#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/18/2201833.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2201833
loop_
_publ_author_name
'Douglas du Boulay'
'Atsuko Oono'
'Nobuo Ishizawa'
_publ_section_title
;
 A reinvestigation of the structure of Cs₃Ta₅O₁₄
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i86
_journal_page_last               i88
_journal_paper_doi               10.1107/S1600536803010122
_journal_volume                  59
_journal_year                    2003
_chemical_formula_iupac          'Cs3 Ta5 O14'
_chemical_formula_moiety         'Cs3 Ta5 O14'
_chemical_formula_sum            'Cs3 O14 Ta5'
_chemical_formula_weight         1527.48
_space_group_IT_number           55
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2 2ab'
_symmetry_space_group_name_H-M   'P b a m'
_cell_angle_alpha                90.00000
_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
_cell_formula_units_Z            4
_cell_length_a                   26.219(6)
_cell_length_b                   7.4283(10)
_cell_length_c                   7.3914(10)
_cell_measurement_reflns_used    20976
_cell_measurement_temperature    295
_cell_measurement_theta_max      30.01
_cell_measurement_theta_min      1.55
_cell_volume                     1439.6(4)
_computing_cell_refinement       Rapid-Auto
_computing_data_collection       'Rapid-Auto (Rigaku, 1999)'
_computing_data_reduction        Rapid-Auto
_computing_molecular_graphics    'ATOMS (Dowty, 1999) and ORTEP in Xtal3.7'
_computing_publication_material  'xtal BONDLA CIFIO in Xtal3.7'
_computing_structure_refinement  'CRYLSQ in Xtal3.7 (Hall et al., 2000)'
_computing_structure_solution    'Serafin & Hoppe (1982)'
_diffrn_ambient_temperature      297
_diffrn_measurement_device_type  'Rigaku Rapid image plate'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Mo K\a tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_R_equivalents  0.0600
_diffrn_reflns_av_sigmaI/netI    .058
_diffrn_reflns_limit_h_max       36
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       0
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2269
_diffrn_reflns_theta_max         30.01
_diffrn_reflns_theta_min         1.55
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    45.17
_exptl_absorpt_correction_T_max  0.349
_exptl_absorpt_correction_T_min  0.113
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details
'Gaussian integration on 8× 8× 8 grid'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    7.048
_exptl_crystal_density_method    none
_exptl_crystal_description       'rectangular block'
_exptl_crystal_F_000             2568
_exptl_crystal_size_max          .06
_exptl_crystal_size_mid          .06
_exptl_crystal_size_min          .04
_refine_diff_density_max         3.693
_refine_diff_density_min         -4.253
_refine_ls_extinction_expression none
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   .909
_refine_ls_goodness_of_fit_ref   .909
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     117
_refine_ls_number_reflns         2269
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          .044
_refine_ls_R_factor_gt           .044
_refine_ls_shift/su_max          .001
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[σ(F)²+0.2+10⁻⁴F²]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         .032
_refine_ls_wR_factor_ref         .032
_reflns_number_gt                2269
_reflns_number_total             2269
_reflns_threshold_expression     F>0
_cod_data_source_file            bt6274.cif
_cod_data_source_block           I
_cod_original_sg_symbol_Hall     -p_2_2ab
_cod_database_code               2201833
_cod_database_fobs_code          2201833
loop_
_symmetry_equiv_pos_as_xyz
+x,+y,+z
-x,-y,+z
1/2+x,1/2-y,-z
1/2-x,1/2+y,-z
-x,-y,-z
+x,+y,-z
1/2-x,1/2+y,+z
1/2+x,1/2-y,+z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_calc_attached_atom
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1 .29149(4) .15909(17) .00000 .0270(5) Uani ? ? 1.00000 ? ?
Cs2 .02229(3) .24078(16) .50000 .0241(5) Uani ? ? 1.00000 ? ?
Cs3 .38046(3) .15651(15) .50000 .0279(5) Uani ? ? 1.00000 ? ?
Ta1 .054631(18) .42585(7) .00000 .0071(2) Uani ? ? 1.00000 ? ?
Ta2 .442909(18) .41007(7) .00000 .0062(2) Uani ? ? 1.00000 ? ?
