#------------------------------------------------------------------------------
#$Date: 2016-08-05 09:33:05 +0300 (Fri, 05 Aug 2016) $
#$Revision: 185010 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/05/2020521.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2020521
loop_
_publ_author_name
'Galding, M. R.'
'Virovets, A. V.'
'Kazakov, I. V.'
'Scheer, M.'
'Smirnov, S. N.'
'Timoshkin, A. Y.'
_publ_section_title
;
 Diminished electron density in the Vaska-type rhodium(I) complex
 trans-[Rh(NCBH₃)(CO)(PPh₃)₂]
;
_journal_coeditor_code           LY3032
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              514
_journal_page_last               517
_journal_paper_doi               10.1107/S2053229616008536
_journal_volume                  72
_journal_year                    2016
_chemical_formula_iupac          '[Rh (C H3 B N) (C O) (C18 H15 P)2]'
_chemical_formula_moiety         'C38 H33 B N O P2 Rh'
_chemical_formula_sum            'C38 H33 B N O P2 Rh'
_chemical_formula_weight         695.31
_chemical_name_systematic
Carbonyl(cyanotrihydridoborato-κN)bis(triphenylphosphine-κP)rhodium(I)
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method
;
Olex2 1.2
(compiled 2014.02.17 svn.r2891 for OlexSys, GUI svn.r4773)
;
_cell_angle_alpha                90
_cell_angle_beta                 105.9870(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.92270(10)
_cell_length_b                   12.35000(10)
_cell_length_c                   19.79660(10)
_cell_measurement_reflns_used    33390
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      73.4940
_cell_measurement_theta_min      4.2140
_cell_volume                     3272.28(4)
_computing_cell_refinement
;
CrysAlis PRO (Agilent, 2014)
;
_computing_data_collection
;
CrysAlis PRO (Agilent, 2014)
;
_computing_data_reduction
;
CrysAlis PRO (Agilent, 2014)
;
_computing_molecular_graphics
;
OLEX2 (Dolomanov et al.,  2009)
;
_computing_publication_material
;
OLEX2 (Dolomanov et al.,  2009)
;
_computing_structure_refinement
;
SHELXL2014 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      123(2)
_diffrn_detector_area_resol_mean 5.1773
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type
'Agilent SuperNova Single Source diffractometer with an Atlas detector'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0273
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            45590
_diffrn_reflns_theta_full        67.500
_diffrn_reflns_theta_max         73.668
_diffrn_reflns_theta_min         3.302
_exptl_absorpt_coefficient_mu    5.381
_exptl_absorpt_correction_T_max  0.706
_exptl_absorpt_correction_T_min  0.186
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
;
(CrysAlis PRO; Agilent, 2014)
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.411
_exptl_crystal_description       plate
_exptl_crystal_F_000             1424
_exptl_crystal_size_max          0.2342
_exptl_crystal_size_mid          0.131
_exptl_crystal_size_min          0.0417
_refine_diff_density_max         0.360
_refine_diff_density_min         -0.562
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.078
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     452
_refine_ls_number_reflns         6570
_refine_ls_number_restraints     72
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.0222
_refine_ls_R_factor_gt           0.0207
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0325P)²+1.0597P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0553
_refine_ls_wR_factor_ref         0.0559
_reflns_number_gt                6129
_reflns_number_total             6570
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ly3032sup1.cif
_cod_data_source_block           I
_cod_depositor_comments          'Adding full bibliography for 2020521.cif.'
_cod_database_code               2020521
_cod_database_fobs_code          2020521
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.366
_shelx_estimated_absorpt_t_max   0.807
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh Rh1 0.73503(2) 0.56499(2) 0.41983(2) 0.02494(5) Uani d 1 . .
N N1 0.82165(11) 0.53014(11) 0.51849(7) 0.0326(3) Uani d 1 . .
C C1 0.87733(15) 0.50901(14) 0.57081(9) 0.0370(4) Uani d 1 . .
B B1 0.9596(3) 0.4798(2) 0.64131(13) 0.0686(9) Uani d 1 . .
H H1A 1.0164 0.4480 0.6303 0.103 Uiso calc 1 . .
H H1B 0.9324 0.4293 0.6680 0.103 Uiso calc 1 . .
H H1C 0.9799 0.5444 0.6684 0.103 Uiso calc 1 . .
C C2 0.65934(13) 0.59485(13) 0.33044(10) 0.0346(4) Uani d 1 . .
O O1 0.61246(11) 0.61247(11) 0.27439(7) 0.0492(4) Uani d 1 . .
P P1 0.69357(3) 0.38432(3) 0.39413(2) 0.02617(9) Uani d 1 . .
