#------------------------------------------------------------------------------
#$Date: 2016-02-20 00:18:51 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176760 $
#$URL: svn://www.crystallography.net/cod/cif/2/01/38/2013897.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2013897
loop_
_publ_author_name
'Yang, Shi-Yao'
'Xie, Zhao-Xiong'
'Ng, Seik Weng'
_publ_section_title
;Bis[tetrakis(triphenylphosphine-κP)silver(I)]
 di-μ-trifluoroacetato-κ⁴O:O'-bis[bis(trifluoroacetato-κO)stannate(IV)]
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m123
_journal_page_last               m125
_journal_paper_doi               10.1107/S0108270104001556
_journal_volume                  60
_journal_year                    2004
_chemical_formula_iupac
'[Ag (C 18 H15 P)4]2 [Sn2 (C1 H3)4 (C2 F3 O2)6]'
_chemical_formula_moiety         '2C72 H60 Ag P4 1+, C16 H12 F18 O12 Sn2 2-'
_chemical_formula_sum            'C160 H132 Ag2 F18 O12 P8 Sn2'
_chemical_formula_weight         3289.54
_chemical_name_systematic
;
Bis[tetrakis(triphenylphosphine-\kP)silver(I)]
di-μ-trifluoroacetato-[dimethylbis(trifluoroacetato-κ²O:O')stannate(IV)]
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                100.3700(10)
_cell_angle_beta                 99.4290(10)
_cell_angle_gamma                95.8990(10)
_cell_formula_units_Z            1
_cell_length_a                   12.9439(6)
_cell_length_b                   14.0499(6)
_cell_length_c                   20.7267(9)
_cell_measurement_reflns_used    5859
_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      27.7
_cell_measurement_theta_min      2.3
_cell_volume                     3623.6(3)
_computing_cell_refinement       'SAINT (Bruker, 2001)'
_computing_data_collection       'SMART (Bruker, 2001)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      223(2)
_diffrn_measured_fraction_theta_full 0.96
_diffrn_measured_fraction_theta_max 0.96
_diffrn_measurement_device_type  'Bruker APEX area-detector diffractometer'
_diffrn_measurement_method       'φ and ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.031
_diffrn_reflns_av_sigmaI/netI    0.065
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            31408
_diffrn_reflns_theta_full        27.5
_diffrn_reflns_theta_max         27.5
_diffrn_reflns_theta_min         1.0
_diffrn_standards_decay_%        0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.78
_exptl_absorpt_correction_T_max  0.837
_exptl_absorpt_correction_T_min  0.672
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 1996)'
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.507
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'Irregular block'
_exptl_crystal_F_000             1664
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.39
_refine_diff_density_min         -0.83
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.92
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     939
_refine_ls_number_reflns         16043
_refine_ls_number_restraints     15
_refine_ls_restrained_S_all      0.92
_refine_ls_R_factor_all          0.064
_refine_ls_R_factor_gt           0.048
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         <0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.058P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.108
_refine_ls_wR_factor_ref         0.113
_reflns_number_gt                11658
_reflns_number_total             16043
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ta1433.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_database_code               2013897
_cod_database_fobs_code          2013897
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
Sn 0.47439(2) 0.37240(2) 0.399750(13) 0.04302(9) Uani d . 1 . . Sn
Ag 0.854661(19) 0.772858(18) 0.211129(12) 0.02934(7) Uani d . 1 . . Ag
P1 0.91374(7) 0.87396(6) 0.12589(4) 0.02685(18) Uani d . 1 . . P
P2 0.64793(6) 0.73477(6) 0.18460(4) 0.02718(19) Uani d . 1 . . P
P3 0.92937(7) 0.60420(6) 0.19892(4) 0.02687(18) Uani d . 1 . . P
P4 0.91833(7) 0.87582(6) 0.33351(4) 0.02861(19) Uani d . 1 . . P
