#------------------------------------------------------------------------------
#$Date: 2022-09-28 18:08:17 +0300 (Wed, 28 Sep 2022) $
#$Revision: 278247 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/10/15/2101552.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2101552
loop_
_publ_author_name
'Wang, Z.'
'Willett, R. D.'
'Elias, A. J.'
'Kirchmeier, R. L.'
'Shreeve, J. M.'
_publ_section_title
;
 Structure of the polytypic β-form of
 P₃N₃(OCH₂CF₂CF₂CH₂O)F₄
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              643
_journal_page_last               650
_journal_paper_doi               10.1107/S0108768195016089
_journal_volume                  52
_journal_year                    1996
_chemical_formula_sum            'C4 H4 F8 N3 O2 P3'
_chemical_formula_weight         371.0
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                110.22(3)
_cell_angle_beta                 90.02(3)
_cell_angle_gamma                97.10(3)
_cell_formula_units_Z            12
_cell_length_a                   12.392(2)
_cell_length_b                   16.569(3)
_cell_length_c                   19.257(4)
_cell_volume                     3677.8(14)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.54184
_exptl_absorpt_coefficient_mu    5.584
_exptl_crystal_density_diffrn    2.010
_exptl_crystal_F_000             2184
_cod_data_source_file            cr0501.cif
_cod_data_source_block           cr0501a
_cod_original_cell_volume        3677.9(12)
_cod_database_code               2101552
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,-z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
P(1) .3483(2) .18020(10) .32440(10) .0430(10)
P(2) .5636(2) .1813(2) .35440(10) .0490(10)
P(3) .4224(2) .20580(10) .46500(10) .0420(10)
N(1) .3298(5) .2002(4) .4091(3) .046(3)
N(2) .4697(5) .1767(4) .3000(3) .051(3)
N(3) .5406(5) .1966(4) .4375(3) .048(3)
O(1) .2938(4) .2515(3) .3052(2) .049(2)
O(2) .2825(4) .0918(3) .2735(3) .049(2)
F(1) .6556(3) .2488(3) .3513(2) .070(2)
F(2) .6233(4) .1018(3) .3237(3) .079(2)
F(3) .3916(3) .1409(3) .5039(2) .063(2)
F(4) .4264(3) .2877(3) .5312(2) .059(2)
F(5) .0232(4) .0755(3) .1885(3) .089(3)
F(6) .1821(4) .0582(3) .1417(3) .088(3)
F(7) .1199(4) .2055(4) .1455(3) .093(3)