Ta3 .25378(2) .40034(7) .50000 .0066(2) Uani ? ? 1.00000 ? ?
Ta4 .151840(12) .16072(5) .25490(4) .00671(15) Uani ? ? 1.00000 ? ?
O1 .00000 .50000 .1740(11) .012(4) Uani ? ? 1.00000 ? ?
O2 .0162(3) .1597(14) .00000 .012(4) Uani ? ? 1.00000 ? ?
O3 .1671(3) .1326(14) .00000 .012(4) Uani ? ? 1.00000 ? ?
O4 .4189(3) .1719(15) .00000 .017(5) Uani ? ? 1.00000 ? ?
O5 .1250(3) .1554(14) .50000 .012(4) Uani ? ? 1.00000 ? ?
O6 .2718(3) .1448(14) .50000 .012(4) Uani ? ? 1.00000 ? ?
O7 .2009(2) .3374(9) .3059(8) .009(3) Uani ? ? 1.00000 ? ?
O8 .3039(2) .4561(9) .6882(8) .009(3) Uani ? ? 1.00000 ? ?
O9 .0979(2) .3408(9) .1915(8) .010(3) Uani ? ? 1.00000 ? ?
O10 .4110(2) .4733(9) .2075(8) .013(3) Uani ? ? 1.00000 ? ?
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cs -.644 2.119 'IT Vol C. Table 6.1.1.4  Table 6.1.1.5'
Ta -1.258 6.523 'IT Vol C. Table 6.1.1.4  Table 6.1.1.5'
O .008 .006 'IT Vol C. Table 6.1.1.4  Table 6.1.1.5'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
O8 Cs1 O8 '6 556' '1 554' 91.87(16)
O8 Cs1 O3 '6 556' . 98.22(16)
O8 Cs1 O7 '6 556' '7 545' 89.98(15)
O8 Cs1 O7 '6 556' '4 545' 170.26(14)
O8 Cs1 O4 '6 556' . 83.03(16)
O8 Cs1 Cs1 '6 556' 4 57.17(11)
O8 Cs1 Cs1 '6 556' '4 545' 130.17(11)
O8 Cs1 Cs3 '6 556' '1 554' 123.80(11)
O8 Cs1 Cs3 '6 556' . 48.78(11)
O8 Cs1 O3 '1 554' . 98.22(16)
O8 Cs1 O7 '1 554' '7 545' 170.26(14)
O8 Cs1 O7 '1 554' '4 545' 89.98(15)
O8 Cs1 O4 '1 554' . 83.03(16)
O8 Cs1 Cs1 '1 554' 4 57.17(11)
O8 Cs1 Cs1 '1 554' '4 545' 130.17(10)
O8 Cs1 Cs3 '1 554' '1 554' 48.78(11)
O8 Cs1 Cs3 '1 554' . 123.80(11)
O3 Cs1 O7 . '7 545' 90.97(16)
O3 Cs1 O7 . '4 545' 90.97(16)
O3 Cs1 O4 . . 178.2(3)
O3 Cs1 Cs1 . 4 63.09(19)
O3 Cs1 Cs1 . '4 545' 56.18(19)
O3 Cs1 Cs3 . '1 554' 122.177(18)
O3 Cs1 Cs3 . . 122.177(18)
O7 Cs1 O7 '7 545' '4 545' 86.64(15)
O7 Cs1 O4 '7 545' . 87.70(16)
O7 Cs1 Cs1 '7 545' 4 131.01(10)
O7 Cs1 Cs1 '7 545' '4 545' 53.50(10)
O7 Cs1 Cs3 '7 545' '1 554' 123.00(11)
O7 Cs1 Cs3 '7 545' . 51.99(10)
O7 Cs1 O4 '4 545' . 87.70(16)