F1 0.8323(10) 0.5074(7) 0.5769(5) 0.117(5) Uani d PD 0.50 A 1 F
F2 0.7756(10) 0.3558(7) 0.5613(6) 0.130(6) Uani d PD 0.50 A 1 F
F3 0.8556(8) 0.4093(9) 0.4912(5) 0.108(5) Uani d PD 0.50 A 1 F
F1' 0.8031(9) 0.4794(8) 0.5946(4) 0.106(4) Uani d PD 0.50 A 2 F
F2' 0.7970(8) 0.3390(5) 0.5363(5) 0.084(3) Uani d PD 0.50 A 2 F
F3' 0.8670(7) 0.4615(9) 0.5051(5) 0.107(5) Uani d PD 0.50 A 2 F
F4 0.1075(2) 0.2683(3) 0.33188(15) 0.1142(13) Uani d . 1 . . F
F5 0.1467(3) 0.1819(2) 0.24693(19) 0.1100(12) Uani d . 1 . . F
F6 0.0926(2) 0.3139(3) 0.24010(16) 0.0959(10) Uani d . 1 . . F
F7 0.5110(4) 0.0680(3) 0.2171(2) 0.1600(19) Uani d . 1 . . F
F8 0.4461(3) 0.1762(4) 0.18131(17) 0.154(2) Uani d . 1 . . F
F9 0.6053(3) 0.1938(3) 0.22205(19) 0.1468(19) Uani d . 1 . . F
O1 0.6522(2) 0.3832(2) 0.43902(14) 0.0528(7) Uani d . 1 . . O
O2 0.6305(3) 0.5039(3) 0.51809(15) 0.0712(9) Uani d . 1 . . O
O3 0.3113(2) 0.3202(2) 0.35532(13) 0.0552(7) Uani d . 1 . . O
O4 0.3039(3) 0.3523(3) 0.25356(16) 0.0877(12) Uani d . 1 . . O
O5 0.5197(2) 0.28646(19) 0.31912(13) 0.0490(7) Uani d . 1 . . O
O6 0.4441(3) 0.1389(2) 0.3231(2) 0.0941(13) Uani d . 1 . . O
C1 0.8705(2) 0.9942(2) 0.12955(17) 0.0294(7) Uani d . 1 . . C
C2 0.8702(3) 1.0505(3) 0.1913(2) 0.0431(9) Uani d . 1 . . C
H2 0.8923 1.0262 0.2300 0.052 Uiso calc R 1 . . H
C3 0.8381(3) 1.1416(3) 0.1973(2) 0.0571(12) Uani d . 1 . . C
H3 0.8395 1.1798 0.2397 0.068 Uiso calc R 1 . . H
C4 0.8038(3) 1.1763(3) 0.1400(3) 0.0604(13) Uani d . 1 . . C
H4 0.7801 1.2378 0.1434 0.072 Uiso calc R 1 . . H
C5 0.8044(3) 1.1217(3) 0.0793(2) 0.0519(11) Uani d . 1 . . C
H5 0.7821 1.1462 0.0407 0.062 Uiso calc R 1 . . H
C6 0.8372(3) 1.0306(3) 0.0729(2) 0.0400(9) Uani d . 1 . . C
H6 0.8369 0.9935 0.0303 0.048 Uiso calc R 1 . . H
C7 1.0565(3) 0.8999(2) 0.13510(16) 0.0288(7) Uani d . 1 . . C
C8 1.1148(3) 0.8256(3) 0.1457(2) 0.0439(9) Uani d . 1 . . C
H8 1.0803 0.7649 0.1490 0.053 Uiso calc R 1 . . H
C9 1.2234(3) 0.8396(3) 0.1516(2) 0.0550(11) Uani d . 1 . . C
H9 1.2626 0.7884 0.1586 0.066 Uiso calc R 1 . . H
C10 1.2738(3) 0.9281(3) 0.1471(2) 0.0541(11) Uani d . 1 . . C
H10 1.3477 0.9382 0.1516 0.065 Uiso calc R 1 . . H
C11 1.2162(3) 1.0017(3) 0.1363(2) 0.0585(12) Uani d . 1 . . C
H11 1.2510 1.0623 0.1331 0.070 Uiso calc R 1 . . H
C12 1.1080(3) 0.9884(3) 0.1300(2) 0.0455(10) Uani d . 1 . . C
H12 1.0693 1.0396 0.1222 0.055 Uiso calc R 1 . . H
C13 0.8732(3) 0.8196(2) 0.03750(16) 0.0297(7) Uani d . 1 . . C
C14 0.9431(3) 0.8119(3) -0.00643(17) 0.0383(8) Uani d . 1 . . C
H14 1.0152 0.8353 0.0092 0.046 Uiso calc R 1 . . H
C15 0.9081(3) 0.7701(3) -0.07298(19) 0.0471(10) Uani d . 1 . . C
H15 0.9565 0.7653 -0.1023 0.057 Uiso calc R 1 . . H
C16 0.8037(3) 0.7358(3) -0.0967(2) 0.0517(11) Uani d . 1 . . C
H16 0.7799 0.7069 -0.1420 0.062 Uiso calc R 1 . . H
C17 0.7342(3) 0.7440(3) -0.0537(2) 0.0594(12) Uani d . 1 . . C
H17 0.6620 0.7216 -0.0698 0.071 Uiso calc R 1 . . H
C18 0.7686(3) 0.7848(3) 0.01294(19) 0.0481(10) Uani d . 1 . . C
H18 0.7198 0.7888 0.0420 0.058 Uiso calc R 1 . . H
C19 0.5884(2) 0.7655(2) 0.25729(16) 0.0287(7) Uani d . 1 . . C
C20 0.6262(3) 0.7310(3) 0.31400(17) 0.0359(8) Uani d . 1 . . C
H20 0.6769 0.6877 0.3128 0.043 Uiso calc R 1 . . H
C21 0.5894(3) 0.7599(3) 0.37201(19) 0.0508(11) Uani d . 1 . . C
H21 0.6150 0.7357 0.4101 0.061 Uiso calc R 1 . . H
C22 0.5165(3) 0.8233(3) 0.3754(2) 0.0565(12) Uani d . 1 . . C
H22 0.4926 0.8429 0.4155 0.068 Uiso calc R 1 . . H
C23 0.4781(3) 0.8583(3) 0.3197(2) 0.0501(10) Uani d . 1 . . C
H23 0.4279 0.9021 0.3217 0.060 Uiso calc R 1 . . H
C24 0.5130(3) 0.8291(3) 0.26097(18) 0.0365(8) Uani d . 1 . . C
H24 0.4856 0.8525 0.2228 0.044 Uiso calc R 1 . . H
C25 0.5964(2) 0.6067(2) 0.15031(17) 0.0319(8) Uani d . 1 . . C
C26 0.6312(3) 0.5628(3) 0.09392(18) 0.0390(9) Uani d . 1 . . C
H26 0.6761 0.6000 0.0737 0.047 Uiso calc R 1 . . H
C27 0.6006(3) 0.4654(3) 0.0676(2) 0.0537(11) Uani d . 1 . . C
H27 0.6239 0.4363 0.0290 0.064 Uiso calc R 1 . . H
C28 0.5363(3) 0.4106(3) 0.0969(3) 0.0667(14) Uani d . 1 . . C
H28 0.5170 0.3435 0.0791 0.080 Uiso calc R 1 . . H
C29 0.4992(3) 0.4525(3) 0.1524(2) 0.0606(13) Uani d . 1 . . C