F(8) .0833(4) .2399(3) .2624(3) .070(2)
C(1) .1673(6) .0805(5) .2678(4) .052(4)
C(2) .1312(7) .1023(6) .2033(5) .054(4)
C(3) .1504(7) .1982(6) .2116(5) .054(4)
C(4) .2649(6) .2432(6) .2300(4) .057(4)
P(4) .3952(2) .50720(10) .85830(10) .0430(10)
P(5) .6036(2) .4880(2) .81710(10) .0480(10)
P(6) .4637(2) .5255(2) .72900(10) .0590(10)
N(4) .5782(5) .5062(5) .7443(3) .062(4)
N(5) .5150(5) .4946(4) .8751(3) .047(3)
N(6) .3731(5) .5255(5) .7848(3) .056(3)
O(3) .3108(4) .4274(3) .8551(3) .051(2)
O(4) .3652(4) .5835(3) .9293(3) .042(2)
F(10) .6461(4) .4008(3) .7957(3) .076(2)
F(11) .7074(3) .5444(3) .8545(3) .077(3)
F(12) .4249(4) .4673(5) .6529(3) .113(4)
F(13) .1525(4) .4180(3) 1.0064(3) .066(2)
F(14) .4745(5) .6121(4) .7157(3) .109(4)
F(15) .1064(3) .4293(3) .9021(2) .059(2)
F(16) .2692(4) .5707(3) 1.0514(2) .060(2)
F(17) .1088(4) .5770(3) 1.0101(3) .068(2)
C(5) .2864(6) .4087(5) .9217(4) .051(4)
C(6) .1871(6) .4515(5) .9542(4) .041(4)
C(7) .2046(6) .5504(5) .9888(4) .040(4)
C(8) .2534(6) .5979(5) .9417(4) .044(4)
P(7) .1075(2) .51040(10) .35870(10) .0440(10)
P(8) -.1072(2) .4953(2) .31840(10) .0530(10)
P(9) .0459(2) .5251(2) .22790(10) .0670(10)
N(7) -.0752(5) .5107(5) .2446(4) .065(4)
N(8) -.0164(5) .5001(4) .3756(3) .049(3)
N(9) .1346(5) .5254(5) .2851(3) .059(3)
O(5) .1634(4) .4294(3) .3570(3) .054(2)
O(6) .1635(4) .5870(3) .4283(3) .043(2)
F(20) -.1878(4) .5571(4) .3561(3) .090(3)
F(21) -.1838(4) .4111(3) .3000(3) .084(3)
F(22) .0672(4) .6094(5) .2114(3) .122(4)
F(23) .0623(4) .4637(5) .1529(3) .126(4)
F(24) .2514(4) .5759(3) .5515(2) .063(2)
F(25) .4148(3) .5807(3) .5130(3) .069(2)
F(26) .3174(4) .4239(3) .5103(3) .068(2)
F(27) .3682(3) .4320(3) .4051(3) .063(2)
C(9) .1827(6) .4131(5) .4247(4) .046(4)
C(10) .2786(6) .6008(5) .4416(4) .043(4)
C(11) .3102(6) .5545(5) .4899(4) .040(4)
C(12) .2936(7) .4550(5) .4561(4) .043(4)
P(10) -.0420(2) .82880(10) .17840(10) .0470(10)
P(11) .1707(2) .81990(10) .14320(10) .0480(10)
P(12) .0195(2) .8088(2) .03770(10) .0540(10)
N(10) .0805(5) .8316(4) .2012(3) .051(3)
N(11) -.0697(5) .8141(4) .0954(3) .057(3)
N(12) .1399(5) .8104(4) .0615(3) .053(3)
O(7) -.1196(4) .7565(3) .1958(3) .052(2)
O(8) -.0763(4) .9165(3) .2329(3) .059(3)
F(30) .2322(4) .7457(3) .1431(3) .071(2)
