#------------------------------------------------------------------------------
#$Date: 2019-12-26 20:53:35 +0200 (Thu, 26 Dec 2019) $
#$Revision: 246089 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/18/2021885.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2021885
loop_
_publ_author_name
'Sabalisck, N. P.'
'Guzmán-Afonso, C.'
'González-Silgo, C.'
'Torres, M. E.'
'Pasán, J.'
'del-Castillo, J.'
'Ramos-Hernández, D.'
'Hernández-Suárez, A.'
'Mestres, L.'
_publ_section_title
;
 Structures and thermal stability of the α-LiNH4SO4 polytypes doped with
 Er3+ and Yb3+ 
;
_journal_issue                   1
_journal_name_full
'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials'
_journal_page_first              122
_journal_paper_doi               10.1107/S2052520616019028
_journal_volume                  73
_journal_year                    2017
_chemical_formula_moiety         'O4 S Yb0.013, 0.961(H4 N), Li'
_chemical_formula_sum            'H3.843 Li N0.961 O4 S Yb0.013'
_chemical_formula_weight         122.51
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   notdet
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 90.20(10)
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   10.177(15)
_cell_length_b                   5.106(4)
_cell_length_c                   34.234(16)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      19
_cell_measurement_theta_min      9
_cell_volume                     1779(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  'ENRAF-Nonius CAD4'
_diffrn_measurement_method       ω/2Θ-scan
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0683
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       0
_diffrn_reflns_limit_l_min       -48
_diffrn_reflns_number            9573
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.961
_diffrn_reflns_theta_min         2.001
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.889
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.831
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1000.0
_exptl_crystal_size_max          0.17
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.09
_refine_diff_density_max         1.887
_refine_diff_density_min         -1.037
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.197
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     256
_refine_ls_number_reflns         5071
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.197
_refine_ls_R_factor_all          0.1029
_refine_ls_R_factor_gt           0.0603
