#------------------------------------------------------------------------------
#$Date: 2020-04-16 09:32:54 +0300 (Thu, 16 Apr 2020) $
#$Revision: 250840 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/10/85/2108596.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108596
loop_
_publ_author_name
'Dudek, Marta K.'
'Paluch, Piotr'
'Pindelska, Edyta'
_publ_section_title
;
 Crystal structures of two furazidin polymorphs revealed by a joint effort
 of crystal structure prediction and NMR crystallography
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S205252062000373X
_journal_volume                  76
_journal_year                    2020
_chemical_formula_sum            'C10 H8 N4 O5'
_chemical_formula_weight         264.2
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_creation_date             2019-12-19T12:58
_audit_creation_method           'created in GSAS-II'
_cell_angle_alpha                90
_cell_angle_beta                 106.848(14)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.670(7)
_cell_length_b                   11.4666(12)
_cell_length_c                   8.494(4)
_cell_measurement_temperature    300
_cell_volume                     1087.8(8)
_computing_structure_refinement
'GSAS-II (Toby & Von Dreele, J. Appl. Cryst. 46, 544-549, 2013)'
_diffrn_ambient_pressure         100
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type  'Bruker D8 with LYNXEYE detector'
_diffrn_radiation_polarisn_ratio 0.7000
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_exptl_crystal_density_diffrn    1.6132
_exptl_crystal_description       powder
_pd_calc_method                  'Rietveld Refinement'
_pd_meas_number_of_points        1921
_pd_proc_ls_background_function
;
Background function: "chebyschev" function with 24 terms:
    6.39(6), -11.28(29), -1.7(8), 1.0(22), 209.4(24), 78(4), 
    -2446.0(10), -1372.6(11), 20455.6(21), 11208(3), -117679.9(15), 
    -34269(4), 414751.5(7), 26568.1(15), -893273.9(17), 87213.0(23), 
    1.1848209(23)e6, -251999(5), -945917.0(18), 281839(4), 417242.8(5), 
    -151823.0(10), -78161(3), 32564(7), 
;
_pd_proc_ls_prof_R_factor        0.07059
_pd_proc_ls_prof_wR_expected     0.31599
_pd_proc_ls_prof_wR_factor       0.09592
_refine_ls_goodness_of_fit_all   0.306
_refine_ls_matrix_type           full
_refine_ls_number_parameters     32
_refine_ls_R_Fsqd_factor         0.04496
_refine_ls_wR_factor_obs         0.09592
_reflns_d_resolution_high        1.552
_reflns_d_resolution_low         11.169
_reflns_limit_h_max              2
_reflns_limit_h_min              2
_reflns_limit_k_max              3
