#------------------------------------------------------------------------------
#$Date: 2023-03-26 11:09:57 +0300 (Sun, 26 Mar 2023) $
#$Revision: 282068 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/10/52/2105249.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2105249
loop_
_publ_author_name
'Moëlo, Yves'
'Guillot-Deudon, Catherine'
'Evain, Michel'
'Orlandi, Paolo'
'Biagioni, Cristian'
_publ_section_title
;
 Comparative modular analysis of two complex sulfosalt structures:
 sterryite, Cu(Ag,Cu)₃Pb₁₉(Sb,As)₂₂(As--As)S₅₆, and parasterryite,
 Ag₄Pb₂₀(Sb,As)₂₄S₅₈
;
_journal_coeditor_code           BP5041
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              480
_journal_page_last               492
_journal_paper_doi               10.1107/S0108768112034027
_journal_volume                  68
_journal_year                    2012
_chemical_compound_source        'Pollone mine, Tuscany, Italy'
_chemical_formula_sum
'Ag1.86 As7.06 Bi0.1 Cu1.73 Hg0.24 Pb19.13 S56 Sb16.47 Tl0.24'
_chemical_formula_weight         8721.7
_chemical_name_common            'Ag2 As7 Cu1.5 Pb19 S56 Sb16.5'
_chemical_name_mineral           Sterryite
_chemical_name_systematic        ' ?'
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_method           'Jana2006 Version : 07/10/2009'
_cell_angle_alpha                90
_cell_angle_beta                 94.896(8)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.1891(10)
_cell_length_b                   28.5294(13)
_cell_length_c                   42.98(2)
_cell_measurement_temperature    293
_cell_measurement_theta_max      35
_cell_measurement_theta_min      6.4
_cell_volume                     10005(5)
_computing_publication_material
'Jana2006 (Petricek, Dusek & Palatinus, 2006)'
_computing_structure_refinement
'Jana2006 (Petricek, Dusek & Palatinus, 2006)'
_database_code_amcsd             0019482
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.99
_diffrn_measurement_device       'four-cycle diffractometer'
_diffrn_measurement_device_type  'Nonius CCD'
_diffrn_measurement_method       'phi, omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.2733
_diffrn_reflns_av_sigmaI/netI    0.1581
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       46
_diffrn_reflns_limit_k_min       -45
_diffrn_reflns_limit_l_max       69
_diffrn_reflns_limit_l_min       -68
_diffrn_reflns_number            177315
_diffrn_reflns_theta_full        35
_diffrn_reflns_theta_max         35
_diffrn_reflns_theta_min         6.4
_exptl_absorpt_coefficient_mu    41.568
_exptl_absorpt_correction_T_max  0.594
_exptl_absorpt_correction_T_min  0.1942
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
'Jana2006  (Petricek, Dusek & Palatinus, 2000)'
_exptl_crystal_density_diffrn    5.7885
_exptl_crystal_description       block
