#------------------------------------------------------------------------------
#$Date: 2016-02-20 18:35:30 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176787 $
#$URL: svn://www.crystallography.net/cod/cif/2/21/72/2217242.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2217242
loop_
_publ_author_name
'Daszkiewicz, M.'
'Gulay, L. D.'
'Shemet, V. Ya.'
'Pietraszko, A.'
_publ_section_title
;
 Dy₈SnS~13.61~O~0.39~ from single-crystal data
;
_journal_coeditor_code           PK2066
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i2
_journal_page_last               i2
_journal_paper_doi               10.1107/S1600536807063416
_journal_volume                  64
_journal_year                    2008
_chemical_formula_iupac          'Dy8 Sn1 S13.61 O0.39'
_chemical_formula_moiety         'Dy8 O0.39 S13.61 Sn'
_chemical_formula_sum            'Dy8 O0.39 S13.61 Sn'
_chemical_formula_weight         1861.27
_chemical_name_systematic
;
Dysprosium tin sulfide oxide
;
_space_group_IT_number           36
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   3.7822(8)
_cell_length_b                   23.620(5)
_cell_length_c                   21.271(4)
_cell_measurement_reflns_used    1910
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      26.72
_cell_measurement_theta_min      2.58
_cell_volume                     1900.3(7)
_computing_cell_refinement       'CrysAlis RED (Oxford Diffraction, 2007)'
_computing_data_collection       'CrysAlis CCD (Oxford Diffraction, 2007)'
_computing_data_reduction        'CrysAlis RED (Oxford Diffraction, 2007)'
_computing_molecular_graphics    'DIAMOND (Brandenburg, 2005)'
_computing_publication_material
'publCIF (Westrip, 2007) and PLATON (Spek, 2003)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean '1024x1024 with blocks 2x2, 33.133pixel/mm'
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'KUMA KM-4 with CCD area-detector'
_diffrn_measurement_method       ω-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0491
_diffrn_reflns_av_sigmaI/netI    0.0477
_diffrn_reflns_limit_h_max       4
_diffrn_reflns_limit_h_min       -4
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            11655
_diffrn_reflns_theta_full        26.72
_diffrn_reflns_theta_max         26.72
_diffrn_reflns_theta_min         2.58
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    33.798
_exptl_absorpt_correction_T_max  0.716
_exptl_absorpt_correction_T_min  0.104
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   '(CrysAlis; Oxford Diffraction, 2007)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    6.506
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             3196
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.01
_exptl_crystal_size_min          0.01
_refine_diff_density_max         3.045
_refine_diff_density_min         -1.561
_refine_ls_abs_structure_details 'Flack (1983), 1089 Friedel pairs'
_refine_ls_abs_structure_Flack   0.0(2)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.888
_refine_ls_matrix_type           full
_refine_ls_number_parameters     141
_refine_ls_number_reflns         2287
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      0.888
_refine_ls_R_factor_all          0.0349
_refine_ls_R_factor_gt           0.0256