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0263P)²+6.4506P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1333
_refine_ls_wR_factor_ref         0.1632
_reflns_number_gt                3231
_reflns_number_total             5071
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            yb5013sup1.cif
_cod_data_source_block           alpha2_LAS
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2021885
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
S S1 0.64805(7) 0.73307(14) 0.20089(2) 0.00608(14) Uani d 1
O O11 0.6399(4) 0.4374(5) 0.20610(11) 0.0406(9) Uani d 1
O O12 0.7859(3) 0.8058(10) 0.20413(11) 0.0521(12) Uani d 1
O O13 0.5709(3) 0.8568(6) 0.23235(9) 0.0274(7) Uani d 1
O O14 0.5950(4) 0.7924(10) 0.16305(10) 0.0566(13) Uani d 1
S S2 0.89820(8) 0.28368(18) 0.04920(3) 0.01657(19) Uani d 1
O O21 0.8934(3) 0.5828(6) 0.04414(10) 0.0324(8) Uani d 1
O O22 1.0370(3) 0.2110(6) 0.04620(9) 0.0298(7) Uani d 1
O O23 0.8456(3) 0.2180(7) 0.08669(9) 0.0368(8) Uani d 1
O O24 0.8213(3) 0.1630(6) 0.01798(9) 0.0280(7) Uani d 1
S S3 0.39959(8) 0.21622(18) 0.04902(3) 0.01718(19) Uani d 1
O O31 0.5355(3) 0.2891(6) 0.04630(10) 0.0304(7) Uani d 1
O O32 0.3211(3) 0.3371(6) 0.01735(9) 0.0273(7) Uani d 1
O O33 0.3916(3) -0.0811(6) 0.04468(10) 0.0330(8) Uani d 1
O O34 0.3434(3) 0.2813(7) 0.08748(9) 0.0324(7) Uani d 1
S S4 0.14878(11) 0.8032(3) 0.20093(4) 0.0364(3) Uani d 1
O O41 0.1414(3) 1.1054(7) 0.20461(9) 0.0314(7) Uani d 1
O O42 0.2864(2) 0.7278(5) 0.20357(8) 0.0211(5) Uani d 1
O O43 0.0927(3) 0.7312(6) 0.16299(9) 0.0272(6) Uani d 1
O O44 0.0714(3) 0.6850(7) 0.23248(9) 0.0292(7) Uani d 1
N N1 0.4006(3) 0.2369(6) 0.16624(10) 0.0417(11) Uani d 0.907(4)
N N2 0.6508(3) 0.7697(7) 0.08377(10) 0.0364(13) Uani d 0.959(4)
N N3 0.1517(3) 0.7309(7) 0.08326(11) 0.0331(14) Uani d 0.978(4)
N N4 0.9005(4) 0.2744(9) 0.16666(12) 0.0381(10) Uani d 1
Yb Yb1 0.4006(3) 0.2369(6) 0.16624(10) 0.0417(11) Uani d 0.0311(15)
Yb Yb2 0.6508(3) 0.7697(7) 0.08377(10) 0.0364(13) Uani d 0.0137(15)
Yb Yb3 0.1517(3) 0.7309(7) 0.08326(11) 0.0331(14) Uani d 0.0074(14)
Li Li1 0.3992(7) 0.7198(14) 0.2497(2) 0.0237(14) Uani d 1
Li Li2 0.1017(7) 0.3041(15) 0.2508(2) 0.0278(16) Uani d 1
Li Li3 0.1488(7) 0.2123(13) 0.0001(2) 0.0218(14) Uani d 1
Li Li4 0.6491(6) 0.2976(12) 0.0013(2) 0.0190(13) Uani d 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
O14 S1 O12 . . 112.0(2)
O14 S1 O13 . . 111.7(2)
O12 S1 O13 . . 110.5(2)
O14 S1 O11 . . 107.2(3)
O12 S1 O11 . . 107.3(3)
O13 S1 O11 . . 108.0(2)
O14 S1 Li1 . . 101.0(2)
O12 S1 Li1 . . 140.2(2)