_exptl_crystal_F_000             14889
_exptl_crystal_size_max          0.142
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.025
_refine_diff_density_max         10.46
_refine_diff_density_min         -8.35
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   3.16
_refine_ls_number_constraints    205
_refine_ls_number_parameters     652
_refine_ls_number_reflns         22702
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.2043
_refine_ls_R_factor_gt           0.1353
_refine_ls_shift/su_max          0.0292
_refine_ls_shift/su_mean         0.0033
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(σ²(F)+0.000484F²)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.1641
_refine_ls_wR_factor_ref         0.1696
_reflns_number_gt                13875
_reflns_number_total             22702
_reflns_threshold_expression     I>3σ(I)
_cod_data_source_file            bp5041.cif
_cod_data_source_block           sterryite
_cod_original_cell_volume        10004.78
_cod_original_sg_symbol_Hall     '-P 2yabc'
_cod_database_code               2105249
_cod_database_fobs_code          2105249
loop_
_symmetry_equiv_pos_site_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x+1/2,y+1/2,-z+1/2
3 -x,-y,-z
4 x+1/2,-y+1/2,z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_symmetry_multiplicity
Pb Pb1 0.7269(3) 0.63980(8) 0.19903(6) 0.0236(7) Uani d 1 4
Pb Pb2 0.2204(3) 0.63585(8) 0.19887(6) 0.0228(7) Uani d 1 4
Pb Pb3 0.6806(3) 0.69994(9) 0.10114(6) 0.0266(7) Uani d 1 4
Pb Pb4 0.1796(3) 0.69914(8) 0.10211(6) 0.0239(7) Uani d 1 4
Pb Pb5 0.6827(3) 0.54811(8) 0.11574(7) 0.0248(7) Uani d 1 4
Pb Pb6 0.1880(3) 0.54785(8) 0.11636(7) 0.0257(7) Uani d 1 4
Pb Pb7 0.6785(3) 0.40767(8) 0.10849(6) 0.0215(7) Uani d 0.9 4
Bi Bi7 0.6785(3) 0.40767(8) 0.10849(6) 0.0215(7) Uani d 0.1 4
Pb Pb8 0.1896(3) 0.40343(8) 0.11030(6) 0.0239(7) Uani d 1 4
Sb Sb9 0.5305(5) 0.01042(12) 0.29831(10) 0.0216(12) Uani d 1 4
Sb Sb10 0.4706(5) 0.49980(13) 0.19294(11) 0.0182(12) Uani d 0.7 4
As As10 0.4706(5) 0.49980(13) 0.19294(11) 0.0182(12) Uani d 0.3 4
Sb Sb11 0.4951(5) 0.08142(13) 0.22572(10) 0.0191(11) Uani d 0.91 4
As As11 0.4951(5) 0.08142(13) 0.22572(10) 0.0191(11) Uani d 0.09 4
Sb Sb12 -0.0004(5) 0.09558(14) 0.21938(12) 0.0177(13) Uani d 0.5 4
As As12 -0.0004(5) 0.09558(14) 0.21938(12) 0.0177(13) Uani d 0.5 4
Pb Pb13 0.7355(3) 0.21623(8) 0.21405(6) 0.0258(7) Uani d 1 4
Pb Pb14 0.2337(3) 0.21029(8) 0.20834(7) 0.0282(8) Uani d 0.76 4
Tl Tl14 0.2337(3) 0.21029(8) 0.20834(7) 0.0282(8) Uani d 0.24 4
Sb Sb15 0.9557(7) 0.76196(17) 0.17837(14) 0.0154(15) Uani d 0.07 4
As As15 0.9557(7) 0.76196(17) 0.17837(14) 0.0154(15) Uani d 0.93 4
Sb Sb16 0.4342(5) 0.76744(14) 0.17674(11) 0.0229(13) Uani d 0.86 4
As As16 0.4342(5) 0.76744(14) 0.17674(11) 0.0229(13) Uani d 0.14 4