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         <0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0128P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0364
_refine_ls_wR_factor_ref         0.0383
_reflns_number_gt                1910
_reflns_number_total             2287
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            pk2066.cif
_cod_data_source_block           I
_cod_database_code               2217242
_cod_database_fobs_code          2217242
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x, -y, z+1/2'
'-x, y, z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
Dy Dy1 0.0000 0.69122(4) 0.08524(3) 0.0086(2) Uani d S 1
Dy Dy2 0.0000 0.44849(4) 0.24158(5) 0.0242(3) Uani d S 1
Dy Dy3 0.0000 0.10373(4) 0.23391(4) 0.0132(2) Uani d S 1
Dy Dy4 0.0000 0.04543(4) 0.40541(5) 0.0125(2) Uani d S 1
Dy Dy5 0.0000 0.85422(4) 0.07459(5) 0.0106(2) Uani d S 1
Dy Dy6 0.0000 0.27636(4) 0.24724(4) 0.0100(2) Uani d S 1
Dy Dy7 0.0000 0.37415(4) 0.41648(5) 0.0109(2) Uani d S 1
Dy Dy8 0.5000 0.52208(3) 0.07589(4) 0.01244(19) Uani d S 1
Sn Sn1 0.0000 0.70904(6) 0.40908(8) 0.0076(2) Uani d S 1
S S1 0.0000 0.85740(18) 0.2105(2) 0.0088(11) Uani d S 1
S S2 0.5000 0.43628(19) 0.3487(2) 0.0100(10) Uani d S 1
S S3 0.5000 0.7734(2) 0.1121(2) 0.0089(10) Uani d S 1
S S4 0.0000 0.48205(18) 0.4751(2) 0.0086(9) Uani d S 1
S S5 0.0000 0.55462(18) 0.3115(2) 0.0100(10) Uani d S 1
S S6 0.5000 0.63430(18) 0.0139(2) 0.0084(10) Uani d S 1
S S7 0.0000 0.4362(2) 0.1072(2) 0.0121(11) Uani d S 1
S S8 0.0000 0.58602(18) 0.13619(19) 0.0105(9) Uani d S 1
S S9 0.5000 0.7460(2) 0.4772(2) 0.0141(10) Uani d S 1
S S10 0.0000 0.1733(2) 0.3409(2) 0.0169(10) Uani d S 1
S S11 0.0000 0.69522(18) 0.21604(19) 0.0079(9) Uani d S 1
S S12 0.0000 0.6207(2) 0.4722(2) 0.0112(10) Uani d S 1
S S13 0.0000 0.80025(18) 0.3496(2) 0.0096(9) Uani d S 1
O O14 0.0000 0.0010(3) 0.2040(4) 0.034(3) Uani d SP 0.39(4)
S S14 0.0000 0.0010(3) 0.2040(4) 0.034(3) Uani d SP 0.61(4)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
S8 Dy1 S9 . 6_564 146.41(14)
S8 Dy1 S3 . . 124.06(10)
S9 Dy1 S3 6_564 . 78.05(13)
S8 Dy1 S3 . 1_455 124.06(10)
S9 Dy1 S3 6_564 1_455 78.05(13)
S3 Dy1 S3 . 1_455 86.14(13)
S8 Dy1 S6 . 1_455 76.95(11)
S9 Dy1 S6 6_564 1_455 78.66(12)
S3 Dy1 S6 . 1_455 156.70(14)
S3 Dy1 S6 1_455 1_455 89.24(10)
S8 Dy1 S6 . . 76.95(11)
S9 Dy1 S6 6_564 . 78.66(12)
S3 Dy1 S6 . . 89.24(10)
S3 Dy1 S6 1_455 . 156.70(14)
S6 Dy1 S6 1_455 . 86.02(13)
S8 Dy1 S11 . . 68.38(12)
S9 Dy1 S11 6_564 . 145.21(13)
S3 Dy1 S11 . . 76.72(12)
S3 Dy1 S11 1_455 . 76.72(12)
S6 Dy1 S11 1_455 . 124.29(10)
S6 Dy1 S11 . . 124.29(10)
S8 Dy1 Dy1 . 1_455 90.0
S9 Dy1 Dy1 6_564 1_455 90.0
S3 Dy1 Dy1 . 1_455 133.07(7)
S3 Dy1 Dy1 1_455 1_455 46.93(7)
S6 Dy1 Dy1 1_455 1_455 46.99(6)
S6 Dy1 Dy1 . 1_455 133.01(6)
S11 Dy1 Dy1 . 1_455 90.0
S8 Dy1 Dy1 . 1_655 90.0
S9 Dy1 Dy1 6_564 1_655 90.0
S3 Dy1 Dy1 . 1_655 46.93(7)
S3 Dy1 Dy1 1_455 1_655 133.07(7)
S6 Dy1 Dy1 1_455 1_655 133.01(6)
S6 Dy1 Dy1 . 1_655 46.99(6)
S11 Dy1 Dy1 . 1_655 90.0
Dy1 Dy1 Dy1 1_455 1_655 180.00(5)
S8 Dy1 Dy5 . . 159.81(9)
S9 Dy1 Dy5 6_564 . 53.78(10)
S3 Dy1 Dy5 . . 46.56(8)
S3 Dy1 Dy5 1_455 . 46.56(8)
S6 Dy1 Dy5 1_455 . 116.87(9)
S6 Dy1 Dy5 . . 116.87(9)
S11 Dy1 Dy5 . . 91.43(9)
Dy1 Dy1 Dy5 1_455 . 90.0
