#------------------------------------------------------------------------------
#$Date: 2018-02-04 02:45:06 +0200 (Sun, 04 Feb 2018) $
#$Revision: 206145 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/10/81/2108157.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108157
loop_
_publ_author_name
'Yakubovich, Olga'
'Shvanskaya, Larisa'
'Pchelkina, Zlata'
'Dimitrova, Olga'
'Volkov, Anatoliy'
'Volkova, Olga'
'Vasiliev, Alexander'
_publ_section_title
;
 A novel representative in the rare family of trivanadates,
 KMn₂V₃O₁₀: synthesis, crystal structure and magnetic properties
;
_journal_coeditor_code           UM5009SUP1
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              97
_journal_page_last               103
_journal_paper_doi               10.1107/S205252061701811X
_journal_volume                  74
_journal_year                    2018
_chemical_formula_moiety         'K Mn2 O10 V3'
_chemical_formula_sum            'K Mn2 O10 V3'
_chemical_formula_weight         461.80
_chemical_name_common            'Potassium dimanganese trivanadate'
_chemical_name_systematic        'Potassium dimanganese trivanadate'
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2016/6
_cell_angle_alpha                101.858(5)
_cell_angle_beta                 102.627(5)
_cell_angle_gamma                100.669(5)
_cell_formula_units_Z            2
_cell_length_a                   6.912(5)
_cell_length_b                   6.993(5)
_cell_length_c                   9.656(5)
_cell_measurement_reflns_used    4295
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      32.588
_cell_measurement_theta_min      2.698
_cell_volume                     432.6(5)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
;
_computing_molecular_graphics    'DIMOND (Brandenburg, 2006)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 16.0630
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Xcalibur, Sapphire3'
_diffrn_measurement_method       ω
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0329
_diffrn_reflns_av_unetI/netI     0.0337
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            8207
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.000
_diffrn_reflns_theta_min         3.067
_diffrn_source                   'Enhance (Mo) X-ray Source'
_exptl_absorpt_coefficient_mu    6.480
_exptl_absorpt_correction_T_max  0.853
_exptl_absorpt_correction_T_min  0.416
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
Numerical absorption correction based on gaussian integration over
a multifaceted crystal model
;
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    3.545
_exptl_crystal_density_meas      ?
_exptl_crystal_description       plate
_exptl_crystal_F_000             436
_exptl_crystal_size_max          0.420
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.050
_refine_diff_density_max         0.589
_refine_diff_density_min         -0.590
_refine_diff_density_rms         0.124
_refine_ls_extinction_coef       0.0054(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.113
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     146
_refine_ls_number_reflns         2514
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.113
_refine_ls_R_factor_all          0.0272
_refine_ls_R_factor_gt           0.0240
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0253P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0591
_refine_ls_wR_factor_ref         0.0612
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2293
_reflns_number_total             2514
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            um5009sup1.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 2108157.cif.