O7 Cs1 Cs1 '4 545' 4 131.01(10)
O7 Cs1 Cs1 '4 545' '4 545' 53.50(10)
O7 Cs1 Cs3 '4 545' '1 554' 51.99(10)
O7 Cs1 Cs3 '4 545' . 123.00(11)
O4 Cs1 Cs1 . 4 118.73(19)
O4 Cs1 Cs1 . '4 545' 121.99(19)
O4 Cs1 Cs3 . '1 554' 57.763(17)
O4 Cs1 Cs3 . . 57.763(17)
Cs1 Cs1 Cs1 4 '4 545' 119.27(3)
Cs1 Cs1 Cs3 4 '1 554' 105.88(2)
Cs1 Cs1 Cs3 4 . 105.88(2)
Cs1 Cs1 Cs3 '4 545' '1 554' 105.43(3)
Cs1 Cs1 Cs3 '4 545' . 105.43(3)
Cs3 Cs1 Cs3 '1 554' . 115.48(3)
O5 Cs2 O9 . '6 556' 55.59(14)
O5 Cs2 O9 . . 55.59(14)
O5 Cs2 O1 . '5 566' 108.77(13)
O5 Cs2 O1 . . 108.77(13)
O5 Cs2 O10 . '7 545' 50.87(16)
O5 Cs2 O10 . '4 546' 50.87(16)
O5 Cs2 Cs2 . 2 94.8(2)
O5 Cs2 Cs3 . '3 456' 178.3(2)
O5 Cs2 Cs3 . '4 556' 63.7(2)
O5 Cs2 Cs2 . '2 565' 120.1(2)
O9 Cs2 O9 '6 556' . 94.29(15)
O9 Cs2 O1 '6 556' '5 566' 53.80(12)
O9 Cs2 O1 '6 556' . 122.33(14)
O9 Cs2 O10 '6 556' '7 545' 106.08(15)
O9 Cs2 O10 '6 556' '4 546' 49.41(17)
O9 Cs2 Cs2 '6 556' 2 115.14(13)
O9 Cs2 Cs3 '6 556' '3 456' 125.16(11)
O9 Cs2 Cs3 '6 556' '4 556' 53.87(12)
O9 Cs2 Cs2 '6 556' '2 565' 87.50(12)
O9 Cs2 O1 . '5 566' 122.33(14)
O9 Cs2 O1 . . 53.80(12)
O9 Cs2 O10 . '7 545' 49.41(17)
O9 Cs2 O10 . '4 546' 106.08(15)
O9 Cs2 Cs2 . 2 115.14(12)
O9 Cs2 Cs3 . '3 456' 125.16(11)
O9 Cs2 Cs3 . '4 556' 53.87(12)
O9 Cs2 Cs2 . '2 565' 87.50(12)
O1 Cs2 O1 '5 566' . 100.27(14)
O1 Cs2 O10 '5 566' '7 545' 159.63(11)
O1 Cs2 O10 '5 566' '4 546' 88.07(14)
O1 Cs2 Cs2 '5 566' 2 121.68(7)
O1 Cs2 Cs3 '5 566' '3 456' 72.20(4)
O1 Cs2 Cs3 '5 566' '4 556' 69.24(5)
O1 Cs2 Cs2 '5 566' '2 565' 50.14(10)
O1 Cs2 O10 . '7 545' 88.07(14)
O1 Cs2 O10 . '4 546' 159.63(11)
O1 Cs2 Cs2 . 2 121.68(7)
O1 Cs2 Cs3 . '3 456' 72.20(4)
O1 Cs2 Cs3 . '4 556' 69.24(5)
O1 Cs2 Cs2 . '2 565' 50.14(10)
O10 Cs2 O10 '7 545' '4 546' 78.49(15)
O10 Cs2 Cs2 '7 545' 2 66.80(11)
O10 Cs2 Cs3 '7 545' '3 456' 128.16(10)
O10 Cs2 Cs3 '7 545' '4 556' 97.05(11)
O10 Cs2 Cs2 '7 545' '2 565' 134.83(11)
O10 Cs2 Cs2 '4 546' 2 66.80(11)
O10 Cs2 Cs3 '4 546' '3 456' 128.16(10)
O10 Cs2 Cs3 '4 546' '4 556' 97.05(11)
