#------------------------------------------------------------------------------
#$Date: 2020-04-16 09:32:54 +0300 (Thu, 16 Apr 2020) $
#$Revision: 250840 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/10/85/2108597.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108597
loop_
_publ_author_name
'Dudek, Marta K.'
'Paluch, Piotr'
'Pindelska, Edyta'
_publ_section_title
;
 Crystal structures of two furazidin polymorphs revealed by a joint effort
 of crystal structure prediction and NMR crystallography
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S205252062000373X
_journal_volume                  76
_journal_year                    2020
_chemical_formula_sum            'C20 H16 N8 O10'
_chemical_formula_weight         528.39
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             2019-12-19T13:42
_audit_creation_method           'created in GSAS-II'
_cell_angle_alpha                51.074(3)
_cell_angle_beta                 92.16(3)
_cell_angle_gamma                97.31(11)
_cell_formula_units_Z            2
_cell_length_a                   22.183(22)
_cell_length_b                   12.546(7)
_cell_length_c                   5.3092(16)
_cell_measurement_temperature    300
_cell_volume                     1138.5(14)
_computing_structure_refinement
'GSAS-II (Toby & Von Dreele, J. Appl. Cryst. 46, 544-549, 2013)'
_diffrn_ambient_pressure         100
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type  'Bruker D8 with LYNXEYE detector'
_diffrn_radiation_polarisn_ratio 0.7000
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_exptl_crystal_density_diffrn    1.5414
_exptl_crystal_description       powder
_pd_calc_method                  'Rietveld Refinement'
_pd_meas_number_of_points        1921
_pd_proc_ls_background_function
;
Background function: "chebyschev" function with 24 terms:
    4846.854, -11028.729, -20160.862, 256317.539, 592987.724, 
    -5.249158441e6, -3.631253229e6, 4.6716624983e7, 2.478157997e6, 
    -2.22566966249e8, 5.3300222852e7, 6.38125053237e8, -2.55142761173e8, 
    -1.156971410908e9, 5.82828782201e8, 1.333696204767e9, -7.80463244314e8, 
    -9.38678820304e8, 6.25995183217e8, 3.54965933309e8, -2.79499578917e8, 
    -4.3505635500e7, 5.3561337350e7, -6.779782588e6, 
;
_pd_proc_ls_prof_R_factor        0.07305
_pd_proc_ls_prof_wR_expected     0.01291
_pd_proc_ls_prof_wR_factor       0.13230
_refine_ls_goodness_of_fit_all   10.274
_refine_ls_matrix_type           full
_refine_ls_number_parameters     10
_refine_ls_R_Fsqd_factor         0.00000
_refine_ls_wR_factor_obs         0.13230
_reflns_d_resolution_high        1.524
_reflns_d_resolution_low         21.970
_reflns_limit_h_max              9
_reflns_limit_h_min              9
_reflns_limit_k_max              -7
_reflns_limit_k_min              -7
_reflns_limit_l_max              -2
_reflns_limit_l_min              -2
