#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/74/2207488.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2207488
loop_
_publ_author_name
'K. Palani'
'M. N. Ponnuswamy'
'A. R. Suresh Babu'
'R. Raghunathan'
'M. Nethaji'
_publ_section_title
4'-(4-Chlorobenzoyl)-1'-methyldispiro[indole-3(2H),2'-pyrrolidine-3',3''(2''H)-indole]-2,2''-dione
_journal_coeditor_code           CI6683
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o4257
_journal_page_last               o4259
_journal_paper_doi               10.1107/S160053680503789X
_journal_volume                  61
_journal_year                    2005
_chemical_formula_iupac          'C26 H20 Cl N3 O3'
_chemical_formula_moiety         'C26 H20 Cl N3 O3'
_chemical_formula_sum            'C26 H20 Cl N3 O3'
_chemical_formula_weight         457.90
_chemical_name_systematic
;
4'-(4-Chlorobenzoyl)-1'-methyl-dispiro[indole-3(2H),2'-pyrrolidine-
3',3''(2''H)-indole]-2,2''-dione
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                104.275(9)
_cell_angle_beta                 93.998(10)
_cell_angle_gamma                102.305(9)
_cell_formula_units_Z            2
_cell_length_a                   9.795(6)
_cell_length_b                   10.316(6)
_cell_length_c                   11.670(7)
_cell_measurement_reflns_used    6234
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.29
_cell_measurement_theta_min      2.10
_cell_volume                     1107.2(11)
_computing_cell_refinement       'SAINT (Bruker, 2001)'
_computing_data_collection       'SMART (Bruker, 2001)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'ZORTEP (Zsolnai, 1997)'
_computing_publication_material  'PLATON (Spek, 2003)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.901
_diffrn_measurement_device_type  'Bruker SMART APEX area-detector'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0163
_diffrn_reflns_av_sigmaI/netI    0.0183
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            11608
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         27.29
_diffrn_reflns_theta_min         2.10
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.207
_exptl_absorpt_correction_T_max  0.959
_exptl_absorpt_correction_T_min  0.955
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 1996)'
_exptl_crystal_colour            Colourless
_exptl_crystal_density_diffrn    1.373
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             476
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.284
_refine_diff_density_min         -0.299
_refine_ls_extinction_coef       0.0105(18)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL97
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    refall
_refine_ls_matrix_type           full
_refine_ls_number_parameters     379
_refine_ls_number_reflns         4491
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_all          0.0481
_refine_ls_R_factor_gt           0.0397
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0518P)²+0.2477P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1018
_refine_ls_wR_factor_ref         0.1079
_reflns_number_gt                3746
_reflns_number_total             4491
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ci6683.cif
_cod_data_source_block           I