Sb Sb17 0.9015(5) 0.83817(12) 0.09471(11) 0.0224(12) Uani d 1 4
Sb Sb18 0.4294(6) 0.82664(18) 0.09887(13) 0.0231(15) Uani d 0.45 4
As As18 0.4294(6) 0.82664(18) 0.09887(13) 0.0231(15) Uani d 0.55 4
Sb Sb19 0.8984(5) 0.90892(15) 0.02117(12) 0.0261(14) Uani d 0.82 4
As As19 0.8984(5) 0.90892(15) 0.02117(12) 0.0261(14) Uani d 0.18 4
Sb Sb20 0.3796(5) 0.92081(14) 0.01144(12) 0.0227(13) Uani d 0.8 4
As As20 0.3796(5) 0.92081(14) 0.01144(12) 0.0227(13) Uani d 0.2 4
Sb Sb21 0.3380(5) 0.49779(13) 0.42995(12) 0.0280(13) Uani d 1 4
Pb Pb22 0.8526(4) 0.49900(13) 0.43845(8) 0.0367(10) Uani d 0.67 4
Sb Sb22 0.8526(4) 0.49900(13) 0.43845(8) 0.0367(10) Uani d 0.33 4
Pb Pb23 0.1804(3) 0.91576(10) 0.14472(7) 0.0298(8) Uani d 0.83 4
Sb Sb23 0.1804(3) 0.91576(10) 0.14472(7) 0.0298(8) Uani d 0.17 4
Sb Sb24 0.7048(5) 0.91749(12) 0.15226(11) 0.0218(12) Uani d 1 4
Ag Ag25 0.2343(8) 0.8281(2) 0.23710(18) 0.048(2) Uani d 0.9 4
Cu Cu25 0.2343(8) 0.8281(2) 0.23710(18) 0.048(2) Uani d 0.1 4
Sb Sb26 0.7330(5) 0.83424(15) 0.23460(12) 0.0241(13) Uani d 0.85 4
As As26 0.7330(5) 0.83424(15) 0.23460(12) 0.0241(13) Uani d 0.15 4
Pb Pb27 0.0042(3) 0.38059(8) 0.19626(7) 0.0282(8) Uani d 1 4
Sb Sb28 0.4792(6) 0.36806(18) 0.19252(13) 0.0262(15) Uani d 0.55 4
As As28 0.4792(6) 0.36806(18) 0.19252(13) 0.0262(15) Uani d 0.45 4
Sb Sb29 0.4575(6) 0.95474(17) 0.22192(12) 0.0331(15) Uani d 1 4
Pb Pb30 0.5218(3) 0.46856(9) 0.27371(7) 0.0321(8) Uani d 1 4
Pb Pb31 0.4385(3) 0.04969(9) 0.14240(7) 0.0301(8) Uani d 1 4
Pb Pb32 0.9344(3) 0.05142(9) 0.14031(7) 0.0330(8) Uani d 1 4
Ag Ag33b 0.355(2) 0.1216(4) 0.0548(4) 0.021(4) Uani d 0.6 4
Cu Cu33a 0.385(6) 0.1125(13) 0.0603(11) 0.021(4) Uani d 0.4 4
Ag Ag34b 0.9174(9) 0.11888(18) 0.05761(14) 0.0462(19) Uani d 0.36 4
Hg Hg34b 0.9174(9) 0.11888(18) 0.05761(14) 0.0462(19) Uani d 0.24 4
Cu Cu34b 0.9174(9) 0.11888(18) 0.05761(14) 0.0462(19) Uani d 0.4 4
Pb Pb35 0.6432(3) 0.78361(9) 0.01656(6) 0.0271(7) Uani d 1 4
Pb Pb36 0.1376(3) 0.78670(9) 0.01835(7) 0.0290(8) Uani d 1 4
Sb Sb37 0.8970(6) 0.62016(16) 0.03928(13) 0.0183(15) Uani d 0.27 4
As As37 0.8970(6) 0.62016(16) 0.03928(13) 0.0183(15) Uani d 0.73 4
Sb Sb38 0.3930(5) 0.61302(14) 0.03657(10) 0.0220(12) Uani d 1 4
Sb Sb39 0.8961(5) 0.46983(13) 0.03944(10) 0.0219(12) Uani d 1 4
Sb Sb40 0.3994(6) 0.48411(15) 0.04011(13) 0.0174(14) Uani d 0.36 4
As As40 0.3994(6) 0.48411(15) 0.04011(13) 0.0174(14) Uani d 0.64 4
Pb Pb41 0.9048(4) 0.33727(12) 0.03897(10) 0.0220(11) Uani d 0.14 4
Sb Sb41 0.9048(4) 0.33727(12) 0.03897(10) 0.0220(11) Uani d 0.86 4
Sb Sb42 0.3870(5) 0.32966(14) 0.03506(11) 0.0203(12) Uani d 0.8 4
As As42 0.3870(5) 0.32966(14) 0.03506(11) 0.0203(12) Uani d 0.2 4
Cu Cu43 0.6465(11) 0.2133(4) 0.0582(2) 0.041(4) Uani d 0.83 4
Pb Pb44a 0.6792(3) 0.27434(8) 0.11949(7) 0.0274(8) Uani d 0.83 4