H29 0.4541 0.4147 0.1721 0.073 Uiso calc R 1 . . H
C30 0.5292(3) 0.5513(3) 0.1789(2) 0.0430(9) Uani d . 1 . . C
H30 0.5038 0.5807 0.2165 0.052 Uiso calc R 1 . . H
C31 0.5761(3) 0.7966(3) 0.12532(16) 0.0309(7) Uani d . 1 . . C
C32 0.4893(3) 0.7509(3) 0.07824(18) 0.0417(9) Uani d . 1 . . C
H32 0.4663 0.6842 0.0749 0.050 Uiso calc R 1 . . H
C33 0.4358(3) 0.8028(3) 0.0358(2) 0.0540(11) Uani d . 1 . . C
H33 0.3772 0.7710 0.0032 0.065 Uiso calc R 1 . . H
C34 0.4680(3) 0.8997(3) 0.0411(2) 0.0541(11) Uani d . 1 . . C
H34 0.4311 0.9347 0.0124 0.065 Uiso calc R 1 . . H
C35 0.5539(3) 0.9469(3) 0.0883(2) 0.0498(10) Uani d . 1 . . C
H35 0.5755 1.0139 0.0920 0.060 Uiso calc R 1 . . H
C36 0.6085(3) 0.8954(3) 0.13019(18) 0.0393(9) Uani d . 1 . . C
H36 0.6678 0.9273 0.1621 0.047 Uiso calc R 1 . . H
C37 0.8860(3) 0.5191(2) 0.24914(16) 0.0301(7) Uani d . 1 . . C
C38 0.9539(3) 0.4870(3) 0.29654(19) 0.0408(9) Uani d . 1 . . C
H38 1.0269 0.5081 0.3037 0.049 Uiso calc R 1 . . H
C39 0.9152(3) 0.4241(3) 0.3335(2) 0.0527(11) Uani d . 1 . . C
H39 0.9621 0.4019 0.3654 0.063 Uiso calc R 1 . . H
C40 0.8100(4) 0.3940(3) 0.3243(2) 0.0510(11) Uani d . 1 . . C
H40 0.7841 0.3518 0.3502 0.061 Uiso calc R 1 . . H
C41 0.7412(3) 0.4253(3) 0.2772(2) 0.0524(11) Uani d . 1 . . C
H41 0.6684 0.4032 0.2701 0.063 Uiso calc R 1 . . H
C42 0.7790(3) 0.4886(3) 0.2406(2) 0.0437(9) Uani d . 1 . . C
H42 0.7315 0.5115 0.2095 0.052 Uiso calc R 1 . . H
C43 0.8995(2) 0.5292(2) 0.11468(16) 0.0284(7) Uani d . 1 . . C
C44 0.8864(3) 0.5753(3) 0.06148(18) 0.0389(9) Uani d . 1 . . C
H44 0.8945 0.6439 0.0693 0.047 Uiso calc R 1 . . H
C45 0.8615(3) 0.5229(3) -0.00337(19) 0.0498(10) Uani d . 1 . . C
H45 0.8511 0.5556 -0.0392 0.060 Uiso calc R 1 . . H
C46 0.8521(3) 0.4232(3) -0.0153(2) 0.0496(10) Uani d . 1 . . C
H46 0.8357 0.3872 -0.0594 0.060 Uiso calc R 1 . . H
C47 0.8666(3) 0.3758(3) 0.0372(2) 0.0485(10) Uani d . 1 . . C
H47 0.8605 0.3072 0.0289 0.058 Uiso calc R 1 . . H
C48 0.8903(3) 0.4282(2) 0.10212(18) 0.0385(8) Uani d . 1 . . C
H48 0.9002 0.3952 0.1378 0.046 Uiso calc R 1 . . H
C49 1.0725(2) 0.6158(2) 0.22105(16) 0.0291(7) Uani d . 1 . . C
C50 1.1326(3) 0.5512(3) 0.1915(2) 0.0420(9) Uani d . 1 . . C
H50 1.0999 0.4989 0.1567 0.050 Uiso calc R 1 . . H
C51 1.2409(3) 0.5635(3) 0.2130(2) 0.0548(11) Uani d . 1 . . C
H51 1.2816 0.5201 0.1921 0.066 Uiso calc R 1 . . H
C52 1.2894(3) 0.6382(3) 0.2644(2) 0.0503(10) Uani d . 1 . . C
H52 1.3631 0.6459 0.2788 0.060 Uiso calc R 1 . . H
C53 1.2310(3) 0.7009(3) 0.2945(2) 0.0514(11) Uani d . 1 . . C
H53 1.2637 0.7518 0.3302 0.062 Uiso calc R 1 . . H
C54 1.1233(3) 0.6899(3) 0.27253(19) 0.0425(9) Uani d . 1 . . C
H54 1.0835 0.7344 0.2934 0.051 Uiso calc R 1 . . H
C55 0.8861(3) 0.8118(2) 0.39839(16) 0.0308(7) Uani d . 1 . . C
C56 0.8572(3) 0.8581(3) 0.45632(17) 0.0355(8) Uani d . 1 . . C
H56 0.8535 0.9255 0.4635 0.043 Uiso calc R 1 . . H
C57 0.8339(3) 0.8057(3) 0.50347(18) 0.0411(9) Uani d . 1 . . C
H57 0.8138 0.8379 0.5424 0.049 Uiso calc R 1 . . H
C58 0.8395(3) 0.7086(3) 0.4946(2) 0.0510(10) Uani d . 1 . . C
H58 0.8235 0.6735 0.5271 0.061 Uiso calc R 1 . . H
C59 0.8692(4) 0.6618(3) 0.4373(2) 0.0565(12) Uani d . 1 . . C
H59 0.8741 0.5945 0.4309 0.068 Uiso calc R 1 . . H
C60 0.8915(3) 0.7133(3) 0.38981(19) 0.0452(10) Uani d . 1 . . C
H60 0.9109 0.6807 0.3508 0.054 Uiso calc R 1 . . H
C61 0.8638(3) 0.9897(2) 0.35458(16) 0.0311(7) Uani d . 1 . . C
C62 0.9234(3) 1.0777(3) 0.38586(19) 0.0444(9) Uani d . 1 . . C
H62 0.9975 1.0822 0.3954 0.053 Uiso calc R 1 . . H
C63 0.8752(3) 1.1596(3) 0.4034(2) 0.0504(10) Uani d . 1 . . C
H63 0.9169 1.2196 0.4240 0.060 Uiso calc R 1 . . H
C64 0.7678(3) 1.1540(3) 0.3911(2) 0.0485(10) Uani d . 1 . . C
H64 0.7354 1.2093 0.4044 0.058 Uiso calc R 1 . . H
C65 0.7074(3) 1.0679(3) 0.3594(2) 0.0514(11) Uani d . 1 . . C
H65 0.6334 1.0642 0.3499 0.062 Uiso calc R 1 . . H
C66 0.7549(3) 0.9857(3) 0.3412(2) 0.0434(9) Uani d . 1 . . C
H66 0.7127 0.9265 0.3195 0.052 Uiso calc R 1 . . H
C67 1.0604(3) 0.9149(2) 0.35946(17) 0.0318(8) Uani d . 1 . . C
C68 1.1184(3) 0.8999(3) 0.41823(19) 0.0430(9) Uani d . 1 . . C
H68 1.0850 0.8664 0.4462 0.052 Uiso calc R 1 . . H
