#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/22/2202284.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2202284
loop_
_publ_author_name
'Smith, Michele L.'
'Almond, Philip M.'
'Albrecht-Schmitt, Thomas E.'
'Hill, William E.'
_publ_section_title
;
 Bis[μ-1,3-bis(diphenylphosphino)propane]disilver(I)
 bis(tetrafluoroborate)
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1013
_journal_page_last               m1014
_journal_paper_doi               10.1107/S1600536803022554
_journal_volume                  59
_journal_year                    2003
_chemical_formula_iupac          '[Ag2 (C27 H26 P2)2] (B F4)2'
_chemical_formula_moiety         'C54 H52 Ag2 P4 2+, 2B F4 1-'
_chemical_formula_sum            'C54 H52 Ag2 B2 F8 P4'
_chemical_formula_weight         1214.20
_chemical_name_common
'Bis[μ-1,3-bis(diphenylphosphino)propane]disilver bis(tetrafluoroborate)'
_chemical_name_systematic
;
Bis[μ-1,3-bis(diphenylphosphino)propane]disilver bis(tetrafluoroborate)
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                90.908(2)
_cell_angle_beta                 114.075(2)
_cell_angle_gamma                112.741(2)
_cell_formula_units_Z            1
_cell_length_a                   10.6882(7)
_cell_length_b                   11.3911(7)
_cell_length_c                   12.9037(8)
_cell_measurement_reflns_used    9950
_cell_measurement_temperature    193(2)
_cell_measurement_theta_max      28.305
_cell_measurement_theta_min      2.308
_cell_volume                     1294.46(15)
_computing_cell_refinement       'SMART and SAINT-Plus (Bruker, 1999)'
_computing_data_collection       'SMART (Bruker, 2000)'
_computing_data_reduction        SAINT-Plus
_computing_molecular_graphics    'SHELXP97 in SHELXTL97'
_computing_publication_material  'XCIF in SHELXTL97'
_computing_structure_refinement  'SHELXL97 in SHELXTL97'
_computing_structure_solution    'SHELXS97 in SHELXTL97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker APEX'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0203
_diffrn_reflns_av_sigmaI/netI    0.0312
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            13475
_diffrn_reflns_theta_full        28.31
_diffrn_reflns_theta_max         28.31
_diffrn_reflns_theta_min         1.77
_diffrn_standards_decay_%        <1
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.945
_exptl_absorpt_correction_T_max  0.8774
_exptl_absorpt_correction_T_min  0.7117
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   '(XPREP in SHELXTL97; Sheldrick, 1997)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.558
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             612
_exptl_crystal_size_max          0.39
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.14