F(31) .2640(3) .8939(3) .1735(3) .067(2)
F(32) .0155(4) .8797(3) .0054(3) .084(3)
F(33) -.0121(4) .7306(3) -.0317(2) .079(2)
F(34) -.2824(5) .7948(4) .3522(3) .111(4)
F(35) -.3267(4) .7677(3) .2361(3) .075(3)
F(36) -.3329(5) .9297(4) .3159(3) .101(3)
F(37) -.1695(5) .9431(4) .3635(3) .106(3)
C(13) -.2480(8) .8063(7) .2888(5) .067(5)
C(14) -.2342(8) .9025(7) .3022(5) .062(5)
C(15) -.1885(7) .9281(5) .2386(5) .064(4)
C(16) -.1469(7) .7613(6) .2690(4) .058(4)
P(13) .4579(2) .81760(10) .96370(10) .0460(10)
P(14) .6668(2) .7966(2) .99130(10) .0500(10)
P(15) .5135(2) .7886(2) 1.08940(10) .0550(10)
N(13) .4254(5) .7990(4) 1.0358(3) .045(3)
N(14) .6336(5) .7869(4) 1.0666(3) .058(3)
N(15) .5797(5) .8106(4) .9400(3) .054(3)
O(9) .3747(4) .7544(3) .9010(3) .056(3)
O(10) .4359(4) .9112(3) .9677(3) .051(2)
F(40) .7635(3) .8668(3) 1.0041(3) .072(2)
F(41) .7229(4) .7200(3) .9474(3) .088(3)
F(42) .4777(4) .7092(3) 1.1103(3) .089(3)
F(43) .5122(4) .8579(4) 1.1653(2) .085(3)
F(44) .1737(4) .7842(3) .8777(3) .079(3)
F(45) .2169(4) .8220(4) .7831(3) .099(3)
F(46) .1804(4) .9508(4) .9114(3) .098(3)
F(47) .3408(5) .9614(4) .8662(3) .096(3)
C(17) .3492(7) .7721(6) .8366(4) .059(4)
C(18) .2549(8) .8235(7) .8499(5) .064(5)
C(19) .2765(7) .9169(6) .9017(6) .064(5)
C(20) .3271(7) .9335(5) .9756(5) .062(4)
P(16) .1437(2) .82230(10) .46380(10) .0440(10)
P(17) -.0704(2) .8110(2) .49640(10) .0540(10)
P(18) .0799(2) .78830(10) .58740(10) .0460(10)
N(16) -.0399(5) .7936(4) .5680(3) .054(3)
N(17) .1706(5) .8006(4) .5347(3) .041(3)
N(18) .0213(5) .8192(4) .4421(3) .053(3)
O(11) .2001(4) .9145(3) .4691(3) .052(2)
O(12) .2031(4) .7575(3) .3988(3) .050(2)
F(50) .0841(4) .7049(3) .6028(3) .077(3)
F(51) .1095(4) .8506(3) .6656(2) .075(2)
F(52) -.1621(4) .7422(4) .4543(3) .088(3)
F(53) -.1315(4) .8895(3) .5167(3) .088(3)
F(54) .4155(4) .7844(3) .3768(3) .077(3)
F(55) .3865(4) .8252(3) .2832(3) .085(3)
F(56) .4683(4) .9518(4) .4109(3) .092(3)
F(57) .3101(4) .9646(3) .3676(3) .085(3)
C(21) .2372(6) .7776(5) .3353(4) .049(4)
C(22) .3495(7) .8260(6) .3500(4) .052(4)
C(23) .3618(7) .9199(6) .4019(5) .058(5)
C(24) .3170(7) .9344(5) .4774(4) .054(4)
H(1A) .1400 .0213 .2608 .080
H(1B) .1400 .1181 .3123 .080
H(4A) .2695 .2997 .2260 .080
H(4B) .3134 .2096 .1965 .080
