#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/38/2203854.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2203854
loop_
_publ_author_name
'Zhu, Hai-Liang'
'Ng, Seik Weng'
_publ_section_title
;
 μ-2-Methylpyrazine-μ-trifluoroacetato-silver(I)
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m939
_journal_page_last               m940
_journal_paper_doi               10.1107/S1600536804013510
_journal_volume                  60
_journal_year                    2004
_chemical_formula_iupac          '[Ag (C5 H6 N2) (C F3 O2]'
_chemical_formula_moiety         'C2 O2 F3, C5 H6 N2, Ag'
_chemical_formula_sum            'C7 H6 Ag F3 N2 O2'
_chemical_formula_weight         315.01
_chemical_name_systematic
;
 (2-Methylpyrazine)trifluoroacetatosilver(I)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.963(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   12.479(2)
_cell_length_b                   12.611(2)
_cell_length_c                   12.597(2)
_cell_measurement_reflns_used    2633
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      24.2
_cell_measurement_theta_min      2.3
_cell_volume                     1971.7(5)
_computing_cell_refinement       'SAINT (Bruker, 2002)'
_computing_data_collection       'SMART (Bruker, 2002)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.98
_diffrn_measured_fraction_theta_max 0.98
_diffrn_measurement_device_type  'Bruker APEX area-detector diffractometer'
_diffrn_measurement_method       'φ and ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.041
_diffrn_reflns_av_sigmaI/netI    0.056
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            10949
_diffrn_reflns_theta_full        27.1
_diffrn_reflns_theta_max         27.1
_diffrn_reflns_theta_min         1.6
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.071
_exptl_absorpt_correction_T_max  0.732
_exptl_absorpt_correction_T_min  0.398
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 2002)'
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    2.122
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             1216
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.50
_refine_diff_density_min         -0.71
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.07
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     330
_refine_ls_number_reflns         4234
_refine_ls_number_restraints     96