_refine_diff_density_max         1.612
_refine_diff_density_min         -1.047
_refine_ls_extinction_coef       0
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.055
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     340
_refine_ls_number_reflns         6396
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.055
_refine_ls_R_factor_all          0.0437
_refine_ls_R_factor_gt           0.0403
_refine_ls_shift/su_max          0.028
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0747P)²+1.0875P] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1154
_refine_ls_wR_factor_ref         0.1187
_reflns_number_gt                5813
_reflns_number_total             6396
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ac6065.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'nm' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        1294.46(14)
_cod_database_code               2202284
_cod_database_fobs_code          2202284
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
Ag1 0.10140(2) 0.114748(19) 0.200649(17) 0.03275(9) Uani d . 1 . . Ag
P1 0.35391(7) 0.23940(6) 0.22321(6) 0.02631(14) Uani d . 1 . . P
P2 -0.13909(7) 0.06654(7) 0.19735(6) 0.02743(14) Uani d . 1 . . P
C1 0.5034(3) 0.2790(3) 0.3706(2) 0.0304(5) Uani d . 1 . . C
C2 0.5758(4) 0.4029(3) 0.4400(3) 0.0407(6) Uani d . 1 . . C
H2A 0.5504 0.4704 0.4097 0.049 Uiso calc R 1 . . H
C3 0.6854(4) 0.4274(4) 0.5538(3) 0.0512(8) Uani d . 1 . . C
H3A 0.7343 0.5118 0.6011 0.061 Uiso calc R 1 . . H
C4 0.7238(4) 0.3297(4) 0.5988(3) 0.0521(9) Uani d . 1 . . C
H4A 0.7991 0.3473 0.6765 0.063 Uiso calc R 1 . . H
C5 0.6525(4) 0.2071(4) 0.5305(3) 0.0472(8) Uani d . 1 . . C
H5A 0.6797 0.1404 0.5610 0.057 Uiso calc R 1 . . H
C6 0.5406(3) 0.1802(3) 0.4168(3) 0.0377(6) Uani d . 1 . . C
H6A 0.4897 0.0948 0.3709 0.045 Uiso calc R 1 . . H
C7 0.3804(3) 0.3931(3) 0.1779(2) 0.0324(5) Uani d . 1 . . C
C8 0.2674(4) 0.4355(3) 0.1511(3) 0.0454(7) Uani d . 1 . . C
H8A 0.1766 0.3835 0.1559 0.054 Uiso calc R 1 . . H
C9 0.2872(6) 0.5543(4) 0.1171(4) 0.0639(11) Uani d . 1 . . C
H9A 0.2110 0.5844 0.1006 0.077 Uiso calc R 1 . . H
C10 0.4169(6) 0.6277(4) 0.1076(4) 0.0678(13) Uani d . 1 . . C
H10A 0.4295 0.7081 0.0834 0.081 Uiso calc R 1 . . H
C11 0.5286(5) 0.5860(4) 0.1327(4) 0.0683(12) Uani d . 1 . . C
H11A 0.6181 0.6376 0.1260 0.082 Uiso calc R 1 . . H
C12 0.5111(4) 0.4687(3) 0.1680(3) 0.0500(8) Uani d . 1 . . C
H12A 0.5886 0.4400 0.1853 0.060 Uiso calc R 1 . . H
C13 -0.1947(3) -0.0395(3) 0.2889(3) 0.0368(6) Uani d . 1 . . C
C14 -0.1077(4) -0.1018(3) 0.3478(3) 0.0517(8) Uani d . 1 . . C
H14A -0.0176 -0.0882 0.3419 0.062 Uiso calc R 1 . . H
C15 -0.1547(7) -0.1865(4) 0.4174(4) 0.0820(17) Uani d . 1 . . C