C69 1.2253(3) 0.9340(3) 0.4360(2) 0.0525(11) Uani d . 1 . . C
H69 1.2644 0.9226 0.4755 0.063 Uiso calc R 1 . . H
C70 1.2744(3) 0.9845(3) 0.3961(2) 0.0513(11) Uani d . 1 . . C
H70 1.3465 1.0095 0.4091 0.062 Uiso calc R 1 . . H
C71 1.2188(3) 0.9982(3) 0.3377(2) 0.0490(10) Uani d . 1 . . C
H71 1.2530 1.0315 0.3099 0.059 Uiso calc R 1 . . H
C72 1.1127(3) 0.9639(3) 0.31900(19) 0.0407(9) Uani d . 1 . . C
H72 1.0752 0.9736 0.2784 0.049 Uiso calc R 1 . . H
C73 0.4916(4) 0.5019(3) 0.3648(2) 0.0573(12) Uani d . 1 . . C
H73a 0.5459 0.5486 0.3957 0.086 Uiso calc R 1 . . H
H73b 0.4252 0.5285 0.3610 0.086 Uiso calc R 1 . . H
H73c 0.5119 0.4891 0.3213 0.086 Uiso calc R 1 . . H
C74 0.4543(4) 0.2896(3) 0.4708(2) 0.0579(12) Uani d . 1 . . C
H74a 0.4719 0.2248 0.4561 0.087 Uiso calc R 1 . . H
H74b 0.3813 0.2849 0.4767 0.087 Uiso calc R 1 . . H
H74c 0.5003 0.3204 0.5128 0.087 Uiso calc R 1 . . H
C75 0.6807(3) 0.4412(3) 0.4935(2) 0.0483(10) Uani d . 1 A . C
C76 0.7883(4) 0.4301(3) 0.5323(2) 0.0650(13) Uani d D 1 . . C
C77 0.2668(4) 0.3204(3) 0.2971(2) 0.0549(11) Uani d . 1 . . C
C78 0.1518(4) 0.2711(4) 0.2806(2) 0.0629(13) Uani d . 1 . . C
C79 0.4884(3) 0.1979(3) 0.2973(2) 0.0539(11) Uani d . 1 . . C
C80 0.5142(4) 0.1639(4) 0.2278(3) 0.0712(15) Uani d . 1 . . C
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C73 Sn C74 . . 154.6(2) yes
C73 Sn O1 . . 92.9(2) yes
C73 Sn O2 . 2_666 77.30(10) yes
C73 Sn O3 . . 99.5(2) yes
C73 Sn O5 . . 95.50(10) yes
C74 Sn O1 . . 86.20(10) yes
C74 Sn O2 . 2_666 79.9(2) yes
C74 Sn O3 . . 86.90(10) yes
C74 Sn O5 . . 109.2(2) yes
O1 Sn O2 . 2_666 114.00(10) yes
O1 Sn O3 . . 164.20(10) yes
O1 Sn O5 . . 79.70(10) yes
O2 Sn O3 2_666 . 78.70(10) yes
O2 Sn O5 2_666 . 164.60(10) yes
O3 Sn O5 . . 89.30(10) yes
P1 Ag P2 . . 108.16(3) no
P1 Ag P3 . . 111.35(3) no
P1 Ag P4 . . 109.45(3) no
P2 Ag P3 . . 107.36(3) no
P2 Ag P4 . . 109.94(3) no
P3 Ag P4 . . 110.51(3) no
C7 P1 C13 . . 102.48(15) no
C7 P1 C1 . . 103.44(15) no
C13 P1 C1 . . 101.84(15) no
C7 P1 Ag . . 113.19(11) no
C13 P1 Ag . . 117.39(11) no
C1 P1 Ag . . 116.52(11) no
C19 P2 C31 . . 102.57(15) no
C19 P2 C25 . . 104.58(15) no
C31 P2 C25 . . 102.41(16) no
C19 P2 Ag . . 113.11(10) no
C31 P2 Ag . . 117.91(11) no
C25 P2 Ag . . 114.59(10) no
C49 P3 C37 . . 102.65(15) no
C49 P3 C43 . . 103.67(15) no
C37 P3 C43 . . 102.48(15) no
C49 P3 Ag . . 113.79(11) no
C37 P3 Ag . . 117.34(11) no
C43 P3 Ag . . 115.09(11) no
C61 P4 C55 . . 101.87(15) no
C61 P4 C67 . . 102.37(15) no
C55 P4 C67 . . 103.14(15) no
C61 P4 Ag . . 117.20(11) no
C55 P4 Ag . . 113.99(11) no
C67 P4 Ag . . 116.21(11) no
C75 O1 Sn . . 112.0(3) no
C77 O3 Sn . . 127.0(3) no
C79 O5 Sn . . 125.5(3) no
C2 C1 C6 . . 118.8(3) no
C2 C1 P1 . . 118.4(3) no
C6 C1 P1 . . 122.7(3) no
C3 C2 C1 . . 121.2(4) no
C3 C2 H2 . . 119.4 no
C1 C2 H2 . . 119.4 no
C2 C3 C4 . . 119.2(4) no
C2 C3 H3 . . 120.4 no
C4 C3 H3 . . 120.4 no
C5 C4 C3 . . 119.9(4) no
C5 C4 H4 . . 120.0 no
C3 C4 H4 . . 120.0 no
C4 C5 C6 . . 121.2(4) no
C4 C5 H5 . . 119.4 no
C6 C5 H5 . . 119.4 no
C5 C6 C1 . . 119.7(4) no
C5 C6 H6 . . 120.1 no
C1 C6 H6 . . 120.1 no
C8 C7 C12 . . 119.1(3) no
C8 C7 P1 . . 117.5(3) no
C12 C7 P1 . . 123.4(3) no
C7 C8 C9 . . 120.5(4) no
C7 C8 H8 . . 119.7 no
C9 C8 H8 . . 119.7 no
C10 C9 C8 . . 119.9(4) no
C10 C9 H9 . . 120.1 no
C8 C9 H9 . . 120.1 no
C11 C10 C9 . . 119.7(4) no
C11 C10 H10 . . 120.1 no
C9 C10 H10 . . 120.1 no
C10 C11 C12 . . 120.9(4) no
C10 C11 H11 . . 119.5 no
C12 C11 H11 . . 119.5 no
C11 C12 C7 . . 119.9(4) no
C11 C12 H12 . . 120.1 no
C7 C12 H12 . . 120.1 no
C18 C13 C14 . . 118.1(3) no
C18 C13 P1 . . 118.8(3) no
C14 C13 P1 . . 123.1(3) no
C15 C14 C13 . . 120.6(3) no
C15 C14 H14 . . 119.7 no
C13 C14 H14 . . 119.7 no
C16 C15 C14 . . 120.5(4) no
C16 C15 H15 . . 119.7 no
C14 C15 H15 . . 119.7 no
C15 C16 C17 . . 119.1(4) no
C15 C16 H16 . . 120.4 no
C17 C16 H16 . . 120.4 no
C16 C17 C18 . . 120.7(4) no
C16 C17 H17 . . 119.6 no
C18 C17 H17 . . 119.6 no
C13 C18 C17 . . 120.8(4) no
C13 C18 H18 . . 119.6 no
C17 C18 H18 . . 119.6 no
C20 C19 C24 . . 118.3(3) no
C20 C19 P2 . . 118.4(3) no
C24 C19 P2 . . 123.0(3) no
