#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/08/2200859.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2200859
loop_
_publ_author_name
'Flörke, Ulrich'
'Petters, Dina'
_publ_section_title
;
 Heptacarbonyl(α-ethoxybenzylidene)di-μ-diethylphosphidodirhenium
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m88
_journal_page_last               m89
_journal_paper_doi               10.1107/S1600536802002258
_journal_volume                  58
_journal_year                    2002
_chemical_formula_iupac          '[Re2 (C9 H10 O1) (C4 H10 P)2 (C O)7]'
_chemical_formula_moiety         'C24 H30 O8 P2 Re2'
_chemical_formula_sum            'C24 H30 O8 P2 Re2'
_chemical_formula_weight         880.82
_chemical_name_systematic
;
 Bis(μ-diethylphosphido)heptacarbonyl-
 α-ethoxybenzylidene-di-rhenium
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                73.040(10)
_cell_angle_beta                 78.820(10)
_cell_angle_gamma                88.590(10)
_cell_formula_units_Z            2
_cell_length_a                   8.425(2)
_cell_length_b                   10.5040(10)
_cell_length_c                   17.674(4)
_cell_measurement_reflns_used    29
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      23.679
_cell_measurement_theta_min      7.764
_cell_volume                     1466.8(5)
_computing_cell_refinement       XSCANS
_computing_data_collection       'XSCANS (Bruker, 1996)'
_computing_data_reduction        'SHELXTL (Bruker, 1998)'
_computing_molecular_graphics    SHELXTL
_computing_publication_material  SHELXTL
_computing_structure_refinement  SHELXTL
_computing_structure_solution    SHELXTL
_diffrn_ambient_temperature      200(2)
_diffrn_measured_fraction_theta_full .989
_diffrn_measured_fraction_theta_max .989
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_R_equivalents  .0227
_diffrn_reflns_av_sigmaI/netI    .0441
_diffrn_reflns_limit_h_max       1
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            8026
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         2.46
_diffrn_standards_decay_%        1
_diffrn_standards_interval_count 397
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    8.396
_exptl_absorpt_correction_T_max  .608
_exptl_absorpt_correction_T_min  .083
_exptl_absorpt_correction_type   '\y scan'
_exptl_absorpt_process_details   '(North et al., 1968)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.994
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    none
_exptl_crystal_description       needle
_exptl_crystal_F_000             836
_exptl_crystal_size_max          .38
_exptl_crystal_size_mid          .15
_exptl_crystal_size_min          .06
_refine_diff_density_max         .940
_refine_diff_density_min         -.822
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   .983
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     330
_refine_ls_number_reflns         6665
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      .983
_refine_ls_R_factor_all          .0556
_refine_ls_R_factor_gt           .0377
_refine_ls_shift/su_max          <0.001
_refine_ls_shift/su_mean         .000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0575P)²] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          .0868
_refine_ls_wR_factor_ref         .0958
_reflns_number_gt                5086
_reflns_number_total             6665
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            cf6148.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_database_code               2200859
_cod_database_fobs_code          2200859
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
Re1 -.00177(3) .37089(3) .358736(14) .02719(10) Uani d . 1 . . Re
Re2 .29648(3) .26519(2) .186324(13) .02267(9) Uani d . 1 . . Re