;
_cod_database_code               2108157
_cod_database_fobs_code          2108157
_shelx_shelxl_version_number     2016/6
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.172
_shelx_estimated_absorpt_t_max   0.738
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
Mn1 Mn -0.05715(5) -0.23945(5) 0.20586(4) 0.00979(9) Uani 1 1 d
Mn2 Mn 0.68277(5) 0.20730(5) 0.51821(4) 0.00951(9) Uani 1 1 d
V2 V 0.45866(6) -0.11174(6) 0.17904(4) 0.00759(9) Uani 1 1 d
V3 V 0.16188(6) 0.23648(6) 0.45149(4) 0.00782(10) Uani 1 1 d
V1 V 0.08777(6) -0.22435(6) 0.88229(4) 0.00812(10) Uani 1 1 d
K1 K 0.45437(9) 0.39821(10) 0.18908(8) 0.02634(16) Uani 1 1 d
O1 O 0.3568(2) 0.1315(3) 0.50399(18) 0.0112(3) Uani 1 1 d
O2 O 0.0248(3) 0.1073(3) 0.25920(18) 0.0113(3) Uani 1 1 d
O3 O 0.7223(2) 0.2313(3) 0.74941(18) 0.0107(3) Uani 1 1 d
O4 O 0.0021(3) 0.2181(3) 0.56376(18) 0.0116(3) Uani 1 1 d
O5 O 0.3122(3) -0.0721(3) 0.01147(19) 0.0135(4) Uani 1 1 d
O6 O -0.3792(3) -0.2570(3) 0.14679(19) 0.0129(3) Uani 1 1 d
O7 O 0.1326(3) -0.4411(3) 0.8119(2) 0.0161(4) Uani 1 1 d
O8 O 0.5892(3) 0.1142(3) 0.28848(18) 0.0123(3) Uani 1 1 d
O9 O -0.0760(3) -0.2680(3) 0.97995(19) 0.0166(4) Uani 1 1 d
O10 O 0.2639(3) 0.4749(3) 0.4604(2) 0.0171(4) Uani 1 1 d
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
V V 0.3005 0.5294 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O9 Mn1 O4 173.03(6) 1_554 2_556
O9 Mn1 O6 86.00(7) 1_554 .
O4 Mn1 O6 100.78(6) 2_556 .
O9 Mn1 O7 95.60(7) 1_554 2_546
O4 Mn1 O7 83.15(7) 2_556 2_546
O6 Mn1 O7 87.71(7) . 2_546
O9 Mn1 O3 90.11(6) 1_554 2_656
O4 Mn1 O3 83.07(6) 2_556 2_656
O6 Mn1 O3 175.87(6) . 2_656
O7 Mn1 O3 91.29(7) 2_546 2_656
O9 Mn1 O2 92.45(7) 1_554 .
O4 Mn1 O2 88.90(6) 2_556 .
O6 Mn1 O2 92.56(6) . .
O7 Mn1 O2 171.95(6) 2_546 .
O3 Mn1 O2 88.98(6) 2_656 .
O9 Mn1 Mn2 132.02(6) 1_554 2_656
O4 Mn1 Mn2 41.16(5) 2_556 2_656
O6 Mn1 Mn2 141.93(5) . 2_656
O7 Mn1 Mn2 86.58(5) 2_546 2_656
O3 Mn1 Mn2 41.91(5) 2_656 2_656
O2 Mn1 Mn2 88.26(4) . 2_656
O9 Mn1 K1 101.83(5) 1_554 1_445
O4 Mn1 K1 82.42(5) 2_556 1_445
O6 Mn1 K1 42.32(6) . 1_445
O7 Mn1 K1 47.62(5) 2_546 1_445
O3 Mn1 K1 137.71(6) 2_656 1_445
O2 Mn1 K1 130.09(5) . 1_445
Mn2 Mn1 K1 113.91(4) 2_656 1_445
O9 Mn1 K1 37.58(6) 1_554 2
O4 Mn1 K1 148.34(5) 2_556 2
O6 Mn1 K1 50.17(5) . 2
O7 Mn1 K1 83.35(5) 2_546 2
O3 Mn1 K1 125.73(5) 2_656 2
O2 Mn1 K1 102.98(4) . 2
Mn2 Mn1 K1 163.970(17) 2_656 2
K1 Mn1 K1 67.39(3) 1_445 2
O8 Mn2 O4 102.27(6) . 1_655
O8 Mn2 O10 97.48(7) . 2_666
O4 Mn2 O10 92.26(7) 1_655 2_666
O8 Mn2 O3 164.99(7) . .
O4 Mn2 O3 85.38(6) 1_655 .
O10 Mn2 O3 95.07(7) 2_666 .
O8 Mn2 O1 84.99(7) . .
O4 Mn2 O1 164.18(7) 1_655 .
O10 Mn2 O1 100.79(7) 2_666 .
O3 Mn2 O1 84.61(6) . .