Sb Sb44b 0.6792(3) 0.27434(8) 0.11949(7) 0.0274(8) Uani d 0.17 4
Pb Pb45 0.1849(3) 0.25801(9) 0.10565(7) 0.0321(8) Uani d 1 4
As As46 0.8587(6) 0.16461(18) 0.13154(18) 0.0177(19) Uani d 1 4
As As47 0.5386(7) 0.1595(2) 0.13276(17) 0.0207(19) Uani d 1 4
S S1 0.9531(17) 0.6910(4) 0.1541(3) 0.013(3) Uiso d 1 4
S S2 0.4445(17) 0.6913(4) 0.1557(3) 0.012(3) Uiso d 1 4
S S3 0.9261(18) 0.6229(5) 0.0934(3) 0.017(3) Uiso d 1 4
S S4 0.4250(17) 0.6236(4) 0.0928(3) 0.012(3) Uiso d 1 4
S S5 0.9576(17) 0.5726(4) 0.1659(3) 0.012(3) Uiso d 1 4
S S6 0.4561(18) 0.5722(4) 0.1681(3) 0.015(3) Uiso d 1 4
S S7 0.4965(17) 0.1560(4) 0.2505(3) 0.014(3) Uiso d 1 4
S S8 0.4911(19) 0.6647(5) 0.2476(4) 0.021(3) Uiso d 1 4
S S9 0.9184(19) 0.7632(5) 0.0698(4) 0.019(3) Uiso d 1 4
S S10 0.4102(19) 0.7606(5) 0.0657(4) 0.020(3) Uiso d 1 4
S S11 0.929(2) 0.4786(5) 0.0971(4) 0.021(3) Uiso d 1 4
S S12 0.419(2) 0.4767(5) 0.0958(4) 0.023(3) Uiso d 1 4
S S13 0.6860(18) 0.4736(5) 0.1638(4) 0.017(3) Uiso d 1 4
S S14 0.2269(19) 0.4722(5) 0.1645(4) 0.021(3) Uiso d 1 4
S S15 0.7736(19) 0.5510(5) 0.2375(4) 0.020(3) Uiso d 1 4
S S16 0.2122(18) 0.5490(5) 0.2369(4) 0.019(3) Uiso d 1 4
S S17 -0.2423(18) 0.1171(5) 0.1902(4) 0.018(3) Uiso d 1 4
S S18 0.194(2) 0.1228(6) 0.1845(4) 0.031(4) Uiso d 1 4
S S19 0.7711(18) 0.7414(5) 0.2129(4) 0.020(3) Uiso d 1 4
S S20 0.1966(17) 0.7520(5) 0.2109(3) 0.015(3) Uiso d 1 4
S S21 0.6611(19) 0.8036(5) 0.1314(4) 0.022(3) Uiso d 1 4
S S22 0.2374(17) 0.7988(5) 0.1343(4) 0.016(3) Uiso d 1 4
S S23 0.6861(19) 0.8715(5) 0.0573(4) 0.022(3) Uiso d 1 4
S S24 1.127(2) 0.8737(6) 0.0547(4) 0.027(3) Uiso d 1 4
S S25 0.4128(18) 0.0476(5) 0.0236(4) 0.019(3) Uiso d 1 4
S S26 0.8642(19) 0.0485(5) 0.0203(4) 0.021(3) Uiso d 1 4
S S27 0.0958(19) 0.4683(5) 0.3964(4) 0.020(3) Uiso d 1 4
S S28 0.946(2) 0.9678(6) 0.1042(4) 0.028(4) Uiso d 1 4
S S29 0.4855(15) 0.8880(4) 0.1847(3) 0.007(2) Uiso d 1 4
S S30 0.9445(19) 0.8893(5) 0.1860(4) 0.021(3) Uiso d 1 4
S S31 0.529(2) 0.8020(5) 0.2666(4) 0.023(3) Uiso d 1 4
S S32 0.5237(17) 0.3087(5) 0.2307(3) 0.016(3) Uiso d 1 4
S S33 0.2517(19) 0.3288(6) 0.1675(4) 0.025(3) Uiso d 1 4
S S34 0.6994(19) 0.3460(5) 0.1635(3) 0.019(3) Uiso d 1 4
S S35 0.2415(19) 0.4100(5) 0.2491(4) 0.020(3) Uiso d 1 4
S S36 0.7711(19) 0.4164(5) 0.2414(4) 0.021(3) Uiso d 1 4
S S37 0.285(2) 0.4922(5) 0.3206(4) 0.022(3) Uiso d 1 4
S S38 0.7090(17) 0.9942(4) 0.1756(3) 0.013(3) Uiso d 1 4
S S39 0.1696(18) 0.0743(5) 0.0959(3) 0.016(3) Uiso d 1 4
S S40 0.8211(17) 0.5742(5) 0.4030(3) 0.015(3) Uiso d 1 4
S S41 0.131(2) 0.1556(5) 0.0145(4) 0.025(3) Uiso d 1 4
S S42 0.6231(19) 0.1573(5) 0.0100(3) 0.020(3) Uiso d 1 4
S S43 0.690(2) 0.6769(6) 0.0346(4) 0.029(4) Uiso d 1 4
S S44 0.112(2) 0.6702(6) 0.0311(4) 0.028(4) Uiso d 1 4
S S45 0.613(2) 0.5396(5) 0.0390(4) 0.025(3) Uiso d 1 4