_reflns_limit_k_min              3
_reflns_limit_l_max              -5
_reflns_limit_l_min              -5
_reflns_number_total             308
_cod_data_source_file            xk5066sup1.cif
_cod_data_source_block           furazidin_formII
_cod_original_cell_volume        1087.80(18)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2108596
_refine_ls_r_f_factor            0.05249
_gsas_proc_ls_prof_r_b_factor    0.08841
_gsas_proc_ls_prof_wr_b_factor   0.11867
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,1/2+y,1/2-z
3 -x,-y,-z
4 x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
H1 H 0.82787 -0.06253 1.00513 1.000 Uiso 0.010 4
H5 H 0.84740 0.19903 1.07817 1.000 Uiso 0.010 4
H9 H 0.68180 0.04856 0.80219 1.000 Uiso 0.010 4
H13 H 0.39344 0.37273 0.39885 1.000 Uiso 0.010 4
H17 H 0.59001 0.09301 0.52272 1.000 Uiso 0.010 4
H21 H 0.49048 0.07430 0.64569 1.000 Uiso 0.010 4
H25 H 0.99900 -0.18311 1.23761 1.000 Uiso 0.010 4
H29 H 1.18276 -0.11085 1.50229 1.000 Uiso 0.010 4
C1 C 1.10762 0.05823 1.41747 1.000 Uiso 0.010 4
C5 C 0.96242 0.00211 1.20938 1.000 Uiso 0.010 4
C9 C 1.02283 -0.09617 1.28110 1.000 Uiso 0.010 4
C13 C 0.86302 0.01664 1.06979 1.000 Uiso 0.010 4
C17 C 0.81292 0.11971 1.01347 1.000 Uiso 0.010 4
C21 C 0.71606 0.12834 0.86814 1.000 Uiso 0.010 4
C25 C 0.53259 0.33898 0.61528 1.000 Uiso 0.010 4
C29 C 0.43200 0.19445 0.44159 1.000 Uiso 0.010 4
C33 C 0.52767 0.13693 0.57693 1.000 Uiso 0.010 4
C37 C 1.11655 -0.05989 1.41512 1.000 Uiso 0.010 4
N1 N 0.67265 0.22973 0.81809 1.000 Uiso 0.010 4
N5 N 0.58263 0.23383 0.67964 1.000 Uiso 0.010 4
N9 N 0.44356 0.31104 0.47203 1.000 Uiso 0.010 4
N13 N 1.17586 0.13997 1.52647 1.000 Uiso 0.010 4
O1 O 1.01514 0.09787 1.29468 1.000 Uiso 0.010 4
O5 O 1.26275 0.10219 1.63454 1.000 Uiso 0.010 4
O9 O 1.14515 0.24256 1.50909 1.000 Uiso 0.010 4
O13 O 0.56028 0.43441 0.67232 1.000 Uiso 0.010 4
O17 O 0.36065 0.14639 0.32818 1.000 Uiso 0.010 4
loop_
_atom_type_symbol
_atom_type_number_in_cell
C 40
H 32
N 16
O 20
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_wavelength_id
1.54050 1.0 1
1.54430 0.5000 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C37 C1 N13 130.432 1_555 1_555 1_555 yes
C37 C1 O1 111.923 1_555 1_555 1_555 yes
N13 C1 O1 117.625 1_555 1_555 1_555 yes
C9 C5 C13 131.449 1_555 1_555 1_555 yes
C9 C5 O1 109.328 1_555 1_555 1_555 yes
C13 C5 O1 119.214 1_555 1_555 1_555 yes
H25 C9 C5 124.159 1_555 1_555 1_555 yes
H25 C9 C37 128.531 1_555 1_555 1_555 yes
C5 C9 C37 107.31 1_555 1_555 1_555 yes
H1 C13 C5 115.348 1_555 1_555 1_555 yes
H1 C13 C17 119.802 1_555 1_555 1_555 yes
