#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/66/2206659.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2206659
loop_
_publ_author_name
'Li, Zong-Xiao'
'Zhang, Xin-Li'
_publ_section_title
;
 Bis[4-chloro-2-(cyclohexyliminomethyl)phenolato]zinc(II)
;
_journal_coeditor_code           CI6629
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1755
_journal_page_last               m1756
_journal_paper_doi               10.1107/S1600536805025250
_journal_volume                  61
_journal_year                    2005
_chemical_formula_iupac          '{Zn (C13 H15 Cl1 N1 O1)2]'
_chemical_formula_moiety         'C26 H30 Cl2 N2 O2 Zn'
_chemical_formula_sum            'C26 H30 Cl2 N2 O2 Zn'
_chemical_formula_weight         538.79
_chemical_name_systematic
;
Bis[4-chloro-2-(cyclohexyliminomethyl)phenolato]zinc(II)
;
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   14.848(2)
_cell_length_b                   13.567(2)
_cell_length_c                   24.993(5)
_cell_measurement_reflns_used    30
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      13.57
_cell_measurement_theta_min      2.19
_cell_volume                     5034.7(14)
_computing_cell_refinement       XSCANS
_computing_data_collection       'XSCANS (Siemens, 1995)'
_computing_data_reduction        'SHELXTL (Siemens, 1995)'
_computing_molecular_graphics    SHELXTL
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Siemens P4'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'normal-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0237
_diffrn_reflns_av_sigmaI/netI    0.0694
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       1
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            5714
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         1.63
_diffrn_standards_decay_%        3.41
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.214
_exptl_absorpt_correction_T_max  0.747
_exptl_absorpt_correction_T_min  0.472
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(XSCANS; Siemens, 1995)'
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.422
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             2240
_exptl_crystal_size_max          0.68
_exptl_crystal_size_mid          0.50
_exptl_crystal_size_min          0.24
_refine_diff_density_max         0.227
_refine_diff_density_min         -0.341
_refine_ls_extinction_coef       0.00191(12)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL97
_refine_ls_goodness_of_fit_ref   0.901
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     299
_refine_ls_number_reflns         4687
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.901
_refine_ls_R_factor_all          0.0899
_refine_ls_R_factor_gt           0.0373
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0308P)²] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0661
_refine_ls_wR_factor_ref         0.0746
_reflns_number_gt                2587
_reflns_number_total             4687
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ci6629.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        5034.5(13)
_cod_database_code               2206659
_cod_database_fobs_code          2206659
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z-1/2'
'-x-1/2, y-1/2, z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_type_symbol
Zn 0.64196(2) 0.58257(3) 0.305777(14) 0.04529(13) Uani d . 1 Zn
Cl1 0.82237(6) 0.26492(7) 0.10343(3) 0.0691(3) Uani d . 1 Cl