O8 Mn2 O1 82.74(6) . 2_656
O4 Mn2 O1 84.82(6) 1_655 2_656
O10 Mn2 O1 177.05(6) 2_666 2_656
O3 Mn2 O1 85.15(6) . 2_656
O1 Mn2 O1 82.16(6) . 2_656
O8 Mn2 Mn1 141.81(5) . 2_656
O4 Mn2 Mn1 41.25(5) 1_655 2_656
O10 Mn2 Mn1 95.27(5) 2_666 2_656
O3 Mn2 Mn1 44.13(5) . 2_656
O1 Mn2 Mn1 127.50(5) . 2_656
O1 Mn2 Mn1 82.83(4) 2_656 2_656
O8 Mn2 K1 40.14(6) . .
O4 Mn2 K1 116.76(5) 1_655 .
O10 Mn2 K1 60.80(5) 2_666 .
O3 Mn2 K1 146.11(5) . .
O1 Mn2 K1 77.83(5) . .
O1 Mn2 K1 120.22(5) 2_656 .
Mn1 Mn2 K1 149.99(2) 2_656 .
O8 Mn2 K1 133.48(5) . 2_666
O4 Mn2 K1 113.29(5) 1_655 2_666
O10 Mn2 K1 53.78(6) 2_666 2_666
O3 Mn2 K1 50.97(5) . 2_666
O1 Mn2 K1 68.88(5) . 2_666
O1 Mn2 K1 127.92(5) 2_656 2_666
Mn1 Mn2 K1 82.15(4) 2_656 2_666
K1 Mn2 K1 95.41(5) . 2_666
O8 V2 O6 109.89(10) . 1_655
O8 V2 O3 112.53(9) . 2_656
O6 V2 O3 110.04(9) 1_655 2_656
O8 V2 O5 107.60(9) . .
O6 V2 O5 112.20(9) 1_655 .
O3 V2 O5 104.50(9) 2_656 .
O8 V2 K1 134.81(7) . 1_545
O6 V2 K1 47.68(6) 1_655 1_545
O3 V2 K1 62.87(6) 2_656 1_545
O5 V2 K1 117.16(6) . 1_545
O8 V2 K1 43.57(6) . .
O6 V2 K1 134.77(7) 1_655 .
O3 V2 K1 114.25(6) 2_656 .
O5 V2 K1 65.02(6) . .
K1 V2 K1 176.51(3) 1_545 .
O8 V2 K1 128.23(6) . 2_655
O6 V2 K1 48.46(6) 1_655 2_655
O3 V2 K1 119.08(7) 2_656 2_655
O5 V2 K1 63.86(7) . 2_655
K1 V2 K1 71.15(3) 1_545 2_655
K1 V2 K1 112.31(3) . 2_655
O10 V3 O1 106.93(10) . .
O10 V3 O4 111.79(9) . .
O1 V3 O4 109.89(9) . .
O10 V3 O2 108.43(9) . .
O1 V3 O2 108.69(8) . .
O4 V3 O2 110.97(9) . .
O10 V3 K1 56.00(6) . .
O1 V3 K1 84.38(7) . .
O4 V3 K1 164.35(6) . .
O2 V3 K1 68.45(7) . .
O10 V3 K1 58.04(7) . 2_666
O1 V3 K1 71.28(7) . 2_666
O4 V3 K1 82.99(8) . 2_666
O2 V3 K1 164.32(6) . 2_666
K1 V3 K1 96.15(5) . 2_666
O7 V1 O9 107.40(10) . .