_reflns_number_total             681
_cod_data_source_file            xk5066sup1.cif
_cod_data_source_block           furazidin_formI
_cod_original_cell_volume        1138.5(4)
_cod_database_code               2108597
_refine_ls_r_f_factor            0.00000
_gsas_proc_ls_prof_r_b_factor    0.09494
_gsas_proc_ls_prof_wr_b_factor   0.14168
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,-z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
H1 H 0.73437 0.64832 0.61697 1.000 Uiso 0.010 2
H3 H 0.62066 0.52561 0.48475 1.000 Uiso 0.010 2
H5 H 0.63637 0.70515 0.70368 1.000 Uiso 0.010 2
H7 H 0.39286 0.75947 0.76895 1.000 Uiso 0.010 2
H9 H 0.56380 0.71649 1.02060 1.000 Uiso 0.010 2
H11 H 0.57257 0.86694 0.60450 1.000 Uiso 0.010 2
H13 H 0.67816 0.42391 0.32840 1.000 Uiso 0.010 2
H15 H 0.78138 0.35187 0.24815 1.000 Uiso 0.010 2
C1 C 0.82279 0.46783 0.40575 1.000 Uiso 0.010 2
C3 C 0.74039 0.52654 0.46840 1.000 Uiso 0.010 2
C5 C 0.72384 0.44947 0.36647 1.000 Uiso 0.010 2
C7 C 0.70785 0.59186 0.54957 1.000 Uiso 0.010 2
C9 C 0.64674 0.58407 0.54803 1.000 Uiso 0.010 2
C11 C 0.61283 0.64767 0.63013 1.000 Uiso 0.010 2
C13 C 0.45912 0.67848 0.67324 1.000 Uiso 0.010 2
C15 C 0.48324 0.81449 0.82113 1.000 Uiso 0.010 2
C17 C 0.54189 0.77530 0.78740 1.000 Uiso 0.010 2
C19 C 0.77679 0.41206 0.32570 1.000 Uiso 0.010 2
N1 N 0.55450 0.63368 0.61499 1.000 Uiso 0.010 2
N3 N 0.52151 0.69179 0.69055 1.000 Uiso 0.010 2
N5 N 0.43833 0.75280 0.75654 1.000 Uiso 0.010 2
N7 N 0.88518 0.46110 0.41877 1.000 Uiso 0.010 2
O1 O 0.80179 0.53803 0.49165 1.000 Uiso 0.010 2
O3 O 0.90364 0.39190 0.35136 1.000 Uiso 0.010 2
O5 O 0.91767 0.52278 0.49571 1.000 Uiso 0.010 2
O7 O 0.42825 0.61607 0.60001 1.000 Uiso 0.010 2
O9 O 0.47708 0.88773 0.89374 1.000 Uiso 0.010 2
H17 H 0.04669 0.90902 0.96963 1.000 Uiso 0.010 2
H19 H 0.10363 0.76403 0.75563 1.000 Uiso 0.010 2
H21 H 0.15591 0.92637 0.99388 1.000 Uiso 0.010 2
H23 H 0.40287 0.90144 0.95446 1.000 Uiso 0.010 2
H25 H 0.24945 1.06139 0.86481 1.000 Uiso 0.010 2
H27 H 0.24527 0.90839 1.27639 1.000 Uiso 0.010 2
H29 H 0.00265 0.69269 0.64518 1.000 Uiso 0.010 2
H31 H -0.11852 0.68967 0.59237 1.000 Uiso 0.010 2
C21 C -0.10609 0.80451 0.77935 1.000 Uiso 0.010 2
C23 C -0.00865 0.81021 0.81570 1.000 Uiso 0.010 2
C25 C -0.02653 0.73908 0.69938 1.000 Uiso 0.010 2
C27 C 0.04779 0.85095 0.88210 1.000 Uiso 0.010 2
C29 C 0.10147 0.82288 0.84010 1.000 Uiso 0.010 2
C31 C 0.15694 0.86719 0.90797 1.000 Uiso 0.010 2
C33 C 0.31258 0.84759 0.89330 1.000 Uiso 0.010 2
C35 C 0.33497 0.98019 1.05233 1.000 Uiso 0.010 2
C37 C 0.26695 0.96216 1.03632 1.000 Uiso 0.010 2
C39 C -0.08910 0.73637 0.67384 1.000 Uiso 0.010 2
N9 N 0.20693 0.83653 0.86463 1.000 Uiso 0.010 2
N11 N 0.25843 0.88000 0.92881 1.000 Uiso 0.010 2
N13 N 0.35739 0.90881 0.96795 1.000 Uiso 0.010 2
N15 N -0.16289 0.83235 0.80984 1.000 Uiso 0.010 2
O11 O -0.05809 0.84979 0.86689 1.000 Uiso 0.010 2