P1 .0457(2) .39188(17) .21057(9) .0229(3) Uani d . 1 . . P
P2 .2345(2) .22693(18) .33571(10) .0265(4) Uani d . 1 . . P
C1 .1543(10) .5263(8) .3305(5) .0409(18) Uani d . 1 . . C
O1 .2431(8) .6143(6) .3136(4) .0615(18) Uani d . 1 . . O
C2 -.0091(10) .3383(8) .4742(5) .0415(19) Uani d . 1 . . C
O2 -.0171(8) .3213(7) .5422(3) .0628(19) Uani d . 1 . . O
C3 -.1901(10) .4838(8) .3595(5) .045(2) Uani d . 1 . . C
O3 -.3029(8) .5454(7) .3635(5) .073(2) Uani d . 1 . . O
C4 -.1455(9) .2136(7) .3829(4) .0339(16) Uani d . 1 . . C
O4 -.2281(6) .1207(6) .3990(3) .0450(14) Uani d . 1 . . O
C5 .4216(8) .4263(7) .1823(4) .0291(15) Uani d . 1 . . C
O5 .4946(6) .5173(5) .1794(3) .0405(13) Uani d . 1 . . O
C6 .4908(8) .1617(7) .1847(4) .0292(15) Uani d . 1 . . C
O6 .6060(6) .0997(6) .1838(3) .0462(14) Uani d . 1 . . O
C7 .3244(9) .3250(7) .0684(4) .0335(16) Uani d . 1 . . C
O7 .3471(8) .3634(6) .0003(3) .0541(16) Uani d . 1 . . O
C8 .1666(8) .0945(7) .1907(4) .0265(14) Uani d . 1 . . C
O8 .0338(6) .0492(5) .2426(3) .0371(12) Uani d . 1 . . O
C9 -.0559(10) -.0722(8) .2430(5) .050(2) Uani d . 1 . . C
H9A -.1004 -.0545 .1932 .060 Uiso calc R 1 . . H
H9B .0185 -.1470 .2450 .060 Uiso calc R 1 . . H
C10 -.1868(11) -.1067(9) .3133(5) .053(2) Uani d . 1 . . C
H10A -.2426 -.1890 .3159 .080 Uiso calc R 1 . . H
H10B -.2635 -.0345 .3092 .080 Uiso calc R 1 . . H
H10C -.1423 -.1198 .3622 .080 Uiso calc R 1 . . H
C11 .2245(8) .0148(7) .1321(4) .0296(15) Uani d . 1 . . C
C12 .1800(10) .0474(8) .0582(4) .0400(18) Uani d . 1 . . C
H12 .1097 .1188 .0440 .048 Uiso calc R 1 . . H
C13 .2379(10) -.0239(9) .0043(5) .046(2) Uani d . 1 . . C
H13 .2057 -.0024 -.0464 .055 Uiso calc R 1 . . H
C14 .3422(10) -.1259(8) .0244(5) .043(2) Uani d . 1 . . C
H14 .3835 -.1736 -.0129 .051 Uiso calc R 1 . . H
C15 .3859(10) -.1583(8) .0976(5) .0416(19) Uani d . 1 . . C
H15 .4569 -.2293 .1112 .050 Uiso calc R 1 . . H
C16 .3277(9) -.0883(7) .1530(4) .0380(17) Uani d . 1 . . C
H16 .3586 -.1112 .2041 .046 Uiso calc R 1 . . H
C17 .0751(9) .5669(7) .1445(4) .0317(15) Uani d . 1 . . C
H17A .1675 .6080 .1570 .038 Uiso calc R 1 . . H
H17B .1061 .5649 .0879 .038 Uiso calc R 1 . . H
C18 -.0674(11) .6565(7) .1501(5) .047(2) Uani d . 1 . . C
H18A -.1542 .6261 .1292 .070 Uiso calc R 1 . . H
H18B -.0334 .7481 .1182 .070 Uiso calc R 1 . . H
H18C -.1067 .6533 .2066 .070 Uiso calc R 1 . . H
C19 -.1352(8) .3378(7) .1830(4) .0313(15) Uani d . 1 . . C
H19A -.1599 .2429 .2136 .038 Uiso calc R 1 . . H
H19B -.2276 .3895 .2004 .038 Uiso calc R 1 . . H
C20 -.1223(9) .3529(8) .0934(4) .0398(18) Uani d . 1 . . C
H20A -.2211 .3158 .0852 .060 Uiso calc R 1 . . H
H20B -.0287 .3051 .0746 .060 Uiso calc R 1 . . H
H20C -.1090 .4475 .0628 .060 Uiso calc R 1 . . H
C21 .4149(8) .2711(9) .3697(4) .0372(18) Uani d . 1 . . C
H21A .5053 .2165 .3536 .045 Uiso calc R 1 . . H
H21B .4463 .3654 .3404 .045 Uiso calc R 1 . . H
C22 .3971(11) .2533(10) .4593(4) .056(2) Uani d . 1 . . C
H22A .4998 .2780 .4704 .084 Uiso calc R 1 . . H
H22B .3680 .1600 .4895 .084 Uiso calc R 1 . . H
H22C .3120 .3104 .4760 .084 Uiso calc R 1 . . H
C23 .1916(9) .0525(7) .3982(4) .0346(16) Uani d . 1 . . C
H23A .1642 .0509 .4556 .042 Uiso calc R 1 . . H
H23B .0949 .0188 .3850 .042 Uiso calc R 1 . . H
C24 .3292(10) -.0431(8) .3886(5) .049(2) Uani d . 1 . . C
H24A .2955 -.1326 .4244 .074 Uiso calc R 1 . . H
H24B .4253 -.0124 .4027 .074 Uiso calc R 1 . . H
H24C .3548 -.0456 .3326 .074 Uiso calc R 1 . . H
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C .0033 .0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H .0000 .0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O .0106 .0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P .1023 .0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
C2 Re1 C3 92.9(4) ?