O13 S1 Li1 . . 33.14(19)
O11 S1 Li1 . . 82.4(2)
O14 S1 Li1 . 2_655 105.6(2)
O12 S1 Li1 . 2_655 84.5(2)
O13 S1 Li1 . 2_655 32.91(18)
O11 S1 Li1 . 2_655 137.4(2)
Li1 S1 Li1 . 2_655 65.12(16)
S1 O11 Li1 . 2_645 132.7(3)
S1 O12 Li2 . 2_655 129.2(3)
S1 O13 Li1 . 2_655 123.1(3)
S1 O13 Li1 . . 122.7(3)
Li1 O13 Li1 2_655 . 112.0(3)
S1 O14 Yb1 . 1_565 111.8(2)
O23 S2 O24 . . 110.9(2)
O23 S2 O22 . . 111.5(2)
O24 S2 O22 . . 110.9(2)
O23 S2 O21 . . 108.8(2)
O24 S2 O21 . . 108.67(18)
O22 S2 O21 . . 105.90(19)
O23 S2 Li4 . . 100.2(2)
O24 S2 Li4 . . 33.25(17)
O22 S2 Li4 . . 140.99(19)
O21 S2 Li4 . . 83.62(17)
S2 O21 Li3 . 3_665 130.3(3)
S2 O21 Yb3 . 1_655 99.80(16)
Li3 O21 Yb3 3_665 1_655 114.2(3)
S2 O22 Li3 . 1_655 128.5(3)
S2 O22 Yb3 . 1_645 123.5(2)
Li3 O22 Yb3 1_655 1_645 96.8(2)
S2 O23 Yb2 . 1_545 113.19(18)
S2 O24 Li4 . . 122.7(3)
S2 O24 Li3 . 3_655 122.7(3)
Li4 O24 Li3 . 3_655 112.0(3)
O31 S3 O34 . . 112.1(2)
O31 S3 O32 . . 111.2(2)
O34 S3 O32 . . 110.49(19)
O31 S3 O33 . . 107.58(19)
O34 S3 O33 . . 106.9(2)
O32 S3 O33 . . 108.37(18)
O31 S3 Li3 . . 140.5(2)
O34 S3 Li3 . . 99.5(2)
O32 S3 Li3 . . 31.90(19)
O33 S3 Li3 . . 84.04(17)
S3 O31 Li4 . . 129.6(3)
S3 O32 Li3 . . 124.5(3)
S3 O32 Li4 . 3_665 122.8(3)
Li3 O32 Li4 . 3_665 110.2(3)
S3 O33 Li4 . 3_655 130.4(3)
S3 O33 Yb3 . 1_545 108.95(19)
Li4 O33 Yb3 3_655 1_545 90.2(2)
S3 O33 Yb2 . 1_545 99.22(15)
Li4 O33 Yb2 3_655 1_545 113.0(2)
Yb3 O33 Yb2 1_545 1_545 116.06(16)
O42 S4 O43 . . 111.2(2)
O42 S4 O44 . . 111.4(2)
O43 S4 O44 . . 109.9(2)
O42 S4 O41 . . 107.78(18)
O43 S4 O41 . . 107.7(2)
O44 S4 O41 . . 108.9(2)
O42 S4 Li2 . 2 140.8(2)
O43 S4 Li2 . 2 99.1(2)
O44 S4 Li2 . 2 31.65(19)
O41 S4 Li2 . 2 85.04(19)
S4 O41 Li2 . 1_565 127.1(3)
S4 O41 Yb1 . 1_565 98.23(15)
Li2 O41 Yb1 1_565 1_565 115.2(3)
S4 O42 Li1 . . 128.3(3)
S4 O44 Li2 . 2 125.1(3)
S4 O44 Li2 . . 122.0(3)
Li2 O44 Li2 2 . 109.8(3)
O11 Li1 O42 2_655 . 120.2(4)
O11 Li1 O13 2_655 2_645 109.3(4)
O42 Li1 O13 . 2_645 111.2(4)
O11 Li1 O13 2_655 . 102.6(4)
O42 Li1 O13 . . 105.5(4)
O13 Li1 O13 2_645 . 106.9(3)
O11 Li1 S1 2_655 . 126.6(3)
O42 Li1 S1 . . 92.5(3)
O13 Li1 S1 2_645 . 93.7(3)
O13 Li1 S1 . . 24.12(14)
O11 Li1 S1 2_655 2_645 90.1(3)
O42 Li1 S1 . 2_645 111.9(3)
O13 Li1 S1 2_645 2_645 23.96(13)
O13 Li1 S1 . 2_645 126.7(3)
S1 Li1 S1 . 2_645 117.2(2)
O11 Li1 Li1 2_655 2_645 125.3(4)
O42 Li1 Li1 . 2_645 112.8(4)
O13 Li1 Li1 2_645 2_645 34.03(11)
O13 Li1 Li1 . 2_645 73.9(3)
S1 Li1 Li1 . 2_645 59.8(2)
S1 Li1 Li1 2_645 2_645 57.36(15)
O11 Li1 Li1 2_655 2_655 71.1(2)
O42 Li1 Li1 . 2_655 110.8(3)