O10 Cs2 Cs2 '4 546' '2 565' 134.83(11)
Cs2 Cs2 Cs3 2 '3 456' 83.50(3)
Cs2 Cs2 Cs3 2 '4 556' 158.56(3)
Cs2 Cs2 Cs2 2 '2 565' 145.02(3)
Cs3 Cs2 Cs3 '3 456' '4 556' 117.95(4)
Cs3 Cs2 Cs2 '3 456' '2 565' 61.52(3)
Cs3 Cs2 Cs2 '4 556' '2 565' 56.43(3)
O6 Cs3 O10 . '6 556' 105.37(18)
O6 Cs3 O10 . . 105.37(18)
O6 Cs3 O8 . '6 556' 54.1(2)
O6 Cs3 O8 . . 54.1(2)
O6 Cs3 O9 . '7 545' 98.60(17)
O6 Cs3 O9 . '4 546' 98.60(17)
O6 Cs3 Cs2 . '3 556' 170.2(2)
O6 Cs3 Cs2 . '4 546' 127.8(2)
O6 Cs3 Cs1 . '1 556' 57.766(17)
O6 Cs3 Cs1 . . 57.766(17)
O10 Cs3 O10 '6 556' . 82.03(16)
O10 Cs3 O8 '6 556' '6 556' 86.74(15)
O10 Cs3 O8 '6 556' . 52.43(14)
O10 Cs3 O9 '6 556' '7 545' 156.01(14)
O10 Cs3 O9 '6 556' '4 546' 90.69(16)
O10 Cs3 Cs2 '6 556' '3 556' 67.55(10)
O10 Cs3 Cs2 '6 556' '4 546' 113.32(11)
O10 Cs3 Cs1 '6 556' '1 556' 64.65(11)
O10 Cs3 Cs1 '6 556' . 132.98(12)
O10 Cs3 O8 . '6 556' 52.43(14)
O10 Cs3 O8 . . 86.74(15)
O10 Cs3 O9 . '7 545' 90.69(16)
O10 Cs3 O9 . '4 546' 156.01(14)
O10 Cs3 Cs2 . '3 556' 67.55(10)
O10 Cs3 Cs2 . '4 546' 113.32(11)
O10 Cs3 Cs1 . '1 556' 132.98(12)
O10 Cs3 Cs1 . . 64.65(11)
O8 Cs3 O8 '6 556' . 49.82(14)
O8 Cs3 O9 '6 556' '7 545' 106.89(15)
O8 Cs3 O9 '6 556' '4 546' 150.35(14)
O8 Cs3 Cs2 '6 556' '3 556' 117.36(11)
O8 Cs3 Cs2 '6 556' '4 546' 154.98(10)
O8 Cs3 Cs1 '6 556' '1 556' 91.66(10)
O8 Cs3 Cs1 '6 556' . 46.90(10)
O8 Cs3 O9 . '7 545' 150.35(14)
O8 Cs3 O9 . '4 546' 106.89(14)
O8 Cs3 Cs2 . '3 556' 117.36(11)
O8 Cs3 Cs2 . '4 546' 154.98(10)
O8 Cs3 Cs1 . '1 556' 46.90(10)
O8 Cs3 Cs1 . . 91.66(10)
O9 Cs3 O9 '7 545' '4 546' 86.77(16)
O9 Cs3 Cs2 '7 545' '3 556' 88.53(10)
O9 Cs3 Cs2 '7 545' '4 546' 49.18(10)
O9 Cs3 Cs1 '7 545' '1 556' 132.48(11)
O9 Cs3 Cs1 '7 545' . 60.90(10)
O9 Cs3 Cs2 '4 546' '3 556' 88.53(10)
O9 Cs3 Cs2 '4 546' '4 546' 49.18(10)
O9 Cs3 Cs1 '4 546' '1 556' 60.90(10)
O9 Cs3 Cs1 '4 546' . 132.48(11)
Cs2 Cs3 Cs2 '3 556' '4 546' 62.05(3)
Cs2 Cs3 Cs1 '3 556' '1 556' 121.466(18)
Cs2 Cs3 Cs1 '3 556' . 121.466(18)
Cs2 Cs3 Cs1 '4 546' '1 556' 110.07(2)