Cl2 0.38801(8) 0.88393(8) 0.48846(4) 0.0945(4) Uani d . 1 Cl
O1 0.71863(13) 0.59206(15) 0.24402(8) 0.0511(6) Uani d . 1 O
O2 0.66003(13) 0.66812(15) 0.36550(9) 0.0556(6) Uani d . 1 O
N1 0.67360(16) 0.44078(17) 0.32149(9) 0.0413(6) Uani d . 1 N
N2 0.51475(15) 0.62634(17) 0.29080(9) 0.0399(6) Uani d . 1 N
C1 0.5955(2) 0.7105(2) 0.39229(13) 0.0447(8) Uani d . 1 C
C2 0.6150(2) 0.7521(2) 0.44308(14) 0.0569(9) Uani d . 1 C
H2 0.6721 0.7433 0.4575 0.068 Uiso calc R 1 H
C3 0.5532(3) 0.8042(2) 0.47122(13) 0.0605(10) Uani d . 1 C
H3 0.5697 0.8327 0.5036 0.073 Uiso calc R 1 H
C4 0.4660(2) 0.8156(2) 0.45262(13) 0.0557(9) Uani d . 1 C
C5 0.4424(2) 0.7732(2) 0.40463(12) 0.0517(9) Uani d . 1 C
H5 0.3837 0.7799 0.3921 0.062 Uiso calc R 1 H
C6 0.5052(2) 0.7199(2) 0.37418(12) 0.0417(8) Uani d . 1 C
C7 0.4726(2) 0.6810(2) 0.32398(12) 0.0446(8) Uani d . 1 C
H7 0.4139 0.6977 0.3147 0.054 Uiso calc R 1 H
C8 0.4671(2) 0.5996(2) 0.24119(12) 0.0424(8) Uani d . 1 C
H8 0.4029 0.6142 0.2458 0.051 Uiso calc R 1 H
C9 0.4774(2) 0.4906(2) 0.22997(12) 0.0510(9) Uani d . 1 C
H9A 0.4500 0.4530 0.2587 0.061 Uiso calc R 1 H
H9B 0.5408 0.4738 0.2285 0.061 Uiso calc R 1 H
C10 0.4327(2) 0.4638(3) 0.17712(13) 0.0651(10) Uani d . 1 C
H10A 0.4421 0.3943 0.1699 0.078 Uiso calc R 1 H
H10B 0.3684 0.4752 0.1798 0.078 Uiso calc R 1 H
C11 0.4702(2) 0.5235(3) 0.13173(14) 0.0728(11) Uani d . 1 C
H11A 0.4393 0.5063 0.0989 0.087 Uiso calc R 1 H
H11B 0.5336 0.5083 0.1272 0.087 Uiso calc R 1 H
C12 0.4593(3) 0.6326(3) 0.14229(13) 0.0720(11) Uani d . 1 C
H12A 0.3957 0.6490 0.1432 0.086 Uiso calc R 1 H
H12B 0.4869 0.6698 0.1135 0.086 Uiso calc R 1 H
C13 0.5028(2) 0.6612(2) 0.19529(12) 0.0608(10) Uani d . 1 C
H13A 0.5675 0.6525 0.1927 0.073 Uiso calc R 1 H
H13B 0.4910 0.7303 0.2025 0.073 Uiso calc R 1 H
C14 0.74025(19) 0.5145(2) 0.21489(12) 0.0422(8) Uani d . 1 C
C15 0.7690(2) 0.5304(3) 0.16133(13) 0.0537(9) Uani d . 1 C
H15 0.7709 0.5945 0.1482 0.064 Uiso calc R 1 H
C16 0.7937(2) 0.4551(3) 0.12867(13) 0.0526(9) Uani d . 1 C
H16 0.8119 0.4684 0.0938 0.063 Uiso calc R 1 H
C17 0.7921(2) 0.3594(2) 0.14683(13) 0.0470(8) Uani d . 1 C
C18 0.76606(18) 0.3398(2) 0.19832(12) 0.0443(8) Uani d . 1 C
H18 0.7668 0.2752 0.2108 0.053 Uiso calc R 1 H
C19 0.73829(17) 0.4160(2) 0.23249(11) 0.0375(7) Uani d . 1 C
C20 0.71104(19) 0.3870(2) 0.28612(12) 0.0442(8) Uani d . 1 C
H20 0.7222 0.3219 0.2957 0.053 Uiso calc R 1 H
C21 0.65493(19) 0.3976(2) 0.37475(12) 0.0473(8) Uani d . 1 C
H21 0.6650 0.3263 0.3731 0.057 Uiso calc R 1 H
C22 0.55684(19) 0.4166(2) 0.38920(12) 0.0509(8) Uani d . 1 C
H22A 0.5180 0.3831 0.3639 0.061 Uiso calc R 1 H
H22B 0.5444 0.4867 0.3871 0.061 Uiso calc R 1 H
C23 0.5369(2) 0.3798(2) 0.44557(12) 0.0583(9) Uani d . 1 C
H23A 0.4748 0.3945 0.4547 0.070 Uiso calc R 1 H
H23B 0.5449 0.3089 0.4470 0.070 Uiso calc R 1 H
C24 0.5988(2) 0.4284(2) 0.48561(13) 0.0603(10) Uani d . 1 C
H24A 0.5856 0.4037 0.5212 0.072 Uiso calc R 1 H
H24B 0.5885 0.4990 0.4856 0.072 Uiso calc R 1 H
C25 0.6968(2) 0.4075(3) 0.47208(12) 0.0670(10) Uani d . 1 C
H25A 0.7083 0.3374 0.4751 0.080 Uiso calc R 1 H
H25B 0.7355 0.4414 0.4974 0.080 Uiso calc R 1 H
C26 0.71891(19) 0.4419(3) 0.41536(12) 0.0578(10) Uani d . 1 C
H26A 0.7151 0.5132 0.4137 0.069 Uiso calc R 1 H
H26B 0.7801 0.4230 0.4066 0.069 Uiso calc R 1 H
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
O2 Zn O1 120.24(9) y
O2 Zn N2 95.61(9) y
O1 Zn N2 112.72(9) y
O2 Zn N1 113.23(9) y
O1 Zn N1 94.72(9) y
N2 Zn N1 122.35(9) y
C14 O1 Zn 122.25(18) ?