H(5A) .2710 .3471 .9099 .080
H(5B) .3473 .4313 .9567 .080
H(8A) .2505 .6588 .9658 .080
H(8B) .2131 .5778 .8950 .080
H(9A) .1296 .4368 .4597 .080
H(9B) .1774 .3517 .4143 .080
H(10A) .3129 .5797 .3952 .080
H(10B) .3022 .6618 .4651 .080
H(15A) -.1958 .9878 .2476 .080
H(15B) -.2278 .8922 .1933 .080
H(16A) -.1612 .7038 .2708 .080
H(16B) -.0877 .7936 .3034 .080
H(17A) .4113 .8048 .8247 .080
H(17B) .3302 .7185 .7962 .080
H(20A) .2851 .8989 .9995 .080
H(20B) .3293 .9938 1.0049 .080
H(21A) .2369 .7248 .2937 .080
H(21B) .1881 .8127 .3246 .080
H(24A) .3367 .9939 .5085 .080
H(24B) .3460 .8973 .4994 .080
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N(1) P(1) O(1) 104.4(3)
N(1) P(1) O(2) 113.0(3)
O(1) P(1) O(2) 104.2(3)
N(2) P(2) F(1) 109.4(4)
N(2) P(2) F(2) 110.3(3)
F(1) P(2) F(2) 97.7(3)
N(1) P(3) F(3) 109.9(3)
N(1) P(3) F(4) 110.6(3)
F(3) P(3) F(4) 98.2(3)
P(1) N(2) P(2) 121.8(4)
P(1) O(1) C(4) 122.6(5)
O(2) C(1) C(2) 109.2(7)
F(5) C(2) C(1) 109.5(8)
F(5) C(2) C(3) 107.2(8)
C(1) C(2) C(3) 116.3(6)
F(7) C(3) C(2) 108.3(6)
F(7) C(3) C(4) 106.0(8)
C(2) C(3) C(4) 117.1(8)
N(5) P(4) O(3) 112.3(4)
N(5) P(4) O(4) 105.2(3)
O(3) P(4) O(4) 104.2(3)
N(4) P(5) F(10) 108.5(3)
N(4) P(5) F(11) 108.8(4)
F(10) P(5) F(11) 97.7(3)
N(4) P(6) F(12) 108.2(3)
N(4) P(6) F(14) 108.9(4)
F(12) P(6) F(14) 98.4(4)
P(4) N(5) P(5) 121.3(4)
P(4) O(3) C(5) 120.3(4)
O(3) C(5) C(6) 108.3(7)
F(13) C(6) C(5) 106.7(7)
F(13) C(6) C(7) 109.0(6)
C(5) C(6) C(7) 116.2(6)
F(16) C(7) C(6) 106.6(7)
N(1) P(1) N(2) 116.5(3)
N(2) P(1) O(1) 112.5(4)
N(2) P(1) O(2) 105.7(3)
N(2) P(2) N(3) 119.7(3)
N(3) P(2) F(1) 108.4(3)
N(3) P(2) F(2) 109.0(4)
N(1) P(3) N(3) 119.1(3)
N(3) P(3) F(3) 108.7(4)
N(3) P(3) F(4) 108.3(3)
P(1) N(1) P(3) 122.4(4)
P(2) N(3) P(3) 120.0(4)
P(1) O(2) C(1) 121.0(4)
F(5) C(2) F(6) 106.5(6)
F(6) C(2) C(1) 109.8(8)
F(6) C(2) C(3) 107.1(8)
F(7) C(3) F(8) 107.0(8)
F(8) C(3) C(2) 107.7(7)
F(8) C(3) C(4) 110.4(6)
O(1) C(4) C(3) 108.1(7)
N(5) P(4) N(6) 117.0(3)
N(6) P(4) O(3) 105.9(3)
N(6) P(4) O(4) 111.5(3)
N(4) P(5) N(5) 119.6(4)
N(5) P(5) F(10) 110.5(4)
N(5) P(5) F(11) 109.5(3)
N(4) P(6) N(6) 120.1(4)
N(6) P(6) F(12) 110.5(3)
N(6) P(6) F(14) 108.6(4)
P(5) N(4) P(6) 119.8(4)
P(4) N(6) P(6) 121.7(4)
P(4) O(4) C(8) 120.3(4)
F(13) C(6) F(15) 106.9(6)