Cs2 Cs3 Cs1 '4 546' . 110.07(2)
Cs1 Cs3 Cs1 '1 556' . 115.48(3)
O9 Ta1 O9 6 . 95.0(2)
O9 Ta1 O4 6 4 95.6(3)
O9 Ta1 O1 6 '5 565' 92.3(2)
O9 Ta1 O1 6 . 170.5(2)
O9 Ta1 O2 6 . 88.5(2)
O9 Ta1 O4 . 4 95.6(3)
O9 Ta1 O1 . '5 565' 170.5(2)
O9 Ta1 O1 . . 92.3(2)
O9 Ta1 O2 . . 88.5(2)
O4 Ta1 O1 4 '5 565' 89.8(2)
O4 Ta1 O1 4 . 89.8(2)
O4 Ta1 O2 4 . 173.8(4)
O1 Ta1 O1 '5 565' . 79.9(3)
O1 Ta1 O2 '5 565' . 85.45(17)
O1 Ta1 O2 . . 85.45(17)
O10 Ta2 O10 6 . 116.0(3)
O10 Ta2 O4 6 . 95.1(3)
O10 Ta2 O2 6 3 120.9(2)
O10 Ta2 O2 6 4 90.4(2)
O10 Ta2 O4 . . 95.1(3)
O10 Ta2 O2 . 3 120.9(2)
O10 Ta2 O2 . 4 90.4(2)
O4 Ta2 O2 . 3 94.5(4)
O4 Ta2 O2 . 4 169.6(4)
O2 Ta2 O2 3 4 75.1(4)
O6 Ta3 O6 '4 556' . 173.7(4)
O6 Ta3 O8 '4 556' '6 556' 91.9(3)
O6 Ta3 O8 '4 556' . 91.9(3)
O6 Ta3 O7 '4 556' '6 556' 88.8(3)
O6 Ta3 O7 '4 556' . 88.8(3)
O6 Ta3 O8 . '6 556' 92.5(3)
O6 Ta3 O8 . . 92.5(3)
O6 Ta3 O7 . '6 556' 86.7(3)
O6 Ta3 O7 . . 86.7(3)
O8 Ta3 O8 '6 556' . 90.5(2)
O8 Ta3 O7 '6 556' '6 556' 178.8(3)
O8 Ta3 O7 '6 556' . 90.3(2)
O8 Ta3 O7 . '6 556' 90.3(2)
O8 Ta3 O7 . . 178.8(3)
O7 Ta3 O7 '6 556' . 88.8(2)
O7 Ta4 O3 . . 97.4(3)
O7 Ta4 O5 . . 94.3(3)
O7 Ta4 O8 . '4 546' 95.4(3)
O7 Ta4 O9 . . 93.7(3)
O7 Ta4 O10 . '7 545' 174.2(2)
O3 Ta4 O5 . . 168.2(4)
O3 Ta4 O8 . '4 546' 90.2(3)
O3 Ta4 O9 . . 89.4(3)
O3 Ta4 O10 . '7 545' 86.0(3)
O5 Ta4 O8 . '4 546' 89.9(3)
O5 Ta4 O9 . . 88.6(3)
O5 Ta4 O10 . '7 545' 82.2(3)
O8 Ta4 O9 '4 546' . 170.9(2)
O8 Ta4 O10 '4 546' '7 545' 89.2(2)
O9 Ta4 O10 . '7 545' 81.7(2)
Ta1 O1 Ta1 . '2 565' 100.1(4)
Ta1 O1 Cs2 . '2 565' 142.64(9)
Ta1 O1 Cs2 . . 101.01(8)
Ta1 O1 Cs2 '2 565' '2 565' 101.01(8)
Ta1 O1 Cs2 '2 565' . 142.64(10)
Cs2 O1 Cs2 '2 565' . 79.7(2)
Ta2 O2 Ta2 '3 455' '4 545' 104.9(4)
Ta2 O2 Ta1 '3 455' . 132.1(5)
Ta2 O2 Ta1 '4 545' . 123.0(4)
Ta4 O3 Ta4 6 . 153.1(5)
Ta4 O3 Cs1 6 . 101.5(3)
Ta4 O3 Cs1 . . 101.5(3)
Ta2 O4 Ta1 . '4 545' 139.6(5)
Ta2 O4 Cs1 . . 111.2(4)
Ta1 O4 Cs1 '4 545' . 109.1(4)
Ta4 O5 Ta4 '6 556' . 137.5(4)
Ta4 O5 Cs2 '6 556' . 110.3(2)
Ta4 O5 Cs2 . . 110.3(2)