C5 C13 C17 124.841 1_555 1_555 1_555 yes
H5 C17 C13 120.056 1_555 1_555 1_555 yes
H5 C17 C21 118.114 1_555 1_555 1_555 yes
C13 C17 C21 121.822 1_555 1_555 1_555 yes
H9 C21 C17 118.189 1_555 1_555 1_555 yes
H9 C21 N1 122.557 1_555 1_555 1_555 yes
C17 C21 N1 119.251 1_555 1_555 1_555 yes
N5 C25 N9 105.567 1_555 1_555 1_555 yes
N5 C25 O13 126.973 1_555 1_555 1_555 yes
N9 C25 O13 127.458 1_555 1_555 1_555 yes
C33 C29 N9 105.961 1_555 1_555 1_555 yes
C33 C29 O17 126.661 1_555 1_555 1_555 yes
N9 C29 O17 127.372 1_555 1_555 1_555 yes
H17 C33 H21 109.84 1_555 1_555 1_555 yes
H17 C33 C29 108.566 1_555 1_555 1_555 yes
H21 C33 C29 112.046 1_555 1_555 1_555 yes
H17 C33 N5 112.139 1_555 1_555 1_555 yes
H21 C33 N5 111.035 1_555 1_555 1_555 yes
C29 C33 N5 103.056 1_555 1_555 1_555 yes
H29 C37 C1 125.073 1_555 1_555 1_555 yes
H29 C37 C9 129.608 1_555 1_555 1_555 yes
C1 C37 C9 105.312 1_555 1_555 1_555 yes
C21 N1 N5 117.189 1_555 1_555 1_555 yes
C25 N5 C33 111.713 1_555 1_555 1_555 yes
C25 N5 N1 121.01 1_555 1_555 1_555 yes
C33 N5 N1 127.253 1_555 1_555 1_555 yes
H13 N9 C25 122.056 1_555 1_555 1_555 yes
H13 N9 C29 124.317 1_555 1_555 1_555 yes
C25 N9 C29 113.627 1_555 1_555 1_555 yes
C1 N13 O5 116.533 1_555 1_555 1_555 yes
C1 N13 O9 118.324 1_555 1_555 1_555 yes
O5 N13 O9 125.141 1_555 1_555 1_555 yes
C1 O1 C5 106.127 1_555 1_555 1_555 yes
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
H1 C13 1.07861 1_555 1_555 yes
H5 C17 1.07841 1_555 1_555 yes
H9 C21 1.08658 1_555 1_555 yes
H13 N9 1.00905 1_555 1_555 yes
H17 C33 1.09043 1_555 1_555 yes
H21 C33 1.09186 1_555 1_555 yes
H25 C9 1.07152 1_555 1_555 yes
H29 C37 1.07475 1_555 1_555 yes
C1 C37 1.35902 1_555 1_555 yes
C1 N13 1.39366 1_555 1_555 yes
C1 O1 1.34416 1_555 1_555 yes
C5 C9 1.37447 1_555 1_555 yes
C5 C13 1.40776 1_555 1_555 yes
C5 O1 1.36047 1_555 1_555 yes
C9 H25 1.07152 1_555 1_555 yes
C9 C5 1.37447 1_555 1_555 yes
C9 C37 1.394 1_555 1_555 yes
C13 H1 1.07861 1_555 1_555 yes
C13 C5 1.40776 1_555 1_555 yes
C13 C17 1.34354 1_555 1_555 yes
C17 H5 1.07841 1_555 1_555 yes
C17 C13 1.34354 1_555 1_555 yes
C17 C21 1.41503 1_555 1_555 yes
C21 H9 1.08658 1_555 1_555 yes
C21 C17 1.41503 1_555 1_555 yes
C21 N1 1.29002 1_555 1_555 yes
C25 N5 1.3814 1_555 1_555 yes
C25 N9 1.38913 1_555 1_555 yes
C25 O13 1.20243 1_555 1_555 yes
C29 C33 1.50301 1_555 1_555 yes
C29 N9 1.3609 1_555 1_555 yes
C29 O17 1.20831 1_555 1_555 yes
C33 H17 1.09043 1_555 1_555 yes
C33 H21 1.09186 1_555 1_555 yes
C33 C29 1.50301 1_555 1_555 yes
C33 N5 1.44316 1_555 1_555 yes
C37 H29 1.07475 1_555 1_555 yes
C37 C1 1.35902 1_555 1_555 yes
C37 C9 1.394 1_555 1_555 yes