Dy1 Dy1 Dy5 1_655 . 90.0
S8 Dy1 Dy7 . 2_564 90.29(9)
S9 Dy1 Dy7 6_564 2_564 56.12(10)
S3 Dy1 Dy7 . 2_564 117.79(10)
S3 Dy1 Dy7 1_455 2_564 117.79(10)
S6 Dy1 Dy7 1_455 2_564 46.02(7)
S6 Dy1 Dy7 . 2_564 46.02(7)
S11 Dy1 Dy7 . 2_564 158.67(9)
Dy1 Dy1 Dy7 1_455 2_564 90.0
Dy1 Dy1 Dy7 1_655 2_564 90.0
Dy5 Dy1 Dy7 . 2_564 109.91(3)
S14 Dy2 O14 5 5 0.0(5)
S14 Dy2 S14 5 5_455 104.1(3)
O14 Dy2 S14 5 5_455 104.1(3)
S14 Dy2 O14 5 5_455 104.1(3)
O14 Dy2 O14 5 5_455 104.1(3)
S14 Dy2 O14 5_455 5_455 0.0(4)
S14 Dy2 S7 5 . 73.79(19)
O14 Dy2 S7 5 . 73.79(19)
S14 Dy2 S7 5_455 . 73.79(19)
O14 Dy2 S7 5_455 . 73.79(19)
S14 Dy2 S5 5 . 74.03(17)
O14 Dy2 S5 5 . 74.03(17)
S14 Dy2 S5 5_455 . 74.03(17)
O14 Dy2 S5 5_455 . 74.03(17)
S7 Dy2 S5 . . 126.46(14)
S14 Dy2 S1 5 5_445 144.2(2)
O14 Dy2 S1 5 5_445 144.2(2)
S14 Dy2 S1 5_455 5_445 78.26(16)
O14 Dy2 S1 5_455 5_445 78.26(16)
S7 Dy2 S1 . 5_445 72.68(12)
S5 Dy2 S1 . 5_445 138.10(7)
S14 Dy2 S1 5 5_545 78.26(16)
O14 Dy2 S1 5 5_545 78.26(16)
S14 Dy2 S1 5_455 5_545 144.2(2)
O14 Dy2 S1 5_455 5_545 144.2(2)
S7 Dy2 S1 . 5_545 72.68(12)
S5 Dy2 S1 . 5_545 138.10(7)
S1 Dy2 S1 5_445 5_545 80.07(11)
S14 Dy2 S2 5 . 78.71(18)
O14 Dy2 S2 5 . 78.71(18)
S14 Dy2 S2 5_455 . 143.7(2)
O14 Dy2 S2 5_455 . 143.7(2)
S7 Dy2 S2 . . 138.79(7)
S5 Dy2 S2 . . 72.10(11)
S1 Dy2 S2 5_445 . 120.68(12)
S1 Dy2 S2 5_545 . 72.10(11)
S14 Dy2 S2 5 1_455 143.7(2)
O14 Dy2 S2 5 1_455 143.7(2)
S14 Dy2 S2 5_455 1_455 78.71(18)
O14 Dy2 S2 5_455 1_455 78.71(18)
S7 Dy2 S2 . 1_455 138.79(7)
S5 Dy2 S2 . 1_455 72.10(11)
S1 Dy2 S2 5_445 1_455 72.10(11)
S1 Dy2 S2 5_545 1_455 120.68(12)
S2 Dy2 S2 . 1_455 78.91(12)
S14 Dy2 Dy2 5 1_455 142.03(14)
O14 Dy2 Dy2 5 1_455 142.03(14)
S14 Dy2 Dy2 5_455 1_455 37.97(14)
O14 Dy2 Dy2 5_455 1_455 37.97(14)
S7 Dy2 Dy2 . 1_455 90.0
S5 Dy2 Dy2 . 1_455 90.0
S1 Dy2 Dy2 5_445 1_455 49.97(6)
S1 Dy2 Dy2 5_545 1_455 130.03(6)
S2 Dy2 Dy2 . 1_455 129.46(6)
S2 Dy2 Dy2 1_455 1_455 50.54(6)
S14 Dy2 Dy2 5 1_655 37.97(14)
O14 Dy2 Dy2 5 1_655 37.97(14)
S14 Dy2 Dy2 5_455 1_655 142.03(14)
O14 Dy2 Dy2 5_455 1_655 142.03(14)
S7 Dy2 Dy2 . 1_655 90.0
S5 Dy2 Dy2 . 1_655 90.0
S1 Dy2 Dy2 5_445 1_655 130.03(6)
S1 Dy2 Dy2 5_545 1_655 49.97(6)
S2 Dy2 Dy2 . 1_655 50.54(6)
S2 Dy2 Dy2 1_455 1_655 129.46(6)
Dy2 Dy2 Dy2 1_455 1_655 180.00(6)
O14 Dy3 S5 . 5_545 75.25(16)
O14 Dy3 S5 . 5_445 75.25(16)
S5 Dy3 S5 5_545 5_445 86.32(13)
O14 Dy3 S10 . . 140.5(2)
S5 Dy3 S10 5_545 . 76.23(12)
S5 Dy3 S10 5_445 . 76.23(12)
O14 Dy3 S8 . 5_445 70.86(16)
S5 Dy3 S8 5_545 5_445 146.11(13)
S5 Dy3 S8 5_445 5_445 85.38(10)
S10 Dy3 S8 . 5_445 132.79(8)
O14 Dy3 S8 . 5_545 70.86(16)
S5 Dy3 S8 5_545 5_545 85.38(10)
S5 Dy3 S8 5_445 5_545 146.11(13)
S10 Dy3 S8 . 5_545 132.79(8)
S8 Dy3 S8 5_445 5_545 83.46(11)
O14 Dy3 S11 . 5_545 133.50(11)
S5 Dy3 S11 5_545 5_545 86.83(9)
S5 Dy3 S11 5_445 5_545 146.92(13)
S10 Dy3 S11 . 5_545 70.70(11)
S8 Dy3 S11 5_445 5_545 116.65(11)
S8 Dy3 S11 5_545 5_545 65.12(11)
O14 Dy3 S11 . 5_445 133.50(11)
S5 Dy3 S11 5_545 5_445 146.92(13)
S5 Dy3 S11 5_445 5_445 86.83(9)
S10 Dy3 S11 . 5_445 70.70(11)
S8 Dy3 S11 5_445 5_445 65.12(11)
S8 Dy3 S11 5_545 5_445 116.65(11)
S11 Dy3 S11 5_545 5_445 81.52(11)
O14 Dy3 Dy3 . 1_455 90.0
S5 Dy3 Dy3 5_545 1_455 133.16(6)
S5 Dy3 Dy3 5_445 1_455 46.84(6)
S10 Dy3 Dy3 . 1_455 90.0
S8 Dy3 Dy3 5_445 1_455 48.27(6)