S S46 0.1871(17) 0.5450(5) 0.0390(4) 0.017(3) Uiso d 1 4
S S47 0.6814(17) 0.4106(5) 0.0393(3) 0.014(3) Uiso d 1 4
S S48 0.1160(18) 0.4065(5) 0.0406(3) 0.018(3) Uiso d 1 4
S S49 0.610(2) 0.2766(6) 0.0255(4) 0.033(4) Uiso d 1 4
S S50 0.172(2) 0.2728(5) 0.0380(4) 0.024(3) Uiso d 1 4
S S51 0.8951(19) 0.1968(5) 0.0839(4) 0.019(3) Uiso d 1 4
S S52 0.4391(19) 0.1899(5) 0.0868(4) 0.019(3) Uiso d 1 4
S S53 0.9368(15) 0.2276(4) 0.1613(3) 0.007(2) Uiso d 1 4
S S54 0.4812(18) 0.2237(5) 0.1629(3) 0.017(3) Uiso d 1 4
S S55 0.9296(19) 0.3349(5) 0.0993(3) 0.019(3) Uiso d 1 4
S S56 0.4231(17) 0.3338(4) 0.0932(3) 0.014(3) Uiso d 1 4
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Pb -3.394 10.111 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Sb -0.587 1.546 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
As 0.050 2.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Ag -0.897 1.102 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Cu 0.320 1.265 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
S 0.125 0.123 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Hg -2.389 9.227 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Tl -2.836 9.669 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Bi -4.108 10.257 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Pb1 S1 . 3.146(14)
Pb1 S2 . 3.201(13)
Pb1 S5 . 3.118(14)
Pb1 S6 . 3.147(14)
Pb1 S7 2_655 3.034(14)
Pb1 S8 . 3.047(16)
Pb1 S15 . 3.032(15)
Pb1 S19 . 2.975(15)
Pb2 S1 1_455 3.201(13)
Pb2 S2 . 3.147(14)
Pb2 S5 1_455 3.062(13)
Pb2 S6 . 3.034(14)
Pb2 S7 2_555 2.979(15)
Pb2 S8 . 3.031(15)
Pb2 S16 . 2.973(15)
Pb2 S20 . 3.362(14)
Pb3 S1 . 3.060(14)
Pb3 S2 . 3.172(14)
Pb3 S3 . 3.017(14)
Pb3 S4 . 3.021(13)
Pb3 S9 . 3.051(15)
Pb3 S10 . 3.106(15)
Pb3 S21 . 3.240(15)
Pb3 S43 . 2.940(19)
Pb4 S1 1_455 3.033(15)
Pb4 S2 . 3.034(13)
Pb4 S3 1_455 3.008(14)
Pb4 S4 . 2.998(13)
Pb4 S9 1_455 3.055(15)
Pb4 S10 . 3.098(16)
Pb4 S22 . 3.180(14)
Pb4 S44 . 3.165(18)
Pb5 S3 . 3.126(15)
Pb5 S4 . 3.115(13)
Pb5 S5 . 3.062(13)
Pb5 S6 . 3.114(15)
Pb5 S11 . 2.986(16)
Pb5 S12 . 3.038(15)
Pb5 S13 . 2.962(15)
Pb5 S45 . 3.309(17)
Pb6 S3 1_455 3.130(14)
Pb6 S4 . 3.130(13)
Pb6 S5 1_455 3.047(15)
Pb6 S6 . 3.069(14)
Pb6 S11 1_455 2.966(15)
Pb6 S12 . 2.960(16)
Pb6 S14 . 2.988(15)
Pb6 S46 . 3.325(16)
Pb7 S11 . 2.951(16)
Pb7 S12 . 2.914(16)
Pb7 S13 . 3.029(15)
Pb7 S34 . 2.939(15)
Pb7 S47 . 2.976(15)
Pb7 S55 . 2.971(15)
Pb7 S56 . 3.002(13)
Bi7 S11 . 2.951(16)
Bi7 S12 . 2.914(16)
Bi7 S13 . 3.029(15)
Bi7 S34 . 2.939(15)
Bi7 S47 . 2.976(15)
Bi7 S55 . 2.971(15)
Bi7 S56 . 3.002(13)
Pb8 S11 1_455 3.046(15)
Pb8 S12 . 2.913(16)
Pb8 S14 . 3.042(15)
Pb8 S33 . 3.260(17)
Pb8 S48 . 3.006(15)
Pb8 S55 1_455 2.899(15)
Pb8 S56 . 2.896(14)
Sb9 S5 2_645 2.345(13)
Sb9 S13 2_645 2.915(15)
Sb9 S14 2_545 2.960(17)
Sb9 S15 2_645 2.590(16)
Sb9 S16 2_545 2.635(15)
