n
C6 C7 C8 . 112.8(8) n
C6 C7 H7A . 109.0 n
C8 C7 H7A . 109.0 n
C6 C7 H7B . 109.0 n
C8 C7 H7B . 109.0 n
H7A C7 H7B . 107.8 n
C7 C8 H8A . 109.5 n
C7 C8 H8B . 109.5 n
H8A C8 H8B . 109.5 n
C7 C8 H8C . 109.5 n
H8A C8 H8C . 109.5 n
H8B C8 H8C . 109.5 n
C10 C9 Sn1 . 111.6(5) n
C10 C9 H9A . 109.3 n
Sn1 C9 H9A . 109.3 n
C10 C9 H9B . 109.3 n
Sn1 C9 H9B . 109.3 n
H9A C9 H9B . 108.0 n
C11 C10 C9 . 116.4(8) n
C11 C10 H10A . 108.2 n
C9 C10 H10A . 108.2 n
C11 C10 H10B . 108.2 n
C9 C10 H10B . 108.2 n
H10A C10 H10B . 107.3 n
C12 C11 C10 . 115.3(9) n
C12 C11 H11A . 108.4 n
C10 C11 H11A . 108.4 n
C12 C11 H11B . 108.4 n
C10 C11 H11B . 108.4 n
H11A C11 H11B . 107.5 n
C11 C12 H12A . 109.5 n
C11 C12 H12B . 109.5 n
H12A C12 H12B . 109.5 n
C11 C12 H12C . 109.5 n
H12A C12 H12C . 109.5 n
H12B C12 H12C . 109.5 n
O2 C13 O1 . 124.3(6) n
O2 C13 C14 . 123.0(6) n
O1 C13 C14 . 112.7(6) n
C15 C14 C13 . 130.7(7) n
C15 C14 H14 . 114.6 n
C13 C14 H14 . 114.6 n
C14 C15 C16 . 134.2(6) n
C14 C15 H15 . 112.9 n
C16 C15 H15 . 112.9 n
O3 C16 N1 . 123.0(6) n
O3 C16 C15 . 118.1(6) n
N1 C16 C15 . 119.0(6) n
C18 C17 N1 . 121.5(7) n
C18 C17 C26 . 120.1(7) n
N1 C17 C26 . 118.4(6) n
C17 C18 C19 . 120.4(8) n
C17 C18 H18 . 119.8 n
C19 C18 H18 . 119.8 n
C20 C19 C18 . 121.2(8) n
C20 C19 H19 . 119.4 n
C18 C19 H19 . 119.4 n
C19 C20 C21 . 120.8(8) n
C19 C20 H20 . 119.6 n
C21 C20 H20 . 119.6 n
C22 C21 C20 . 122.5(8) n
C22 C21 C26 . 118.4(8) n
C20 C21 C26 . 119.1(7) n
C23 C22 C21 . 121.8(8) n
C23 C22 H22 . 119.1 n
C21 C22 H22 . 119.1 n
C22 C23 C24 . 120.1(8) n
C22 C23 H23 . 120.0 n
C24 C23 H23 . 120.0 n
C25 C24 C23 . 120.1(8) n
C25 C24 H24 . 119.9 n
C23 C24 H24 . 119.9 n
C24 C25 C26 . 121.4(7) n
C24 C25 H25 . 119.3 n
C26 C25 H25 . 119.3 n
C25 C26 C21 . 118.2(7) n
C25 C26 C17 . 123.5(7) n
C21 C26 C17 . 118.3(7) n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sn1 C1 . 2.129(7) y
Sn1 C9 . 2.127(8) y
Sn1 C5 . 2.142(7) y
Sn1 O1 . 2.167(5) y
Sn1 O3 1_655 2.457(4) y
O1 C13 . 1.293(8) y
O2 C13 . 1.226(9) y
O3 C16 . 1.231(8) y
O3 Sn1 1_455 2.457(4) n
N1 C16 . 1.339(9) y
N1 C17 . 1.412(9) y
N1 H1 . 0.8800 n
C1 C2 . 1.529(11) n
C1 H1A . 0.9900 n
C1 H1B . 0.9900 n
C2 C3 . 1.521(11) n
C2 H2A . 0.9900 n
C2 H2B . 0.9900 n
C3 C4 . 1.511(11) n
C3 H3A . 0.9900 n
C3 H3B . 0.9900 n
C4 H4A . 0.9800 n
C4 H4B . 0.9800 n
C4 H4C . 0.9800 n
C5 C6 . 1.524(11) n
C5 H5A . 0.9900 n
C5 H5B . 0.9900 n
C6 C7 . 1.499(12) n
C6 H6A . 0.9900 n
C6 H6B . 0.9900 n
C7 C8 . 1.519(12) n
C7 H7A . 0.9900 n
C7 H7B . 0.9900 n