C2 Re1 C4 89.8(3) ?
C3 Re1 C4 89.9(3) ?
C2 Re1 C1 91.8(3) ?
C3 Re1 C1 92.8(3) ?
C4 Re1 C1 176.8(3) ?
C2 Re1 P2 96.0(3) ?
C3 Re1 P2 170.9(3) ?
C4 Re1 P2 88.3(2) ?
C1 Re1 P2 88.7(2) ?
C2 Re1 P1 171.2(3) ?
C3 Re1 P1 95.9(3) ?
C4 Re1 P1 90.6(2) ?
C1 Re1 P1 87.4(2) ?
P2 Re1 P1 75.23(5) y
C6 Re2 C7 93.4(3) ?
C6 Re2 C5 91.4(3) ?
C7 Re2 C5 89.8(3) ?
C6 Re2 C8 88.1(3) ?
C7 Re2 C8 90.3(3) ?
C5 Re2 C8 179.5(3) ?
C6 Re2 P2 95.78(19) ?
C7 Re2 P2 169.7(2) ?
C5 Re2 P2 85.28(19) ?
C8 Re2 P2 94.66(17) ?
C6 Re2 P1 171.38(19) ?
C7 Re2 P1 95.1(2) ?
C5 Re2 P1 87.2(2) ?
C8 Re2 P1 93.27(19) ?
P2 Re2 P1 75.63(6) y
C19 P1 C17 101.3(3) ?
C19 P1 Re2 116.5(2) ?
C17 P1 Re2 110.2(2) ?
C19 P1 Re1 111.1(2) ?
C17 P1 Re1 113.8(2) ?
Re2 P1 Re1 104.30(6) y
C23 P2 C21 101.7(4) ?
C23 P2 Re2 116.1(2) ?
C21 P2 Re2 110.0(2) ?
C23 P2 Re1 111.7(2) ?
C21 P2 Re1 113.2(3) ?
Re2 P2 Re1 104.40(6) y
O1 C1 Re1 179.3(7) ?
O2 C2 Re1 178.1(8) ?
O3 C3 Re1 176.7(8) ?
O4 C4 Re1 178.2(7) ?
O5 C5 Re2 178.9(6) ?
O6 C6 Re2 179.7(6) ?
O7 C7 Re2 176.5(7) ?
O8 C8 C11 115.4(6) ?
O8 C8 Re2 123.6(5) y
C11 C8 Re2 121.0(4) ?
C8 O8 C9 121.8(6) ?
C10 C9 O8 108.7(7) ?
C10 C9 H9A 109.9 ?
O8 C9 H9A 109.9 ?
C10 C9 H9B 109.9 ?
O8 C9 H9B 109.9 ?
H9A C9 H9B 108.3 ?
C9 C10 H10A 109.5 ?
C9 C10 H10B 109.5 ?
H10A C10 H10B 109.5 ?
C9 C10 H10C 109.5 ?
H10A C10 H10C 109.5 ?
H10B C10 H10C 109.5 ?
C12 C11 C16 120.3(7) ?
C12 C11 C8 120.7(7) ?
C16 C11 C8 119.0(6) ?
C11 C12 C13 120.0(8) ?
C11 C12 H12 120.0 ?
C13 C12 H12 120.0 ?
C14 C13 C12 120.0(8) ?
C14 C13 H13 120.0 ?
C12 C13 H13 120.0 ?
C15 C14 C13 120.1(7) ?
C15 C14 H14 120.0 ?
C13 C14 H14 120.0 ?
C14 C15 C16 120.8(8) ?
C14 C15 H15 119.6 ?
C16 C15 H15 119.6 ?
C11 C16 C15 118.9(7) ?
C11 C16 H16 120.6 ?
C15 C16 H16 120.6 ?
C18 C17 P1 117.0(5) ?
C18 C17 H17A 108.1 ?
P1 C17 H17A 108.1 ?