C1 O2 Zn 124.50(19) ?
C20 N1 C21 118.6(2) ?
C20 N1 Zn 120.8(2) ?
C21 N1 Zn 120.56(18) ?
C7 N2 C8 117.0(2) ?
C7 N2 Zn 120.7(2) ?
C8 N2 Zn 122.27(19) ?
O2 C1 C2 119.0(3) ?
O2 C1 C6 124.8(3) ?
C2 C1 C6 116.2(3) ?
C3 C2 C1 122.3(3) ?
C3 C2 H2 118.9 ?
C1 C2 H2 118.9 ?
C2 C3 C4 121.2(3) ?
C2 C3 H3 119.4 ?
C4 C3 H3 119.4 ?
C5 C4 C3 118.9(3) ?
C5 C4 Cl2 120.3(3) ?
C3 C4 Cl2 120.8(3) ?
C4 C5 C6 121.3(3) ?
C4 C5 H5 119.4 ?
C6 C5 H5 119.4 ?
C5 C6 C1 120.0(3) ?
C5 C6 C7 115.9(3) ?
C1 C6 C7 124.0(3) ?
N2 C7 C6 127.8(3) ?
N2 C7 H7 116.1 ?
C6 C7 H7 116.1 ?
N2 C8 C9 110.4(2) ?
N2 C8 C13 109.5(2) ?
C9 C8 C13 111.3(3) ?
N2 C8 H8 108.5 ?
C9 C8 H8 108.5 ?
C13 C8 H8 108.5 ?
C8 C9 C10 110.5(3) ?
C8 C9 H9A 109.5 ?
C10 C9 H9A 109.5 ?
C8 C9 H9B 109.5 ?
C10 C9 H9B 109.5 ?
H9A C9 H9B 108.1 ?
C11 C10 C9 111.4(3) ?
C11 C10 H10A 109.3 ?
C9 C10 H10A 109.3 ?
C11 C10 H10B 109.3 ?
C9 C10 H10B 109.3 ?
H10A C10 H10B 108.0 ?
C10 C11 C12 110.9(3) ?
C10 C11 H11A 109.5 ?
C12 C11 H11A 109.5 ?
C10 C11 H11B 109.5 ?
C12 C11 H11B 109.5 ?
H11A C11 H11B 108.1 ?
C11 C12 C13 110.8(3) ?
C11 C12 H12A 109.5 ?
C13 C12 H12A 109.5 ?
C11 C12 H12B 109.5 ?
C13 C12 H12B 109.5 ?
H12A C12 H12B 108.1 ?
C8 C13 C12 111.7(3) ?
C8 C13 H13A 109.3 ?
C12 C13 H13A 109.3 ?
C8 C13 H13B 109.3 ?
C12 C13 H13B 109.3 ?
H13A C13 H13B 107.9 ?
O1 C14 C19 125.4(3) ?
O1 C14 C15 118.1(3) ?
C19 C14 C15 116.4(3) ?
C16 C15 C14 122.2(3) ?
C16 C15 H15 118.9 ?
C14 C15 H15 118.9 ?
C15 C16 C17 120.5(3) ?
C15 C16 H16 119.8 ?
C17 C16 H16 119.8 ?
C18 C17 C16 119.9(3) ?
C18 C17 Cl1 121.1(3) ?
C16 C17 Cl1 119.1(3) ?