Sb9 S36 2_645 3.635(16)
Sb10 S6 . 2.322(14)
Sb10 S13 . 2.369(16)
Sb10 S14 . 2.383(16)
Sb10 S15 . 3.339(15)
Sb10 S16 . 3.273(16)
As10 S6 . 2.322(14)
As10 S13 . 2.369(16)
As10 S14 . 2.383(16)
As10 S15 . 3.339(15)
As10 S16 . 3.273(16)
Sb11 S7 . 2.379(13)
Sb11 S15 2_645 2.515(15)
Sb11 S16 2_545 2.603(16)
Sb11 S17 1_655 2.925(16)
Sb11 S18 . 3.139(18)
As11 S7 . 2.379(13)
As11 S15 2_645 2.515(15)
As11 S16 2_545 2.603(16)
As11 S17 1_655 2.925(16)
As11 S18 . 3.139(18)
Sb12 S8 2_545 2.427(15)
Sb12 S15 2_545 3.280(17)
Sb12 S16 2_545 3.178(15)
Sb12 S17 . 2.335(15)
Sb12 S18 . 2.410(19)
As12 S8 2_545 2.427(15)
As12 S15 2_545 3.280(17)
As12 S16 2_545 3.178(15)
As12 S17 . 2.335(15)
As12 S18 . 2.410(19)
Pb13 S7 . 3.125(14)
Pb13 S8 2_645 3.043(15)
Pb13 S17 1_655 3.018(14)
Pb13 S19 2_645 3.227(16)
Pb13 S31 2_645 3.179(15)
Pb13 S32 . 3.270(14)
Pb13 S53 . 2.934(13)
Pb13 S54 . 2.903(14)
Pb14 S7 . 3.107(13)
Pb14 S8 2_545 3.042(16)
Pb14 S18 . 2.708(17)
Pb14 S20 2_545 3.667(15)
Pb14 S31 2_545 3.610(16)
Pb14 S32 . 3.750(14)
Pb14 S53 1_455 3.068(12)
Pb14 S54 . 2.956(16)
Tl14 S7 . 3.107(13)
Tl14 S8 2_545 3.042(16)
Tl14 S18 . 2.708(17)
Tl14 S20 2_545 3.667(15)
Tl14 S31 2_545 3.610(16)
Tl14 S32 . 3.750(14)
Tl14 S53 1_455 3.068(12)
Tl14 S54 . 2.956(16)
Sb15 S1 . 2.277(14)
Sb15 S19 . 2.283(17)
Sb15 S20 1_655 2.337(14)
Sb15 S21 . 3.236(16)
Sb15 S22 1_655 3.280(16)
Sb15 S30 . 3.651(15)
As15 S1 . 2.277(14)
As15 S19 . 2.283(17)
As15 S20 1_655 2.337(14)
As15 S21 . 3.236(16)
As15 S22 1_655 3.280(16)
As15 S30 . 3.651(15)
Sb16 S2 . 2.358(13)
Sb16 S19 . 3.137(15)
Sb16 S20 . 2.574(15)
Sb16 S21 . 2.988(17)
Sb16 S22 . 2.494(15)
Sb16 S29 . 3.479(12)
As16 S2 . 2.358(13)
As16 S19 . 3.137(15)
As16 S20 . 2.574(15)
As16 S21 . 2.988(17)
As16 S22 . 2.494(15)
As16 S29 . 3.479(12)
Sb17 S9 . 2.401(15)
Sb17 S21 . 2.805(17)
Sb17 S22 1_655 3.305(14)
Sb17 S23 . 2.475(16)
Sb17 S24 . 2.820(18)
Sb17 S28 . 3.735(17)
Sb18 S10 . 2.359(15)
Sb18 S21 . 2.353(16)
Sb18 S22 . 2.415(16)
Sb18 S23 . 3.146(17)
Sb18 S24 1_455 3.275(17)
As18 S10 . 2.359(15)
As18 S21 . 2.353(16)
As18 S22 . 2.415(16)
As18 S23 . 3.146(17)
As18 S24 1_455 3.275(17)
Sb19 S23 . 2.651(17)
Sb19 S24 . 2.478(17)
Sb19 S25 3_665 3.302(15)
Sb19 S26 3_765 3.004(17)
Sb19 S41 3_665 2.395(16)
As19 S23 . 2.651(17)
As19 S24 . 2.478(17)
As19 S25 3_665 3.302(15)
As19 S26 3_765 3.004(17)
As19 S41 3_665 2.395(16)
Sb20 S23 . 3.363(16)
Sb20 S24 1_455 3.190(18)
Sb20 S25 1_565 3.662(15)
Sb20 S25 3_665 2.532(16)
Sb20 S26 3_665 2.480(16)
Sb20 S42 3_665 2.410(15)
As20 S23 . 3.363(16)
As20 S24 1_455 3.190(18)
As20 S25 1_565 3.662(15)
As20 S25 3_665 2.532(16)
As20 S26 3_665 2.480(16)
As20 S42 3_665 2.410(15)
Sb21 S24 2_645 3.607(17)
Sb21 S25 2_555 3.305(16)
Sb21 S26 2_655 3.423(16)
Sb21 S27 . 2.496(15)
Sb21 S28 2_645 2.543(19)
Sb21 S39 2_555 2.447(14)