_cod_original_cell_volume        1107.2(12)
_cod_database_code               2207488
_cod_database_fobs_code          2207488
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_type_symbol
H3 0.391(2) 0.3927(19) 0.8816(17) 0.065(5) Uiso d 1 H
H2 0.636(2) 0.019(2) 1.0695(18) 0.072(6) Uiso d 1 H
Cl1 0.03103(6) 0.24821(8) 0.46553(6) 0.0998(2) Uani d 1 Cl
N3 0.46756(14) 0.37456(13) 0.86284(12) 0.0483(3) Uani d 1 N
O2 0.40878(12) 0.14756(12) 0.86139(10) 0.0565(3) Uani d 1 O
C16 0.68904(15) 0.40253(14) 0.81108(12) 0.0406(3) Uani d 1 C
C17 0.58261(15) 0.46926(15) 0.84269(12) 0.0433(3) Uani d 1 C
C8 0.76452(15) 0.30381(15) 1.02912(13) 0.0423(3) Uani d 1 C
N2 0.66605(15) 0.08616(15) 1.04051(13) 0.0551(3) Uani d 1 N
O1 0.62657(14) -0.03960(11) 0.84430(11) 0.0642(3) Uani d 1 O
N1 0.85893(14) 0.20505(13) 0.83758(11) 0.0490(3) Uani d 1 N
C11 0.49094(15) 0.24701(15) 0.84700(12) 0.0426(3) Uani d 1 C
O3 0.70782(14) 0.23271(16) 0.52152(11) 0.0741(4) Uani d 1 O
C20 0.47083(17) 0.20710(15) 0.55448(12) 0.0481(3) Uani d 1 C
C19 0.61905(18) 0.19908(16) 0.58304(13) 0.0514(4) Uani d 1 C
C7 0.82088(16) 0.44351(16) 1.07676(15) 0.0492(4) Uani d 1 C
C10 0.64044(15) 0.25375(14) 0.81173(12) 0.0404(3) Uani d 1 C
C15 0.81347(17) 0.47508(17) 0.78572(15) 0.0512(4) Uani d 1 C
C3 0.66632(16) 0.06898(15) 0.92135(14) 0.0478(3) Uani d 1 C
C18 0.65428(18) 0.15023(16) 0.69213(13) 0.0481(4) Uani d 1 C
C9 0.71919(16) 0.22292(16) 1.10575(13) 0.0482(3) Uani d 1 C
C2 0.73605(15) 0.21217(14) 0.90215(12) 0.0416(3) Uani d 1 C
C25 0.3562(2) 0.12365(18) 0.58535(14) 0.0576(4) Uani d 1 C
C12 0.5985(2) 0.60811(17) 0.85248(15) 0.0566(4) Uani d 1 C
C6 0.82829(18) 0.4998(2) 1.19976(16) 0.0594(4) Uani d 1 C
C21 0.4466(2) 0.30173(19) 0.49361(15) 0.0583(4) Uani d 1 C
C4 0.72862(19) 0.2777(2) 1.22824(15) 0.0619(4) Uani d 1 C
C22 0.3127(2) 0.3159(2) 0.46736(17) 0.0649(5) Uani d 1 C
C24 0.2208(2) 0.1353(2) 0.55710(16) 0.0655(5) Uani d 1 C
C14 0.8318(2) 0.61476(18) 0.79736(16) 0.0597(4) Uani d 1 C
C23 0.20077(19) 0.2316(2) 0.49921(15) 0.0633(4) Uani d 1 C
C5 0.7836(2) 0.4173(2) 1.27360(16) 0.0664(5) Uani d 1 C
C26 0.8054(2) 0.1334(2) 0.71131(15) 0.0605(5) Uani d 1 C
C13 0.7258(2) 0.67970(18) 0.83050(16) 0.0624(5) Uani d 1 C
C1 0.9658(2) 0.1488(2) 0.8887(2) 0.0647(5) Uani d 1 C
H18 0.5871(18) 0.0637(18) 0.6842(14) 0.051(4) Uiso d 1 H
H7 0.8562(17) 0.5013(17) 1.0269(15) 0.052(4) Uiso d 1 H
H15 0.886(2) 0.4296(18) 0.7639(16) 0.061(5) Uiso d 1 H
H26A 0.803(2) 0.030(2) 0.6935(17) 0.074(6) Uiso d 1 H
H1C 0.996(2) 0.199(2) 0.974(2) 0.090(7) Uiso d 1 H
H26B 0.865(2) 0.1748(19) 0.6611(18) 0.069(5) Uiso d 1 H
H1B 0.933(2) 0.051(2) 0.8828(19) 0.079(6) Uiso d 1 H
H21 0.528(2) 0.360(2) 0.4716(18) 0.076(6) Uiso d 1 H
H25 0.3706(19) 0.0558(19) 0.6282(17) 0.064(5) Uiso d 1 H
H24 0.141(2) 0.077(2) 0.5779(18) 0.076(6) Uiso d 1 H
H6 0.8676(19) 0.598(2) 1.2335(17) 0.064(5) Uiso d 1 H
H4 0.698(2) 0.2179(19) 1.2785(18) 0.068(5) Uiso d 1 H
H12 0.525(2) 0.6519(19) 0.8710(16) 0.065(5) Uiso d 1 H
H1A 1.050(2) 0.158(2) 0.8435(19) 0.079(6) Uiso d 1 H
H14 0.921(2) 0.6698(19) 0.7817(17) 0.068(5) Uiso d 1 H
H22 0.301(2) 0.383(2) 0.4250(18) 0.077(6) Uiso d 1 H
H13 0.737(2) 0.772(2) 0.8369(18) 0.075(6) Uiso d 1 H
H5 0.792(2) 0.456(2) 1.3556(19) 0.071(6) Uiso d 1 H
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
C11 N3 C17 112.62(13) ?