C18 C17 H17B 108.1 ?
P1 C17 H17B 108.1 ?
H17A C17 H17B 107.3 ?
C17 C18 H18A 109.5 ?
C17 C18 H18B 109.5 ?
H18A C18 H18B 109.5 ?
C17 C18 H18C 109.5 ?
H18A C18 H18C 109.5 ?
H18B C18 H18C 109.5 ?
C20 C19 P1 115.5(5) ?
C20 C19 H19A 108.4 ?
P1 C19 H19A 108.4 ?
C20 C19 H19B 108.4 ?
P1 C19 H19B 108.4 ?
H19A C19 H19B 107.5 ?
C19 C20 H20A 109.5 ?
C19 C20 H20B 109.5 ?
H20A C20 H20B 109.5 ?
C19 C20 H20C 109.5 ?
H20A C20 H20C 109.5 ?
H20B C20 H20C 109.5 ?
C22 C21 P2 116.6(5) ?
C22 C21 H21A 108.2 ?
P2 C21 H21A 108.2 ?
C22 C21 H21B 108.2 ?
P2 C21 H21B 108.2 ?
H21A C21 H21B 107.3 ?
C21 C22 H22A 109.5 ?
C21 C22 H22B 109.5 ?
H22A C22 H22B 109.5 ?
C21 C22 H22C 109.5 ?
H22A C22 H22C 109.5 ?
H22B C22 H22C 109.5 ?
C24 C23 P2 115.5(5) ?
C24 C23 H23A 108.4 ?
P2 C23 H23A 108.4 ?
C24 C23 H23B 108.4 ?
P2 C23 H23B 108.4 ?
H23A C23 H23B 107.5 ?
C23 C24 H24A 109.5 ?
C23 C24 H24B 109.5 ?
H24A C24 H24B 109.5 ?
C23 C24 H24C 109.5 ?
H24A C24 H24C 109.5 ?
H24B C24 H24C 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Re1 C2 . 1.956(8) ?
Re1 C3 . 1.958(9) ?
Re1 C4 . 1.966(8) ?
Re1 C1 . 2.004(8) ?
Re1 P2 . 2.5122(19) y
Re1 P1 . 2.5154(17) y
Re2 C6 . 1.943(7) ?
Re2 C7 . 1.962(7) ?
Re2 C5 . 1.993(7) ?
Re2 C8 . 2.098(7) y
Re2 P2 . 2.5023(17) y
Re2 P1 . 2.5024(18) y
P1 C19 . 1.837(7) ?
P1 C17 . 1.861(6) ?
P2 C23 . 1.846(7) ?
P2 C21 . 1.854(7) ?
C1 O1 . 1.136(9) ?
C2 O2 . 1.152(9) ?
C3 O3 . 1.139(10) ?
C4 O4 . 1.145(9) ?
C5 O5 . 1.132(8) ?
C6 O6 . 1.155(8) ?
C7 O7 . 1.130(8) ?
C8 O8 . 1.300(8) y
C8 C11 . 1.517(9) y
O8 C9 . 1.495(9) y
C9 C10 . 1.455(11) ?
C9 H9A . .990 ?
C9 H9B . .990 ?
C10 H10A . .980 ?
C10 H10B . .980 ?
C10 H10C . .980 ?
C11 C12 . 1.374(10) ?
C11 C16 . 1.382(10) ?
C12 C13 . 1.387(10) ?
C12 H12 . .950 ?
C13 C14 . 1.377(12) ?
C13 H13 . .950 ?
C14 C15 . 1.358(11) ?
C14 H14 . .950 ?
C15 C16 . 1.399(10) ?
C15 H15 . .950 ?
C16 H16 . .950 ?
C17 C18 . 1.513(11) ?
C17 H17A . .990 ?
C17 H17B . .990 ?
C18 H18A . .980 ?
C18 H18B . .980 ?
C18 H18C . .980 ?
C19 C20 . 1.529(9) ?
C19 H19A . .990 ?
C19 H19B . .990 ?
C20 H20A . .980 ?
C20 H20B . .980 ?
C20 H20C . .980 ?
C21 C22 . 1.518(9) ?
C21 H21A . .990 ?
C21 H21B . .990 ?
C22 H22A . .980 ?
C22 H22B . .980 ?
C22 H22C . .980 ?
C23 C24 . 1.532(10) ?
C23 H23A . .990 ?
C23 H23B . .990 ?