C17 C18 C19 120.8(3) ?
C17 C18 H18 119.6 ?
C19 C18 H18 119.6 ?
C18 C19 C14 120.2(3) ?
C18 C19 C20 116.3(3) ?
C14 C19 C20 123.4(3) ?
N1 C20 C19 127.3(3) ?
N1 C20 H20 116.4 ?
C19 C20 H20 116.4 ?
N1 C21 C26 109.2(2) ?
N1 C21 C22 109.0(2) ?
C26 C21 C22 111.9(2) ?
N1 C21 H21 108.9 ?
C26 C21 H21 108.9 ?
C22 C21 H21 108.9 ?
C21 C22 C23 110.5(3) ?
C21 C22 H22A 109.6 ?
C23 C22 H22A 109.6 ?
C21 C22 H22B 109.6 ?
C23 C22 H22B 109.6 ?
H22A C22 H22B 108.1 ?
C24 C23 C22 110.6(3) ?
C24 C23 H23A 109.5 ?
C22 C23 H23A 109.5 ?
C24 C23 H23B 109.5 ?
C22 C23 H23B 109.5 ?
H23A C23 H23B 108.1 ?
C23 C24 C25 110.7(3) ?
C23 C24 H24A 109.5 ?
C25 C24 H24A 109.5 ?
C23 C24 H24B 109.5 ?
C25 C24 H24B 109.5 ?
H24A C24 H24B 108.1 ?
C24 C25 C26 110.8(3) ?
C24 C25 H25A 109.5 ?
C26 C25 H25A 109.5 ?
C24 C25 H25B 109.5 ?
C26 C25 H25B 109.5 ?
H25A C25 H25B 108.1 ?
C21 C26 C25 111.5(3) ?
C21 C26 H26A 109.3 ?
C25 C26 H26A 109.3 ?
C21 C26 H26B 109.3 ?
C25 C26 H26B 109.3 ?
H26A C26 H26B 108.0 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
Zn O2 1.910(2) y
Zn O1 1.922(2) y
Zn N2 2.015(2) y
Zn N1 2.019(2) y
Cl1 C17 1.738(3) ?
Cl2 C4 1.733(3) ?
O1 C14 1.320(3) ?
O2 C1 1.302(3) ?
N1 C20 1.274(3) ?
N1 C21 1.480(3) ?
N2 C7 1.276(3) ?
N2 C8 1.473(3) ?
C1 C2 1.419(4) ?
C1 C6 1.421(4) ?
C2 C3 1.354(4) ?
C2 H2 0.93 ?
C3 C4 1.385(4) ?
C3 H3 0.93 ?
C4 C5 1.376(4) ?
C5 C6 1.404(4) ?
C5 H5 0.93 ?
C6 C7 1.444(4) ?
C7 H7 0.93 ?
C8 C9 1.513(4) ?
C8 C13 1.515(4) ?
C8 H8 0.98 ?
C9 C10 1.522(4) ?
C9 H9A 0.97 ?
C9 H9B 0.97 ?
C10 C11 1.501(4) ?
C10 H10A 0.97 ?
C10 H10B 0.97 ?
C11 C12 1.512(4) ?
C11 H11A 0.97 ?
C11 H11B 0.97 ?
C12 C13 1.524(4) ?
C12 H12A 0.97 ?
C12 H12B 0.97 ?
C13 H13A 0.97 ?
C13 H13B 0.97 ?
C14 C19 1.406(4) ?
C14 C15 1.422(4) ?
C15 C16 1.358(4) ?
C15 H15 0.93 ?
C16 C17 1.376(4) ?
C16 H16 0.93 ?
C17 C18 1.370(4) ?
C18 C19 1.403(4) ?
C18 H18 0.93 ?
C19 C20 1.455(4) ?
C20 H20 0.93 ?
C21 C26 1.515(4) ?
C21 C22 1.523(4) ?
C21 H21 0.98 ?
C22 C23 1.524(4) ?
C22 H22A 0.97 ?
C22 H22B 0.97 ?
C23 C24 1.510(4) ?
C23 H23A 0.97 ?
C23 H23B 0.97 ?
C24 C25 1.520(4) ?
C24 H24A 0.97 ?