N1 C21 1.29002 1_555 1_555 yes
N1 N5 1.33144 1_555 1_555 yes
N5 C25 1.3814 1_555 1_555 yes
N5 C33 1.44316 1_555 1_555 yes
N5 N1 1.33144 1_555 1_555 yes
N9 H13 1.00905 1_555 1_555 yes
N9 C25 1.38913 1_555 1_555 yes
N9 C29 1.3609 1_555 1_555 yes
N13 C1 1.39366 1_555 1_555 yes
N13 O5 1.23248 1_555 1_555 yes
N13 O9 1.22612 1_555 1_555 yes
O1 C1 1.34416 1_555 1_555 yes
O1 C5 1.36047 1_555 1_555 yes
O5 N13 1.23248 1_555 1_555 yes
O9 N13 1.22612 1_555 1_555 yes
O13 C25 1.20243 1_555 1_555 yes
O17 C29 1.20831 1_555 1_555 yes
loop_
_pd_meas_2theta_scan
_pd_meas_intensity_total
_pd_calc_intensity_total
_pd_proc_intensity_bkg_calc
_pd_proc_ls_weight
2.92870 14.13 10.7920159 10.7900777 0.0707714
2.95840 12.76 10.5702553 10.5682952 0.0783699
2.98810 11.59 10.354609 10.3526266 0.0862813
3.01780 10.29 10.1451696 10.1431645 0.0971817
3.04750 9.71 9.9420059 9.9399777 0.1029866
3.07710 9.38 9.745817 9.7437654 0.1066098
3.10680 9.07 9.5553039 9.5532284 0.1102536
3.13650 8.71 9.3711478 9.3690479 0.1148106
3.16620 8.68 9.1933391 9.1912144 0.1152074
3.19590 8.29 9.021852 9.0197021 0.1206273
3.22550 8.39 8.857192 8.8550165 0.1191895
3.25520 8.22 8.6981928 8.6959911 0.1216545
3.28490 8.04 8.545355 8.5431266 0.1243781
3.31460 7.77 8.3986011 8.3963456 0.1287001
3.34430 7.59 8.2578436 8.2555605 0.1317523
3.37390 7.82 8.1234301 8.1211188 0.1278772
3.40360 7.43 7.9943475 7.9920075 0.1345895
3.43330 7.76 7.8709476 7.8685783 0.128866
3.46300 7.51 7.7531115 7.7507124 0.1331558
3.49270 7.32 7.6407146 7.6382851 0.136612
3.52230 7.31 7.5339792 7.5315187 0.1367989
3.55200 7.37 7.4320505 7.4295584 0.1356852
3.58170 7.1 7.3351607 7.3326363 0.1408451
3.61140 7.13 7.2431691 7.2406118 0.1402525
3.64110 7.15 7.1559328 7.153342 0.1398601
3.67070 6.97 7.0735777 7.0709527 0.143472
3.70040 6.98 6.9954014 6.9927415 0.1432665
3.73010 6.92 6.9215426 6.918847 0.1445087
3.75980 7.02 6.8518537 6.8491217 0.1424501
3.78950 7.03 6.7861868 6.7834177 0.1422475
3.81910 6.79 6.7245963 6.7217893 0.1472754
3.84880 6.7 6.6665196 6.6636738 0.1492537
3.87850 6.64 6.6120253 6.6091399 0.1506024
3.90820 6.75 6.5609687 6.5580429 0.1481481
3.93790 6.51 6.5132068 6.5102397 0.1536098
3.96750 6.47 6.4691696 6.4657341 0.1545595
3.99720 6.41 6.4277809 6.4240865 0.1560062
4.02690 6.45 6.389058 6.3853155 0.1550388
4.05660 6.55 6.3530779 6.3492861 0.1526718
4.08630 6.5 6.3197084 6.3158664 0.1538462
4.11590 6.53 6.2889202 6.2850269 0.1531394
4.14560 6.38 6.260379 6.2564332 0.1567398
4.17530 6.4 6.2340693 6.2300699 0.15625
4.20500 6.46 6.2098708 6.2058165 0.1547988
4.23470 6.44 6.187666 6.1835557 0.1552795
4.26430 6.28 6.1674063 6.1632388 0.1592357