_refine_ls_restrained_S_all      1.07
_refine_ls_R_factor_all          0.075
_refine_ls_R_factor_gt           0.055
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         <0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0899P)²+2.7689P] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.157
_refine_ls_wR_factor_ref         0.180
_reflns_number_gt                3041
_reflns_number_total             4234
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            bt6467.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2203854
_cod_database_fobs_code          2203854
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
Ag1 0.39816(6) 0.24636(6) 0.22983(6) 0.0462(2) Uani d . 1 . . Ag
Ag2 0.27038(6) 0.23843(4) 0.60454(6) 0.0447(2) Uani d . 1 . . Ag
F1 0.4301(11) 0.2503(14) -0.1479(10) 0.129(8) Uani d PDU 0.76(3) A 1 F
F2 0.4342(11) 0.4118(9) -0.0929(16) 0.142(9) Uani d PDU 0.76(3) A 1 F
F3 0.3464(7) 0.2970(14) -0.0173(9) 0.113(7) Uani d PDU 0.76(3) A 1 F
F1' 0.384(4) 0.220(2) -0.084(4) 0.16(3) Uani d PDU 0.24(3) A 2 F
F2' 0.462(2) 0.351(3) -0.1532(18) 0.097(16) Uani d PDU 0.24(3) A 2 F
F3' 0.371(3) 0.378(3) -0.021(2) 0.119(19) Uani d PDU 0.24(3) A 2 F
F4 0.6498(14) 0.247(2) 0.5696(15) 0.138(13) Uani d PDU 0.56(3) B 3 F
F5 0.5171(12) 0.2954(19) 0.6492(8) 0.097(8) Uani d PDU 0.56(3) B 3 F
F6 0.591(2) 0.4098(12) 0.5581(14) 0.143(13) Uani d PDU 0.56(3) B 3 F
F4' 0.580(3) 0.2259(17) 0.626(2) 0.143(15) Uani d PDU 0.44(3) B 4 F
F5' 0.5289(18) 0.389(2) 0.617(2) 0.141(16) Uani d PDU 0.44(3) B 4 F
F6' 0.6615(12) 0.337(3) 0.5372(14) 0.095(9) Uani d PDU 0.44(3) B 4 F
O1 0.5286(6) 0.2772(6) 0.1075(5) 0.0676(19) Uani d . 1 . . O
O2 0.6219(5) 0.2803(6) -0.0302(5) 0.0651(18) Uani d . 1 . . O
O3 0.3936(6) 0.2643(5) 0.4728(5) 0.0628(18) Uani d . 1 . . O
O4 0.5319(5) 0.2747(5) 0.3791(5) 0.0556(16) Uani d . 1 . . O
N1 0.3167(5) 0.0850(5) 0.2394(5) 0.0411(15) Uani d . 1 . . N
N2 0.2000(6) -0.0986(5) 0.2601(6) 0.0475(17) Uani d . 1 . . N
N3 0.2720(5) 0.0842(5) 0.6988(5) 0.0430(15) Uani d . 1 . . N
N4 0.2508(5) -0.1019(5) 0.8141(5) 0.0405(15) Uani d . 1 . . N
C1 0.5388(6) 0.2882(7) 0.0154(6) 0.0419(18) Uani d . 1 A . C
C2 0.4363(7) 0.3108(8) -0.0615(6) 0.065(3) Uani d D 1 . . C
C3 0.4862(6) 0.2799(6) 0.4606(6) 0.0364(16) Uani d . 1 B . C
C4 0.5629(6) 0.3084(7) 0.5599(7) 0.063(2) Uani d D 1 . . C
C5 0.2449(7) 0.0776(6) 0.3095(7) 0.053(2) Uani d . 1 . . C