F(15) C(6) C(5) 110.0(6)
F(15) C(6) C(7) 107.7(7)
F(16) C(7) F(17) 107.1(6)
F(17) C(7) C(6) 108.1(6)
F(16) C(7) C(8) 109.4(6)
C(6) C(7) C(8) 116.4(6)
N(8) P(7) O(5) 112.2(4)
N(8) P(7) O(6) 105.3(3)
O(5) P(7) O(6) 104.6(3)
N(7) P(8) F(20) 108.3(4)
N(7) P(8) F(21) 109.2(3)
F(20) P(8) F(21) 97.8(3)
N(7) P(9) F(22) 108.5(4)
N(7) P(9) F(23) 108.3(3)
F(22) P(9) F(23) 98.2(4)
P(7) N(8) P(8) 121.9(4)
P(7) O(5) C(9) 120.3(4)
O(5) C(9) C(12) 108.9(7)
F(24) C(11) F(25) 106.4(6)
F(25) C(11) C(10) 109.7(7)
F(25) C(11) C(12) 108.3(7)
F(26) C(12) F(27) 106.6(7)
F(27) C(12) C(9) 111.0(6)
F(27) C(12) C(11) 107.3(6)
N(10) P(10) O(7) 112.9(4)
N(10) P(10) O(8) 104.6(3)
O(7) P(10) O(8) 104.1(3)
N(10) P(11) F(30) 109.9(4)
N(10) P(11) F(31) 109.0(3)
F(30) P(11) F(31) 97.9(3)
N(11) P(12) F(32) 110.0(4)
N(11) P(12) F(33) 109.8(3)
F(32) P(12) F(33) 99.0(3)
P(10) N(11) P(12) 122.5(4)
P(10) O(7) C(16) 123.5(4)
F(34) C(13) F(35) 107.7(8)
F(35) C(13) C(14) 108.0(9)
F(35) C(13) C(16) 109.9(7)
F(36) C(14) F(37) 107.7(7)
F(37) C(14) C(13) 108.1(9)
F(37) C(14) C(15) 109.6(7)
F(17) C(7) C(8) 108.8(7)
O(4) C(8) C(7) 110.4(7)
N(8) P(7) N(9) 116.2(4)
N(9) P(7) O(5) 106.0(3)
N(9) P(7) O(6) 112.0(3)
N(7) P(8) N(8) 119.5(4)
N(8) P(8) F(20) 109.4(3)
N(8) P(8) F(21) 110.5(4)
N(7) P(9) N(9) 119.3(4)
N(9) P(9) F(22) 109.0(4)
N(9) P(9) F(23) 111.5(4)
P(8) N(7) P(9) 119.7(5)
P(7) N(9) P(9) 123.1(4)
P(7) O(6) C(10) 121.0(4)
O(6) C(10) C(11) 110.6(6)
F(24) C(11) C(10) 109.4(6)
F(24) C(11) C(12) 106.4(7)
C(10) C(11) C(12) 116.1(6)
F(26) C(12) C(9) 107.2(7)
F(26) C(12) C(11) 107.7(6)
C(9) C(12) C(11) 116.6(7)
N(10) P(10) N(11) 117.2(3)
N(11) P(10) O(7) 104.8(3)
N(11) P(10) O(8) 112.6(4)
N(10) P(11) N(12) 119.6(3)
N(12) P(11) F(30) 109.7(3)
N(12) P(11) F(31) 108.7(3)
N(11) P(12) N(12) 119.1(4)
N(12) P(12) F(32) 108.0(4)
N(12) P(12) F(33) 109.1(3)
P(10) N(10) P(11) 121.3(4)
P(11) N(12) P(12) 120.1(4)
P(10) O(8) C(15) 119.8(4)
F(34) C(13) C(14) 107.9(7)
F(34) C(13) C(16) 106.3(9)
C(14) C(13) C(16) 116.6(8)
F(36) C(14) C(13) 107.8(8)
F(36) C(14) C(15) 108.2(9)
C(13) C(14) C(15) 115.2(7)
O(8) C(15) C(14) 109.4(8)
N(13) P(13) O(9) 105.4(3)
N(13) P(13) O(10) 112.0(3)
O(9) P(13) O(10) 103.9(3)
N(14) P(14) F(40) 109.9(3)
N(14) P(14) F(41) 109.0(4)
F(40) P(14) F(41) 97.9(3)