C21 C20 C19 . . 120.0(4) no
C21 C20 H20 . . 120.0 no
C19 C20 H20 . . 120.0 no
C22 C21 C20 . . 121.2(4) no
C22 C21 H21 . . 119.4 no
C20 C21 H21 . . 119.4 no
C21 C22 C23 . . 119.6(4) no
C21 C22 H22 . . 120.2 no
C23 C22 H22 . . 120.2 no
C22 C23 C24 . . 120.0(4) no
C22 C23 H23 . . 120.0 no
C24 C23 H23 . . 120.0 no
C23 C24 C19 . . 120.8(4) no
C23 C24 H24 . . 119.6 no
C19 C24 H24 . . 119.6 no
C30 C25 C26 . . 119.1(3) no
C30 C25 P2 . . 123.8(3) no
C26 C25 P2 . . 117.0(3) no
C27 C26 C25 . . 120.3(4) no
C27 C26 H26 . . 119.8 no
C25 C26 H26 . . 119.8 no
C28 C27 C26 . . 120.3(4) no
C28 C27 H27 . . 119.9 no
C26 C27 H27 . . 119.9 no
C27 C28 C29 . . 120.7(4) no
C27 C28 H28 . . 119.7 no
C29 C28 H28 . . 119.7 no
C28 C29 C30 . . 119.2(4) no
C28 C29 H29 . . 120.4 no
C30 C29 H29 . . 120.4 no
C25 C30 C29 . . 120.4(4) no
C25 C30 H30 . . 119.8 no
C29 C30 H30 . . 119.8 no
C32 C31 C36 . . 119.2(3) no
C32 C31 P2 . . 122.9(3) no
C36 C31 P2 . . 117.8(3) no
C31 C32 C33 . . 120.2(4) no
C31 C32 H32 . . 119.9 no
C33 C32 H32 . . 119.9 no
C34 C33 C32 . . 120.1(4) no
C34 C33 H33 . . 119.9 no
C32 C33 H33 . . 119.9 no
C33 C34 C35 . . 120.5(4) no
C33 C34 H34 . . 119.8 no
C35 C34 H34 . . 119.8 no
C34 C35 C36 . . 119.7(4) no
C34 C35 H35 . . 120.1 no
C36 C35 H35 . . 120.1 no
C35 C36 C31 . . 120.2(4) no
C35 C36 H36 . . 119.9 no
C31 C36 H36 . . 119.9 no
C38 C37 C42 . . 118.7(3) no
C38 C37 P3 . . 123.4(3) no
C42 C37 P3 . . 117.8(3) no
C39 C38 C37 . . 120.2(4) no
C39 C38 H38 . . 119.9 no
C37 C38 H38 . . 119.9 no
C40 C39 C38 . . 120.5(4) no
C40 C39 H39 . . 119.8 no
C38 C39 H39 . . 119.8 no
C39 C40 C41 . . 120.0(4) no
C39 C40 H40 . . 120.0 no
C41 C40 H40 . . 120.0 no
C42 C41 C40 . . 119.9(4) no
C42 C41 H41 . . 120.1 no
C40 C41 H41 . . 120.1 no
C41 C42 C37 . . 120.6(4) no
C41 C42 H42 . . 119.7 no
C37 C42 H42 . . 119.7 no
C44 C43 C48 . . 118.6(3) no
C44 C43 P3 . . 118.3(3) no
C48 C43 P3 . . 123.1(3) no
C43 C44 C45 . . 121.2(3) no
C43 C44 H44 . . 119.4 no
C45 C44 H44 . . 119.4 no
C46 C45 C44 . . 119.8(4) no
C46 C45 H45 . . 120.1 no
C44 C45 H45 . . 120.1 no
C45 C46 C47 . . 119.9(4) no
C45 C46 H46 . . 120.1 no
C47 C46 H46 . . 120.1 no
C46 C47 C48 . . 120.4(4) no
C46 C47 H47 . . 119.8 no
C48 C47 H47 . . 119.8 no
C47 C48 C43 . . 120.1(4) no
C47 C48 H48 . . 119.9 no
C43 C48 H48 . . 119.9 no
C54 C49 C50 . . 118.0(3) no
C54 C49 P3 . . 118.1(3) no
C50 C49 P3 . . 123.7(3) no
C51 C50 C49 . . 120.0(4) no
C51 C50 H50 . . 120.0 no
C49 C50 H50 . . 120.0 no
C52 C51 C50 . . 120.7(4) no
C52 C51 H51 . . 119.6 no
C50 C51 H51 . . 119.6 no
C53 C52 C51 . . 119.8(4) no
C53 C52 H52 . . 120.1 no
C51 C52 H52 . . 120.1 no
C52 C53 C54 . . 119.8(4) no
C52 C53 H53 . . 120.1 no
C54 C53 H53 . . 120.1 no
C49 C54 C53 . . 121.8(3) no
C49 C54 H54 . . 119.1 no
C53 C54 H54 . . 119.1 no
C60 C55 C56 . . 118.3(3) no
C60 C55 P4 . . 118.6(3) no
C56 C55 P4 . . 123.1(3) no
C57 C56 C55 . . 120.3(3) no
C57 C56 H56 . . 119.8 no
C55 C56 H56 . . 119.8 no
C58 C57 C56 . . 121.0(4) no
C58 C57 H57 . . 119.5 no
C56 C57 H57 . . 119.5 no
C57 C58 C59 . . 119.2(4) no
C57 C58 H58 . . 120.4 no
C59 C58 H58 . . 120.4 no
C60 C59 C58 . . 120.1(4) no
C60 C59 H59 . . 120.0 no
C58 C59 H59 . . 120.0 no
C59 C60 C55 . . 121.1(4) no
C59 C60 H60 . . 119.5 no
C55 C60 H60 . . 119.5 no
C62 C61 C66 . . 118.2(3) no
C62 C61 P4 . . 124.3(3) no
C66 C61 P4 . . 117.4(3) no
C61 C62 C63 . . 120.6(4) no
C61 C62 H62 . . 119.7 no
C63 C62 H62 . . 119.7 no
C64 C63 C62 . . 120.5(4) no
C64 C63 H63 . . 119.8 no
C62 C63 H63 . . 119.8 no
C65 C64 C63 . . 119.8(4) no
C65 C64 H64 . . 120.1 no
C63 C64 H64 . . 120.1 no
C64 C65 C66 . . 120.2(4) no
C64 C65 H65 . . 119.9 no
C66 C65 H65 . . 119.9 no
C65 C66 C61 . . 120.7(4) no
C65 C66 H66 . . 119.6 no
C61 C66 H66 . . 119.6 no
C68 C67 C72 . . 118.2(3) no
C68 C67 P4 . . 123.2(3) no
C72 C67 P4 . . 118.6(3) no
C69 C68 C67 . . 120.3(4) no
C69 C68 H68 . . 119.8 no
C67 C68 H68 . . 119.8 no
C70 C69 C68 . . 120.3(4) no
C70 C69 H69 . . 119.8 no
C68 C69 H69 . . 119.8 no
C71 C70 C69 . . 119.9(4) no
C71 C70 H70 . . 120.0 no
C69 C70 H70 . . 120.0 no
C70 C71 C72 . . 120.4(4) no
C70 C71 H71 . . 119.8 no
C72 C71 H71 . . 119.8 no