O13 O -0.20670 0.79634 0.71446 1.000 Uiso 0.010 2
O15 O -0.16667 0.89097 0.92750 1.000 Uiso 0.010 2
O17 O 0.31939 0.77775 0.81175 1.000 Uiso 0.010 2
O19 O 0.36417 1.04487 1.12393 1.000 Uiso 0.010 2
loop_
_atom_type_symbol
_atom_type_number_in_cell
C 40
H 32
N 16
O 20
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_wavelength_id
1.54050 1.0 1
1.54430 0.5000 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C19 C1 N7 131.106 1_555 1_555 1_555 yes
C19 C1 O1 111.839 1_555 1_555 1_555 yes
N7 C1 O1 117.038 1_555 1_555 1_555 yes
C5 C3 C7 134.101 1_555 1_555 1_555 yes
C5 C3 O1 109.435 1_555 1_555 1_555 yes
C7 C3 O1 116.464 1_555 1_555 1_555 yes
H13 C5 C3 125.354 1_555 1_555 1_555 yes
H13 C5 C19 127.272 1_555 1_555 1_555 yes
C3 C5 C19 107.374 1_555 1_555 1_555 yes
H1 C7 C3 116.82 1_555 1_555 1_555 yes
H1 C7 C9 120.819 1_555 1_555 1_555 yes
C3 C7 C9 122.356 1_555 1_555 1_555 yes
H3 C9 C7 120.134 1_555 1_555 1_555 yes
H3 C9 C11 116.188 1_555 1_555 1_555 yes
C7 C9 C11 123.672 1_555 1_555 1_555 yes
H5 C11 C9 119.676 1_555 1_555 1_555 yes
H5 C11 N1 122.828 1_555 1_555 1_555 yes
C9 C11 N1 117.495 1_555 1_555 1_555 yes
N3 C13 N5 105.705 1_555 1_555 1_555 yes
N3 C13 O7 127.975 1_555 1_555 1_555 yes
N5 C13 O7 126.319 1_555 1_555 1_555 yes
C17 C15 N5 106.775 1_555 1_555 1_555 yes
C17 C15 O9 126.879 1_555 1_555 1_555 yes
N5 C15 O9 126.346 1_555 1_555 1_555 yes
H9 C17 H11 109.402 1_555 1_555 1_555 yes
H9 C17 C15 110.123 1_555 1_555 1_555 yes
H11 C17 C15 110.441 1_555 1_555 1_555 yes
H9 C17 N3 112.349 1_555 1_555 1_555 yes
H11 C17 N3 112.096 1_555 1_555 1_555 yes
C15 C17 N3 102.255 1_555 1_555 1_555 yes
H15 C19 C1 126.564 1_555 1_555 1_555 yes
H15 C19 C5 128.088 1_555 1_555 1_555 yes
C1 C19 C5 105.348 1_555 1_555 1_555 yes
C11 N1 N3 118.95 1_555 1_555 1_555 yes
C13 N3 C17 111.706 1_555 1_555 1_555 yes
C13 N3 N1 119.565 1_555 1_555 1_555 yes
C17 N3 N1 128.71 1_555 1_555 1_555 yes
H7 N5 C13 122.941 1_555 1_555 1_555 yes
H7 N5 C15 123.529 1_555 1_555 1_555 yes
C13 N5 C15 113.529 1_555 1_555 1_555 yes
C1 N7 O3 116.476 1_555 1_555 1_555 yes
C1 N7 O5 118.547 1_555 1_555 1_555 yes
O3 N7 O5 124.977 1_555 1_555 1_555 yes
C1 O1 C3 106.003 1_555 1_555 1_555 yes
C39 C21 N15 131.144 1_555 1_555 1_555 yes
C39 C21 O11 111.9 1_555 1_555 1_555 yes
N15 C21 O11 116.955 1_555 1_555 1_555 yes
C25 C23 C27 134.363 1_555 1_555 1_555 yes
C25 C23 O11 109.899 1_555 1_555 1_555 yes
C27 C23 O11 115.72 1_555 1_555 1_555 yes
H29 C25 C23 126.248 1_555 1_555 1_555 yes
H29 C25 C39 126.794 1_555 1_555 1_555 yes
C23 C25 C39 106.941 1_555 1_555 1_555 yes
H17 C27 C23 116.428 1_555 1_555 1_555 yes
H17 C27 C29 119.78 1_555 1_555 1_555 yes
C23 C27 C29 123.789 1_555 1_555 1_555 yes
H19 C29 C27 121.082 1_555 1_555 1_555 yes
H19 C29 C31 117.375 1_555 1_555 1_555 yes
C27 C29 C31 121.539 1_555 1_555 1_555 yes
H21 C31 C29 118.714 1_555 1_555 1_555 yes