S8 Dy3 Dy3 5_545 1_455 131.73(6)
S11 Dy3 Dy3 5_545 1_455 130.76(5)
S11 Dy3 Dy3 5_445 1_455 49.24(5)
O14 Dy3 Dy3 . 1_655 90.0
S5 Dy3 Dy3 5_545 1_655 46.84(6)
S5 Dy3 Dy3 5_445 1_655 133.16(6)
S10 Dy3 Dy3 . 1_655 90.0
S8 Dy3 Dy3 5_445 1_655 131.73(6)
S8 Dy3 Dy3 5_545 1_655 48.27(6)
S11 Dy3 Dy3 5_545 1_655 49.24(5)
S11 Dy3 Dy3 5_445 1_655 130.76(5)
Dy3 Dy3 Dy3 1_455 1_655 180.00(3)
O14 Dy3 Dy8 . 5_445 45.47(18)
S5 Dy3 Dy8 5_545 5_445 107.98(9)
S5 Dy3 Dy8 5_445 5_445 107.98(9)
S10 Dy3 Dy8 . 5_445 174.01(11)
S8 Dy3 Dy8 5_445 5_445 44.94(7)
S8 Dy3 Dy8 5_545 5_445 44.94(7)
S11 Dy3 Dy8 5_545 5_445 104.92(9)
S11 Dy3 Dy8 5_445 5_445 104.92(8)
Dy3 Dy3 Dy8 1_455 5_445 90.0
Dy3 Dy3 Dy8 1_655 5_445 90.0
S5 Dy4 S5 5_445 5_545 86.51(13)
S5 Dy4 S4 5_445 5_545 151.45(13)
S5 Dy4 S4 5_545 5_545 87.87(10)
S5 Dy4 S4 5_445 5_445 87.87(10)
S5 Dy4 S4 5_545 5_445 151.45(13)
S4 Dy4 S4 5_545 5_445 83.83(12)
S5 Dy4 S2 5_445 5_445 76.38(11)
S5 Dy4 S2 5_545 5_445 76.38(11)
S4 Dy4 S2 5_545 5_445 75.09(11)
S4 Dy4 S2 5_445 5_445 75.09(11)
S5 Dy4 S12 5_445 5_545 137.58(12)
S5 Dy4 S12 5_545 5_545 82.10(11)
S4 Dy4 S12 5_545 5_545 68.88(12)
S4 Dy4 S12 5_445 5_545 119.56(13)
S2 Dy4 S12 5_445 5_545 138.40(7)
S5 Dy4 S12 5_445 5_445 82.10(11)
S5 Dy4 S12 5_545 5_445 137.58(12)
S4 Dy4 S12 5_545 5_445 119.56(13)
S4 Dy4 S12 5_445 5_445 68.88(12)
S2 Dy4 S12 5_445 5_445 138.40(7)
S12 Dy4 S12 5_545 5_445 79.43(12)
S5 Dy4 Dy4 5_445 1_655 133.25(7)
S5 Dy4 Dy4 5_545 1_655 46.75(7)
S4 Dy4 Dy4 5_545 1_655 48.09(6)
S4 Dy4 Dy4 5_445 1_655 131.91(6)
S2 Dy4 Dy4 5_445 1_655 90.0
S12 Dy4 Dy4 5_545 1_655 50.28(6)
S12 Dy4 Dy4 5_445 1_655 129.72(6)
S5 Dy4 Dy4 5_445 1_455 46.75(7)
S5 Dy4 Dy4 5_545 1_455 133.25(7)
S4 Dy4 Dy4 5_545 1_455 131.91(6)
S4 Dy4 Dy4 5_445 1_455 48.09(6)
S2 Dy4 Dy4 5_445 1_455 90.0
S12 Dy4 Dy4 5_545 1_455 129.72(6)
S12 Dy4 Dy4 5_445 1_455 50.28(6)
Dy4 Dy4 Dy4 1_655 1_455 180.00(5)
S5 Dy4 Dy3 5_445 . 45.15(7)
S5 Dy4 Dy3 5_545 . 45.15(7)
S4 Dy4 Dy3 5_545 . 132.57(7)
S4 Dy4 Dy3 5_445 . 132.57(7)
S2 Dy4 Dy3 5_445 . 85.62(10)
S12 Dy4 Dy3 5_545 . 103.71(10)
S12 Dy4 Dy3 5_445 . 103.71(10)
Dy4 Dy4 Dy3 1_655 . 90.0
Dy4 Dy4 Dy3 1_455 . 90.0
S5 Dy4 Dy8 5_445 6 133.99(7)
S5 Dy4 Dy8 5_545 6 133.99(7)
S4 Dy4 Dy8 5_545 6 46.20(7)
S4 Dy4 Dy8 5_445 6 46.20(7)
S2 Dy4 Dy8 5_445 6 91.32(10)
S12 Dy4 Dy8 5_545 6 78.60(10)
S12 Dy4 Dy8 5_445 6 78.60(10)
Dy4 Dy4 Dy8 1_655 6 90.0
Dy4 Dy4 Dy8 1_455 6 90.0
Dy3 Dy4 Dy8 . 6 176.94(3)
S7 Dy5 S7 5 5_455 85.19(13)
S7 Dy5 S3 5 . 86.84(11)
S7 Dy5 S3 5_455 . 149.10(16)
S7 Dy5 S3 5 1_455 149.10(16)
S7 Dy5 S3 5_455 1_455 86.84(11)
S3 Dy5 S3 . 1_455 84.86(13)
S7 Dy5 S1 5 . 74.57(12)
S7 Dy5 S1 5_455 . 74.57(12)
S3 Dy5 S1 . . 74.54(12)
S3 Dy5 S1 1_455 . 74.54(12)
S7 Dy5 S12 5 6_464 118.62(13)
S7 Dy5 S12 5_455 6_464 67.02(12)
S3 Dy5 S12 . 6_464 141.31(14)
S3 Dy5 S12 1_455 6_464 85.06(11)
S1 Dy5 S12 . 6_464 137.24(8)
S7 Dy5 S12 5 6_564 67.02(12)
S7 Dy5 S12 5_455 6_564 118.62(13)
S3 Dy5 S12 . 6_564 85.06(11)
S3 Dy5 S12 1_455 6_564 141.31(14)
S1 Dy5 S12 . 6_564 137.24(8)
S12 Dy5 S12 6_464 6_564 79.93(13)
S7 Dy5 S9 5 6_564 133.23(9)
S7 Dy5 S9 5_455 6_564 133.23(9)
S3 Dy5 S9 . 6_564 71.02(11)
S3 Dy5 S9 1_455 6_564 71.02(11)
S1 Dy5 S9 . 6_564 132.68(13)
S12 Dy5 S9 6_464 6_564 70.38(11)
S12 Dy5 S9 6_564 6_564 70.38(11)