C C111 0.74308(13) 0.28177(13) 0.46076(8) 0.0300(3) Uani d 1 . .
C C112 0.84580(14) 0.28016(14) 0.49117(9) 0.0344(4) Uani d 1 . .
H H112 0.8858 0.3332 0.4794 0.041 Uiso calc 1 . .
C C113 0.88900(15) 0.19970(14) 0.53907(9) 0.0395(4) Uani d 1 . .
H H113 0.9576 0.1994 0.5597 0.047 Uiso calc 1 . .
C C114 0.82958(17) 0.12001(14) 0.55588(9) 0.0417(5) Uani d 1 . .
H H114 0.8584 0.0660 0.5878 0.050 Uiso calc 1 . .
C C115 0.72795(17) 0.12046(14) 0.52548(10) 0.0436(5) Uani d 1 . .
H H115 0.6885 0.0664 0.5367 0.052 Uiso calc 1 . .
C C116 0.68388(15) 0.20139(13) 0.47805(10) 0.0373(4) Uani d 1 . .
H H116 0.6151 0.2017 0.4580 0.045 Uiso calc 1 . .
C C121 0.55822(12) 0.37601(11) 0.37490(8) 0.0252(3) Uani d 1 . .
C C122 0.51429(12) 0.39827(12) 0.42911(8) 0.0279(3) Uani d 1 . .
H H122 0.5546 0.4086 0.4746 0.033 Uiso calc 1 . .
C C123 0.41169(13) 0.40499(14) 0.41564(9) 0.0323(3) Uani d 1 . .
H H123 0.3832 0.4190 0.4521 0.039 Uiso calc 1 . .
C C124 0.35131(14) 0.39082(17) 0.34787(10) 0.0419(4) Uani d 1 . .
H H124 0.2823 0.3961 0.3386 0.050 Uiso calc 1 . .
C C125 0.39386(15) 0.36882(19) 0.29399(10) 0.0482(5) Uani d 1 . .
H H125 0.3531 0.3591 0.2485 0.058 Uiso calc 1 . .
C C126 0.49690(14) 0.36117(15) 0.30718(9) 0.0374(4) Uani d 1 . .
H H126 0.5249 0.3461 0.2706 0.045 Uiso calc 1 . .
C C131 0.7183(7) 0.3134(6) 0.3137(4) 0.0225(14) Uani d 0.5 A 1
C C132 0.7846(6) 0.3640(5) 0.2844(4) 0.0324(14) Uani d 0.5 A 1
H H132 0.8072 0.4336 0.2983 0.039 Uiso calc 0.5 A 1
C C133 0.8175(5) 0.3098(7) 0.2336(3) 0.0413(16) Uani d 0.5 A 1
H H133 0.8650 0.3418 0.2148 0.050 Uiso calc 0.5 A 1
C C134 0.7806(5) 0.2101(6) 0.2111(3) 0.0482(15) Uani d 0.5 A 1
H H134 0.8020 0.1747 0.1764 0.058 Uiso calc 0.5 A 1
C C135 0.7119(5) 0.1615(4) 0.2395(3) 0.0502(13) Uani d 0.5 A 1
H H135 0.6865 0.0937 0.2235 0.060 Uiso calc 0.5 A 1
C C136 0.6799(4) 0.2130(5) 0.2921(3) 0.0361(11) Uani d 0.5 A 1
H H136 0.6339 0.1803 0.3119 0.043 Uiso calc 0.5 A 1
C C141 0.7377(7) 0.3386(7) 0.3256(5) 0.0234(14) Uani d 0.5 A 2
C C142 0.7972(6) 0.3993(5) 0.2942(4) 0.0253(11) Uani d 0.5 A 2
H H142 0.8127 0.4703 0.3090 0.030 Uiso calc 0.5 A 2
C C143 0.8349(4) 0.3567(4) 0.2405(3) 0.0316(12) Uani d 0.5 A 2
H H143 0.8722 0.4000 0.2187 0.038 Uiso calc 0.5 A 2
C C144 0.8157(5) 0.2506(6) 0.2208(3) 0.0350(13) Uani d 0.5 A 2
H H144 0.8410 0.2219 0.1858 0.042 Uiso calc 0.5 A 2
C C145 0.7602(4) 0.1862(4) 0.2518(3) 0.0367(10) Uani d 0.5 A 2
H H145 0.7480 0.1144 0.2381 0.044 Uiso calc 0.5 A 2
C C146 0.7218(4) 0.2292(5) 0.3043(3) 0.0302(11) Uani d 0.5 A 2
H H146 0.6849 0.1849 0.3257 0.036 Uiso calc 0.5 A 2
P P2 0.74681(3) 0.74960(3) 0.44377(2) 0.02491(8) Uani d 1 . .