N(13) P(15) F(42) 110.1(3)
N(13) P(15) F(43) 110.0(3)
F(42) P(15) F(43) 98.7(3)
P(14) N(14) P(15) 120.4(5)
P(13) O(9) C(17) 122.2(5)
O(9) C(17) C(18) 109.8(7)
F(44) C(18) C(17) 109.4(9)
F(44) C(18) C(19) 106.8(7)
C(17) C(18) C(19) 116.8(7)
F(46) C(19) C(18) 108.5(7)
F(46) C(19) C(20) 108.1(7)
C(18) C(19) C(20) 117.5(10)
N(17) P(16) O(11) 111.9(3)
N(17) P(16) O(12) 105.1(3)
O(11) P(16) O(12) 103.9(3)
N(16) P(17) F(52) 108.3(4)
N(16) P(17) F(53) 109.5(3)
F(52) P(17) F(53) 98.6(3)
N(16) P(18) F(50) 108.6(3)
N(16) P(18) F(51) 108.5(3)
F(50) P(18) F(51) 97.2(3)
P(16) N(17) P(18) 121.1(4)
P(16) O(11) C(24) 120.1(5)
O(12) C(21) C(22) 109.8(6)
F(54) C(22) C(21) 110.2(8)
F(54) C(22) C(23) 107.6(7)
C(21) C(22) C(23) 117.0(7)
F(56) C(23) C(22) 108.7(7)
F(56) C(23) C(24) 108.3(6)
C(22) C(23) C(24) 115.4(8)
O(7) C(16) C(13) 108.6(8)
N(13) P(13) N(15) 117.6(4)
N(15) P(13) O(9) 111.6(3)
N(15) P(13) O(10) 105.6(4)
N(14) P(14) N(15) 119.8(4)
N(15) P(14) F(40) 109.1(4)
N(15) P(14) F(41) 109.0(3)
N(13) P(15) N(14) 119.4(4)
N(14) P(15) F(42) 108.7(4)
N(14) P(15) F(43) 107.9(3)
P(13) N(13) P(15) 121.2(4)
P(13) N(15) P(14) 121.1(5)
P(13) O(10) C(20) 119.9(5)
F(44) C(18) F(45) 106.6(7)
F(45) C(18) C(17) 107.9(7)
F(45) C(18) C(19) 108.8(9)
F(46) C(19) F(47) 106.3(9)
F(47) C(19) C(18) 107.1(8)
F(47) C(19) C(20) 108.9(7)
O(10) C(20) C(19) 109.5(5)
N(17) P(16) N(18) 117.9(4)
N(18) P(16) O(11) 105.8(4)
N(18) P(16) O(12) 111.5(3)
N(16) P(17) N(18) 119.0(4)
N(18) P(17) F(52) 109.5(3)
N(18) P(17) F(53) 109.9(4)
N(16) P(18) N(17) 119.5(4)
N(17) P(18) F(50) 110.8(3)
N(17) P(18) F(51) 109.9(3)
P(17) N(16) P(18) 120.8(4)
P(16) N(18) P(17) 120.9(5)
P(16) O(12) C(21) 122.0(5)
F(54) C(22) F(55) 107.3(7)
F(55) C(22) C(21) 106.6(6)
F(55) C(22) C(23) 107.7(8)
F(56) C(23) F(57) 108.1(8)
F(57) C(23) C(22) 106.9(7)
F(57) C(23) C(24) 109.2(7)
O(11) C(24) C(23) 108.6(6)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
P(1) N(2) 1.578(6)
P(1) O(2) 1.576(5)
P(2) N(3) 1.564(7)
P(2) F(2) 1.528(6)
P(3) N(3) 1.565(6)
P(3) F(4) 1.503(4)
O(2) C(1) 1.416(9)
F(6) C(2) 1.362(9)
F(8) C(3) 1.341(10)
C(2) C(3) 1.529(14)
P(4) N(6) 1.577(8)
P(4) O(4) 1.589(4)
P(5) N(5) 1.553(6)
P(5) F(11) 1.511(5)
P(6) N(6) 1.554(7)
P(6) F(14) 1.531(8)
O(4) C(8) 1.441(9)
