#------------------------------------------------------------------------------
#$Date: 2016-02-20 22:30:07 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176789 $
#$URL: svn://www.crystallography.net/cod/cif/2/22/10/2221006.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2221006
loop_
_publ_author_name
'Fazaeli, Yousef'
'Najafi, Ezzatollah'
'Amini, Mostafa M.'
'Ng, Seik Weng'
_publ_section_title
;
 Dichloridobis(5,7-dichloroquinolin-8-olato-κ²N,O)tin(IV)
;
_journal_coeditor_code           BT2866
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m270
_journal_paper_doi               10.1107/S1600536809004371
_journal_volume                  65
_journal_year                    2009
_chemical_formula_iupac          '[Sn (C9 H4 Cl2 N O)2 Cl2]'
_chemical_formula_moiety         'C18 H8 Cl6 N2 O2 Sn'
_chemical_formula_sum            'C18 H8 Cl6 N2 O2 Sn'
_chemical_formula_weight         615.65
_chemical_name_systematic
;
Dichloridobis(5,7-dichloroquinolin-8-olato-κ²N,O)tin(IV)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 110.3810(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   15.2459(2)
_cell_length_b                   8.92620(10)
_cell_length_c                   15.8541(2)
_cell_measurement_reflns_used    9940
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.3
_cell_measurement_theta_min      2.6
_cell_volume                     2022.48(5)
_computing_cell_refinement       'SAINT (Bruker, 2008)'
_computing_data_collection       'APEX2 (Bruker, 2008)'
_computing_data_reduction        'SAINT (Bruker, 2008)'
_computing_molecular_graphics    'X-SEED (Barbour, 2001)'
_computing_publication_material  'publCIF (Westrip, 2009)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker SMART APEX'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0213
_diffrn_reflns_av_sigmaI/netI    0.0193
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            18582
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.42
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.076
_exptl_absorpt_correction_T_max  0.7064
_exptl_absorpt_correction_T_min  0.5941
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 1996)'
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    2.022
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Polyhedron
_exptl_crystal_F_000             1192
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.18
_refine_diff_density_max         0.591
_refine_diff_density_min         -1.250
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.056
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     262
_refine_ls_number_reflns         4651
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.0301
_refine_ls_R_factor_gt           0.0259
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0394P)²+4.6706P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0712
_refine_ls_wR_factor_ref         0.0794
_reflns_number_gt                4218
_reflns_number_total             4651
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            bt2866.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        2022.48(4)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2221006
_cod_database_fobs_code          2221006
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn Sn1 0.778941(13) 0.92337(2) 0.344613(13) 0.01736(7) Uani d . 1 . .
Cl Cl1 0.93987(6) 0.32043(9) 0.64058(5) 0.02934(17) Uani d . 1 . .
Cl Cl2 0.84159(6) 0.38698(8) 0.28352(5) 0.02702(17) Uani d . 1 . .
Cl Cl3 0.34831(5) 1.07293(11) 0.39582(6) 0.0343(2) Uani d . 1 . .
Cl Cl4 0.66222(6) 1.38854(9) 0.45378(7) 0.03409(19) Uani d . 1 . .
Cl Cl5 0.70590(6) 0.98399(10) 0.19137(5) 0.02889(17) Uani d . 1 . .
Cl Cl6 0.92679(6) 1.01709(10) 0.36724(6) 0.03319(19) Uani d . 1 . .
O O1 0.80174(15) 0.7039(2) 0.31888(13) 0.0191(4) Uani d . 1 . .
O O2 0.73412(14) 1.1077(2) 0.39671(15) 0.0205(4) Uani d . 1 . .
N N1 0.83134(16) 0.8252(3) 0.48199(16) 0.0171(5) Uani d . 1 . .
N N2 0.63835(17) 0.8521(3) 0.34618(16) 0.0192(5) Uani d . 1 . .
C C1 0.83654(19) 0.6170(3) 0.39116(19) 0.0169(5) Uani d . 1 . .
C C2 0.8582(2) 0.4680(3) 0.38683(19) 0.0183(6) Uani d . 1 . .
C C3 0.8920(2) 0.3773(3) 0.4644(2) 0.0198(6) Uani d . 1 . .