S7 Dy5 Dy5 5 1_455 132.60(7)
S7 Dy5 Dy5 5_455 1_455 47.40(7)
S3 Dy5 Dy5 . 1_455 132.43(7)
S3 Dy5 Dy5 1_455 1_455 47.57(7)
S1 Dy5 Dy5 . 1_455 90.0
S12 Dy5 Dy5 6_464 1_455 50.03(6)
S12 Dy5 Dy5 6_564 1_455 129.97(6)
S9 Dy5 Dy5 6_564 1_455 90.0
S7 Dy5 Dy5 5 1_655 47.40(7)
S7 Dy5 Dy5 5_455 1_655 132.60(7)
S3 Dy5 Dy5 . 1_655 47.57(7)
S3 Dy5 Dy5 1_455 1_655 132.43(7)
S1 Dy5 Dy5 . 1_655 90.0
S12 Dy5 Dy5 6_464 1_655 129.97(6)
S12 Dy5 Dy5 6_564 1_655 50.03(6)
S9 Dy5 Dy5 6_564 1_655 90.0
Dy5 Dy5 Dy5 1_455 1_655 180.0
S7 Dy5 Dy1 5 . 132.63(8)
S7 Dy5 Dy1 5_455 . 132.63(8)
S3 Dy5 Dy1 . . 45.84(7)
S3 Dy5 Dy1 1_455 . 45.84(7)
S1 Dy5 Dy1 . . 88.12(9)
S12 Dy5 Dy1 6_464 . 104.13(10)
S12 Dy5 Dy1 6_564 . 104.13(10)
S9 Dy5 Dy1 6_564 . 44.56(9)
Dy5 Dy5 Dy1 1_455 . 90.0
Dy5 Dy5 Dy1 1_655 . 90.0
S7 Dy5 Dy8 5 5_455 45.99(8)
S7 Dy5 Dy8 5_455 5_455 45.99(8)
S3 Dy5 Dy8 . 5_455 132.78(8)
S3 Dy5 Dy8 1_455 5_455 132.78(8)
S1 Dy5 Dy8 . 5_455 88.11(9)
S12 Dy5 Dy8 6_464 5_455 78.71(9)
S12 Dy5 Dy8 6_564 5_455 78.71(9)
S9 Dy5 Dy8 6_564 5_455 139.21(9)
Dy5 Dy5 Dy8 1_455 5_455 90.0
Dy5 Dy5 Dy8 1_655 5_455 90.0
Dy1 Dy5 Dy8 . 5_455 176.23(4)
S11 Dy6 S11 5_445 5_545 85.99(12)
S11 Dy6 S1 5_445 5_545 149.95(14)
S11 Dy6 S1 5_545 5_545 86.85(10)
S11 Dy6 S1 5_445 5_445 86.85(9)
S11 Dy6 S1 5_545 5_445 149.95(14)
S1 Dy6 S1 5_545 5_445 84.89(12)
S11 Dy6 S3 5_445 5_445 75.16(11)
S11 Dy6 S3 5_545 5_445 75.16(11)
S1 Dy6 S3 5_545 5_445 74.79(12)
S1 Dy6 S3 5_445 5_445 74.79(12)
S11 Dy6 S13 5_445 5_545 138.49(12)
S11 Dy6 S13 5_545 5_545 82.60(10)
S1 Dy6 S13 5_545 5_545 68.99(11)
S1 Dy6 S13 5_445 5_545 120.66(12)
S3 Dy6 S13 5_445 5_545 138.20(6)
S11 Dy6 S13 5_445 5_445 82.60(10)
S11 Dy6 S13 5_545 5_445 138.49(12)
S1 Dy6 S13 5_545 5_445 120.66(12)
S1 Dy6 S13 5_445 5_445 68.99(11)
S3 Dy6 S13 5_445 5_445 138.20(6)
S13 Dy6 S13 5_545 5_445 80.09(11)
S11 Dy6 S10 5_445 . 67.46(10)
S11 Dy6 S10 5_545 . 67.46(10)
S1 Dy6 S10 5_545 . 134.86(8)
S1 Dy6 S10 5_445 . 134.86(8)
S3 Dy6 S10 5_445 . 127.89(13)
S13 Dy6 S10 5_545 . 71.30(10)
S13 Dy6 S10 5_445 . 71.30(10)
S11 Dy6 Dy6 5_445 1_655 133.00(6)
S11 Dy6 Dy6 5_545 1_655 47.00(6)
S1 Dy6 Dy6 5_545 1_655 47.55(6)
S1 Dy6 Dy6 5_445 1_655 132.45(6)
S3 Dy6 Dy6 5_445 1_655 90.0
S13 Dy6 Dy6 5_545 1_655 49.95(5)
S13 Dy6 Dy6 5_445 1_655 130.05(5)
S10 Dy6 Dy6 . 1_655 90.0
S11 Dy6 Dy6 5_445 1_455 47.00(6)
S11 Dy6 Dy6 5_545 1_455 133.00(6)
S1 Dy6 Dy6 5_545 1_455 132.45(6)
S1 Dy6 Dy6 5_445 1_455 47.55(6)
S3 Dy6 Dy6 5_445 1_455 90.0
S13 Dy6 Dy6 5_545 1_455 130.05(5)
S13 Dy6 Dy6 5_445 1_455 49.95(5)
S10 Dy6 Dy6 . 1_455 90.0
Dy6 Dy6 Dy6 1_655 1_455 180.00(5)
S2 Dy7 S2 . 1_455 85.20(14)
S2 Dy7 S6 . 2_665 87.83(11)
S2 Dy7 S6 1_455 2_665 150.73(13)
S2 Dy7 S6 . 2_565 150.73(13)
S2 Dy7 S6 1_455 2_565 87.83(11)
S6 Dy7 S6 2_665 2_565 84.49(13)
S2 Dy7 S4 . . 75.80(11)
S2 Dy7 S4 1_455 . 75.80(11)
S6 Dy7 S4 2_665 . 74.93(11)
S6 Dy7 S4 2_565 . 74.93(11)
S2 Dy7 S13 . 5_445 119.86(13)
S2 Dy7 S13 1_455 5_445 68.11(12)
S6 Dy7 S13 2_665 5_445 138.30(12)
S6 Dy7 S13 2_565 5_445 83.21(10)
S4 Dy7 S13 . 5_445 138.23(6)
S2 Dy7 S13 . 5_545 68.11(12)
S2 Dy7 S13 1_455 5_545 119.86(13)
S6 Dy7 S13 2_665 5_545 83.21(10)
S6 Dy7 S13 2_565 5_545 138.30(12)
S4 Dy7 S13 . 5_545 138.23(6)
S13 Dy7 S13 5_445 5_545 80.06(11)
S2 Dy7 Dy7 . 1_455 132.60(7)
S2 Dy7 Dy7 1_455 1_455 47.40(7)