C8 H8A . 0.9800 n
C8 H8B . 0.9800 n
C8 H8C . 0.9800 n
C9 C10 . 1.537(11) n
C9 H9A . 0.9900 n
C9 H9B . 0.9900 n
C10 C11 . 1.490(13) n
C10 H10A . 0.9900 n
C10 H10B . 0.9900 n
C11 C12 . 1.451(15) n
C11 H11A . 0.9900 n
C11 H11B . 0.9900 n
C12 H12A . 0.9800 n
C12 H12B . 0.9800 n
C12 H12C . 0.9800 n
C13 C14 . 1.499(9) n
C14 C15 . 1.321(10) n
C14 H14 . 0.9500 n
C15 C16 . 1.491(10) n
C15 H15 . 0.9500 n
C17 C18 . 1.375(10) n
C17 C26 . 1.429(10) n
C18 C19 . 1.402(12) n
C18 H18 . 0.9500 n
C19 C20 . 1.345(13) n
C19 H19 . 0.9500 n
C20 C21 . 1.416(12) n
C20 H20 . 0.9500 n
C21 C22 . 1.405(12) n
C21 C26 . 1.428(10) n
C22 C23 . 1.350(13) n
C22 H22 . 0.9500 n
C23 C24 . 1.397(12) n
C23 H23 . 0.9500 n
C24 C25 . 1.364(11) n
C24 H24 . 0.9500 n
C25 C26 . 1.403(10) n
C25 H25 . 0.9500 n
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
N1 H1 O2 0.88 1.82 2.669(7) 162
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion
_geom_torsion_publ_flag
C1 Sn1 O1 C13 . 171.1(6) n
C9 Sn1 O1 C13 . 56.7(6) n
C5 Sn1 O1 C13 . -73.5(6) n
C9 Sn1 C1 C2 . 173.8(5) n
C5 Sn1 C1 C2 . -19.2(6) n
O1 Sn1 C1 C2 . 76.2(5) n
O3 Sn1 C1 C2 1_655 -104.7(5) n
Sn1 C1 C2 C3 . -180.0(5) n
C1 C2 C3 C4 . -70.2(10) n
C1 Sn1 C5 C6 . -134.8(5) n
C9 Sn1 C5 C6 . 30.0(7) n
O1 Sn1 C5 C6 . 134.8(5) n
O3 Sn1 C5 C6 1_655 -46.5(5) n
Sn1 C5 C6 C7 . -71.0(8) n
C5 C6 C7 C8 . -177.7(7) n
C1 Sn1 C9 C10 . 17.1(6) n
C5 Sn1 C9 C10 . -147.8(5) n
O1 Sn1 C9 C10 . 108.3(5) n
O3 Sn1 C9 C10 1_655 -69.6(5) n
Sn1 C9 C10 C11 . -177.8(6) n
C9 C10 C11 C12 . -61.2(13) n
Sn1 O1 C13 O2 . 6.8(10) n
Sn1 O1 C13 C14 . -174.8(5) n
O2 C13 C14 C15 . -19.2(13) n
O1 C13 C14 C15 . 162.4(8) n
C13 C14 C15 C16 . 0.4(15) n
Sn1 O3 C16 N1 1_455 142.2(7) n
Sn1 O3 C16 C15 1_455 -37.2(11) n
C17 N1 C16 O3 . -2.4(11) n
C17 N1 C16 C15 . 177.0(6) n
C14 C15 C16 O3 . -168.7(8) n
C14 C15 C16 N1 . 11.9(12) n
C16 N1 C17 C18 . 34.8(11) n
C16 N1 C17 C26 . -147.5(7) n
N1 C17 C18 C19 . 178.7(7) n
C26 C17 C18 C19 . 1.0(11) n
C17 C18 C19 C20 . -2.1(13) n
C18 C19 C20 C21 . 2.6(13) n
C19 C20 C21 C22 . 178.3(8) n
C19 C20 C21 C26 . -2.0(12) n
C20 C21 C22 C23 . -179.8(8) n
C26 C21 C22 C23 . 0.5(13) n
C21 C22 C23 C24 . 0.0(14) n
C22 C23 C24 C25 . -0.4(14) n
C23 C24 C25 C26 . 0.4(12) n
C24 C25 C26 C21 . 0.2(11) n
C24 C25 C26 C17 . 178.9(7) n
C22 C21 C26 C25 . -0.6(10) n
C20 C21 C26 C25 . 179.7(7) n
C22 C21 C26 C17 . -179.4(7) n
C20 C21 C26 C17 . 0.9(10) n
C18 C17 C26 C25 . -179.2(7) n
N1 C17 C26 C25 . 3.1(10) n
C18 C17 C26 C21 . -0.4(10) n
N1 C17 C26 C21 . -178.2(6) n