C C211 0.62427(13) 0.81437(15) 0.41329(8) 0.0348(4) Uani d 1 . .
C C212 0.61247(17) 0.92239(17) 0.39291(10) 0.0448(5) Uani d 1 . .
H H212 0.6681 0.9649 0.3945 0.054 Uiso calc 1 . .
C C213 0.51675(19) 0.9667(2) 0.37006(11) 0.0607(7) Uani d 1 . .
H H213 0.5088 1.0388 0.3559 0.073 Uiso calc 1 . .
C C214 0.43431(18) 0.9047(2) 0.36835(11) 0.0644(8) Uani d 1 . .
H H214 0.3708 0.9348 0.3529 0.077 Uiso calc 1 . .
C C215 0.44537(15) 0.7987(2) 0.38930(11) 0.0574(6) Uani d 1 . .
H H215 0.3893 0.7575 0.3889 0.069 Uiso calc 1 . .
C C216 0.54004(13) 0.75242(19) 0.41123(9) 0.0430(5) Uani d 1 . .
H H216 0.5470 0.6800 0.4245 0.052 Uiso calc 1 . .
C C221 0.79140(12) 0.78914(12) 0.53606(8) 0.0287(3) Uani d 1 . .
C C222 0.72855(14) 0.83414(13) 0.57257(9) 0.0341(4) Uani d 1 . .
H H222 0.6612 0.8449 0.5500 0.041 Uiso calc 1 . .
C C223 0.76682(17) 0.86292(14) 0.64285(10) 0.0413(4) Uani d 1 . .
H H223 0.7247 0.8928 0.6671 0.050 Uiso calc 1 . .
C C224 0.86659(17) 0.84758(14) 0.67696(9) 0.0412(4) Uani d 1 . .
H H224 0.8918 0.8685 0.7236 0.049 Uiso calc 1 . .
C C225 0.92912(15) 0.80071(14) 0.64131(9) 0.0372(4) Uani d 1 . .
H H225 0.9961 0.7889 0.6644 0.045 Uiso calc 1 . .
C C226 0.89155(13) 0.77142(13) 0.57118(9) 0.0314(3) Uani d 1 . .
H H226 0.9336 0.7398 0.5475 0.038 Uiso calc 1 . .
C C231 0.82451(12) 0.82938(12) 0.40206(8) 0.0255(3) Uani d 1 . .
C C232 0.85997(15) 0.93094(12) 0.42820(9) 0.0338(4) Uani d 1 . .
H H232 0.8507 0.9548 0.4705 0.041 Uiso calc 1 . .
C C233 0.90894(15) 0.99662(13) 0.39167(10) 0.0370(4) Uani d 1 . .
H H233 0.9319 1.0645 0.4093 0.044 Uiso calc 1 . .
C C234 0.92371(14) 0.96111(13) 0.32870(9) 0.0325(3) Uani d 1 . .
H H234 0.9553 1.0058 0.3036 0.039 Uiso calc 1 . .
C C235 0.89148(12) 0.85938(13) 0.30336(8) 0.0289(3) Uani d 1 . .
H H235 0.9027 0.8351 0.2617 0.035 Uiso calc 1 . .
C C236 0.84240(11) 0.79315(12) 0.33991(8) 0.0259(3) Uani d 1 . .
H H236 0.8214 0.7244 0.3229 0.031 Uiso calc 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh 0.0927 3.6045 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
N1 Rh1 P1 93.02(4) y
N1 Rh1 P2 91.25(4) y
C2 Rh1 N1 178.72(7) y
C2 Rh1 P1 86.54(5) y
C2 Rh1 P2 89.37(5) y
P2 Rh1 P1 169.933(14) y
C1 N1 Rh1 173.47(15) y
N1 C1 B1 176.7(2) y
C1 B1 H1A 109.5 ?
C1 B1 H1B 109.5 ?
C1 B1 H1C 109.5 ?
H1A B1 H1B 109.5 ?
H1A B1 H1C 109.5 ?
H1B B1 H1C 109.5 ?
O1 C2 Rh1 179.25(18) y
C111 P1 Rh1 119.15(6) ?
C111 P1 C131 99.4(3) ?
C121 P1 Rh1 106.28(5) ?
C121 P1 C111 106.02(7) ?
C121 P1 C131 102.2(3) ?
C131 P1 Rh1 121.8(2) ?
C141 P1 Rh1 111.3(3) ?