Ta3 O6 Ta3 '4 546' . 145.8(5)
Ta3 O6 Cs3 '4 546' . 112.0(4)
Ta3 O6 Cs3 . . 102.2(4)
Ta4 O7 Ta3 . . 139.8(3)
Ta4 O7 Cs1 . 4 114.3(2)
Ta3 O7 Cs1 . 4 105.9(2)
Ta4 O8 Ta3 '4 556' . 135.6(3)
Ta4 O8 Cs1 '4 556' '1 556' 116.1(2)
Ta4 O8 Cs3 '4 556' . 104.7(2)
Ta3 O8 Cs1 . '1 556' 107.3(2)
Ta3 O8 Cs3 . . 88.1(2)
Cs1 O8 Cs3 '1 556' . 84.32(15)
Ta1 O9 Ta4 . . 144.0(3)
Ta1 O9 Cs2 . . 104.1(2)
Ta1 O9 Cs3 . '4 556' 112.0(3)
Ta4 O9 Cs2 . . 96.8(2)
Ta4 O9 Cs3 . '4 556' 101.0(2)
Cs2 O9 Cs3 . '4 556' 76.95(14)
Ta2 O10 Ta4 . 7 130.5(3)
Ta2 O10 Cs3 . . 118.9(3)
Ta2 O10 Cs2 . '4 556' 116.8(3)
Ta4 O10 Cs3 7 . 99.6(2)
Ta4 O10 Cs2 7 '4 556' 85.1(2)
Cs3 O10 Cs2 . '4 556' 97.16(16)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cs1 O8 . '6 556' 3.207(6) ?
Cs1 O8 . '1 554' 3.207(6) ?
Cs1 O3 . . 3.268(9) ?
Cs1 O7 . '7 545' 3.296(6) ?
Cs1 O7 . '4 545' 3.296(6) ?
Cs1 O4 . . 3.342(9) ?
Cs1 Cs1 . 4 4.3046(17) ?
Cs1 Cs1 . '4 545' 4.3046(17) ?
Cs1 Cs3 . '1 554' 4.3704(9) ?
Cs1 Cs3 . . 4.3704(9) ?
Cs2 O5 . . 2.767(8) ?
Cs2 O9 . '6 556' 3.111(6) ?
Cs2 O9 . . 3.111(6) ?
Cs2 O1 . '5 566' 3.140(6) ?
Cs2 O1 . . 3.140(6) ?
Cs2 O10 . '7 545' 3.417(6) ?
Cs2 O10 . '4 546' 3.417(6) ?
Cs2 Cs2 . 2 3.7634(18) ?
Cs2 Cs3 . '3 456' 3.7961(15) ?
Cs2 Cs3 . '4 556' 4.0047(16) ?
Cs2 Cs2 . '2 565' 4.0247(18) ?
Cs3 O6 . . 2.851(8) ?
Cs3 O10 . '6 556' 3.294(7) ?
Cs3 O10 . . 3.294(7) ?
Cs3 O8 . '6 556' 3.304(6) ?
Cs3 O8 . . 3.304(6) ?
Cs3 O9 . '7 545' 3.320(6) ?
Cs3 O9 . '4 546' 3.320(6) ?
Ta1 O9 . 6 1.920(6) ?
Ta1 O9 . . 1.920(6) ?
Ta1 O4 . 4 1.955(11) ?
Ta1 O1 . '5 565' 2.002(5) ?
Ta1 O1 . . 2.002(5) ?
Ta1 O2 . . 2.219(10) ?
Ta2 O10 . 6 1.808(6) ?
Ta2 O10 . . 1.808(6) ?
Ta2 O4 . . 1.878(11) ?
Ta2 O2 . 3 1.991(8) ?
Ta2 O2 . 4 2.141(10) ?
Ta3 O6 . '4 556' 1.936(10) ?
Ta3 O6 . . 1.956(10) ?
Ta3 O8 . '6 556' 1.959(6) ?
Ta3 O8 . . 1.959(6) ?
Ta3 O7 . '6 556' 2.050(6) ?
Ta3 O7 . . 2.050(6) ?
Ta4 O7 . . 1.876(6) ?
Ta4 O3 . . 1.937(2) ?
Ta4 O5 . . 1.944(3) ?
Ta4 O8 . '4 546' 1.957(6) ?
Ta4 O9 . . 2.003(6) ?
Ta4 O10 . '7 545' 2.186(6) ?