4.29400 6.57 6.1488443 6.1446182 0.152207
4.32370 6.3 6.1319442 6.1276582 0.1587302
4.35340 6.24 6.1168383 6.1122546 0.1602564
4.38310 6.23 6.1030729 6.0983068 0.1605136
4.41270 6.23 6.0905903 6.085758 0.1605136
4.44240 6.21 6.0793302 6.0744298 0.1610306
4.47210 6.16 6.0692467 6.0642765 0.1623377
4.50180 6.34 6.0602531 6.0552115 0.1577287
4.53150 6.08 6.052266 6.0471514 0.1644737
4.56110 6.27 6.0452279 6.0400387 0.1594896
4.59080 6.33 6.039015 6.0337491 0.1579779
4.62050 6.11 6.0335795 6.028235 0.1636661
4.65020 6.06 6.0288516 6.0234265 0.1650165
4.67990 6.3 6.0247647 6.0192571 0.1587302
4.70950 5.91 6.0212666 6.0156746 0.1692047
4.73920 6.09 6.0182738 6.0125948 0.1642036
4.76890 6.09 6.015742 6.0099739 0.1642036
4.79860 6.07 6.0136174 6.0077578 0.1647446
4.82830 6.14 6.0118492 6.0058957 0.1628664
4.85790 5.96 6.0103939 6.0043442 0.1677852
4.88760 6 6.0091968 6.0030481 0.1666667
4.91730 6.08 6.0082211 6.0019706 0.1644737
4.94700 6.11 6.0074273 6.0010722 0.1636661
4.97670 6.11 6.0067788 6.0003161 0.1636661
5.00630 5.97 6.0062428 5.9996699 0.1675042
5.03600 5.95 6.0057843 5.9990976 0.1680672
5.06570 6.12 6.0053759 5.9985722 0.1633987
5.09540 6.02 6.0049908 5.9980665 0.166113
5.12510 6.02 6.0046045 5.997556 0.166113
5.15470 6.02 6.0041958 5.99702 0.166113
5.18440 6.09 6.003742 5.9964344 0.1642036
5.21410 5.92 6.0032261 5.9957828 0.1689189
5.24380 5.85 6.002632 5.9950486 0.1709402
5.27350 5.95 6.0019452 5.9942174 0.1680672
5.30310 5.86 6.0011562 5.9932798 0.1706485
5.33280 5.83 6.0002489 5.9922186 0.1715266
5.36250 5.98 5.9992166 5.9910274 0.1672241
5.39220 5.98 5.9980519 5.9896985 0.1672241
5.42190 5.94 5.9967489 5.9882257 0.1683502
5.45150 6.1 5.9953079 5.9866099 0.1639344
5.48120 5.92 5.9937163 5.9848366 0.1689189
5.51090 5.92 5.9919767 5.9829091 0.1689189
5.54060 5.9 5.9900885 5.9808264 0.1694915
5.57030 5.89 5.9880523 5.9785885 0.1697793
5.59990 5.95 5.9858773 5.9762053 0.1680672
5.62960 5.77 5.9835514 5.9736628 0.1733102
5.65930 5.93 5.9811422 5.9709721 0.1686341
5.68900 5.97 5.9785694 5.9681373 0.1675042
5.71870 5.9 5.9758383 5.9651634 0.1694915
5.74830 5.88 5.9729932 5.9620668 0.170068
5.77800 6.03 5.9700217 5.9588329 0.1658375
5.80770 5.89 5.9669408 5.9554791 0.1697793
5.83740 5.8 5.9637589 5.952013 0.1724138
5.86710 5.88 5.9604846 5.9484428 0.170068
5.89670 5.88 5.9571389 5.9447896 0.170068
5.92640 5.81 5.9537089 5.941038 0.172117
5.95610 5.7 5.950216 5.9372095 0.1754386
5.98580 5.75 5.9479867 5.9333139 0.173913
6.01550 5.89 5.9444086 5.9293615 0.1697793
6.04510 5.93 5.9414735 5.925376 0.1686341
6.07480 5.86 5.9378519 5.9213412 0.1706485