H15A -0.0969 -0.2312 0.4579 0.098 Uiso calc R 1 . . H
C16 -0.2852(8) -0.2036(5) 0.4259(5) 0.095(2) Uani d . 1 . . C
H16A -0.3156 -0.2589 0.4739 0.114 Uiso calc R 1 . . H
C17 -0.3712(7) -0.1419(5) 0.3659(5) 0.0861(19) Uani d . 1 . . C
H17A -0.4606 -0.1547 0.3727 0.103 Uiso calc R 1 . . H
C18 -0.3295(5) -0.0619(4) 0.2963(4) 0.0584(10) Uani d . 1 . . C
H18A -0.3915 -0.0217 0.2530 0.070 Uiso calc R 1 . . H
C19 -0.1423(3) 0.2192(3) 0.2368(2) 0.0309(5) Uani d . 1 . . C
C20 -0.1473(3) 0.2540(3) 0.3382(3) 0.0367(6) Uani d . 1 . . C
H20A -0.1588 0.1936 0.3874 0.044 Uiso calc R 1 . . H
C21 -0.1356(4) 0.3776(3) 0.3680(3) 0.0444(7) Uani d . 1 . . C
H21A -0.1392 0.4012 0.4373 0.053 Uiso calc R 1 . . H
C22 -0.1187(4) 0.4651(3) 0.2971(3) 0.0483(8) Uani d . 1 . . C
H22A -0.1089 0.5496 0.3185 0.058 Uiso calc R 1 . . H
C23 -0.1159(4) 0.4313(3) 0.1951(3) 0.0465(7) Uani d . 1 . . C
H23A -0.1059 0.4916 0.1457 0.056 Uiso calc R 1 . . H
C24 -0.1276(4) 0.3086(3) 0.1652(3) 0.0391(6) Uani d . 1 . . C
H24A -0.1256 0.2853 0.0951 0.047 Uiso calc R 1 . . H
C25 0.4083(3) 0.1555(3) 0.1389(2) 0.0309(5) Uani d . 1 . . C
H25A 0.5109 0.2132 0.1485 0.037 Uiso calc R 1 . . H
H25B 0.4120 0.0766 0.1684 0.037 Uiso calc R 1 . . H
C26 0.2950(3) 0.1168(3) 0.0099(2) 0.0309(5) Uani d . 1 . . C
H26A 0.1913 0.0910 0.0020 0.037 Uiso calc R 1 . . H
H26B 0.3197 0.1927 -0.0269 0.037 Uiso calc R 1 . . H
C27 0.2992(3) 0.0044(3) -0.0522(2) 0.0332(5) Uani d . 1 . . C
H27A 0.2971 -0.0638 -0.0055 0.040 Uiso calc R 1 . . H
H27B 0.3954 0.0360 -0.0588 0.040 Uiso calc R 1 . . H
B1 0.1140(6) -0.1745(4) 0.1470(4) 0.0499(9) Uani d . 1 . . B
F1 0.1749(5) -0.0923(4) 0.2478(3) 0.1059(13) Uani d . 1 . . F
F2 0.0530(3) -0.1148(2) 0.0584(2) 0.0587(6) Uani d . 1 . . F
F3 0.0292(7) -0.2880(4) 0.1389(6) 0.252(5) Uani d . 1 . . F
F4 0.2450(7) -0.1726(6) 0.1475(5) 0.166(2) Uani d . 1 . . F
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
P2 Ag1 P1 . . 159.66(3) yes
C7 P1 C1 . . 105.66(13) no
C7 P1 C25 . . 105.34(13) no
C1 P1 C25 . . 103.68(12) no
C7 P1 Ag1 . . 113.23(10) no
C1 P1 Ag1 . . 114.76(9) no
C25 P1 Ag1 . . 113.20(9) no
C13 P2 C19 . . 107.23(13) no
C13 P2 C27 . 2 104.94(14) no
C19 P2 C27 . 2 103.39(12) no
C13 P2 Ag1 . . 118.32(11) no
C19 P2 Ag1 . . 108.34(9) no
C27 P2 Ag1 2 . 113.47(9) no
C2 C1 C6 . . 119.4(3) no
C2 C1 P1 . . 121.8(2) no
C6 C1 P1 . . 118.7(2) no
C3 C2 C1 . . 119.8(3) no
C3 C2 H2A . . 120.1 no
C1 C2 H2A . . 120.1 no
C4 C3 C2 . . 120.6(3) no
C4 C3 H3A . . 119.7 no
C2 C3 H3A . . 119.7 no
C5 C4 C3 . . 119.8(3) no
C5 C4 H4A . . 120.1 no
C3 C4 H4A . . 120.1 no
C4 C5 C6 . . 120.4(3) no
C4 C5 H5A . . 119.8 no
C6 C5 H5A . . 119.8 no
C5 C6 C1 . . 119.9(3) no
C5 C6 H6A . . 120.0 no
C1 C6 H6A . . 120.0 no
C12 C7 C8 . . 119.4(3) no
C12 C7 P1 . . 121.1(2) no