C11 N3 H3 122.5(13) ?
C17 N3 H3 124.9(13) ?
C15 C16 C17 119.62(14) yes
C15 C16 C10 131.53(13) ?
C17 C16 C10 108.85(13) ?
C12 C17 C16 121.93(15) yes
C12 C17 N3 129.09(14) ?
C16 C17 N3 108.96(13) ?
C7 C8 C9 118.93(15) yes
C7 C8 C2 132.50(14) ?
C9 C8 C2 108.55(13) ?
C3 N2 C9 112.40(13) ?
C3 N2 H2 122.0(14) ?
C9 N2 H2 125.6(14) ?
C1 N1 C2 115.58(14) yes
C1 N1 C26 113.85(14) yes
C2 N1 C26 107.34(13) yes
O2 C11 N3 125.38(14) ?
O2 C11 C10 127.24(13) ?
N3 C11 C10 107.36(12) ?
C25 C20 C21 118.69(16) ?
C25 C20 C19 122.90(15) ?
C21 C20 C19 118.41(15) ?
O3 C19 C20 120.26(15) ?
O3 C19 C18 121.95(16) ?
C20 C19 C18 117.79(13) ?
C8 C7 C6 118.95(16) ?
C8 C7 H7 120.9(10) ?
C6 C7 H7 120.1(10) ?
C16 C10 C11 102.20(11) ?
C16 C10 C2 112.97(12) ?
C11 C10 C2 111.61(11) ?
C16 C10 C18 113.06(12) ?
C11 C10 C18 116.86(12) ?
C2 C10 C18 100.62(11) ?
C16 C15 C14 119.02(15) ?
C16 C15 H15 119.7(11) ?
C14 C15 H15 121.3(11) ?
O1 C3 N2 126.03(14) ?
O1 C3 C2 126.36(14) ?
N2 C3 C2 107.50(13) ?
C19 C18 C26 115.33(14) ?
C19 C18 C10 112.52(12) ?
C26 C18 C10 103.37(13) ?
C19 C18 H18 106.9(10) ?
C26 C18 H18 110.4(10) ?
C10 C18 H18 108.2(10) ?
C4 C9 N2 127.64(15) ?
C4 C9 C8 122.44(16) yes
N2 C9 C8 109.92(14) ?
N1 C2 C8 116.50(13) ?
N1 C2 C10 99.76(11) ?
C8 C2 C10 116.31(11) ?
N1 C2 C3 111.39(11) ?
C8 C2 C3 101.54(12) ?
C10 C2 C3 111.79(12) ?
C24 C25 C20 120.69(17) ?
C24 C25 H25 119.1(11) ?
C20 C25 H25 120.2(11) ?
C17 C12 C13 117.42(15) ?
C17 C12 H12 121.5(12) ?
C13 C12 H12 121.0(11) ?
C5 C6 C7 120.90(17) ?
C5 C6 H6 119.9(11) ?
C7 C6 H6 119.2(11) ?
C22 C21 C20 120.98(17) ?
C22 C21 H21 120.7(12) ?
C20 C21 H21 118.3(12) ?
C5 C4 C9 117.66(17) ?
C5 C4 H4 122.4(12) ?
C9 C4 H4 119.9(12) ?
C21 C22 C23 119.04(18) ?
C21 C22 H22 118.1(13) ?
C23 C22 H22 122.8(12) ?
C23 C24 C25 119.15(18) ?
C23 C24 H24 119.7(12) ?
C25 C24 H24 121.1(12) ?
C13 C14 C15 120.51(17) ?
C13 C14 H14 118.7(11) ?
C15 C14 H14 120.8(11) ?
C24 C23 C22 121.42(18) ?
C24 C23 Cl1 119.25(15) ?
C22 C23 Cl1 119.33(15) ?
C4 C5 C6 121.11(17) ?
C4 C5 H5 119.1(12) ?
C6 C5 H5 119.8(12) ?