6.10450 5.94 5.9342241 5.9172812 0.1683502
6.13420 5.9 5.9306024 5.9132067 0.1694915
6.16390 6.01 5.9269991 5.9091289 0.1663894
6.19350 5.92 5.9234386 5.9050723 0.1689189
6.22320 5.97 5.9199095 5.9010205 0.1675042
6.25290 5.86 5.9164367 5.8969984 0.1706485
6.28260 5.88 5.913033 5.8930169 0.170068
6.31230 5.88 5.9097115 5.8890868 0.170068
6.34190 6.12 5.906496 5.8852319 0.1633987
6.37160 5.95 5.9033779 5.8814369 0.1680672
6.40130 5.85 5.9003815 5.8777253 0.1709402
6.43100 5.76 5.8975203 5.8741076 0.1736111
6.46070 5.84 5.8948078 5.8705938 0.1712329
6.49030 6.01 5.8922658 5.8672052 0.1663894
6.52000 6.02 5.8898911 5.8639286 0.166113
6.54970 6.13 5.8877065 5.8607851 0.1631321
6.57940 6 5.8857263 5.8577838 0.1666667
6.60910 5.76 5.883965 5.8549337 0.1736111
6.63870 6.11 5.8824422 5.8522522 0.1636661
6.66840 6 5.881163 5.8497294 0.1666667
6.69810 5.94 5.8801488 5.8473827 0.1683502
6.72780 5.97 5.8794161 5.8452197 0.1675042
6.75750 5.93 5.8789823 5.8432476 0.1686341
6.78710 5.99 5.8788656 5.8414792 0.1669449
6.81680 5.92 5.8790847 5.8399091 0.1689189
6.84650 6.09 5.8796614 5.8385497 0.1642036
6.87620 5.92 5.8806184 5.8374071 0.1689189
6.90590 6.05 5.8819806 5.8364866 0.1652893
6.93550 6.1 5.8837685 5.8357955 0.1639344
6.96520 5.95 5.8860247 5.8353336 0.1680672
6.99490 6.03 5.8890542 5.8351083 0.1658375
7.02460 5.88 5.8923452 5.8351234 0.170068
7.05430 6.06 5.8963553 5.8353827 0.1650165
7.08390 6.14 5.9008435 5.8358872 0.1628664
7.11360 6.06 5.9060376 5.8366432 0.1650165
7.14330 6.12 5.9119944 5.8376519 0.1633987
7.17300 6.15 5.9187978 5.8389156 0.1626016
7.20270 5.99 5.9265485 5.8404358 0.1669449
7.23230 6.09 5.9353369 5.8422078 0.1642036
7.26200 5.81 5.9500391 5.8442444 0.172117
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57.59930 3.88 3.9339737 1.4048991 0.257732
57.62900 3.69 3.9275146 1.4102324 0.2710027
57.65870 3.74 3.9285548 1.4158678 0.2673797
57.68830 3.75 3.9298855 1.4217845 0.2666667
57.71800 3.87 3.9253835 1.4280221 0.2583979
57.74770 3.63 3.9097925 1.4345607 0.2754821
57.77740 3.77 3.8803777 1.4414001 0.265252
57.80710 3.75 3.8368449 1.44854 0.2666667
57.83670 3.6 3.7799488 1.4559543 0.2777778
57.86640 3.67 3.7106979 1.4636931 0.2724796
57.89610 3.61 3.631685 1.4717316 0.2770083
57.92580 3.44 3.5468024 1.4800695 0.2906977
57.95550 3.61 3.4609099 1.488707 0.2770083
57.98510 3.48 3.3791034 1.4976133 0.2873563
58.01480 3.5 3.3046746 1.5068489 0.2857143
58.04450 3.54 3.240479 1.5163842 0.2824859
58.07420 3.51 3.1878242 1.5262196 0.2849003
58.10390 3.51 3.1467443 1.5363556 0.2849003
58.13350 3.45 3.1160414 1.5467571 0.2898551