S6 Dy7 Dy7 2_665 1_455 132.25(6)
S6 Dy7 Dy7 2_565 1_455 47.75(6)
S4 Dy7 Dy7 . 1_455 90.0
S13 Dy7 Dy7 5_445 1_455 49.97(6)
S13 Dy7 Dy7 5_545 1_455 130.03(6)
S2 Dy7 Dy7 . 1_655 47.40(7)
S2 Dy7 Dy7 1_455 1_655 132.60(7)
S6 Dy7 Dy7 2_665 1_655 47.75(6)
S6 Dy7 Dy7 2_565 1_655 132.25(6)
S4 Dy7 Dy7 . 1_655 90.0
S13 Dy7 Dy7 5_445 1_655 130.03(6)
S13 Dy7 Dy7 5_545 1_655 49.97(6)
Dy7 Dy7 Dy7 1_455 1_655 180.00(8)
S2 Dy7 Dy1 . 2_565 132.94(8)
S2 Dy7 Dy1 1_455 2_565 132.94(8)
S6 Dy7 Dy1 2_665 2_565 45.18(7)
S6 Dy7 Dy1 2_565 2_565 45.18(7)
S4 Dy7 Dy1 . 2_565 87.21(9)
S13 Dy7 Dy1 5_445 2_565 102.10(8)
S13 Dy7 Dy1 5_545 2_565 102.10(8)
Dy7 Dy7 Dy1 1_455 2_565 90.0
Dy7 Dy7 Dy1 1_655 2_565 90.0
S8 Dy8 S8 1_655 . 87.33(13)
S8 Dy8 S14 1_655 5 68.79(14)
S8 Dy8 S14 . 5 68.79(14)
S8 Dy8 O14 1_655 5 68.79(14)
S8 Dy8 O14 . 5 68.79(14)
S14 Dy8 O14 5 5 0.0(3)
S8 Dy8 S7 1_655 . 137.78(12)
S8 Dy8 S7 . . 79.92(11)
S14 Dy8 S7 5 . 69.06(15)
O14 Dy8 S7 5 . 69.06(15)
S8 Dy8 S7 1_655 1_655 79.92(11)
S8 Dy8 S7 . 1_655 137.78(12)
S14 Dy8 S7 5 1_655 69.06(15)
O14 Dy8 S7 5 1_655 69.06(15)
S7 Dy8 S7 . 1_655 83.07(13)
S8 Dy8 S4 1_655 2_564 145.71(13)
S8 Dy8 S4 . 2_564 85.03(10)
S14 Dy8 S4 5 2_564 136.99(8)
O14 Dy8 S4 5 2_564 136.99(8)
S7 Dy8 S4 . 2_564 73.29(12)
S7 Dy8 S4 1_655 2_564 126.09(13)
S8 Dy8 S4 1_655 2_664 85.03(10)
S8 Dy8 S4 . 2_664 145.71(13)
S14 Dy8 S4 5 2_664 136.99(8)
O14 Dy8 S4 5 2_664 136.99(8)
S7 Dy8 S4 . 2_664 126.09(13)
S7 Dy8 S4 1_655 2_664 73.29(12)
S4 Dy8 S4 2_564 2_664 82.77(12)
S8 Dy8 S6 1_655 . 73.43(10)
S8 Dy8 S6 . . 73.43(10)
S14 Dy8 S6 5 . 126.78(17)
O14 Dy8 S6 5 . 126.78(17)
S7 Dy8 S6 . . 137.80(7)
S7 Dy8 S6 1_655 . 137.80(7)
S4 Dy8 S6 2_564 . 72.35(11)
S4 Dy8 S6 2_664 . 72.35(11)
S8 Dy8 Dy8 1_655 1_455 133.66(6)
S8 Dy8 Dy8 . 1_455 46.34(6)
S14 Dy8 Dy8 5 1_455 90.0
O14 Dy8 Dy8 5 1_455 90.0
S7 Dy8 Dy8 . 1_455 48.47(7)
S7 Dy8 Dy8 1_655 1_455 131.53(7)
S4 Dy8 Dy8 2_564 1_455 48.62(6)
S4 Dy8 Dy8 2_664 1_455 131.38(6)
S6 Dy8 Dy8 . 1_455 90.0
S8 Dy8 Dy8 1_655 1_655 46.34(6)
S8 Dy8 Dy8 . 1_655 133.66(6)
S14 Dy8 Dy8 5 1_655 90.0
O14 Dy8 Dy8 5 1_655 90.0
S7 Dy8 Dy8 . 1_655 131.53(7)
S7 Dy8 Dy8 1_655 1_655 48.47(7)
S4 Dy8 Dy8 2_564 1_655 131.38(6)
S4 Dy8 Dy8 2_664 1_655 48.62(6)
S6 Dy8 Dy8 . 1_655 90.0
Dy8 Dy8 Dy8 1_455 1_655 180.0
S8 Dy8 Dy3 1_655 5 47.11(7)
S8 Dy8 Dy3 . 5 47.11(7)
S14 Dy8 Dy3 5 5 40.19(15)
O14 Dy8 Dy3 5 5 40.19(15)
S7 Dy8 Dy3 . 5 98.71(10)
S7 Dy8 Dy3 1_655 5 98.71(10)
S4 Dy8 Dy3 2_564 5 131.84(7)
S4 Dy8 Dy3 2_664 5 131.84(7)
S6 Dy8 Dy3 . 5 86.59(9)
Dy8 Dy8 Dy3 1_455 5 90.0
Dy8 Dy8 Dy3 1_655 5 90.0
S12 Sn1 S13 . . 177.64(19)
S12 Sn1 S10 . 5_455 91.72(15)
S13 Sn1 S10 . 5_455 89.85(14)
S12 Sn1 S10 . 5 91.72(15)
S13 Sn1 S10 . 5 89.85(14)
S10 Sn1 S10 5_455 5 96.82(16)
S12 Sn1 S9 . . 88.85(14)
S13 Sn1 S9 . . 89.58(14)
S10 Sn1 S9 5_455 . 179.39(19)
S10 Sn1 S9 5 . 83.40(8)
S12 Sn1 S9 . 1_455 88.85(14)
S13 Sn1 S9 . 1_455 89.58(13)
S10 Sn1 S9 5_455 1_455 83.40(8)
S10 Sn1 S9 5 1_455 179.39(19)
S9 Sn1 S9 . 1_455 96.38(16)
Dy6 S1 Dy6 5_455 5 84.89(12)
Dy6 S1 Dy5 5_455 . 105.14(12)
Dy6 S1 Dy5 5 . 105.14(12)
Dy6 S1 Dy2 5_455 5 150.61(19)
Dy6 S1 Dy2 5 5 90.17(6)
Dy5 S1 Dy2 . 5 104.12(12)
Dy6 S1 Dy2 5_455 5_455 90.17(6)
Dy6 S1 Dy2 5 5_455 150.61(19)
Dy5 S1 Dy2 . 5_455 104.12(12)
Dy2 S1 Dy2 5 5_455 80.07(11)
Dy7 S2 Dy7 . 1_655 85.20(14)