H21 C31 N9 122.561 1_555 1_555 1_555 yes
C29 C31 N9 118.725 1_555 1_555 1_555 yes
N11 C33 N13 106.558 1_555 1_555 1_555 yes
N11 C33 O17 126.455 1_555 1_555 1_555 yes
N13 C33 O17 126.987 1_555 1_555 1_555 yes
C37 C35 N13 106.3 1_555 1_555 1_555 yes
C37 C35 O19 126.98 1_555 1_555 1_555 yes
N13 C35 O19 126.719 1_555 1_555 1_555 yes
H25 C37 H27 108.787 1_555 1_555 1_555 yes
H25 C37 C35 112.057 1_555 1_555 1_555 yes
H27 C37 C35 109.642 1_555 1_555 1_555 yes
H25 C37 N11 111.487 1_555 1_555 1_555 yes
H27 C37 N11 112.44 1_555 1_555 1_555 yes
C35 C37 N11 102.349 1_555 1_555 1_555 yes
H31 C39 C21 126.816 1_555 1_555 1_555 yes
H31 C39 C25 127.654 1_555 1_555 1_555 yes
C21 C39 C25 105.524 1_555 1_555 1_555 yes
C31 N9 N11 117.485 1_555 1_555 1_555 yes
C33 N11 C37 111.818 1_555 1_555 1_555 yes
C33 N11 N9 119.72 1_555 1_555 1_555 yes
C37 N11 N9 128.461 1_555 1_555 1_555 yes
H23 N13 C33 121.648 1_555 1_555 1_555 yes
H23 N13 C35 125.396 1_555 1_555 1_555 yes
C33 N13 C35 112.943 1_555 1_555 1_555 yes
C21 N15 O13 116.843 1_555 1_555 1_555 yes
C21 N15 O15 118.694 1_555 1_555 1_555 yes
O13 N15 O15 124.462 1_555 1_555 1_555 yes
C21 O11 C23 105.729 1_555 1_555 1_555 yes
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
H1 C7 1.08279 1_555 1_555 yes
H3 C9 1.08301 1_555 1_555 yes
H5 C11 1.09 1_555 1_555 yes
H7 N5 1.03077 1_555 1_555 yes
H7 O17 1.71715 1_555 1_555 yes
H9 C17 1.10062 1_555 1_555 yes
H11 C17 1.08436 1_555 1_555 yes
H13 C5 1.07435 1_555 1_555 yes
H15 C19 1.07865 1_555 1_555 yes
C1 C19 1.36784 1_555 1_555 yes
C1 N7 1.39371 1_555 1_555 yes
C1 O1 1.35121 1_555 1_555 yes
C3 C5 1.38376 1_555 1_555 yes
C3 C7 1.41272 1_555 1_555 yes
C3 O1 1.36049 1_555 1_555 yes
C5 H13 1.07435 1_555 1_555 yes
C5 C3 1.38376 1_555 1_555 yes
C5 C19 1.39047 1_555 1_555 yes
C7 H1 1.08279 1_555 1_555 yes
C7 C3 1.41272 1_555 1_555 yes
C7 C9 1.34676 1_555 1_555 yes
C9 H3 1.08301 1_555 1_555 yes
C9 C7 1.34676 1_555 1_555 yes
C9 C11 1.41667 1_555 1_555 yes
C11 H5 1.09 1_555 1_555 yes
C11 C9 1.41667 1_555 1_555 yes
C11 N1 1.28976 1_555 1_555 yes
C13 N3 1.37922 1_555 1_555 yes
C13 N5 1.38583 1_555 1_555 yes
C13 O7 1.20809 1_555 1_555 yes
C15 C17 1.50256 1_555 1_555 yes
C15 N5 1.3494 1_555 1_555 yes
C15 O9 1.22175 1_555 1_555 yes
C17 H9 1.10062 1_555 1_555 yes
C17 H11 1.08436 1_555 1_555 yes
C17 C15 1.50256 1_555 1_555 yes
C17 N3 1.45104 1_555 1_555 yes
C19 H15 1.07865 1_555 1_555 yes
C19 C1 1.36784 1_555 1_555 yes
C19 C5 1.39047 1_555 1_555 yes
N1 C11 1.28976 1_555 1_555 yes
N1 N3 1.32413 1_555 1_555 yes
N3 C13 1.37922 1_555 1_555 yes
N3 C17 1.45104 1_555 1_555 yes
N3 N1 1.32413 1_555 1_555 yes
N5 H7 1.03077 1_555 1_555 yes
N5 C13 1.38583 1_555 1_555 yes
N5 C15 1.3494 1_555 1_555 yes
N7 C1 1.39371 1_555 1_555 yes
N7 O3 1.24152 1_555 1_555 yes
N7 O5 1.23222 1_555 1_555 yes
O1 C1 1.35121 1_555 1_555 yes
O1 C3 1.36049 1_555 1_555 yes
O3 N7 1.24152 1_555 1_555 yes