C141 P1 C111 101.3(3) ?
C141 P1 C121 112.9(3) ?
C112 C111 P1 117.54(12) ?
C112 C111 C116 119.43(15) ?
C116 C111 P1 122.84(14) ?
C111 C112 H112 119.8 ?
C111 C112 C113 120.36(17) ?
C113 C112 H112 119.8 ?
C112 C113 H113 120.1 ?
C114 C113 C112 119.82(19) ?
C114 C113 H113 120.1 ?
C113 C114 H114 119.9 ?
C115 C114 C113 120.16(16) ?
C115 C114 H114 119.9 ?
C114 C115 H115 119.8 ?
C114 C115 C116 120.44(18) ?
C116 C115 H115 119.8 ?
C111 C116 C115 119.79(19) ?
C111 C116 H116 120.1 ?
C115 C116 H116 120.1 ?
C122 C121 P1 118.29(12) ?
C126 C121 P1 122.36(12) ?
C126 C121 C122 118.90(15) ?
C121 C122 H122 119.7 ?
C123 C122 C121 120.68(15) ?
C123 C122 H122 119.7 ?
C122 C123 H123 120.0 ?
C122 C123 C124 119.94(16) ?
C124 C123 H123 120.0 ?
C123 C124 H124 120.1 ?
C125 C124 C123 119.87(17) ?
C125 C124 H124 120.1 ?
C124 C125 H125 119.7 ?
C124 C125 C126 120.55(17) ?
C126 C125 H125 119.7 ?
C121 C126 C125 120.07(16) ?
C121 C126 H126 120.0 ?
C125 C126 H126 120.0 ?
C132 C131 P1 115.9(4) ?
C132 C131 C136 122.0(7) ?
C136 C131 P1 121.7(6) ?
C131 C132 H132 120.5 ?
C131 C132 C133 118.9(6) ?
C133 C132 H132 120.5 ?
C132 C133 H133 119.9 ?
C134 C133 C132 120.2(6) ?
C134 C133 H133 119.9 ?
C133 C134 H134 119.9 ?
C133 C134 C135 120.3(5) ?
C135 C134 H134 119.9 ?
C134 C135 H135 119.7 ?
C134 C135 C136 120.5(6) ?
C136 C135 H135 119.7 ?
C131 C136 C135 118.0(7) ?
C131 C136 H136 121.0 ?
C135 C136 H136 121.0 ?
C142 C141 P1 124.1(5) ?
C142 C141 C146 116.6(8) ?
C146 C141 P1 119.0(7) ?
C141 C142 H142 119.0 ?
C141 C142 C143 121.9(5) ?
C143 C142 H142 119.0 ?
C142 C143 H143 120.4 ?
C144 C143 C142 119.1(6) ?
C144 C143 H143 120.4 ?
C143 C144 H144 119.4 ?
C145 C144 C143 121.2(6) ?
C145 C144 H144 119.4 ?
C144 C145 H145 120.3 ?
C144 C145 C146 119.5(5) ?
C146 C145 H145 120.3 ?
C141 C146 H146 119.2 ?
C145 C146 C141 121.6(6) ?
C145 C146 H146 119.2 ?
C211 P2 Rh1 110.76(7) ?
C221 P2 Rh1 116.83(5) ?
C221 P2 C211 104.01(8) ?
C231 P2 Rh1 117.10(5) ?
C231 P2 C211 103.32(7) ?
C231 P2 C221 103.19(7) ?
C212 C211 P2 122.69(15) ?
C212 C211 C216 119.20(17) ?
C216 C211 P2 118.10(14) ?
C211 C212 H212 120.1 ?
C211 C212 C213 119.8(2) ?
C213 C212 H212 120.1 ?
C212 C213 H213 119.8 ?
C214 C213 C212 120.4(2) ?
C214 C213 H213 119.8 ?
C213 C214 H214 119.9 ?
C215 C214 C213 120.18(19) ?
C215 C214 H214 119.9 ?
C214 C215 H215 119.8 ?
C214 C215 C216 120.4(2) ?
C216 C215 H215 119.8 ?
C211 C216 C215 120.1(2) ?
C211 C216 H216 120.0 ?
C215 C216 H216 120.0 ?
C222 C221 P2 122.41(13) ?
C226 C221 P2 118.35(12) ?
C226 C221 C222 119.24(16) ?
C221 C222 H222 120.1 ?
C223 C222 C221 119.85(18) ?
C223 C222 H222 120.1 ?
C222 C223 H223 119.6 ?
C224 C223 C222 120.71(16) ?
C224 C223 H223 119.6 ?