Pb22 S23 2_645 3.657(16)
Pb22 S25 2_655 2.782(15)
Pb22 S26 2_655 2.971(16)
Pb22 S27 1_655 2.934(16)
Pb22 S28 2_645 3.062(17)
Pb22 S40 . 2.632(14)
Sb22 S23 2_645 3.657(16)
Sb22 S25 2_655 2.782(15)
Sb22 S26 2_655 2.971(16)
Sb22 S27 1_655 2.934(16)
Sb22 S28 2_645 3.062(17)
Sb22 S40 . 2.632(14)
Pb23 S22 . 3.404(14)
Pb23 S27 2_555 3.048(16)
Pb23 S28 1_455 2.888(17)
Pb23 S29 . 3.014(12)
Pb23 S30 1_455 2.835(17)
Pb23 S37 2_555 2.643(15)
Sb23 S22 . 3.404(14)
Sb23 S27 2_555 3.048(16)
Sb23 S28 1_455 2.888(17)
Sb23 S29 . 3.014(12)
Sb23 S30 1_455 2.835(17)
Sb23 S37 2_555 2.643(15)
Sb24 S21 . 3.382(15)
Sb24 S27 2_555 3.415(15)
Sb24 S28 . 3.304(18)
Sb24 S29 . 2.509(14)
Sb24 S30 . 2.473(16)
Sb24 S38 . 2.407(13)
Ag25 S20 . 2.452(15)
Ag25 S29 . 3.610(15)
Ag25 S30 1_455 3.553(16)
Ag25 S31 . 2.735(17)
Ag25 S32 2_555 2.680(17)
Ag25 S35 2_555 2.415(15)
Cu25 S20 . 2.452(15)
Cu25 S29 . 3.610(15)
Cu25 S30 1_455 3.553(16)
Cu25 S31 . 2.735(17)
Cu25 S32 2_555 2.680(17)
Cu25 S35 2_555 2.415(15)
Sb26 S19 . 2.834(15)
Sb26 S29 . 3.214(13)
Sb26 S30 . 3.232(17)
Sb26 S31 . 2.432(17)
Sb26 S32 2_655 2.494(15)
Sb26 S36 2_655 2.563(15)
As26 S19 . 2.834(15)
As26 S29 . 3.214(13)
As26 S30 . 3.232(17)
As26 S31 . 2.432(17)
As26 S32 2_655 2.494(15)
As26 S36 2_655 2.563(15)
Pb27 S14 . 3.528(15)
Pb27 S31 2_545 2.779(16)
Pb27 S33 . 2.871(17)
Pb27 S34 1_455 2.931(15)
Pb27 S35 . 2.980(15)
Pb27 S36 1_455 3.013(16)
Sb28 S13 . 3.718(15)
Sb28 S14 . 3.758(15)
Sb28 S32 . 2.364(15)
Sb28 S33 . 2.354(16)
Sb28 S34 . 2.365(17)
Sb28 S35 . 3.454(17)
Sb28 S36 . 3.342(16)
As28 S13 . 3.718(15)
As28 S14 . 3.758(15)
As28 S32 . 2.364(15)
As28 S33 . 2.354(16)
As28 S34 . 2.365(17)
As28 S35 . 3.454(17)
As28 S36 . 3.342(16)
Sb29 S16 2_555 3.565(16)
Sb29 S29 . 2.511(13)
Sb29 S35 2_555 2.487(16)
Sb29 S36 2_655 2.834(16)
Sb29 S37 2_555 2.792(16)
Sb29 S38 . 3.191(15)
Pb30 S15 . 3.570(16)
Pb30 S16 . 3.676(15)
Pb30 S30 2_645 2.846(15)
Pb30 S35 . 2.961(15)
Pb30 S36 . 2.966(16)
Pb30 S37 . 2.991(17)
Pb30 S38 2_645 3.054(13)
Pb31 S17 1_655 3.720(14)
Pb31 S18 . 3.497(18)
Pb31 S27 2_545 2.860(15)
Pb31 S37 2_545 3.011(16)
Pb31 S38 1_545 2.985(13)
Pb31 S39 . 2.928(14)
Pb31 S40 2_645 2.970(15)
Pb32 S17 1_655 3.277(16)
Pb32 S18 1_655 3.405(17)
Pb32 S28 1_545 2.852(17)
Pb32 S37 2_645 3.211(15)
Pb32 S38 1_545 2.974(14)
Pb32 S39 1_655 2.898(15)
Pb32 S40 2_645 2.756(14)
Ag33b S25 . 2.57(2)
Ag33b S39 . 2.78(2)
Ag33b S40 2_645 3.37(2)
Ag33b S41 . 2.60(2)
Ag33b S42 . 3.21(2)
Ag33b S52 . 2.449(19)
Cu33a S25 . 2.45(4)
Cu33a S39 . 2.67(5)
Cu33a S40 2_645 2.97(5)
Cu33a S41 . 3.00(5)
Cu33a S42 . 3.29(5)
Cu33a S52 . 2.51(4)
Ag34b S26 . 2.583(16)
Ag34b S39 1_655 2.832(15)
Ag34b S40 2_645 2.980(16)
Ag34b S41 1_655 2.853(18)
Ag34b S42 . 3.218(16)
Ag34b S51 . 2.507(15)
Hg34b S26 . 2.583(16)
Hg34b S39 1_655 2.832(15)
Hg34b S40 2_645 2.980(16)