C71 C72 C67 . . 120.7(4) no
C71 C72 H72 . . 119.6 no
C67 C72 H72 . . 119.6 no
Sn C73 H73a . . 109.5 no
Sn C73 H73b . . 109.5 no
H73a C73 H73b . . 109.5 no
Sn C73 H73c . . 109.5 no
H73a C73 H73c . . 109.5 no
H73b C73 H73c . . 109.5 no
Sn C74 H74a . . 109.5 no
Sn C74 H74b . . 109.5 no
H74a C74 H74b . . 109.5 no
Sn C74 H74c . . 109.5 no
H74a C74 H74c . . 109.5 no
H74b C74 H74c . . 109.5 no
O2 C75 O1 . . 126.3(4) no
O2 C75 C76 . . 119.1(4) no
O1 C75 C76 . . 114.6(4) no
F1 C76 F2 . . 109.4(7) no
F2 C76 F3' . . 130.6(8) no
F2' C76 F3' . . 107.1(7) no
F2' C76 F1' . . 105.9(6) no
F3' C76 F1' . . 107.9(7) no
F1 C76 F3 . . 107.7(7) no
F2 C76 F3 . . 106.7(7) no
F1 C76 C75 . . 113.8(7) no
F2 C76 C75 . . 108.0(7) no
F2' C76 C75 . . 112.4(5) no
F3' C76 C75 . . 112.4(6) no
F1' C76 C75 . . 110.7(6) no
F3 C76 C75 . . 111.0(6) no
O4 C77 O3 . . 128.4(4) no
O4 C77 C78 . . 118.5(4) no
O3 C77 C78 . . 113.1(4) no
F4 C78 F6 . . 107.5(4) no
F4 C78 F5 . . 109.0(5) no
F6 C78 F5 . . 104.2(4) no
F4 C78 C77 . . 114.7(4) no
F6 C78 C77 . . 111.4(4) no
F5 C78 C77 . . 109.5(4) no
O6 C79 O5 . . 129.6(5) no
O6 C79 C80 . . 118.9(4) no
O5 C79 C80 . . 111.5(4) no
F9 C80 F8 . . 112.5(6) no
F9 C80 F7 . . 103.9(5) no
F8 C80 F7 . . 103.0(5) no
F9 C80 C79 . . 114.5(4) no
F8 C80 C79 . . 113.7(4) no
F7 C80 C79 . . 108.0(5) no
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sn C73 . 2.081(4) yes
Sn C74 . 2.065(4) yes
Sn O1 . 2.291(3) yes
Sn O2 2_666 2.818(3) yes
Sn O3 . 2.155(3) yes
Sn O5 . 2.082(3) yes
Ag P1 . 2.6167(9) no
Ag P2 . 2.6204(9) no
Ag P3 . 2.6363(9) no
Ag P4 . 2.6373(9) no
P1 C7 . 1.818(3) no
P1 C13 . 1.820(3) no
P1 C1 . 1.826(3) no
P2 C19 . 1.807(3) no
P2 C31 . 1.818(3) no
P2 C25 . 1.824(3) no
P3 C49 . 1.817(3) no
P3 C37 . 1.825(3) no
P3 C43 . 1.828(3) no
P4 C61 . 1.825(3) no
P4 C55 . 1.825(3) no
P4 C67 . 1.826(3) no
F1 C76 . 1.304(7) no
F2 C76 . 1.304(7) no
F3 C76 . 1.332(8) no
F1' C76 . 1.326(7) no
F2' C76 . 1.312(7) no
F3' C76 . 1.317(7) no
F4 C78 . 1.291(5) no
F5 C78 . 1.309(5) no
F6 C78 . 1.312(5) no
F7 C80 . 1.321(6) no
F8 C80 . 1.243(6) no
F9 C80 . 1.243(5) no
O1 C75 . 1.244(5) no
O2 C75 . 1.234(5) no
O3 C77 . 1.249(5) no
O4 C77 . 1.220(5) no
O5 C79 . 1.245(5) no
O6 C79 . 1.210(5) no
C1 C2 . 1.379(5) no
C1 C6 . 1.387(5) no
C2 C3 . 1.377(5) no
C2 H2 . 0.9400 no
C3 C4 . 1.388(6) no
C3 H3 . 0.9400 no
C4 C5 . 1.354(6) no
C4 H4 . 0.9400 no
C5 C6 . 1.379(5) no
C5 H5 . 0.9400 no
C6 H6 . 0.9400 no
C7 C8 . 1.377(5) no
C7 C12 . 1.379(5) no
C8 C9 . 1.381(5) no
C8 H8 . 0.9400 no
C9 C10 . 1.370(6) no
C9 H9 . 0.9400 no
C10 C11 . 1.364(6) no
C10 H10 . 0.9400 no
C11 C12 . 1.375(5) no
C11 H11 . 0.9400 no
C12 H12 . 0.9400 no
C13 C18 . 1.371(5) no
C13 C14 . 1.384(5) no
C14 C15 . 1.379(5) no
C14 H14 . 0.9400 no
C15 C16 . 1.366(6) no
C15 H15 . 0.9400 no
C16 C17 . 1.364(6) no
C16 H16 . 0.9400 no
C17 C18 . 1.377(5) no
C17 H17 . 0.9400 no
C18 H18 . 0.9400 no
C19 C20 . 1.387(5) no
C19 C24 . 1.391(5) no
C20 C21 . 1.374(5) no
C20 H20 . 0.9400 no
C21 C22 . 1.364(6) no
C21 H21 . 0.9400 no
C22 C23 . 1.373(6) no
C22 H22 . 0.9400 no
C23 C24 . 1.376(5) no
C23 H23 . 0.9400 no
C24 H24 . 0.9400 no
C25 C30 . 1.382(5) no
C25 C26 . 1.386(5) no
C26 C27 . 1.369(5) no
C26 H26 . 0.9400 no
C27 C28 . 1.364(6) no
C27 H27 . 0.9400 no
C28 C29 . 1.377(6) no
C28 H28 . 0.9400 no
C29 C30 . 1.386(5) no
C29 H29 . 0.9400 no
C30 H30 . 0.9400 no
C31 C32 . 1.376(5) no
C31 C36 . 1.388(5) no
C32 C33 . 1.387(5) no
C32 H32 . 0.9400 no
C33 C34 . 1.362(6) no
C33 H33 . 0.9400 no
C34 C35 . 1.376(6) no
C34 H34 . 0.9400 no
C35 C36 . 1.381(5) no
C35 H35 . 0.9400 no
C36 H36 . 0.9400 no
C37 C38 . 1.378(5) no
C37 C42 . 1.379(5) no
C38 C39 . 1.378(5) no
C38 H38 . 0.9400 no
C39 C40 . 1.355(6) no
C39 H39 . 0.9400 no
C40 C41 . 1.374(6) no
C40 H40 . 0.9400 no
C41 C42 . 1.372(5) no
C41 H41 . 0.9400 no
C42 H42 . 0.9400 no
C43 C44 . 1.373(5) no
C43 C48 . 1.384(4) no
C44 C45 . 1.381(5) no
C44 H44 . 0.9400 no
C45 C46 . 1.366(5) no
C45 H45 . 0.9400 no
C46 C47 . 1.372(6) no
C46 H46 . 0.9400 no
C47 C48 . 1.382(5) no
C47 H47 . 0.9400 no
C48 H48 . 0.9400 no
C49 C54 . 1.373(5) no
C49 C50 . 1.381(5) no
C50 C51 . 1.383(5) no