O5 N7 1.23222 1_555 1_555 yes
O7 C13 1.20809 1_555 1_555 yes
O9 C15 1.22175 1_555 1_555 yes
O9 H23 1.73916 1_555 1_555 yes
H17 C27 1.08529 1_555 1_555 yes
H19 C29 1.08409 1_555 1_555 yes
H21 C31 1.09102 1_555 1_555 yes
H23 O9 1.73916 1_555 1_555 yes
H23 N13 1.03409 1_555 1_555 yes
H25 C37 1.09611 1_555 1_555 yes
H27 C37 1.09283 1_555 1_555 yes
H29 C25 1.0773 1_555 1_555 yes
H31 C39 1.07538 1_555 1_555 yes
C21 C39 1.37341 1_555 1_555 yes
C21 N15 1.39077 1_555 1_555 yes
C21 O11 1.34657 1_555 1_555 yes
C23 C25 1.38534 1_555 1_555 yes
C23 C27 1.4084 1_555 1_555 yes
C23 O11 1.36158 1_555 1_555 yes
C25 H29 1.0773 1_555 1_555 yes
C25 C23 1.38534 1_555 1_555 yes
C25 C39 1.38767 1_555 1_555 yes
C27 H17 1.08529 1_555 1_555 yes
C27 C23 1.4084 1_555 1_555 yes
C27 C29 1.3479 1_555 1_555 yes
C29 H19 1.08409 1_555 1_555 yes
C29 C27 1.3479 1_555 1_555 yes
C29 C31 1.41343 1_555 1_555 yes
C31 H21 1.09102 1_555 1_555 yes
C31 C29 1.41343 1_555 1_555 yes
C31 N9 1.29198 1_555 1_555 yes
C33 N11 1.37157 1_555 1_555 yes
C33 N13 1.37601 1_555 1_555 yes
C33 O17 1.22205 1_555 1_555 yes
C35 C37 1.50414 1_555 1_555 yes
C35 N13 1.37268 1_555 1_555 yes
C35 O19 1.20754 1_555 1_555 yes
C37 H25 1.09611 1_555 1_555 yes
C37 H27 1.09283 1_555 1_555 yes
C37 C35 1.50414 1_555 1_555 yes
C37 N11 1.45111 1_555 1_555 yes
C39 H31 1.07538 1_555 1_555 yes
C39 C21 1.37341 1_555 1_555 yes
C39 C25 1.38767 1_555 1_555 yes
N9 C31 1.29198 1_555 1_555 yes
N9 N11 1.32842 1_555 1_555 yes
N11 C33 1.37157 1_555 1_555 yes
N11 C37 1.45111 1_555 1_555 yes
N11 N9 1.32842 1_555 1_555 yes
N13 H23 1.03409 1_555 1_555 yes
N13 C33 1.37601 1_555 1_555 yes
N13 C35 1.37268 1_555 1_555 yes
N15 C21 1.39077 1_555 1_555 yes
N15 O13 1.24243 1_555 1_555 yes
N15 O15 1.23895 1_555 1_555 yes
O11 C21 1.34657 1_555 1_555 yes
O11 C23 1.36158 1_555 1_555 yes
O13 N15 1.24243 1_555 1_555 yes
O15 N15 1.23895 1_555 1_555 yes
O17 H7 1.71715 1_555 1_555 yes
O17 C33 1.22205 1_555 1_555 yes
O19 C35 1.20754 1_555 1_555 yes
loop_
_pd_meas_2theta_scan
_pd_meas_intensity_total
_pd_calc_intensity_total
_pd_proc_intensity_bkg_calc
_pd_proc_ls_weight
3.02010 8790 7210.0809 7188.5848 0.0001137656
3.04980 7892 6965.4974 6942.556 0.0001267106
3.07950 7341 6739.1569 6714.6041 0.0001362212
3.10910 6775 6530.6117 6504.2611 0.0001476015
3.13880 6342 6337.398 6309.019 0.000157679
3.16850 5958 6159.2561 6128.585 0.0001678416
3.19820 5875 5995.2585 5961.9838 0.0001702128
3.22790 5702 5844.5422 5808.2935 0.0001753771
3.25750 5460 5706.7554 5667.1012 0.0001831502
3.28720 5446 5580.2388 5536.6329 0.000183621
3.31690 5310 5464.8199 5416.6097 0.0001883239
3.34660 5318 5359.9171 5306.3 0.0001880406
3.37630 5224 5265.0362 5205.0144 0.0001914242
3.40590 5057 5180.0563 5112.4032 0.0001977457
3.43560 5041 5104.1368 5027.2313 0.0001983733
3.46530 5031 5037.4762 4949.2506 0.0001987676
3.49500 4972 4980.1948 4877.9209 0.0002011263