O7 V1 O5 108.65(10) . 1_556
O9 V1 O5 104.64(10) . 1_556
O7 V1 O2 112.46(9) . 2_556
O9 V1 O2 108.31(9) . 2_556
O5 V1 O2 114.85(9) 1_556 2_556
O7 V1 K1 97.08(8) . 2_556
O9 V1 K1 43.43(7) . 2_556
O5 V1 K1 145.00(6) 1_556 2_556
O2 V1 K1 74.18(6) 2_556 2_556
O7 V1 K1 44.53(7) . 2_656
O9 V1 K1 137.74(7) . 2_656
O5 V1 K1 69.42(8) 1_556 2_656
O2 V1 K1 111.94(6) 2_556 2_656
K1 V1 K1 141.35(4) 2_556 2_656
O8 K1 O6 135.70(7) . 1_665
O8 K1 O9 112.21(7) . 2_556
O6 K1 O9 109.09(6) 1_665 2_556
O8 K1 O7 71.00(6) . 2_656
O6 K1 O7 66.40(6) 1_665 2_656
O9 K1 O7 143.56(7) 2_556 2_656
O8 K1 O3 147.36(6) . 2_666
O6 K1 O3 58.06(7) 1_665 2_666
O9 K1 O3 77.19(6) 2_556 2_666
O7 K1 O3 120.76(6) 2_656 2_666
O8 K1 O6 104.49(6) . 2
O6 K1 O6 82.33(6) 1_665 2
O9 K1 O6 60.53(5) 2_556 2
O7 K1 O6 83.24(5) 2_656 2
O3 K1 O6 107.05(5) 2_666 2
O8 K1 O10 87.57(6) . .
O6 K1 O10 109.98(6) 1_665 .
O9 K1 O10 87.17(7) 2_556 .
O7 K1 O10 129.03(6) 2_656 .
O3 K1 O10 61.04(5) 2_666 .
O6 K1 O10 147.69(6) 2 .
O8 K1 O5 56.35(6) . .
O6 K1 O5 137.93(6) 1_665 .
O9 K1 O5 63.21(5) 2_556 .
O7 K1 O5 95.13(5) 2_656 .
O3 K1 O5 140.20(6) 2_666 .
O6 K1 O5 57.31(5) 2 .
O10 K1 O5 110.74(5) . .
O8 K1 O10 63.05(6) . 2_666
O6 K1 O10 92.22(6) 1_665 2_666
O9 K1 O10 143.25(5) 2_556 2_666
O7 K1 O10 72.14(6) 2_656 2_666
O3 K1 O10 90.35(5) 2_666 2_666
O6 K1 O10 154.85(5) 2 2_666
O10 K1 O10 56.98(7) . 2_666
O5 K1 O10 118.78(5) . 2_666
O8 K1 V2 155.14(5) . 1_565
O6 K1 V2 28.29(4) 1_665 1_565
O9 K1 V2 91.82(5) 2_556 1_565
O7 K1 V2 93.70(4) 2_656 1_565
O3 K1 V2 29.98(4) 2_666 1_565
O6 K1 V2 92.57(4) 2 1_565
O10 K1 V2 87.38(4) . 1_565
O5 K1 V2 147.14(5) . 1_565
O10 K1 V2 94.05(4) 2_666 1_565
O8 K1 V2 26.21(4) . .
O6 K1 V2 149.12(5) 1_665 .
O9 K1 V2 87.88(5) 2_556 .
O7 K1 V2 84.50(4) 2_656 .
O3 K1 V2 152.81(4) 2_666 .
O6 K1 V2 84.26(4) 2 .
O10 K1 V2 96.07(4) . .
O5 K1 V2 30.55(4) . .
O10 K1 V2 88.25(4) 2_666 .
V2 K1 V2 176.51(3) 1_565 .
O8 K1 V1 102.49(5) . 2_556
O6 K1 V1 121.77(4) 1_665 2_556
O9 K1 V1 25.44(4) 2_556 2_556
O7 K1 V1 164.88(5) 2_656 2_556
O3 K1 V1 72.22(5) 2_666 2_556
O6 K1 V1 85.36(4) 2 2_556
O10 K1 V1 62.62(4) . 2_556
O5 K1 V1 70.27(3) . 2_556
O10 K1 V1 117.83(4) 2_666 2_556
V2 K1 V1 96.71(3) 1_565 2_556
V2 K1 V1 84.50(3) . 2_556
V3 O1 Mn2 134.27(10) . .
V3 O1 Mn2 123.39(10) . 2_656
Mn2 O1 Mn2 97.84(6) . 2_656
V1 O2 V3 126.47(10) 2_556 .