O13 Li1 Li1 2_645 2_655 129.3(4)
O13 Li1 Li1 . 2_655 34.0(2)
S1 Li1 Li1 . 2_655 57.5(2)
S1 Li1 Li1 2_645 2_655 137.1(4)
Li1 Li1 Li1 2_645 2_655 102.4(4)
O11 Li1 Yb1 2_655 2_655 57.5(2)
O42 Li1 Yb1 . 2_655 177.3(3)
O13 Li1 Yb1 2_645 2_655 71.4(2)
O13 Li1 Yb1 . 2_655 74.2(2)
S1 Li1 Yb1 . 2_655 88.2(2)
S1 Li1 Yb1 2_645 2_655 70.03(16)
Li1 Li1 Yb1 2_645 2_655 69.8(3)
Li1 Li1 Yb1 2_655 2_655 67.4(3)
O11 Li1 Yb1 2_655 1_565 100.8(3)
O42 Li1 Yb1 . 1_565 52.7(2)
O13 Li1 Yb1 2_645 1_565 149.8(3)
O13 Li1 Yb1 . 1_565 62.2(2)
S1 Li1 Yb1 . 1_565 64.90(15)
S1 Li1 Yb1 2_645 1_565 164.3(2)
Li1 Li1 Yb1 2_645 1_565 122.0(3)
Li1 Li1 Yb1 2_655 1_565 58.09(19)
Yb1 Li1 Yb1 2_655 1_565 125.4(2)
O12 Li2 O41 2_645 1_545 122.5(4)
O12 Li2 O44 2_645 2_545 107.6(4)
O41 Li2 O44 1_545 2_545 105.6(4)
O12 Li2 O44 2_645 . 109.1(4)
O41 Li2 O44 1_545 . 106.2(4)
O44 Li2 O44 2_545 . 104.4(3)
O12 Li2 S4 2_645 2_545 93.5(3)
O41 Li2 S4 1_545 2_545 128.7(3)
O44 Li2 S4 2_545 2_545 23.27(15)
O44 Li2 S4 . 2_545 92.4(3)
O12 Li2 Li2 2_645 2 112.5(4)
O41 Li2 Li2 1_545 2 122.1(4)
O44 Li2 Li2 2_545 2 71.2(4)
O44 Li2 Li2 . 2 33.96(10)
S4 Li2 Li2 2_545 2 58.8(3)
O12 Li2 Li2 2_645 2_545 113.0(4)
O41 Li2 Li2 1_545 2_545 73.2(3)
O44 Li2 Li2 2_545 2_545 36.3(3)
O44 Li2 Li2 . 2_545 129.3(4)
S4 Li2 Li2 2_545 2_545 58.6(3)
Li2 Li2 Li2 2 2_545 101.9(4)
O21 Li3 O22 3_665 1_455 121.3(4)
O21 Li3 O32 3_665 . 105.2(4)
O22 Li3 O32 1_455 . 106.4(4)
O21 Li3 O24 3_665 3_655 108.1(3)
O22 Li3 O24 1_455 3_655 109.4(4)
O32 Li3 O24 . 3_655 105.3(3)
O21 Li3 S3 3_665 . 128.6(3)
O22 Li3 S3 1_455 . 92.6(3)
O32 Li3 S3 . . 23.58(14)
O24 Li3 S3 3_655 . 92.7(2)
O21 Li3 Li4 3_665 3_665 72.7(3)
O22 Li3 Li4 1_455 3_665 112.8(3)
O32 Li3 Li4 . 3_665 35.30(19)
O24 Li3 Li4 3_655 3_665 128.8(3)
S3 Li3 Li4 . 3_665 58.17(16)
O21 Li3 Li4 3_665 3_655 124.2(3)
O22 Li3 Li4 1_455 3_655 111.9(3)
O32 Li3 Li4 . 3_655 72.8(2)
O24 Li3 Li4 3_655 3_655 33.33(19)
S3 Li3 Li4 . 3_655 59.68(16)
Li4 Li3 Li4 3_665 3_655 102.3(2)
O21 Li3 Yb2 3_665 3_665 57.5(2)
O22 Li3 Yb2 1_455 3_665 178.6(3)
O32 Li3 Yb2 . 3_665 73.5(3)
O24 Li3 Yb2 3_655 3_665 71.9(2)
S3 Li3 Yb2 . 3_665 87.8(2)
Li4 Li3 Yb2 3_665 3_665 66.37(18)
Li4 Li3 Yb2 3_655 3_665 69.43(18)
O21 Li3 Yb3 3_665 1_545 165.9(3)
O22 Li3 Yb3 1_455 1_545 52.3(2)
O32 Li3 Yb3 . 1_545 88.9(3)
O24 Li3 Yb3 3_655 1_545 67.3(2)
S3 Li3 Yb3 . 1_545 65.44(15)
Li4 Li3 Yb3 3_665 1_545 120.9(2)
Li4 Li3 Yb3 3_655 1_545 59.66(18)
Yb2 Li3 Yb3 3_665 1_545 129.0(2)
O31 Li4 O33 . 3_655 120.1(3)
O31 Li4 O24 . . 107.2(4)
O33 Li4 O24 3_655 . 102.8(3)