C24 H24B 0.97 ?
C25 C26 1.528(4) ?
C25 H25A 0.97 ?
C25 H25B 0.97 ?
C26 H26A 0.97 ?
C26 H26B 0.97 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
O2 Zn O1 C14 147.1(2)
N2 Zn O1 C14 -101.4(2)
N1 Zn O1 C14 26.7(2)
O1 Zn O2 C1 138.6(2)
N2 Zn O2 C1 18.1(2)
N1 Zn O2 C1 -110.7(2)
O2 Zn N1 C20 -142.6(2)
O1 Zn N1 C20 -16.8(2)
N2 Zn N1 C20 103.9(2)
O2 Zn N1 C21 36.5(2)
O1 Zn N1 C21 162.3(2)
N2 Zn N1 C21 -77.0(2)
O2 Zn N2 C7 -10.4(2)
O1 Zn N2 C7 -136.6(2)
N1 Zn N2 C7 111.7(2)
O2 Zn N2 C8 167.9(2)
O1 Zn N2 C8 41.8(2)
N1 Zn N2 C8 -70.0(2)
Zn O2 C1 C2 164.6(2)
Zn O2 C1 C6 -16.3(4)
O2 C1 C2 C3 174.5(3)
C6 C1 C2 C3 -4.6(5)
C1 C2 C3 C4 2.9(5)
C2 C3 C4 C5 -0.1(5)
C2 C3 C4 Cl2 -179.0(3)
C3 C4 C5 C6 -0.8(5)
Cl2 C4 C5 C6 178.2(2)
C4 C5 C6 C1 -1.1(4)
C4 C5 C6 C7 -178.6(3)
O2 C1 C6 C5 -175.4(3)
C2 C1 C6 C5 3.7(4)
O2 C1 C6 C7 1.8(5)
C2 C1 C6 C7 -179.1(3)
C8 N2 C7 C6 -177.7(3)
Zn N2 C7 C6 0.7(4)
C5 C6 C7 N2 -176.1(3)
C1 C6 C7 N2 6.6(5)
C7 N2 C8 C9 -133.9(3)
Zn N2 C8 C9 47.6(3)
C7 N2 C8 C13 103.2(3)
Zn N2 C8 C13 -75.3(3)
N2 C8 C9 C10 -176.8(2)
C13 C8 C9 C10 -55.0(3)
C8 C9 C10 C11 56.7(4)
C9 C10 C11 C12 -57.4(4)
C10 C11 C12 C13 56.0(4)
N2 C8 C13 C12 176.9(3)
C9 C8 C13 C12 54.6(4)
C11 C12 C13 C8 -54.8(4)
Zn O1 C14 C19 -22.5(4)
Zn O1 C14 C15 158.2(2)
O1 C14 C15 C16 179.1(3)
C19 C14 C15 C16 -0.3(4)
C14 C15 C16 C17 -0.3(5)
C15 C16 C17 C18 -0.6(5)
C15 C16 C17 Cl1 178.9(2)
C16 C17 C18 C19 2.0(4)
Cl1 C17 C18 C19 -177.5(2)
C17 C18 C19 C14 -2.6(4)
C17 C18 C19 C20 179.3(3)
O1 C14 C19 C18 -177.6(3)
C15 C14 C19 C18 1.7(4)
O1 C14 C19 C20 0.4(5)
C15 C14 C19 C20 179.7(3)
C21 N1 C20 C19 -177.3(3)
Zn N1 C20 C19 1.8(4)
C18 C19 C20 N1 -170.9(3)
C14 C19 C20 N1 11.0(5)
C20 N1 C21 C26 108.4(3)
Zn N1 C21 C26 -70.7(3)
C20 N1 C21 C22 -129.1(3)
Zn N1 C21 C22 51.8(3)
N1 C21 C22 C23 -175.8(2)
C26 C21 C22 C23 -55.0(3)
C21 C22 C23 C24 57.3(4)
C22 C23 C24 C25 -58.7(4)
C23 C24 C25 C26 56.9(4)
N1 C21 C26 C25 174.5(2)
C22 C21 C26 C25 53.7(4)
C24 C25 C26 C21 -54.3(4)