F(15) C(6) 1.341(9)
F(17) C(7) 1.333(9)
C(6) C(7) 1.528(10)
P(7) N(9) 1.552(8)
P(7) O(6) 1.579(4)
P(8) N(8) 1.550(7)
P(8) F(21) 1.518(5)
P(9) N(9) 1.554(7)
P(9) F(23) 1.483(6)
O(6) C(10) 1.426(8)
F(25) C(11) 1.340(8)
F(27) C(12) 1.339(9)
C(10) C(11) 1.474(13)
P(10) N(11) 1.561(7)
P(10) O(8) 1.579(5)
P(1) N(1) 1.571(6)
P(1) O(1) 1.576(6)
P(2) N(2) 1.542(7)
P(2) F(1) 1.511(5)
P(3) N(1) 1.545(6)
P(3) F(3) 1.522(6)
O(1) C(4) 1.448(10)
F(5) C(2) 1.354(9)
F(7) C(3) 1.378(11)
C(1) C(2) 1.491(14)
C(3) C(4) 1.499(11)
P(4) N(5) 1.574(6)
P(4) O(3) 1.565(5)
P(5) N(4) 1.573(8)
P(5) F(10) 1.519(6)
P(6) N(4) 1.543(7)
P(6) F(12) 1.488(5)
O(3) C(5) 1.443(11)
F(13) C(6) 1.351(10)
F(16) C(7) 1.365(9)
C(5) C(6) 1.522(11)
C(7) C(8) 1.478(13)
P(7) N(8) 1.571(6)
P(7) O(5) 1.575(6)
P(8) N(7) 1.570(8)
P(8) F(20) 1.520(6)
P(9) N(7) 1.542(7)
P(9) F(22) 1.528(9)
O(5) C(9) 1.446(11)
F(24) C(11) 1.356(9)
F(26) C(12) 1.360(11)
C(9) C(12) 1.486(10)
C(11) C(12) 1.536(10)
P(10) N(10) 1.571(6)
P(10) O(7) 1.570(6)
P(11) N(10) 1.561(6)
P(11) N(12) 1.570(7)
P(11) F(31) 1.528(4)
P(12) N(12) 1.555(6)
P(12) F(33) 1.516(4)
O(8) C(15) 1.426(10)
F(35) C(13) 1.338(10)
F(37) C(14) 1.344(10)
C(13) C(16) 1.519(14)
P(13) N(15) 1.583(6)
P(13) O(10) 1.584(6)
P(14) N(15) 1.553(7)
P(14) F(41) 1.513(5)
P(15) N(14) 1.553(7)
P(15) F(43) 1.516(5)
O(10) C(20) 1.435(10)
F(45) C(18) 1.360(11)
F(47) C(19) 1.361(13)
C(18) C(19) 1.513(13)
P(16) N(18) 1.563(6)
P(16) O(12) 1.591(5)
P(17) N(18) 1.569(7)
P(17) F(53) 1.519(6)
P(18) N(17) 1.556(6)
P(18) F(51) 1.516(4)
O(12) C(21) 1.424(10)
F(55) C(22) 1.361(10)
F(57) C(23) 1.361(13)
C(22) C(23) 1.519(12)
P(11) F(30) 1.523(6)
P(12) N(11) 1.557(7)
P(12) F(32) 1.512(7)
O(7) C(16) 1.427(10)
F(34) C(13) 1.359(12)
F(36) C(14) 1.351(12)
C(13) C(14) 1.511(16)
C(14) C(15) 1.515(15)
P(13) N(13) 1.566(7)
P(13) O(9) 1.573(5)
P(14) N(14) 1.563(8)
P(14) F(40) 1.519(5)
P(15) N(13) 1.567(7)
P(15) F(42) 1.519(7)
O(9) C(17) 1.414(11)
F(44) C(18) 1.344(12)
F(46) C(19) 1.364(11)
C(17) C(18) 1.500(14)
C(19) C(20) 1.476(14)
P(16) N(17) 1.572(7)
P(16) O(11) 1.568(6)
P(17) N(16) 1.559(8)
P(17) F(52) 1.513(5)
P(18) N(16) 1.551(7)
P(18) F(50) 1.518(6)
O(11) C(24) 1.441(9)
F(54) C(22) 1.340(12)
F(56) C(23) 1.347(10)
C(21) C(22) 1.493(11)
C(23) C(24) 1.507(12)