58.16320 3.64 3.0933236 1.557495 0.2747253
58.19290 3.49 3.0764329 1.5685357 0.286533
58.22260 3.47 3.0638324 1.5798802 0.2881844
58.25230 3.47 3.0551011 1.5915296 0.2881844
58.28190 3.48 3.0505074 1.6034446 0.2873563
58.31160 3.49 3.0502897 1.6157074 0.286533
58.34130 3.57 3.0544192 1.6282799 0.280112
58.37100 3.51 3.0626369 1.6411642 0.2849003
58.40070 3.64 3.0746121 1.6543625 0.2747253
58.43030 3.6 3.08974 1.6678313 0.2777778
58.46000 3.45 3.1071488 1.6816642 0.2898551
58.48970 3.57 3.1255408 1.6958193 0.280112
58.51940 3.42 3.1439022 1.7102998 0.2923977
58.54910 3.66 3.1617779 1.7251092 0.273224
58.57870 3.66 3.1789753 1.7401997 0.273224
58.60840 3.53 3.1951539 1.7556772 0.2832861
58.63810 3.54 3.2091837 1.7714957 0.2824859
58.66780 3.61 3.2198121 1.7876598 0.2770083
58.69750 3.52 3.2265034 1.8041743 0.2840909
58.72710 3.51 3.2300183 1.820987 0.2849003
58.75680 3.44 3.2322072 1.8382169 0.2906977
58.78650 3.47 3.2351678 1.8558137 0.2881844
58.81620 3.56 3.2402732 1.8737834 0.2808989
58.84590 3.48 3.2481064 1.8921323 0.2873563
58.87550 3.38 3.2588793 1.9108033 0.295858
58.90520 3.41 3.2731068 1.9299293 0.2932551
58.93490 3.37 3.2915698 1.9494552 0.2967359
58.96460 3.48 3.3150052 1.9693884 0.2873563
58.99430 3.36 3.3433463 1.9897364 0.297619
59.02390 3.43 3.3750007 2.0104367 0.2915452
59.05360 3.28 3.4077125 2.031637 0.304878
59.08330 3.35 3.4377646 2.0532766 0.2985075
59.11300 3.41 3.461784 2.0753639 0.2932551
59.14270 3.4 3.4778106 2.0979075 0.2941176
59.17230 3.37 3.4853934 2.1208381 0.2967359
59.20200 3.39 3.4855414 2.1443193 0.2949853
59.23170 3.25 3.4795857 2.1682836 0.3076923
59.26140 3.3 3.4685708 2.1927398 0.3030303
59.29110 3.26 3.4530087 2.217697 0.3067485
59.32070 3.33 3.4332404 2.2430775 0.3003003
59.35040 3.16 3.4095305 2.2690616 0.3164557
59.38010 3.18 3.3827067 2.2955733 0.3144654
59.40980 3.3 3.3538409 2.3226211 0.3030303
59.43950 3.16 3.3240933 2.3502131 0.3164557
59.46910 3.16 3.2944852 2.3782618 0.3164557
59.49880 3.19 3.2653929 2.4069643 0.3134796
59.52850 3.19 3.237418 2.4362338 0.3134796
59.55820 3.15 3.2110288 2.4660769 0.3174603
59.58790 3.01 3.1868231 2.4964998 0.3322259
59.61750 3.23 3.1655484 2.5274023 0.3095975
59.64720 2.98 3.1475823 2.5589977 0.3355705
59.67690 3.1 3.1333997 2.5911863 0.3225806
59.70660 3.12 3.1232857 2.6239707 0.3205128
59.73630 3.09 3.1174129 2.6573523 0.3236246
59.76590 3.18 3.1158365 2.691216 0.3144654
59.79560 3.12 3.1184624 2.7257896 0.3205128
59.82530 3.17 3.1251013 2.760957 0.3154574
59.85500 3.09 3.1354616 2.7967139 0.3236246
59.88470 3.13 3.1492154 2.8330543 0.3194888
59.91430 3.14 3.1659617 2.8698449 0.3184713