O31 Li4 O32 . 3_665 111.6(3)
O33 Li4 O32 3_655 3_665 107.6(4)
O24 Li4 O32 . 3_665 106.5(3)
O31 Li4 S2 . . 94.0(3)
O33 Li4 S2 3_655 . 126.6(3)
O24 Li4 S2 . . 24.01(13)
O32 Li4 S2 3_665 . 93.9(2)
O31 Li4 Li3 . 3_665 114.3(3)
O33 Li4 Li3 3_655 3_665 123.7(3)
O24 Li4 Li3 . 3_665 73.1(2)
O32 Li4 Li3 3_665 3_665 34.47(19)
S2 Li4 Li3 . 3_665 59.59(16)
O31 Li4 Li3 . 3_655 111.5(3)
O33 Li4 Li3 3_655 3_655 71.1(2)
O24 Li4 Li3 . 3_655 34.71(18)
O32 Li4 Li3 3_665 3_655 129.3(3)
S2 Li4 Li3 . 3_655 57.96(15)
Li3 Li4 Li3 3_665 3_655 102.3(2)
O31 Li4 Yb3 . 3_665 175.9(3)
O33 Li4 Yb3 3_655 3_665 56.1(2)
O24 Li4 Yb3 . 3_665 73.2(2)
O32 Li4 Yb3 3_665 3_665 71.9(2)
S2 Li4 Yb3 . 3_665 87.77(18)
Li3 Li4 Yb3 3_665 3_665 69.78(18)
Li3 Li4 Yb3 3_655 3_665 66.38(18)
O31 Li4 Yb2 . 1_545 53.7(2)
O33 Li4 Yb2 3_655 1_545 101.0(3)
O24 Li4 Yb2 . 1_545 63.0(2)
O32 Li4 Yb2 3_665 1_545 151.2(3)
S2 Li4 Yb2 . 1_545 65.70(15)
Li3 Li4 Yb2 3_665 1_545 122.9(2)
Li3 Li4 Yb2 3_655 1_545 57.83(17)
Yb3 Li4 Yb2 3_665 1_545 124.17(19)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
S1 O14 . 1.434(3)
S1 O12 . 1.455(4)
S1 O13 . 1.477(3)
S1 O11 . 1.522(3)
S1 Li1 . 3.040(8)
S1 Li1 2_655 3.045(7)
O11 Li1 2_645 1.920(8)
O12 Li2 2_655 1.918(8)
O13 Li1 2_655 1.976(8)
O13 Li1 . 1.976(8)
O14 Yb1 1_565 3.013(6)
S2 O23 . 1.432(3)
S2 O24 . 1.459(3)
S2 O22 . 1.464(3)
S2 O21 . 1.538(3)
S2 Li4 . 3.016(7)
O21 Li3 3_665 1.890(8)
O21 Yb3 1_655 3.042(6)
O22 Li3 1_655 1.948(8)
O22 Yb3 1_645 2.996(5)
O23 Yb2 1_545 3.030(5)
O24 Li4 . 1.966(7)
O24 Li3 3_655 2.037(7)
S3 O31 . 1.436(3)
S3 O34 . 1.475(3)
S3 O32 . 1.479(3)
S3 O33 . 1.527(3)
S3 Li3 . 3.047(8)
O31 Li4 . 1.930(8)
O32 Li3 . 1.954(8)
O32 Li4 3_665 1.995(7)
O33 Li4 3_655 1.966(7)
O33 Yb3 1_545 2.941(6)
O33 Yb2 1_545 3.050(6)
S4 O42 . 1.455(3)
S4 O43 . 1.464(3)
S4 O44 . 1.469(3)
S4 O41 . 1.550(4)
S4 Li2 2 3.043(9)
O41 Li2 1_565 1.922(9)
O41 Yb1 1_565 3.027(6)
O42 Li1 . 1.950(8)
O44 Li2 2 1.951(8)
O44 Li2 . 2.066(8)
Li1 O11 2_655 1.920(8)
Li1 O13 2_645 1.976(8)
Li1 S1 2_645 3.045(7)
Li1 Li1 2_645 3.275(9)
Li1 Li1 2_655 3.275(9)
Li1 Yb1 2_655 3.520(8)
Li1 Yb1 1_565 3.891(8)
Li2 O12 2_645 1.918(8)
Li2 O41 1_545 1.922(9)
Li2 O44 2_545 1.951(8)
Li2 S4 2_545 3.043(9)
Li2 Li2 2 3.287(9)
Li2 Li2 2_545 3.287(9)
Li3 O21 3_665 1.890(8)
Li3 O22 1_455 1.948(8)
Li3 O24 3_655 2.037(7)
Li3 Li4 3_665 3.239(9)
Li3 Li4 3_655 3.319(9)
Li3 Yb2 3_665 3.530(9)
Li3 Yb3 1_545 3.760(8)
Li4 O33 3_655 1.966(7)
Li4 O32 3_665 1.995(7)
Li4 Li3 3_665 3.239(9)
Li4 Li3 3_655 3.319(9)
Li4 Yb3 3_665 3.542(9)
Li4 Yb2 1_545 3.904(8)