Hg34b S41 1_655 2.853(18)
Hg34b S42 . 3.218(16)
Hg34b S51 . 2.507(15)
Cu34b S26 . 2.583(16)
Cu34b S39 1_655 2.832(15)
Cu34b S40 2_645 2.980(16)
Cu34b S41 1_655 2.853(18)
Cu34b S42 . 3.218(16)
Cu34b S51 . 2.507(15)
Pb35 S9 . 3.127(15)
Pb35 S10 . 3.037(16)
Pb35 S23 . 3.061(16)
Pb35 S41 3_665 2.938(17)
Pb35 S42 3_665 2.912(15)
Pb35 S43 . 3.158(18)
Pb35 S49 3_665 3.146(18)
Pb35 S50 3_665 3.316(17)
Pb36 S9 1_455 3.040(16)
Pb36 S10 . 2.984(15)
Pb36 S24 1_455 2.939(17)
Pb36 S41 3_565 3.003(16)
Pb36 S42 3_665 2.879(16)
Pb36 S44 . 3.379(16)
Pb36 S49 3_665 3.426(19)
Pb36 S50 3_565 3.759(16)
Sb37 S3 . 2.318(16)
Sb37 S43 . 2.341(18)
Sb37 S44 1_655 2.315(18)
Sb37 S45 . 3.267(17)
Sb37 S46 1_655 3.202(15)
Sb37 S48 3_665 3.510(16)
As37 S3 . 2.318(16)
As37 S43 . 2.341(18)
As37 S44 1_655 2.315(18)
As37 S45 . 3.267(17)
As37 S46 1_655 3.202(15)
As37 S48 3_665 3.510(16)
Sb38 S4 . 2.427(14)
Sb38 S43 . 3.044(18)
Sb38 S44 . 2.815(17)
Sb38 S45 . 2.760(16)
Sb38 S46 . 2.580(15)
Sb38 S47 3_665 3.336(15)
Sb39 S11 . 2.481(16)
Sb39 S45 . 3.053(17)
Sb39 S46 1_655 3.206(15)
Sb39 S46 3_665 3.408(16)
Sb39 S47 . 2.438(14)
Sb39 S48 1_655 2.548(15)
Sb40 S12 . 2.397(17)
Sb40 S45 . 2.365(17)
Sb40 S45 3_665 3.458(18)
Sb40 S46 . 2.454(15)
Sb40 S47 . 3.122(14)
Sb40 S48 . 3.208(15)
As40 S12 . 2.397(17)
As40 S45 . 2.365(17)
As40 S45 3_665 3.458(18)
As40 S46 . 2.454(15)
As40 S47 . 3.122(14)
As40 S48 . 3.208(15)
Pb41 S44 3_665 3.010(18)
Pb41 S47 . 2.780(14)
Pb41 S48 1_655 2.624(15)
Pb41 S49 . 2.984(18)
Pb41 S50 1_655 2.861(16)
Pb41 S55 . 2.586(16)
Sb41 S44 3_665 3.010(18)
Sb41 S47 . 2.780(14)
Sb41 S48 1_655 2.624(15)
Sb41 S49 . 2.984(18)
Sb41 S50 1_655 2.861(16)
Sb41 S55 . 2.586(16)
Sb42 S43 3_665 3.014(19)
Sb42 S47 . 3.332(14)
Sb42 S48 . 3.144(15)
Sb42 S49 . 2.436(19)
Sb42 S50 . 2.406(16)
Sb42 S56 . 2.494(15)
As42 S43 3_665 3.014(19)
As42 S47 . 3.332(14)
As42 S48 . 3.144(15)
As42 S49 . 2.436(19)
As42 S50 . 2.406(16)
As42 S56 . 2.494(15)
Cu43 S42 . 2.609(19)
Cu43 S49 . 2.29(2)
Cu43 S51 . 2.282(17)
Cu43 S52 . 2.281(19)
Pb44a S34 . 2.780(15)
Pb44a S51 . 3.289(15)
Pb44a S52 . 3.343(14)
Pb44a S53 . 2.967(12)
Pb44a S54 . 2.952(15)
Pb44a S55 . 2.872(15)
Pb44a S56 . 2.854(13)
Sb44b S34 . 2.780(15)
Sb44b S51 . 3.289(15)
Sb44b S52 . 3.343(14)
Sb44b S53 . 2.967(12)
Sb44b S54 . 2.952(15)
Sb44b S55 . 2.872(15)
Sb44b S56 . 2.854(13)
Pb45 S33 . 3.346(17)
Pb45 S50 . 2.930(17)
Pb45 S51 1_455 3.030(15)
Pb45 S52 . 3.010(15)
Pb45 S53 1_455 3.380(13)
Pb45 S54 . 3.447(14)
Pb45 S55 1_455 3.027(15)
Pb45 S56 . 2.991(14)
As46 S17 1_655 3.038(17)
As46 S18 1_655 3.618(18)
As46 S40 2_645 3.264(14)
As46 S51 . 2.285(17)
As46 S53 . 2.266(13)
As47 S17 1_655 3.165(16)
As47 S40 2_645 3.146(15)
As47 S52 . 2.246(16)
As47 S54 . 2.317(16)
loop_
_cod_related_entry_id
_cod_related_entry_database
_cod_related_entry_code
1 AMCSD 0019482