H5 0.2337 0.1358 0.3523 0.063 Uiso calc R 1 . . H
C6 0.1866(8) -0.0135(7) 0.3207(8) 0.055(2) Uani d . 1 . . C
H6 0.1372 -0.0160 0.3710 0.066 Uiso calc R 1 . . H
C7 0.2704(6) -0.0892(7) 0.1897(7) 0.048(2) Uani d . 1 . . C
H7 0.2809 -0.1468 0.1459 0.058 Uiso calc R 1 . . H
C8 0.3294(6) 0.0019(6) 0.1775(7) 0.0421(18) Uani d . 1 . . C
C9 0.4073(9) 0.0107(8) 0.0953(9) 0.074(3) Uani d . 1 . . C
H9a 0.4276 -0.0590 0.0741 0.111 Uiso calc R 1 . . H
H9b 0.4703 0.0485 0.1248 0.111 Uiso calc R 1 . . H
H9c 0.3741 0.0483 0.0342 0.111 Uiso calc R 1 . . H
C10 0.2042(8) 0.0768(6) 0.7733(7) 0.055(2) Uani d . 1 . . C
H10 0.1628 0.1355 0.7874 0.066 Uiso calc R 1 . . H
C11 0.1936(7) -0.0151(7) 0.8299(7) 0.051(2) Uani d . 1 . . C
H11 0.1449 -0.0168 0.8810 0.061 Uiso calc R 1 . . H
C12 0.3190(6) -0.0926(6) 0.7407(6) 0.0452(19) Uani d . 1 . . C
H12 0.3617 -0.1507 0.7281 0.054 Uiso calc R 1 . . H
C13 0.3302(6) -0.0014(6) 0.6816(7) 0.0415(17) Uani d . 1 . . C
C14 0.4077(10) 0.0047(8) 0.5999(9) 0.082(3) Uani d . 1 . . C
H14a 0.4242 -0.0656 0.5772 0.122 Uiso calc R 1 . . H
H14b 0.4727 0.0388 0.6301 0.122 Uiso calc R 1 . . H
H14c 0.3764 0.0448 0.5398 0.122 Uiso calc R 1 . . H
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N1 Ag1 N2 . 2 120.6(3) yes
N1 Ag1 O1 . . 121.1(2) yes
N1 Ag1 O4 . . 111.5(2) yes
N2 Ag1 O1 2 . 107.3(3) yes
N2 Ag1 O4 2 . 99.2(2) yes
O1 Ag1 O4 . . 90.9(2) yes
N3 Ag2 N4 . 2_556 120.9(2) yes
N3 Ag2 O2 . 4_566 104.5(3) yes
N3 Ag2 O3 . . 120.3(2) yes
N4 Ag2 O2 2_556 4_566 106.7(2) yes
N4 Ag2 O3 2_556 . 107.6(2) yes
O2 Ag2 O3 4_566 . 91.6(2) yes
C1 O1 Ag1 . . 143.0(6) no
C1 O2 Ag2 . 4_665 107.6(5) no
C3 O3 Ag2 . . 143.8(6) no
C3 O4 Ag1 . . 108.5(5) no
C5 N1 C8 . . 117.8(7) no
C5 N1 Ag1 . . 115.7(5) no
C8 N1 Ag1 . . 126.3(5) no
C7 N2 C6 . . 116.3(7) no
C7 N2 Ag1 . 2_545 120.4(5) no
C6 N2 Ag1 . 2_545 123.2(5) no
C10 N3 C13 . . 117.1(7) no
C10 N3 Ag2 . . 117.1(5) no
C13 N3 Ag2 . . 125.6(5) no
C12 N4 C11 . . 115.1(7) no
C12 N4 Ag2 . 2_546 120.2(5) no
C11 N4 Ag2 . 2_546 124.5(5) no
O1 C1 O2 . . 128.5(8) no
O1 C1 C2 . . 117.9(7) no
O2 C1 C2 . . 113.6(7) no
F3 C2 F1 . . 107.0(10) no
F1' C2 F2' . . 107.7(15) no
F1' C2 F3' . . 109.0(18) no
F2' C2 F3' . . 107.9(16) no
F3 C2 F2 . . 105.1(10) no
F1 C2 F2 . . 108.0(10) no
F3 C2 C1 . . 113.3(8) no
F1 C2 C1 . . 112.5(9) no
F1' C2 C1 . . 109(2) no
F2' C2 C1 . . 110.5(14) no
F3' C2 C1 . . 112.4(18) no
F2 C2 C1 . . 110.5(8) no