C8 C7 P1 . . 119.5(2) no
C7 C8 C9 . . 120.0(4) no
C7 C8 H8A . . 120.0 no
C9 C8 H8A . . 120.0 no
C10 C9 C8 . . 119.9(4) no
C10 C9 H9A . . 120.1 no
C8 C9 H9A . . 120.1 no
C9 C10 C11 . . 120.6(3) no
C9 C10 H10A . . 119.7 no
C11 C10 H10A . . 119.7 no
C10 C11 C12 . . 120.1(4) no
C10 C11 H11A . . 119.9 no
C12 C11 H11A . . 119.9 no
C11 C12 C7 . . 120.1(4) no
C11 C12 H12A . . 120.0 no
C7 C12 H12A . . 120.0 no
C14 C13 C18 . . 120.2(3) no
C14 C13 P2 . . 119.8(3) no
C18 C13 P2 . . 120.0(3) no
C13 C14 C15 . . 119.0(4) no
C13 C14 H14A . . 120.5 no
C15 C14 H14A . . 120.5 no
C16 C15 C14 . . 119.6(5) no
C16 C15 H15A . . 120.2 no
C14 C15 H15A . . 120.2 no
C17 C16 C15 . . 120.7(4) no
C17 C16 H16A . . 119.6 no
C15 C16 H16A . . 119.6 no
C18 C17 C16 . . 120.6(5) no
C18 C17 H17A . . 119.7 no
C16 C17 H17A . . 119.7 no
C17 C18 C13 . . 119.9(5) no
C17 C18 H18A . . 120.1 no
C13 C18 H18A . . 120.1 no
C20 C19 C24 . . 118.9(3) no
C20 C19 P2 . . 123.3(2) no
C24 C19 P2 . . 117.6(2) no
C19 C20 C21 . . 120.1(3) no
C19 C20 H20A . . 120.0 no
C21 C20 H20A . . 120.0 no
C22 C21 C20 . . 120.0(3) no
C22 C21 H21A . . 120.0 no
C20 C21 H21A . . 120.0 no
C21 C22 C23 . . 120.6(3) no
C21 C22 H22A . . 119.7 no
C23 C22 H22A . . 119.7 no
C22 C23 C24 . . 119.5(3) no
C22 C23 H23A . . 120.2 no
C24 C23 H23A . . 120.2 no
C23 C24 C19 . . 120.8(3) no
C23 C24 H24A . . 119.6 no
C19 C24 H24A . . 119.6 no
C26 C25 P1 . . 110.97(18) no
C26 C25 H25A . . 109.4 no
P1 C25 H25A . . 109.4 no
C26 C25 H25B . . 109.4 no
P1 C25 H25B . . 109.4 no
H25A C25 H25B . . 108.0 no
C27 C26 C25 . . 111.3(2) no
C27 C26 H26A . . 109.4 no
C25 C26 H26A . . 109.4 no
C27 C26 H26B . . 109.4 no
C25 C26 H26B . . 109.4 no
H26A C26 H26B . . 108.0 no
C26 C27 P2 . 2 112.12(18) no
C26 C27 H27A . . 109.2 no
P2 C27 H27A 2 . 109.2 no
C26 C27 H27B . . 109.2 no
P2 C27 H27B 2 . 109.2 no
H27A C27 H27B . . 107.9 no
F3 B1 F1 . . 116.9(5) no
F3 B1 F4 . . 108.0(6) no
F1 B1 F4 . . 99.8(5) no
F3 B1 F2 . . 115.1(4) no
F1 B1 F2 . . 107.4(3) no
F4 B1 F2 . . 108.4(4) no
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ag1 P2 . 2.3935(7) yes
Ag1 P1 . 2.4016(7) yes
P1 C7 . 1.809(3) no
P1 C1 . 1.820(3) no
P1 C25 . 1.829(3) no
P2 C13 . 1.809(3) no
P2 C19 . 1.821(3) no
P2 C27 2 1.832(3) no
C1 C2 . 1.394(4) no
C1 C6 . 1.397(4) no
C2 C3 . 1.392(4) no
C2 H2A . 0.9500 no
C3 C4 . 1.387(6) no
C3 H3A . 0.9500 no
C4 C5 . 1.378(6) no
C4 H4A . 0.9500 no
C5 C6 . 1.396(4) no
C5 H5A . 0.9500 no
C6 H6A . 0.9500 no
C7 C12 . 1.389(5) no
C7 C8 . 1.389(4) no
C8 C9 . 1.393(5) no
C8 H8A . 0.9500 no
C9 C10 . 1.372(7) no
C9 H9A . 0.9500 no
C10 C11 . 1.373(7) no
C10 H10A . 0.9500 no
C11 C12 . 1.386(5) no
C11 H11A . 0.9500 no
C12 H12A . 0.9500 no
C13 C14 . 1.377(5) no
C13 C18 . 1.406(5) no
C14 C15 . 1.418(6) no