N1 C26 C18 106.04(12) ?
N1 C26 H26A 111.1(11) ?
C18 C26 H26A 109.0(11) ?
N1 C26 H26B 109.1(12) ?
C18 C26 H26B 111.9(12) ?
H26A C26 H26B 109.6(16) ?
C14 C13 C12 121.43(16) ?
C14 C13 H13 120.5(13) ?
C12 C13 H13 118.1(13) ?
N1 C1 H1C 110.5(13) ?
N1 C1 H1B 112.9(13) ?
H1C C1 H1B 108.6(18) ?
N1 C1 H1A 109.3(12) ?
H1C C1 H1A 109.1(18) ?
H1B C1 H1A 106.2(17) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
Cl1 C23 1.735(2) yes
N3 C11 1.354(2) yes
N3 C17 1.400(2) y
N3 H3 0.84(2) ?
O2 C11 1.2166(18) yes
C16 C15 1.380(2) ?
C16 C17 1.390(2) ?
C16 C10 1.509(2) ?
C17 C12 1.382(2) ?
C8 C7 1.383(2) ?
C8 C9 1.400(2) ?
C8 C2 1.519(2) ?
N2 C3 1.358(2) yes
N2 C9 1.394(2) y
N2 H2 0.85(2) ?
O1 C3 1.218(2) yes
N1 C1 1.460(2) yes
N1 C2 1.469(2) yes
N1 C26 1.477(2) yes
C11 C10 1.541(2) ?
O3 C19 1.214(2) y
C20 C25 1.389(2) ?
C20 C21 1.390(2) ?
C20 C19 1.491(2) ?
C19 C18 1.524(2) ?
C7 C6 1.400(3) ?
C7 H7 0.961(17) ?
C10 C2 1.559(2) ?
C10 C18 1.568(2) ?
C15 C14 1.384(3) ?
C15 H15 0.947(19) ?
C3 C2 1.566(2) ?
C18 C26 1.534(2) ?
C18 H18 0.969(17) ?
C9 C4 1.390(2) ?
C25 C24 1.381(3) ?
C25 H25 0.982(19) ?
C12 C13 1.382(3) ?
C12 H12 0.939(19) ?
C6 C5 1.384(3) ?
C6 H6 0.970(19) ?
C21 C22 1.372(3) ?
C21 H21 0.98(2) ?
C4 C5 1.377(3) ?
C4 H4 0.97(2) ?
C22 C23 1.381(3) ?
C22 H22 0.96(2) ?
C24 C23 1.370(3) ?
C24 H24 0.96(2) ?
C14 C13 1.379(3) ?
C14 H14 0.99(2) ?
C5 H5 0.93(2) ?
C26 H26A 1.03(2) ?
C26 H26B 0.97(2) ?
C13 H13 0.92(2) ?
C1 H1C 0.99(2) ?
C1 H1B 0.97(2) ?
C1 H1A 1.01(2) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C18 H18 O1 . 0.97(2) 2.42(2) 2.936(3) 113.0(10) yes
C26 H26B O3 . 0.97(2) 2.43(2) 2.848(3) 106.0(10) yes
N2 H2 O2 2_657 0.85(2) 2.05(2) 2.896(3) 172(2) yes
C13 H13 O1 1_565 0.92(2) 2.40(2) 3.217(3) 148(2) yes
C7 H7 Cg1 . 0.96(2) 2.90(2) 3.572(3) 128.0(10) yes
C12 H12 Cg2 2_665 0.94(2) 2.90(2) 3.730(3) 149(2) yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C15 C16 C17 C12 -1.6(2)
C10 C16 C17 C12 178.41(13)
C15 C16 C17 N3 179.46(13)
C10 C16 C17 N3 -0.55(16)
C11 N3 C17 C12 -178.57(15)
C11 N3 C17 C16 0.29(17)
C17 N3 C11 O2 178.43(13)
C17 N3 C11 C10 0.09(16)
C25 C20 C19 O3 153.18(16)