C24 H24A . .980 ?
C24 H24B . .980 ?
C24 H24C . .980 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C7 Re2 P1 C19 66.8(3)
C5 Re2 P1 C19 156.4(3)
C8 Re2 P1 C19 -23.8(3)
P2 Re2 P1 C19 -117.8(2)
C7 Re2 P1 C17 -47.8(3)
C5 Re2 P1 C17 41.7(3)
C8 Re2 P1 C17 -138.4(3)
P2 Re2 P1 C17 127.6(3)
C7 Re2 P1 Re1 -170.4(2)
C5 Re2 P1 Re1 -80.79(19)
C8 Re2 P1 Re1 99.03(17)
P2 Re2 P1 Re1 5.05(6)
C3 Re1 P1 C19 -56.9(4)
C4 Re1 P1 C19 33.1(3)
C1 Re1 P1 C19 -149.4(3)
P2 Re1 P1 C19 121.2(3)
C3 Re1 P1 C17 56.7(4)
C4 Re1 P1 C17 146.7(3)
C1 Re1 P1 C17 -35.8(3)
P2 Re1 P1 C17 -125.2(3)
C3 Re1 P1 Re2 176.9(2)
C4 Re1 P1 Re2 -93.1(2)
C1 Re1 P1 Re2 84.3(2)
P2 Re1 P1 Re2 -5.04(6)
C6 Re2 P2 C23 -62.5(3)
C5 Re2 P2 C23 -153.4(3)
C8 Re2 P2 C23 26.1(3)
P1 Re2 P2 C23 118.3(3)
C6 Re2 P2 C21 52.3(4)
C5 Re2 P2 C21 -38.6(4)
C8 Re2 P2 C21 140.9(3)
P1 Re2 P2 C21 -126.9(3)
C6 Re2 P2 Re1 174.2(2)
C5 Re2 P2 Re1 83.3(2)
C8 Re2 P2 Re1 -97.25(19)
P1 Re2 P2 Re1 -5.06(6)
C2 Re1 P2 C23 59.5(3)
C4 Re1 P2 C23 -30.1(3)
C1 Re1 P2 C23 151.2(3)
P1 Re1 P2 C23 -121.2(3)
C2 Re1 P2 C21 -54.6(3)
C4 Re1 P2 C21 -144.2(3)
C1 Re1 P2 C21 37.1(3)
P1 Re1 P2 C21 124.7(3)
C2 Re1 P2 Re2 -174.3(2)
C4 Re1 P2 Re2 96.1(2)
C1 Re1 P2 Re2 -82.6(2)
P1 Re1 P2 Re2 5.04(6)
C6 Re2 C8 O8 130.5(6)
C7 Re2 C8 O8 -136.2(6)
P2 Re2 C8 O8 34.8(6)
P1 Re2 C8 O8 -41.0(5)
C6 Re2 C8 C11 -49.3(5)
C7 Re2 C8 C11 44.0(6)
P2 Re2 C8 C11 -145.0(5)
P1 Re2 C8 C11 139.2(5)
C11 C8 O8 C9 -.8(10)
Re2 C8 O8 C9 179.4(6)
C8 O8 C9 C10 173.1(7)
O8 C8 C11 C12 92.7(8)
Re2 C8 C11 C12 -87.5(8)
O8 C8 C11 C16 -89.7(8)
Re2 C8 C11 C16 90.1(7)
C16 C11 C12 C13 .5(11)
C8 C11 C12 C13 178.1(7)
C11 C12 C13 C14 -1.1(12)
C12 C13 C14 C15 1.2(12)
C13 C14 C15 C16 -.7(12)
C12 C11 C16 C15 .1(11)
C8 C11 C16 C15 -177.6(6)
C14 C15 C16 C11 .0(12)
C19 P1 C17 C18 54.6(7)
Re2 P1 C17 C18 178.5(5)
Re1 P1 C17 C18 -64.8(6)
C17 P1 C19 C20 55.9(6)
Re2 P1 C19 C20 -63.7(6)
Re1 P1 C19 C20 177.1(5)
C23 P2 C21 C22 -56.3(7)
Re2 P2 C21 C22 -180.0(6)
Re1 P2 C21 C22 63.7(7)
C21 P2 C23 C24 -58.7(7)
Re2 P2 C23 C24 60.7(6)
Re1 P2 C23 C24 -179.8(5)