C14 H14A . 0.9500 no
C15 C16 . 1.382(9) no
C15 H15A . 0.9500 no
C16 C17 . 1.370(10) no
C16 H16A . 0.9500 no
C17 C18 . 1.369(6) no
C17 H17A . 0.9500 no
C18 H18A . 0.9500 no
C19 C20 . 1.389(4) no
C19 C24 . 1.393(4) no
C20 C21 . 1.398(4) no
C20 H20A . 0.9500 no
C21 C22 . 1.373(5) no
C21 H21A . 0.9500 no
C22 C23 . 1.382(5) no
C22 H22A . 0.9500 no
C23 C24 . 1.387(4) no
C23 H23A . 0.9500 no
C24 H24A . 0.9500 no
C25 C26 . 1.533(4) no
C25 H25A . 0.9900 no
C25 H25B . 0.9900 no
C26 C27 . 1.526(4) no
C26 H26A . 0.9900 no
C26 H26B . 0.9900 no
C27 P2 2 1.832(3) no
C27 H27A . 0.9900 no
C27 H27B . 0.9900 no
B1 F3 . 1.231(5) no
B1 F1 . 1.339(5) no
B1 F4 . 1.389(7) no
B1 F2 . 1.397(4) no
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
P2 Ag1 P1 C7 . . -35.63(12) no
P2 Ag1 P1 C1 . . 85.81(12) no
P2 Ag1 P1 C25 . . -155.45(11) no
P1 Ag1 P2 C13 . . -122.22(12) no
P1 Ag1 P2 C19 . . 0.00(13) no
P1 Ag1 P2 C27 . 2 114.20(12) no
C7 P1 C1 C2 . . 21.8(3) no
C25 P1 C1 C2 . . 132.3(2) no
Ag1 P1 C1 C2 . . -103.7(2) no
C7 P1 C1 C6 . . -161.5(2) no
C25 P1 C1 C6 . . -51.0(2) no
Ag1 P1 C1 C6 . . 73.0(2) no
C6 C1 C2 C3 . . 0.8(5) no
P1 C1 C2 C3 . . 177.5(2) no
C1 C2 C3 C4 . . 0.3(5) no
C2 C3 C4 C5 . . -0.3(5) no
C3 C4 C5 C6 . . -0.8(5) no
C4 C5 C6 C1 . . 1.8(5) no
C2 C1 C6 C5 . . -1.9(4) no
P1 C1 C6 C5 . . -178.6(2) no
C1 P1 C7 C12 . . 63.5(3) no
C25 P1 C7 C12 . . -45.8(3) no
Ag1 P1 C7 C12 . . -170.0(2) no
C1 P1 C7 C8 . . -117.3(2) no
C25 P1 C7 C8 . . 133.3(2) no
Ag1 P1 C7 C8 . . 9.1(3) no
C12 C7 C8 C9 . . -1.4(5) no
P1 C7 C8 C9 . . 179.4(3) no
C7 C8 C9 C10 . . 1.5(6) no
C8 C9 C10 C11 . . -0.9(7) no
C9 C10 C11 C12 . . 0.1(7) no
C10 C11 C12 C7 . . 0.0(6) no
C8 C7 C12 C11 . . 0.7(5) no
P1 C7 C12 C11 . . 179.8(3) no
C19 P2 C13 C14 . . -130.2(3) no
C27 P2 C13 C14 2 . 120.3(3) no
Ag1 P2 C13 C14 . . -7.4(3) no
C19 P2 C13 C18 . . 52.3(3) no
C27 P2 C13 C18 2 . -57.2(3) no
Ag1 P2 C13 C18 . . 175.0(2) no
C18 C13 C14 C15 . . -1.2(5) no
P2 C13 C14 C15 . . -178.8(3) no
C13 C14 C15 C16 . . -0.8(6) no
C14 C15 C16 C17 . . 1.4(7) no
C15 C16 C17 C18 . . 0.0(8) no
C16 C17 C18 C13 . . -2.0(7) no
C14 C13 C18 C17 . . 2.6(5) no
P2 C13 C18 C17 . . -179.8(3) no
C13 P2 C19 C20 . . 15.2(3) no
C27 P2 C19 C20 2 . 125.7(2) no
Ag1 P2 C19 C20 . . -113.6(2) no
C13 P2 C19 C24 . . -169.7(2) no
C27 P2 C19 C24 2 . -59.1(2) no
Ag1 P2 C19 C24 . . 61.5(2) no
C24 C19 C20 C21 . . -0.9(4) no
P2 C19 C20 C21 . . 174.2(2) no
C19 C20 C21 C22 . . -0.1(5) no
C20 C21 C22 C23 . . 1.1(5) no
C21 C22 C23 C24 . . -1.1(5) no
C22 C23 C24 C19 . . 0.0(5) no
C20 C19 C24 C23 . . 1.0(4) no
P2 C19 C24 C23 . . -174.4(3) no
C7 P1 C25 C26 . . -68.0(2) no
C1 P1 C25 C26 . . -178.80(19) no
Ag1 P1 C25 C26 . . 56.2(2) no
P1 C25 C26 C27 . . -157.3(2) no
C25 C26 C27 P2 . 2_444 167.82(19) no