C50 H50 . 0.9400 no
C51 C52 . 1.369(6) no
C51 H51 . 0.9400 no
C52 C53 . 1.354(5) no
C52 H52 . 0.9400 no
C53 C54 . 1.377(5) no
C53 H53 . 0.9400 no
C54 H54 . 0.9400 no
C55 C60 . 1.374(5) no
C55 C56 . 1.386(5) no
C56 C57 . 1.377(5) no
C56 H56 . 0.9400 no
C57 C58 . 1.355(5) no
C57 H57 . 0.9400 no
C58 C59 . 1.383(5) no
C58 H58 . 0.9400 no
C59 C60 . 1.373(5) no
C59 H59 . 0.9400 no
C60 H60 . 0.9400 no
C61 C62 . 1.377(5) no
C61 C66 . 1.385(5) no
C62 C63 . 1.385(5) no
C62 H62 . 0.9400 no
C63 C64 . 1.364(6) no
C63 H63 . 0.9400 no
C64 C65 . 1.363(6) no
C64 H64 . 0.9400 no
C65 C66 . 1.385(5) no
C65 H65 . 0.9400 no
C66 H66 . 0.9400 no
C67 C68 . 1.385(5) no
C67 C72 . 1.391(5) no
C68 C69 . 1.382(5) no
C68 H68 . 0.9400 no
C69 C70 . 1.371(6) no
C69 H69 . 0.9400 no
C70 C71 . 1.360(6) no
C70 H70 . 0.9400 no
C71 C72 . 1.374(5) no
C71 H71 . 0.9400 no
C72 H72 . 0.9400 no
C73 H73a . 0.9700 no
C73 H73b . 0.9700 no
C73 H73c . 0.9700 no
C74 H74a . 0.9700 no
C74 H74b . 0.9700 no
C74 H74c . 0.9700 no
C75 C76 . 1.527(6) no
C77 C78 . 1.533(6) no
C79 C80 . 1.536(6) no
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion
_geom_torsion_publ_flag
P2 Ag P1 C7 . -176.63(12) no
P3 Ag P1 C7 . -58.88(12) no
P4 Ag P1 C7 . 63.60(12) no
P2 Ag P1 C13 . -57.51(13) no
P3 Ag P1 C13 . 60.24(13) no
P4 Ag P1 C13 . -177.28(12) no
P2 Ag P1 C1 . 63.61(12) no
P3 Ag P1 C1 . -178.65(12) no
P4 Ag P1 C1 . -56.16(12) no
P1 Ag P2 C19 . -129.71(12) no
P3 Ag P2 C19 . 110.02(12) no
P4 Ag P2 C19 . -10.24(12) no
P1 Ag P2 C31 . -10.11(13) no
P3 Ag P2 C31 . -130.38(13) no
P4 Ag P2 C31 . 109.35(13) no
P1 Ag P2 C25 . 110.55(13) no
P3 Ag P2 C25 . -9.73(13) no
P4 Ag P2 C25 . -129.99(13) no
P1 Ag P3 C49 . 65.73(12) no
P2 Ag P3 C49 . -176.05(12) no
P4 Ag P3 C49 . -56.14(12) no
P1 Ag P3 C37 . -174.44(13) no
P2 Ag P3 C37 . -56.22(13) no
P4 Ag P3 C37 . 63.69(13) no
P1 Ag P3 C43 . -53.72(12) no
P2 Ag P3 C43 . 64.50(12) no
P4 Ag P3 C43 . -175.60(11) no
P1 Ag P4 C61 . 63.22(13) no
P2 Ag P4 C61 . -55.45(13) no
P3 Ag P4 C61 . -173.79(13) no
P1 Ag P4 C55 . -177.97(12) no
P2 Ag P4 C55 . 63.35(12) no
P3 Ag P4 C55 . -54.99(12) no
P1 Ag P4 C67 . -58.21(13) no
P2 Ag P4 C67 . -176.89(13) no
P3 Ag P4 C67 . 64.77(13) no
C74 Sn O1 C75 . -75.3(3) no
O5 Sn O1 C75 . 174.4(3) no
C73 Sn O1 C75 . 79.3(3) no
O3 Sn O1 C75 . -139.5(4) no
O2 Sn O1 C75 2_666 1.9(3) no
C74 Sn O3 C77 . -161.2(4) no
O5 Sn O3 C77 . -51.9(4) no
C73 Sn O3 C77 . 43.5(4) no
O1 Sn O3 C77 . -97.1(5) no
O2 Sn O3 C77 2_666 118.5(4) no
C74 Sn O5 C79 . 35.5(4) no
C73 Sn O5 C79 . -150.3(4) no
O3 Sn O5 C79 . -50.9(3) no
O1 Sn O5 C79 . 117.8(3) no
O2 Sn O5 C79 2_666 -88.9(5) no
C7 P1 C1 C2 . -85.9(3) no
C13 P1 C1 C2 . 168.0(3) no
Ag P1 C1 C2 . 39.0(3) no
C7 P1 C1 C6 . 94.8(3) no
C13 P1 C1 C6 . -11.3(3) no
Ag P1 C1 C6 . -140.4(3) no
C6 C1 C2 C3 . -0.4(5) no
P1 C1 C2 C3 . -179.8(3) no
C1 C2 C3 C4 . 1.2(6) no
C2 C3 C4 C5 . -1.5(6) no
C3 C4 C5 C6 . 1.0(6) no
C4 C5 C6 C1 . -0.2(6) no
C2 C1 C6 C5 . -0.1(5) no
P1 C1 C6 C5 . 179.3(3) no
C13 P1 C7 C8 . -85.2(3) no
C1 P1 C7 C8 . 169.2(3) no
Ag P1 C7 C8 . 42.2(3) no
C13 P1 C7 C12 . 92.8(3) no
C1 P1 C7 C12 . -12.8(3) no
Ag P1 C7 C12 . -139.8(3) no
C12 C7 C8 C9 . 0.4(6) no
P1 C7 C8 C9 . 178.5(3) no
C7 C8 C9 C10 . 0.3(6) no
C8 C9 C10 C11 . -0.7(7) no
C9 C10 C11 C12 . 0.3(7) no
C10 C11 C12 C7 . 0.4(7) no
C8 C7 C12 C11 . -0.7(6) no
P1 C7 C12 C11 . -178.7(3) no
C7 P1 C13 C18 . 176.0(3) no
C1 P1 C13 C18 . -77.1(3) no
Ag P1 C13 C18 . 51.3(3) no
C7 P1 C13 C14 . -4.1(3) no
C1 P1 C13 C14 . 102.7(3) no
Ag P1 C13 C14 . -128.8(3) no
C18 C13 C14 C15 . -0.1(5) no
P1 C13 C14 C15 . -179.9(3) no
C13 C14 C15 C16 . 0.1(6) no
C14 C15 C16 C17 . 0.5(7) no
C15 C16 C17 C18 . -1.1(7) no
C14 C13 C18 C17 . -0.5(6) no
P1 C13 C18 C17 . 179.3(3) no
C16 C17 C18 C13 . 1.2(7) no
C31 P2 C19 C20 . -178.9(3) no
C25 P2 C19 C20 . 74.5(3) no
Ag P2 C19 C20 . -50.9(3) no
C31 P2 C19 C24 . -4.7(3) no
C25 P2 C19 C24 . -111.3(3) no
Ag P2 C19 C24 . 123.3(3) no
C24 C19 C20 C21 . -0.3(5) no
P2 C19 C20 C21 . 174.2(3) no
C19 C20 C21 C22 . -0.6(6) no
C20 C21 C22 C23 . 0.6(6) no
C21 C22 C23 C24 . 0.2(6) no
C22 C23 C24 C19 . -1.0(6) no
C20 C19 C24 C23 . 1.0(5) no