V1 O2 Mn1 117.49(9) 2_556 .
V3 O2 Mn1 115.19(8) . .
V2 O3 Mn2 123.88(10) 2_656 .
V2 O3 Mn1 129.03(9) 2_656 2_656
Mn2 O3 Mn1 93.95(6) . 2_656
V2 O3 K1 87.15(8) 2_656 2_666
Mn2 O3 K1 95.95(6) . 2_666
Mn1 O3 K1 124.85(7) 2_656 2_666
V3 O4 Mn2 129.35(9) . 1_455
V3 O4 Mn1 132.58(10) . 2_556
Mn2 O4 Mn1 97.59(7) 1_455 2_556
V1 O5 V2 130.36(11) 1_554 .
V1 O5 K1 134.09(8) 1_554 .
V2 O5 K1 84.43(7) . .
V2 O6 Mn1 138.97(11) 1_455 .
V2 O6 K1 104.03(9) 1_455 1_445
Mn1 O6 K1 104.24(7) . 1_445
V2 O6 K1 107.46(7) 1_455 2
Mn1 O6 K1 97.53(6) . 2
K1 O6 K1 97.67(6) 1_445 2
V1 O7 Mn1 144.61(11) . 2_546
V1 O7 K1 111.34(9) . 2_656
Mn1 O7 K1 97.89(6) 2_546 2_656
V2 O8 Mn2 129.12(9) . .
V2 O8 K1 110.22(9) . .
Mn2 O8 K1 108.71(8) . .
V1 O9 Mn1 135.78(11) . 1_556
V1 O9 K1 111.13(10) . 2_556
Mn1 O9 K1 113.08(8) 1_556 2_556
V3 O10 Mn2 164.34(11) . 2_666
V3 O10 K1 98.26(8) . .
Mn2 O10 K1 93.22(6) 2_666 .
V3 O10 K1 97.12(7) . 2_666
Mn2 O10 K1 85.35(6) 2_666 2_666
K1 O10 K1 123.02(7) . 2_666
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mn1 O9 2.122(2) 1_554
Mn1 O4 2.142(2) 2_556
Mn1 O6 2.147(2) .
Mn1 O7 2.160(2) 2_546
Mn1 O3 2.248(2) 2_656
Mn1 O2 2.306(2) .
Mn1 Mn2 3.2202(15) 2_656
Mn1 K1 3.778(2) 1_445
Mn1 K1 3.9834(19) 2
Mn2 O8 2.094(2) .
Mn2 O4 2.138(2) 1_655
Mn2 O10 2.143(2) 2_666
Mn2 O3 2.156(2) .
Mn2 O1 2.184(2) .
Mn2 O1 2.293(2) 2_656
Mn2 K1 3.8347(16) .
Mn2 K1 3.9285(18) 2_666
V2 O8 1.672(2) .
V2 O6 1.6817(18) 1_655
V2 O3 1.7227(18) 2_656
V2 O5 1.8145(18) .
V2 K1 3.443(3) 1_545
V2 K1 3.553(3) .
V2 K1 3.9323(18) 2_655
V3 O10 1.663(2) .
V3 O1 1.6830(18) .
V3 O4 1.7144(18) .
V3 O2 1.8400(19) .
V3 K1 3.7892(16) .
V3 K1 3.9280(17) 2_666
V1 O7 1.643(2) .
V1 O9 1.6498(19) .
V1 O5 1.758(2) 1_556
V1 O2 1.8364(18) 2_556
V1 K1 3.583(3) 2_556
V1 K1 3.742(2) 2_656
K1 O8 2.610(2) .
K1 O6 2.624(2) 1_665
K1 O9 2.641(2) 2_556
K1 O7 2.817(3) 2_656
K1 O3 3.068(2) 2_666
K1 O6 3.086(2) 2
K1 O10 3.174(2) .
K1 O5 3.236(3) .
K1 O10 3.359(2) 2_666