3.52470 4912 4932.7405 4812.7352 0.0002035831
3.55430 4916 4896.4625 4753.409 0.0002034174
3.58400 4710 4872.384 4699.0963 0.0002123142
3.61370 4782 4863.5045 4649.5889 0.0002091175
3.64340 4711 4874.4084 4604.4955 0.0002122692
3.67310 4761 4911.482 4563.4503 0.0002100399
3.70270 4603 4982.6975 4526.2314 0.0002172496
3.73240 4572 5097.1106 4492.2691 0.0002187227
3.76210 4688 5256.9741 4461.398 0.0002133106
3.79180 4781 5440.6532 4433.3411 0.0002091613
3.82150 4645 5578.2333 4407.8409 0.0002152853
3.85110 4615 5576.4204 4384.7324 0.0002166847
3.88080 4716 5420.1309 4363.6383 0.0002120441
3.91050 4785 5192.8289 4344.4346 0.0002089864
3.94020 4757 4975.891 4326.931 0.0002102165
3.96990 4877 4800.7557 4310.9518 0.0002050441
3.99950 5271 4668.6986 4296.382 0.0001897173
4.02920 5062 4570.4113 4282.9744 0.0001975504
4.05890 5234 4497.3227 4270.6431 0.0001910585
4.08860 4945 4442.0525 4259.2626 0.0002022245
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55.19750 2090 2080.1479 2006.6892 0.0004784689
55.22720 2100 2092.4374 2004.3094 0.0004761905
55.25690 2083 2078.8728 2001.9368 0.0004800768
55.28660 2098 2049.969 1999.5731 0.0004766444
55.31630 2093 2075.2632 1997.2199 0.0004777831
55.34590 2055 2120.6672 1994.8867 0.000486618
55.37560 2086 2119.8879 1992.5594 0.0004793864
55.40530 2101 2174.774 1990.2473 0.0004759638
55.43500 2055 2252.1251 1987.9522 0.000486618
55.46470 2040 2148.7541 1985.6756 0.0004901961
55.49430 2065 2051.7998 1983.4266 0.0004842615
55.52400 2122 2029.1406 1981.1917 0.0004712535
55.55370 2120 2053.7404 1978.9799 0.0004716981
55.58340 2177 2098.9413 1976.7928 0.0004593477
55.61310 2202 2043.7007 1974.632 0.0004541326
55.64270 2184 2080.5528 1972.506 0.0004578755
55.67240 2316 2446.6535 1970.4019 0.0004317789
55.70210 2302 2284.628 1968.3284 0.0004344049
55.73180 2185 2002.3172 1966.2869 0.0004576659
55.76150 2295 2093.0124 1964.2788 0.0004357298
55.79110 2244 2382.4684 1962.3119 0.0004456328
55.82080 2254 2462.6963 1960.3744 0.0004436557
55.85050 2155 2278.4359 1958.4741 0.0004640371
55.88020 2143 2017.2516 1956.6123 0.0004666356
55.90990 2091 2081.5644 1954.7902 0.0004782401
55.93950 2097 2177.5404 1953.0149 0.0004768717
55.96920 2082 2091.8311 1951.2755 0.0004803074
55.99890 2116 2044.1526 1949.5791 0.0004725898
56.02860 2058 2035.9207 1947.9267 0.0004859086
56.05830 2019 2064.349 1946.3193 0.0004952947
56.08790 2041 2023.6723 1944.763 0.0004899559
56.11760 2049 2047.0713 1943.248 0.0004880429
56.14730 2006 2011.461 1941.7806 0.0004985045
56.17700 1978 1992.1684 1940.3615 0.0005055612
56.20670 1953 1984.3291 1938.9914 0.0005120328
56.23630 2013 1965.9066 1937.6753 0.000496771
56.26600 1961 1986.2162 1936.4048 0.0005099439
56.29570 1974 1970.6607 1935.185 0.0005065856
56.32540 2001 1970.0821 1934.0164 0.0004997501
56.35510 2007 2004.535 1932.8992 0.0004982561
56.38470 1925 1960.4199 1931.8374 0.0005194805