O3 C3 O4 . . 129.5(8) no
O3 C3 C4 . . 117.4(7) no
O4 C3 C4 . . 113.0(7) no
F5 C4 F4 . . 105.7(11) no
F5 C4 F6 . . 105.9(10) no
F4 C4 F6 . . 110.1(12) no
F5' C4 F4' . . 107.3(13) no
F5' C4 F6' . . 105.1(12) no
F4' C4 F6' . . 104.7(12) no
F5 C4 C3 . . 112.1(8) no
F4 C4 C3 . . 111.9(10) no
F6 C4 C3 . . 110.8(9) no
F5' C4 C3 . . 114.1(11) no
F4' C4 C3 . . 111.6(12) no
F6' C4 C3 . . 113.4(10) no
N1 C5 C6 . . 121.9(7) no
N1 C5 H5 . . 119.0 no
C6 C5 H5 . . 119.0 no
N2 C6 C5 . . 120.9(8) no
N2 C6 H6 . . 119.6 no
C5 C6 H6 . . 119.6 no
N2 C7 C8 . . 123.3(7) no
N2 C7 H7 . . 118.3 no
C8 C7 H7 . . 118.3 no
N1 C8 C7 . . 119.6(7) no
N1 C8 C9 . . 118.4(7) no
C7 C8 C9 . . 122.0(7) no
C8 C9 H9a . . 109.5 no
C8 C9 H9b . . 109.5 no
H9a C9 H9b . . 109.5 no
C8 C9 H9c . . 109.5 no
H9a C9 H9c . . 109.5 no
H9b C9 H9c . . 109.5 no
N3 C10 C11 . . 121.9(8) no
N3 C10 H10 . . 119.1 no
C11 C10 H10 . . 119.1 no
N4 C11 C10 . . 122.2(8) no
N4 C11 H11 . . 118.9 no
C10 C11 H11 . . 118.9 no
N4 C12 C13 . . 123.8(7) no
N4 C12 H12 . . 118.1 no
C13 C12 H12 . . 118.1 no
N3 C13 C12 . . 119.9(7) no
N3 C13 C14 . . 118.5(7) no
C12 C13 C14 . . 121.7(7) no
C13 C14 H14a . . 109.5 no
C13 C14 H14b . . 109.5 no
H14a C14 H14b . . 109.5 no
C13 C14 H14c . . 109.5 no
H14a C14 H14c . . 109.5 no
H14b C14 H14c . . 109.5 no
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ag1 N1 . 2.283(6) yes
Ag1 N2 2 2.318(6) yes
Ag1 O1 . 2.387(7) yes
Ag1 O4 . 2.407(6) yes
Ag2 N3 . 2.278(6) yes
Ag2 N4 2_556 2.288(6) yes
Ag2 O2 4_566 2.392(7) yes
Ag2 O3 . 2.398(6) yes
F1 C2 . 1.325(8) no
F2 C2 . 1.333(8) no
F3 C2 . 1.316(8) no
F1' C2 . 1.331(10) no
F2' C2 . 1.332(10) no
F3' C2 . 1.32(3) no
F4 C4 . 1.325(9) no
F5 C4 . 1.323(8) no
F6 C4 . 1.328(9) no
F4' C4 . 1.333(9) no
F5' C4 . 1.334(9) no
F6' C4 . 1.341(9) no
O1 C1 . 1.189(10) no
O2 C1 . 1.240(9) no
O2 Ag2 4_665 2.392(7) no
O3 C3 . 1.199(10) no
O4 C3 . 1.227(9) no
N1 C5 . 1.324(10) no
N1 C8 . 1.326(9) no
N2 C7 . 1.318(9) no
N2 C6 . 1.336(10) no
N2 Ag1 2_545 2.318(6) no
N3 C10 . 1.330(10) no
N3 C13 . 1.332(9) no
N4 C12 . 1.324(9) no
N4 C11 . 1.333(10) no
N4 Ag2 2_546 2.288(6) no
C1 C2 . 1.549(12) no
C3 C4 . 1.537(11) no
C5 C6 . 1.376(11) no
C5 H5 . 0.9300 no
C6 H6 . 0.9300 no
C7 C8 . 1.382(11) no
C7 H7 . 0.9300 no
C8 C9 . 1.497(13) no
C9 H9a . 0.9600 no
C9 H9b . 0.9600 no
C9 H9c . 0.9600 no
C10 C11 . 1.374(11) no
C10 H10 . 0.9300 no
C11 H11 . 0.9300 no
C12 C13 . 1.385(11) no