Dy7 S2 Dy4 . 5 104.92(13)
Dy7 S2 Dy4 1_655 5 104.92(13)
Dy7 S2 Dy2 . . 90.90(5)
Dy7 S2 Dy2 1_655 . 151.17(18)
Dy4 S2 Dy2 5 . 103.69(13)
Dy7 S2 Dy2 . 1_655 151.17(18)
Dy7 S2 Dy2 1_655 1_655 90.90(5)
Dy4 S2 Dy2 5 1_655 103.69(13)
Dy2 S2 Dy2 . 1_655 78.91(12)
Dy1 S3 Dy1 . 1_655 86.14(13)
Dy1 S3 Dy5 . 1_655 151.58(19)
Dy1 S3 Dy5 1_655 1_655 87.60(5)
Dy1 S3 Dy5 . . 87.60(5)
Dy1 S3 Dy5 1_655 . 151.58(19)
Dy5 S3 Dy5 1_655 . 84.86(13)
Dy1 S3 Dy6 . 5 102.89(13)
Dy1 S3 Dy6 1_655 5 102.89(13)
Dy5 S3 Dy6 1_655 5 105.53(13)
Dy5 S3 Dy6 . 5 105.53(13)
Dy4 S4 Dy4 5 5_455 83.83(12)
Dy4 S4 Dy7 5 . 104.18(12)
Dy4 S4 Dy7 5_455 . 104.18(12)
Dy4 S4 Dy8 5 2_665 88.21(5)
Dy4 S4 Dy8 5_455 2_665 148.43(17)
Dy7 S4 Dy8 . 2_665 107.38(12)
Dy4 S4 Dy8 5 2_565 148.43(17)
Dy4 S4 Dy8 5_455 2_565 88.21(5)
Dy7 S4 Dy8 . 2_565 107.38(12)
Dy8 S4 Dy8 2_665 2_565 82.77(12)
Dy4 S5 Dy4 5 5_455 86.51(13)
Dy4 S5 Dy3 5 5_455 159.03(18)
Dy4 S5 Dy3 5_455 5_455 89.79(4)
Dy4 S5 Dy3 5 5 89.79(4)
Dy4 S5 Dy3 5_455 5 159.03(18)
Dy3 S5 Dy3 5_455 5 86.32(13)
Dy4 S5 Dy2 5 . 107.56(12)
Dy4 S5 Dy2 5_455 . 107.56(12)
Dy3 S5 Dy2 5_455 . 93.24(12)
Dy3 S5 Dy2 5 . 93.24(12)
Dy1 S6 Dy1 1_655 . 86.02(13)
Dy1 S6 Dy7 1_655 2_564 153.67(17)
Dy1 S6 Dy7 . 2_564 88.80(5)
Dy1 S6 Dy7 1_655 2_664 88.80(5)
Dy1 S6 Dy7 . 2_664 153.67(17)
Dy7 S6 Dy7 2_564 2_664 84.49(13)
Dy1 S6 Dy8 1_655 . 100.99(12)
Dy1 S6 Dy8 . . 100.99(12)
Dy7 S6 Dy8 2_564 . 105.34(11)
Dy7 S6 Dy8 2_664 . 105.34(11)
Dy5 S7 Dy5 5_445 5_545 85.19(13)
Dy5 S7 Dy8 5_445 1_455 89.21(5)
Dy5 S7 Dy8 5_545 1_455 152.1(2)
Dy5 S7 Dy8 5_445 . 152.1(2)
Dy5 S7 Dy8 5_545 . 89.21(5)
Dy8 S7 Dy8 1_455 . 83.07(13)
Dy5 S7 Dy2 5_445 . 108.48(14)
Dy5 S7 Dy2 5_545 . 108.48(14)
Dy8 S7 Dy2 1_455 . 99.23(13)
Dy8 S7 Dy2 . . 99.23(13)
Dy1 S8 Dy8 . 1_455 108.55(12)
Dy1 S8 Dy8 . . 108.55(12)
Dy8 S8 Dy8 1_455 . 87.33(13)
Dy1 S8 Dy3 . 5 99.06(12)
Dy8 S8 Dy3 1_455 5 152.05(17)
Dy8 S8 Dy3 . 5 87.95(5)
Dy1 S8 Dy3 . 5_455 99.06(12)
Dy8 S8 Dy3 1_455 5_455 87.95(5)
Dy8 S8 Dy3 . 5_455 152.05(17)
Dy3 S8 Dy3 5 5_455 83.46(11)
Sn1 S9 Sn1 . 1_655 96.38(16)
Sn1 S9 Dy1 . 6_565 131.79(8)
Sn1 S9 Dy1 1_655 6_565 131.79(8)
Sn1 S9 Dy5 . 6_565 96.74(13)
Sn1 S9 Dy5 1_655 6_565 96.74(13)
Dy1 S9 Dy5 6_565 6_565 81.66(13)
Sn1 S10 Sn1 5_545 5_445 96.82(16)
Sn1 S10 Dy3 5_545 . 131.34(8)
Sn1 S10 Dy3 5_445 . 131.34(8)
Sn1 S10 Dy6 5_545 . 96.03(14)
Sn1 S10 Dy6 5_445 . 96.03(14)
Dy3 S10 Dy6 . . 86.55(13)
Dy6 S11 Dy6 5 5_455 85.99(12)
Dy6 S11 Dy1 5 . 105.23(11)
Dy6 S11 Dy1 5_455 . 105.23(11)
Dy6 S11 Dy3 5 5_455 158.35(16)
Dy6 S11 Dy3 5_455 5_455 92.23(4)
Dy1 S11 Dy3 . 5_455 96.07(11)
Dy6 S11 Dy3 5 5 92.23(4)
Dy6 S11 Dy3 5_455 5 158.35(16)
Dy1 S11 Dy3 . 5 96.07(11)
Dy3 S11 Dy3 5_455 5 81.52(11)
Sn1 S12 Dy5 . 6_565 103.38(14)
Sn1 S12 Dy5 . 6_465 103.38(14)
Dy5 S12 Dy5 6_565 6_465 79.93(13)
Sn1 S12 Dy4 . 5_455 104.21(14)
Dy5 S12 Dy4 6_565 5_455 152.42(18)
Dy5 S12 Dy4 6_465 5_455 93.75(5)
Sn1 S12 Dy4 . 5 104.21(14)
Dy5 S12 Dy4 6_565 5 93.75(5)
Dy5 S12 Dy4 6_465 5 152.42(18)
Dy4 S12 Dy4 5_455 5 79.43(12)
Sn1 S13 Dy6 . 5_455 102.09(12)
Sn1 S13 Dy6 . 5 102.09(12)
Dy6 S13 Dy6 5_455 5 80.09(11)
Sn1 S13 Dy7 . 5 105.50(12)
Dy6 S13 Dy7 5_455 5 152.39(16)
Dy6 S13 Dy7 5 5 93.35(5)
Sn1 S13 Dy7 . 5_455 105.50(12)
Dy6 S13 Dy7 5_455 5_455 93.35(5)
Dy6 S13 Dy7 5 5_455 152.39(16)