56.41440 1887 1932.4748 1930.8239 0.0005299417
56.44410 1873 1930.2834 1929.8628 0.0005339028
56.47380 1861 1938.9819 1928.9539 0.0005373455
56.50350 1978 1969.2771 1928.0975 0.0005055612
56.53310 2020 1999.5669 1927.2961 0.0004950495
56.56280 2097 2063.6142 1926.5441 0.0004768717
56.59250 1994 2069.6697 1925.8443 0.0005015045
56.62220 2035 2031.9507 1925.1962 0.0004914005
56.65190 2042 2047.584 1924.5998 0.000489716
56.68150 2094 2078.9819 1924.0562 0.0004775549
56.71120 2135 2127.2857 1923.5614 0.0004683841
56.74090 2156 2148.7432 1923.1168 0.0004638219
56.77060 2084 2028.357 1922.7217 0.0004798464
56.80030 2082 2099.5558 1922.3755 0.0004803074
56.82990 2028 2116.6389 1922.0783 0.0004930966
56.85960 2099 2042.314 1921.8274 0.0004764173
56.88930 1979 2115.8795 1921.6228 0.0005053057
56.91900 2101 2029.8153 1921.4637 0.0004759638
56.94870 2085 1991.7255 1921.349 0.0004796163
56.97830 2020 2046.7445 1921.2777 0.0004950495
57.00800 1995 1997.0665 1921.2483 0.0005012531
57.03770 1981 1976.8449 1921.2598 0.0005047956
57.06740 1968 1969.504 1921.3108 0.0005081301
57.09710 1930 1931.2328 1921.4001 0.0005181347
57.12670 1938 1946.9766 1921.5257 0.0005159959
57.15640 1956 1954.1067 1921.6869 0.0005112474
57.18610 1953 1940.1137 1921.8819 0.0005120328
57.21580 1932 1939.4902 1922.109 0.0005175983
57.24550 2000 1974.0946 1922.3666 0.0005
57.27510 2040 2056.4978 1922.652 0.0004901961
57.30480 1919 1980.0726 1922.9653 0.0005211047
57.33450 1978 1974.0974 1923.3037 0.0005055612
57.36420 1978 2050.1596 1923.6655 0.0005055612
57.39390 1980 1989.6869 1924.0487 0.0005050505
57.42350 1969 1991.3762 1924.45 0.000507872
57.45320 2012 1962.6538 1924.8702 0.0004970179
57.48290 2078 1945.7908 1925.3058 0.000481232
57.51260 2054 2029.7936 1925.7549 0.0004868549
57.54230 1999 2053.6 1926.2153 0.0005002501
57.57190 2069 2029.0243 1926.6834 0.0004833253
57.60160 2033 2016.7275 1927.1603 0.0004918839
57.63130 1958 1993.1924 1927.6422 0.0005107252
57.66100 2004 1987.0544 1928.1269 0.000499002
57.69070 1976 2001.9099 1928.6124 0.0005060729
57.72030 1931 2016.7436 1929.0949 0.0005178664
57.75000 2045 2056.0792 1929.5753 0.0004889976
57.77970 2038 2003.3333 1930.0501 0.0004906771
57.80940 2040 1980.4326 1930.5169 0.0004901961
57.83910 1932 1964.3172 1930.9737 0.0005175983
57.86870 1987 1948.7382 1931.4168 0.0005032713
57.89840 1971 1969.135 1931.8472 0.0005073567
57.92810 1958 1957.9031 1932.2611 0.0005107252
57.95780 1869 1945.2216 1932.6567 0.0005350455
57.98750 1926 1947.0722 1933.0318 0.0005192108
58.01710 1980 1966.0303 1933.3833 0.0005050505
58.04680 1981 2008.7635 1933.7116 0.0005047956
58.07650 2003 1984.1776 1934.0136 0.0004992511
58.10620 1989 1984.2739 1934.2874 0.0005027652
58.13590 1967 1989.417 1934.5313 0.0005083884
58.16550 1968 1958.5598 1934.7428 0.0005081301
58.19520 1986 1985.191 1934.9216 0.0005035247