P2 C19 C24 C23 . -173.2(3) no
C19 P2 C25 C30 . -1.7(3) no
C31 P2 C25 C30 . -108.4(3) no
Ag P2 C25 C30 . 122.7(3) no
C19 P2 C25 C26 . -178.8(3) no
C31 P2 C25 C26 . 74.5(3) no
Ag P2 C25 C26 . -54.4(3) no
C30 C25 C26 C27 . -0.9(5) no
P2 C25 C26 C27 . 176.4(3) no
C25 C26 C27 C28 . -0.6(6) no
C26 C27 C28 C29 . 1.6(7) no
C27 C28 C29 C30 . -0.9(7) no
C26 C25 C30 C29 . 1.5(6) no
P2 C25 C30 C29 . -175.6(3) no
C28 C29 C30 C25 . -0.6(7) no
C19 P2 C31 C32 . -95.2(3) no
C25 P2 C31 C32 . 13.0(3) no
Ag P2 C31 C32 . 139.8(3) no
C19 P2 C31 C36 . 82.0(3) no
C25 P2 C31 C36 . -169.7(3) no
Ag P2 C31 C36 . -42.9(3) no
C36 C31 C32 C33 . 0.7(5) no
P2 C31 C32 C33 . 177.9(3) no
C31 C32 C33 C34 . -1.0(6) no
C32 C33 C34 C35 . 0.4(7) no
C33 C34 C35 C36 . 0.5(6) no
C34 C35 C36 C31 . -0.8(6) no
C32 C31 C36 C35 . 0.1(5) no
P2 C31 C36 C35 . -177.2(3) no
C49 P3 C37 C38 . 7.0(3) no
C43 P3 C37 C38 . 114.3(3) no
Ag P3 C37 C38 . -118.6(3) no
C49 P3 C37 C42 . -175.6(3) no
C43 P3 C37 C42 . -68.3(3) no
Ag P3 C37 C42 . 58.9(3) no
C42 C37 C38 C39 . 1.3(6) no
P3 C37 C38 C39 . 178.7(3) no
C37 C38 C39 C40 . -0.8(6) no
C38 C39 C40 C41 . 0.8(7) no
C39 C40 C41 C42 . -1.5(6) no
C40 C41 C42 C37 . 2.0(6) no
C38 C37 C42 C41 . -1.9(6) no
P3 C37 C42 C41 . -179.5(3) no
C49 P3 C43 C44 . -96.2(3) no
C37 P3 C43 C44 . 157.3(3) no
Ag P3 C43 C44 . 28.7(3) no
C49 P3 C43 C48 . 83.3(3) no
C37 P3 C43 C48 . -23.3(3) no
Ag P3 C43 C48 . -151.8(3) no
C48 C43 C44 C45 . 1.9(5) no
P3 C43 C44 C45 . -178.6(3) no
C43 C44 C45 C46 . -1.6(6) no
C44 C45 C46 C47 . 0.5(6) no
C45 C46 C47 C48 . 0.3(6) no
C46 C47 C48 C43 . 0.0(6) no
C44 C43 C48 C47 . -1.1(5) no
P3 C43 C48 C47 . 179.5(3) no
C37 P3 C49 C54 . -92.2(3) no
C43 P3 C49 C54 . 161.4(3) no
Ag P3 C49 C54 . 35.6(3) no
C37 P3 C49 C50 . 84.1(3) no
C43 P3 C49 C50 . -22.3(3) no
Ag P3 C49 C50 . -148.0(3) no
C54 C49 C50 C51 . -1.3(6) no
P3 C49 C50 C51 . -177.7(3) no
C49 C50 C51 C52 . 1.3(6) no
C50 C51 C52 C53 . -0.2(7) no
C51 C52 C53 C54 . -0.9(7) no
C50 C49 C54 C53 . 0.3(6) no
P3 C49 C54 C53 . 176.9(3) no
C52 C53 C54 C49 . 0.8(6) no
C61 P4 C55 C60 . 164.2(3) no
C67 P4 C55 C60 . -89.9(3) no
Ag P4 C55 C60 . 37.0(3) no
C61 P4 C55 C56 . -16.3(3) no
C67 P4 C55 C56 . 89.5(3) no
Ag P4 C55 C56 . -143.6(3) no
C60 C55 C56 C57 . -0.5(5) no
P4 C55 C56 C57 . -179.9(3) no
C55 C56 C57 C58 . 0.5(6) no
C56 C57 C58 C59 . 0.0(6) no
C57 C58 C59 C60 . -0.6(7) no
C58 C59 C60 C55 . 0.7(7) no
C56 C55 C60 C59 . -0.1(6) no
P4 C55 C60 C59 . 179.3(3) no
C55 P4 C61 C62 . 103.3(3) no
C67 P4 C61 C62 . -3.2(4) no
Ag P4 C61 C62 . -131.6(3) no
C55 P4 C61 C66 . -73.2(3) no
C67 P4 C61 C66 . -179.7(3) no
Ag P4 C61 C66 . 51.9(3) no
C66 C61 C62 C63 . 0.1(6) no
P4 C61 C62 C63 . -176.4(3) no
C61 C62 C63 C64 . 1.2(6) no
C62 C63 C64 C65 . -2.0(7) no
C63 C64 C65 C66 . 1.5(7) no
C64 C65 C66 C61 . -0.2(6) no
C62 C61 C66 C65 . -0.6(6) no
P4 C61 C66 C65 . 176.1(3) no
C61 P4 C67 C68 . 101.9(3) no
C55 P4 C67 C68 . -3.6(3) no
Ag P4 C67 C68 . -129.1(3) no
C61 P4 C67 C72 . -76.8(3) no
C55 P4 C67 C72 . 177.7(3) no
Ag P4 C67 C72 . 52.2(3) no
C72 C67 C68 C69 . 0.7(5) no
P4 C67 C68 C69 . -178.0(3) no
C67 C68 C69 C70 . 1.1(6) no
C68 C69 C70 C71 . -2.2(6) no
C69 C70 C71 C72 . 1.5(6) no
C70 C71 C72 C67 . 0.3(6) no
C68 C67 C72 C71 . -1.4(5) no
P4 C67 C72 C71 . 177.4(3) no
Sn O1 C75 O2 . -16.6(5) no
Sn O1 C75 C76 . 162.7(3) no
O2 C75 C76 F1 . -21.3(9) no
O1 C75 C76 F1 . 159.3(7) no
O2 C75 C76 F2 . 100.4(7) no
O1 C75 C76 F2 . -79.0(7) no
O2 C75 C76 F2' . 130.5(7) no
O1 C75 C76 F2' . -48.8(7) no
O2 C75 C76 F3' . -108.6(7) no
O1 C75 C76 F3' . 72.1(8) no
O2 C75 C76 F1' . 12.2(8) no
O1 C75 C76 F1' . -167.1(7) no
O2 C75 C76 F3 . -142.9(7) no
O1 C75 C76 F3 . 37.7(7) no
Sn O3 C77 O4 . -2.5(7) no
Sn O3 C77 C78 . 175.9(3) no
O4 C77 C78 F4 . -158.2(5) no
O3 C77 C78 F4 . 23.1(6) no
O4 C77 C78 F6 . -35.8(6) no
O3 C77 C78 F6 . 145.6(4) no
O4 C77 C78 F5 . 78.9(6) no
O3 C77 C78 F5 . -99.7(5) no
Sn O5 C79 O6 . -15.6(7) no
Sn O5 C79 C80 . 165.3(3) no
O6 C79 C80 F9 . -134.1(6) no
O5 C79 C80 F9 . 45.0(7) no
O6 C79 C80 F8 . 94.6(7) no
O5 C79 C80 F8 . -86.2(6) no
O6 C79 C80 F7 . -19.0(7) no
O5 C79 C80 F7 . 160.1(4) no