C223 C224 H224 120.1 ?
C223 C224 C225 119.73(17) ?
C225 C224 H224 120.1 ?
C224 C225 H225 120.0 ?
C224 C225 C226 119.99(18) ?
C226 C225 H225 120.0 ?
C221 C226 H226 119.8 ?
C225 C226 C221 120.47(16) ?
C225 C226 H226 119.8 ?
C232 C231 P2 120.82(11) ?
C232 C231 C236 119.01(14) ?
C236 C231 P2 119.95(12) ?
C231 C232 H232 119.7 ?
C233 C232 C231 120.53(15) ?
C233 C232 H232 119.7 ?
C232 C233 H233 120.0 ?
C232 C233 C234 119.98(16) ?
C234 C233 H233 120.0 ?
C233 C234 H234 120.0 ?
C235 C234 C233 119.96(15) ?
C235 C234 H234 120.0 ?
C234 C235 H235 119.9 ?
C234 C235 C236 120.23(14) ?
C236 C235 H235 119.9 ?
C231 C236 H236 119.9 ?
C235 C236 C231 120.22(14) ?
C235 C236 H236 119.9 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
Rh1 N1 2.0389(14) y
Rh1 C2 1.8305(18) y
Rh1 P1 2.3257(4) y
Rh1 P2 2.3253(4) y
N1 C1 1.140(2) y
C1 B1 1.584(3) y
B1 H1A 0.9600 ?
B1 H1B 0.9600 ?
B1 H1C 0.9600 ?
C2 O1 1.143(2) y
P1 C111 1.8216(15) ?
P1 C121 1.8197(16) ?
P1 C131 1.929(8) ?
P1 C141 1.732(10) ?
C111 C112 1.391(3) ?
C111 C116 1.392(2) ?
C112 H112 0.9300 ?
C112 C113 1.391(2) ?
C113 H113 0.9300 ?
C113 C114 1.384(3) ?
C114 H114 0.9300 ?
C114 C115 1.377(3) ?
C115 H115 0.9300 ?
C115 C116 1.393(2) ?
C116 H116 0.9300 ?
C121 C122 1.401(2) ?
C121 C126 1.389(2) ?
C122 H122 0.9300 ?
C122 C123 1.382(2) ?
C123 H123 0.9300 ?
C123 C124 1.384(3) ?
C124 H124 0.9300 ?
C124 C125 1.382(3) ?
C125 H125 0.9300 ?
C125 C126 1.389(3) ?
C126 H126 0.9300 ?
C131 C132 1.370(14) ?
C131 C136 1.371(7) ?
C132 H132 0.9300 ?
C132 C133 1.387(11) ?
C133 H133 0.9300 ?
C133 C134 1.361(9) ?
C134 H134 0.9300 ?
C134 C135 1.375(9) ?
C135 H135 0.9300 ?
C135 C136 1.392(8) ?
C136 H136 0.9300 ?
C141 C142 1.385(14) ?
C141 C146 1.414(7) ?
C142 H142 0.9300 ?
C142 C143 1.410(11) ?
C143 H143 0.9300 ?
C143 C144 1.373(7) ?
C144 H144 0.9300 ?
C144 C145 1.367(8) ?
C145 H145 0.9300 ?
C145 C146 1.398(8) ?
C146 H146 0.9300 ?
P2 C211 1.8296(16) ?
P2 C221 1.8268(17) ?
P2 C231 1.8207(15) ?
C211 C212 1.390(3) ?
C211 C216 1.391(3) ?
C212 H212 0.9300 ?
C212 C213 1.396(3) ?
C213 H213 0.9300 ?
C213 C214 1.373(4) ?
C214 H214 0.9300 ?
C214 C215 1.369(4) ?
C215 H215 0.9300 ?
C215 C216 1.392(3) ?
C216 H216 0.9300 ?
C221 C222 1.395(2) ?
C221 C226 1.394(2) ?
C222 H222 0.9300 ?
C222 C223 1.392(3) ?
C223 H223 0.9300 ?
C223 C224 1.380(3) ?
C224 H224 0.9300 ?
C224 C225 1.389(3) ?
C225 H225 0.9300 ?
C225 C226 1.390(2) ?
C226 H226 0.9300 ?
C231 C232 1.394(2) ?
C231 C236 1.395(2) ?
C232 H232 0.9300 ?
C232 C233 1.385(2) ?
C233 H233 0.9300 ?
C233 C234 1.389(2) ?
C234 H234 0.9300 ?
C234 C235 1.381(2) ?
C235 H235 0.9300 ?
C235 C236 1.390(2) ?
C236 H236 0.9300 ?