C12 H12 . 0.9300 no
C13 C14 . 1.485(13) no
C14 H14a . 0.9600 no
C14 H14b . 0.9600 no
C14 H14c . 0.9600 no
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion
_geom_torsion_publ_flag
N1 Ag1 O1 C1 . 71.5(12) no
N2 Ag1 O1 C1 2 -72.6(11) no
O4 Ag1 O1 C1 . -172.5(11) no
N3 Ag2 O3 C3 . -72.0(10) no
N4 Ag2 O3 C3 2_556 72.1(10) no
O2 Ag2 O3 C3 4_566 -179.8(10) no
N1 Ag1 O4 C3 . -65.8(6) no
N2 Ag1 O4 C3 2 62.3(6) no
O1 Ag1 O4 C3 . 170.0(6) no
N2 Ag1 N1 C5 2 -39.9(7) no
O1 Ag1 N1 C5 . -179.4(6) no
O4 Ag1 N1 C5 . 75.7(6) no
N2 Ag1 N1 C8 2 135.4(7) no
O1 Ag1 N1 C8 . -4.0(8) no
O4 Ag1 N1 C8 . -108.9(7) no
N4 Ag2 N3 C10 2_556 38.2(7) no
O2 Ag2 N3 C10 4_566 -81.8(6) no
O3 Ag2 N3 C10 . 177.6(6) no
N4 Ag2 N3 C13 2_556 -146.0(6) no
O2 Ag2 N3 C13 4_566 94.0(7) no
O3 Ag2 N3 C13 . -6.6(8) no
Ag1 O1 C1 O2 . -162.0(8) no
Ag1 O1 C1 C2 . 15.1(15) no
Ag2 O2 C1 O1 4_665 -7.9(12) no
Ag2 O2 C1 C2 4_665 175.0(6) no
O1 C1 C2 F3 . -11.1(14) no
O2 C1 C2 F3 . 166.5(11) no
O1 C1 C2 F1 . -132.6(12) no
O2 C1 C2 F1 . 44.9(13) no
O1 C1 C2 F1' . -80(3) no
O2 C1 C2 F1' . 98(3) no
O1 C1 C2 F2' . 162(2) no
O2 C1 C2 F2' . -21(2) no
O1 C1 C2 F3' . 41.4(19) no
O2 C1 C2 F3' . -141.1(17) no
O1 C1 C2 F2 . 106.6(14) no
O2 C1 C2 F2 . -75.9(14) no
Ag2 O3 C3 O4 . 167.7(7) no
Ag2 O3 C3 C4 . -10.8(14) no
Ag1 O4 C3 O3 . 6.9(11) no
Ag1 O4 C3 C4 . -174.6(5) no
O3 C3 C4 F5 . 9.9(15) no
O4 C3 C4 F5 . -168.8(13) no
O3 C3 C4 F4 . 128.5(17) no
O4 C3 C4 F4 . -50.3(17) no
O3 C3 C4 F6 . -108.3(16) no
O4 C3 C4 F6 . 73.0(16) no
O3 C3 C4 F5' . -52(2) no
O4 C3 C4 F5' . 129(2) no
O3 C3 C4 F4' . 70(2) no
O4 C3 C4 F4' . -109(2) no
O3 C3 C4 F6' . -172.3(16) no
O4 C3 C4 F6' . 9.0(17) no
C8 N1 C5 C6 . 1.6(14) no
Ag1 N1 C5 C6 . 177.3(7) no
C7 N2 C6 C5 . -0.7(14) no
Ag1 N2 C6 C5 2_545 -178.2(7) no
N1 C5 C6 N2 . -0.4(15) no
C6 N2 C7 C8 . 0.6(14) no
Ag1 N2 C7 C8 2_545 178.2(7) no
C5 N1 C8 C7 . -1.6(13) no
Ag1 N1 C8 C7 . -176.9(6) no
C5 N1 C8 C9 . 177.8(8) no
Ag1 N1 C8 C9 . 2.5(12) no
N2 C7 C8 N1 . 0.5(14) no
N2 C7 C8 C9 . -178.8(9) no
C13 N3 C10 C11 . -0.5(14) no
Ag2 N3 C10 C11 . 175.7(7) no
C12 N4 C11 C10 . 0.5(13) no
Ag2 N4 C11 C10 2_546 -175.2(7) no
N3 C10 C11 N4 . 0.4(15) no
C11 N4 C12 C13 . -1.4(12) no
Ag2 N4 C12 C13 2_546 174.6(6) no
C10 N3 C13 C12 . -0.4(12) no
Ag2 N3 C13 C12 . -176.2(6) no
C10 N3 C13 C14 . -179.2(9) no
Ag2 N3 C13 C14 . 5.0(12) no
N4 C12 C13 N3 . 1.4(13) no
N4 C12 C13 C14 . -179.8(9) no