Dy7 S13 Dy7 5 5_455 80.06(11)
Dy2 O14 Dy2 5_445 5_545 104.1(3)
Dy2 O14 Dy3 5_445 . 114.6(2)
Dy2 O14 Dy3 5_545 . 114.6(2)
Dy2 O14 Dy8 5_445 5_445 114.9(2)
Dy2 O14 Dy8 5_545 5_445 114.9(2)
Dy3 O14 Dy8 . 5_445 94.3(2)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Dy1 S8 . 2.711(4)
Dy1 S9 6_564 2.735(5)
Dy1 S3 . 2.769(3)
Dy1 S3 1_455 2.769(3)
Dy1 S6 1_455 2.772(3)
Dy1 S6 . 2.772(3)
Dy1 S11 . 2.784(4)
Dy1 Dy1 1_455 3.7822(8)
Dy1 Dy1 1_655 3.7822(8)
Dy1 Dy5 . 3.8567(14)
Dy1 Dy7 2_564 3.9078(15)
Dy2 S14 5 2.399(5)
Dy2 O14 5 2.399(5)
Dy2 S14 5_455 2.399(5)
Dy2 O14 5_455 2.399(5)
Dy2 S7 . 2.873(5)
Dy2 S5 . 2.914(5)
Dy2 S1 5_445 2.940(3)
Dy2 S1 5_545 2.940(3)
Dy2 S2 . 2.976(4)
Dy2 S2 1_455 2.976(4)
Dy2 Dy2 1_455 3.7822(8)
Dy2 Dy2 1_655 3.7822(8)
Dy3 O14 . 2.508(7)
Dy3 S5 5_545 2.765(3)
Dy3 S5 5_445 2.765(3)
Dy3 S10 . 2.807(5)
Dy3 S8 5_445 2.841(3)
Dy3 S8 5_545 2.841(3)
Dy3 S11 5_545 2.897(3)
Dy3 S11 5_445 2.897(3)
Dy3 Dy3 1_455 3.7822(8)
Dy3 Dy3 1_655 3.7822(8)
Dy3 Dy8 5_445 3.8753(14)
Dy4 S5 5_445 2.760(3)
Dy4 S5 5_545 2.760(3)
Dy4 S4 5_545 2.831(3)
Dy4 S4 5_445 2.831(3)
Dy4 S2 5_445 2.846(5)
Dy4 S12 5_545 2.960(4)
Dy4 S12 5_445 2.960(4)
Dy4 Dy4 1_655 3.7822(8)
Dy4 Dy4 1_455 3.7822(8)
Dy4 Dy8 6 3.9612(17)
Dy5 S7 5 2.794(4)
Dy5 S7 5_455 2.794(4)
Dy5 S3 . 2.803(4)
Dy5 S3 1_455 2.803(4)
Dy5 S1 . 2.892(5)
Dy5 S12 6_464 2.944(4)
Dy5 S12 6_564 2.944(4)
Dy5 S9 6_564 3.145(5)
Dy5 Dy5 1_455 3.7822(8)
Dy5 Dy5 1_655 3.7822(8)
Dy5 Dy8 5_455 3.9649(15)
Dy6 S11 5_445 2.773(3)
Dy6 S11 5_545 2.773(3)
Dy6 S1 5_545 2.802(3)
Dy6 S1 5_445 2.802(3)
Dy6 S3 5_445 2.876(5)
Dy6 S13 5_545 2.939(3)
Dy6 S13 5_445 2.939(3)
Dy6 S10 . 3.145(5)
Dy6 Dy6 1_655 3.7822(8)
Dy6 Dy6 1_455 3.7822(8)
Dy7 S2 . 2.794(4)
Dy7 S2 1_455 2.794(4)
Dy7 S6 2_665 2.813(3)
Dy7 S6 2_565 2.813(3)
Dy7 S4 . 2.837(5)
Dy7 S13 5_445 2.940(3)
Dy7 S13 5_545 2.940(3)
Dy7 Dy7 1_455 3.7822(8)
Dy7 Dy7 1_655 3.7822(8)
Dy7 Dy1 2_565 3.9078(15)
Dy8 S8 1_655 2.739(3)
Dy8 S8 . 2.739(3)
Dy8 S14 5 2.770(8)
Dy8 O14 5 2.770(8)
Dy8 S7 . 2.852(4)
Dy8 S7 1_655 2.852(4)
Dy8 S4 2_564 2.861(3)
Dy8 S4 2_664 2.861(3)
Dy8 S6 . 2.960(4)
Dy8 Dy8 1_455 3.7822(8)
Dy8 Dy8 1_655 3.7822(8)
Dy8 Dy3 5 3.8753(14)
Sn1 S12 . 2.481(5)
Sn1 S13 . 2.498(5)
Sn1 S10 5_455 2.529(3)
Sn1 S10 5 2.529(3)
Sn1 S9 . 2.537(3)
Sn1 S9 1_455 2.537(3)
S1 Dy6 5_455 2.802(3)
S1 Dy6 5 2.802(3)
S1 Dy2 5 2.940(3)
S1 Dy2 5_455 2.940(3)
S2 Dy7 1_655 2.794(4)
S2 Dy4 5 2.846(5)
S2 Dy2 1_655 2.976(4)
S3 Dy1 1_655 2.769(3)
S3 Dy5 1_655 2.803(4)
S3 Dy6 5 2.876(5)
S4 Dy4 5 2.831(3)
S4 Dy4 5_455 2.831(3)
S4 Dy8 2_665 2.861(3)
S4 Dy8 2_565 2.861(3)
S5 Dy4 5 2.760(3)
S5 Dy4 5_455 2.760(3)
S5 Dy3 5_455 2.765(3)
S5 Dy3 5 2.765(3)
S6 Dy1 1_655 2.772(3)
S6 Dy7 2_564 2.813(3)
S6 Dy7 2_664 2.813(3)
S7 Dy5 5_445 2.794(4)
S7 Dy5 5_545 2.794(4)
S7 Dy8 1_455 2.852(4)
S8 Dy8 1_455 2.739(3)
S8 Dy3 5 2.841(3)
S8 Dy3 5_455 2.841(3)
S9 Sn1 1_655 2.537(3)
S9 Dy1 6_565 2.735(5)
S9 Dy5 6_565 3.145(5)
S10 Sn1 5_545 2.529(3)
S10 Sn1 5_445 2.529(3)
S11 Dy6 5 2.773(3)
S11 Dy6 5_455 2.773(3)
S11 Dy3 5_455 2.897(3)
S11 Dy3 5 2.897(3)
S12 Dy5 6_565 2.944(4)
S12 Dy5 6_465 2.944(4)
S12 Dy4 5_455 2.960(4)
S12 Dy4 5 2.960(4)
S13 Dy6 5_455 2.939(3)
S13 Dy6 5 2.939(3)
S13 Dy7 5 2.940(3)
S13 Dy7 5_455 2.940(3)
O14 Dy2 5_445 2.399(5)
O14 Dy2 5_545 2.399(5)
O14 Dy8 5_445 2.770(8)