58.22490 1993 2000.3177 1935.0654 0.0005017561
58.25460 2046 2026.9911 1935.1725 0.0004887586
58.28430 1996 1998.2169 1935.2416 0.000501002
58.31390 2023 1983.052 1935.2711 0.0004943154
58.34360 1946 1992.7229 1935.26 0.0005138746
58.37330 2034 2002.8919 1935.2067 0.0004916421
58.40300 1955 1987.4132 1935.1101 0.000511509
58.43270 1980 1963.8117 1934.9691 0.0005050505
58.46230 1937 1957.3934 1934.7834 0.0005162623
58.49200 1967 1965.7596 1934.5509 0.0005083884
58.52170 1986 1976.513 1934.2712 0.0005035247
58.55140 2002 2011.5392 1933.9435 0.0004995005
58.58110 2012 1990.8051 1933.5673 0.0004970179
58.61070 1979 2006.5566 1933.1434 0.0005053057
58.64040 2045 2016.6227 1932.6686 0.0004889976
58.67010 1964 1989.8552 1932.1437 0.000509165
58.69980 2079 2043.0739 1931.5686 0.0004810005
58.72950 2030 2109.2299 1930.9428 0.0004926108
58.75910 2120 2143.935 1930.2687 0.0004716981
58.78880 2061 2065.9734 1929.5417 0.0004852014
58.81850 2214 2154.2832 1928.7638 0.0004516712
58.84820 2381 2530.4474 1927.9353 0.0004199916
58.87790 2457 2277.6261 1927.0562 0.0004070004
58.90750 2617 2312.8506 1926.1298 0.0003821169
58.93720 2754 2987.3832 1925.1502 0.0003631082
58.96690 2584 2550.7639 1924.1207 0.0003869969
58.99660 2416 2490.8065 1923.0415 0.0004139073
59.02630 2369 2491.5813 1921.913 0.000422119
59.05590 2340 2314.7968 1920.7394 0.0004273504
59.08560 2436 2404.5785 1919.5132 0.000410509
59.11530 2290 2367.8615 1918.2384 0.0004366812
59.14500 2186 2090.4094 1916.9154 0.0004574565
59.17470 2126 2097.6734 1915.5441 0.0004703669
59.20430 2038 2079.3444 1914.1297 0.0004906771
59.23400 2035 2008.4868 1912.6625 0.0004914005
59.26370 1937 1927.4383 1911.147 0.0005162623
59.29340 1859 1917.999 1909.5829 0.0005379236
59.32310 1904 1909.5909 1907.9698 0.0005252101
59.35270 1871 1906.5204 1906.3127 0.0005344735
59.38240 1882 1904.7267 1904.5995 0.0005313496
59.41210 1892 1903.4569 1902.8346 0.0005285412
59.44180 1902 1908.2136 1901.0164 0.0005257624
59.47150 1923 1916.7821 1899.1432 0.0005200208
59.50110 1921 1939.069 1897.2194 0.0005205622
59.53080 1951 1956.0391 1895.2295 0.0005125577
59.56050 1937 2025.2305 1893.1768 0.0005162623
59.59020 2057 2020.8349 1891.0578 0.0004861449
59.61990 2019 1992.9222 1888.8683 0.0004952947
59.64950 2008 2037.2782 1886.6115 0.000498008
59.67920 2010 1946.2036 1884.2668 0.0004975124
59.70890 1966 1927.7763 1881.8356 0.000508647
59.73860 1939 1956.8338 1879.3111 0.0005157298
59.76830 1963 1920.7907 1876.6856 0.0005094244
59.79790 1940 1942.345 1873.9599 0.0005154639
59.82760 1849 1912.5061 1871.1061 0.0005408329
59.85730 1797 1871.7723 1868.1224 0.000556483
59.88700 1827 1865.0456 1864.9973 0.0005473454
59.91670 1835 1861.7198 1861.7177 0.0005449591
59.94630 1715 1858.2829 1858.2813 0.0005830904
59.97600 1740 1854.6504 1854.6491 0.0005747126
60.00570 1787 1850.8165 1850.8154 0.0005595971

_cod_database_fobs_code 2108597