C21 C20 C19 O3 -26.4(2)
C25 C20 C19 C18 -27.9(2)
C21 C20 C19 C18 152.53(15)
C9 C8 C7 C6 -1.2(2)
C2 C8 C7 C6 177.27(15)
C15 C16 C10 C11 -179.44(15)
C17 C16 C10 C11 0.57(14)
C15 C16 C10 C2 60.5(2)
C17 C16 C10 C2 -119.48(13)
C15 C16 C10 C18 -53.0(2)
C17 C16 C10 C18 127.06(13)
O2 C11 C10 C16 -178.69(14)
N3 C11 C10 C16 -0.40(14)
O2 C11 C10 C2 -57.69(19)
N3 C11 C10 C2 120.60(13)
O2 C11 C10 C18 57.33(19)
N3 C11 C10 C18 -124.38(13)
C17 C16 C15 C14 2.7(2)
C10 C16 C15 C14 -177.24(15)
C9 N2 C3 O1 179.52(15)
C9 N2 C3 C2 3.18(17)
O3 C19 C18 C26 -5.7(2)
C20 C19 C18 C26 175.44(14)
O3 C19 C18 C10 112.59(17)
C20 C19 C18 C10 -66.31(18)
C16 C10 C18 C19 -37.51(18)
C11 C10 C18 C19 80.73(17)
C2 C10 C18 C19 -158.27(13)
C16 C10 C18 C26 87.55(15)
C11 C10 C18 C26 -154.20(13)
C2 C10 C18 C26 -33.20(15)
C3 N2 C9 C4 177.09(16)
C3 N2 C9 C8 -2.80(18)
C7 C8 C9 C4 0.0(2)
C2 C8 C9 C4 -178.79(14)
C7 C8 C9 N2 179.91(13)
C2 C8 C9 N2 1.10(16)
C1 N1 C2 C8 62.32(19)
C26 N1 C2 C8 -169.42(13)
C1 N1 C2 C10 -171.65(14)
C26 N1 C2 C10 -43.39(14)
C1 N1 C2 C3 -53.49(19)
C26 N1 C2 C3 74.76(15)
C7 C8 C2 N1 60.9(2)
C9 C8 C2 N1 -120.49(13)
C7 C8 C2 C10 -56.3(2)
C9 C8 C2 C10 122.27(14)
C7 C8 C2 C3 -177.89(15)
C9 C8 C2 C3 0.69(14)
C16 C10 C2 N1 -74.52(13)
C11 C10 C2 N1 170.98(11)
C18 C10 C2 N1 46.31(13)
C16 C10 C2 C8 51.65(16)
C11 C10 C2 C8 -62.86(16)
C18 C10 C2 C8 172.47(12)
C16 C10 C2 C3 167.62(11)
C11 C10 C2 C3 53.12(15)
C18 C10 C2 C3 -71.55(14)
O1 C3 C2 N1 -53.9(2)
N2 C3 C2 N1 122.40(14)
O1 C3 C2 C8 -178.62(15)
N2 C3 C2 C8 -2.29(15)
O1 C3 C2 C10 56.7(2)
N2 C3 C2 C10 -126.96(13)
C21 C20 C25 C24 -0.6(2)
C19 C20 C25 C24 179.84(15)
C16 C17 C12 C13 -0.5(2)
N3 C17 C12 C13 178.19(15)
C8 C7 C6 C5 1.7(2)
C25 C20 C21 C22 1.9(3)
C19 C20 C21 C22 -178.47(16)
N2 C9 C4 C5 -179.15(16)
C8 C9 C4 C5 0.7(3)
C20 C21 C22 C23 -1.9(3)
C20 C25 C24 C23 -0.8(3)
C16 C15 C14 C13 -1.8(3)
C25 C24 C23 C22 0.8(3)
C25 C24 C23 Cl1 -179.07(14)
C21 C22 C23 C24 0.5(3)
C21 C22 C23 Cl1 -179.61(15)
C9 C4 C5 C6 -0.3(3)
C7 C6 C5 C4 -0.9(3)
C1 N1 C26 C18 151.80(15)
C2 N1 C26 C18 22.55(17)
C19 C18 C26 N1 131.25(15)
C10 C18 C26 N1 8.02(17)
C15 C14 C13 C12 -0.3(3)
C17 C12 C13 C14 1.5(3)