H H3 0.9064 0.2750 0.4591 0.024 Uiso calc R 1 . .
C C4 0.9038(2) 0.4366(3) 0.5468(2) 0.0198(6) Uani d . 1 . .
C C5 0.8855(2) 0.5884(3) 0.55734(19) 0.0180(6) Uani d . 1 . .
C C6 0.85181(19) 0.6765(3) 0.47856(19) 0.0160(5) Uani d . 1 . .
C C7 0.8970(2) 0.6608(4) 0.64017(19) 0.0208(6) Uani d . 1 . .
H H7 0.9187 0.6058 0.6949 0.025 Uiso calc R 1 . .
C C8 0.8765(2) 0.8106(4) 0.6412(2) 0.0230(6) Uani d . 1 . .
H H8 0.8843 0.8598 0.6964 0.028 Uiso calc R 1 . .
C C9 0.8441(2) 0.8900(3) 0.5600(2) 0.0202(6) Uani d . 1 . .
H H9 0.8310 0.9939 0.5612 0.024 Uiso calc R 1 . .
C C10 0.6471(2) 1.1032(3) 0.39562(19) 0.0183(6) Uani d . 1 . .
C C11 0.6027(2) 1.2221(3) 0.4198(2) 0.0217(6) Uani d . 1 . .
C C12 0.5108(2) 1.2119(4) 0.4191(2) 0.0248(6) Uani d . 1 . .
H H12 0.4824 1.2963 0.4356 0.030 Uiso calc R 1 . .
C C13 0.4617(2) 1.0813(4) 0.3950(2) 0.0250(7) Uani d . 1 . .
C C14 0.5014(2) 0.9536(4) 0.37007(19) 0.0218(6) Uani d . 1 . .
C C15 0.5937(2) 0.9681(3) 0.37025(19) 0.0185(5) Uani d . 1 . .
C C16 0.4580(2) 0.8118(4) 0.3460(2) 0.0288(7) Uani d . 1 . .
H H16 0.3959 0.7965 0.3449 0.035 Uiso calc R 1 . .
C C17 0.5055(2) 0.6976(4) 0.3246(2) 0.0299(7) Uani d . 1 . .
H H17 0.4771 0.6018 0.3099 0.036 Uiso calc R 1 . .
C C18 0.5961(2) 0.7209(4) 0.3242(2) 0.0251(6) Uani d . 1 . .
H H18 0.6280 0.6409 0.3077 0.030 Uiso calc R 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 Sn1 O2 . . 160.55(8) ?
O1 Sn1 N1 . . 77.91(8) ?
O2 Sn1 N1 . . 88.76(9) ?
O1 Sn1 N2 . . 87.73(9) ?
O2 Sn1 N2 . . 76.73(9) ?
N1 Sn1 N2 . . 84.03(9) ?
O1 Sn1 Cl6 . . 98.77(6) ?
O2 Sn1 Cl6 . . 95.19(6) ?
N1 Sn1 Cl6 . . 89.56(7) ?
N2 Sn1 Cl6 . . 169.75(7) ?
O1 Sn1 Cl5 . . 93.79(6) ?
O2 Sn1 Cl5 . . 97.26(6) ?
N1 Sn1 Cl5 . . 168.73(7) ?
N2 Sn1 Cl5 . . 88.07(6) ?
Cl6 Sn1 Cl5 . . 99.32(3) ?
C1 O1 Sn1 . . 115.39(17) ?
C10 O2 Sn1 . . 116.24(18) ?
C9 N1 C6 . . 120.2(3) ?
C9 N1 Sn1 . . 129.2(2) ?
C6 N1 Sn1 . . 110.64(18) ?
C18 N2 C15 . . 120.1(3) ?
C18 N2 Sn1 . . 128.8(2) ?
C15 N2 Sn1 . . 111.08(19) ?
O1 C1 C2 . . 123.4(3) ?
O1 C1 C6 . . 120.0(3) ?
C2 C1 C6 . . 116.6(3) ?
C1 C2 C3 . . 122.1(3) ?
C1 C2 Cl2 . . 119.5(2) ?
C3 C2 Cl2 . . 118.4(2) ?
C4 C3 C2 . . 120.0(3) ?
C4 C3 H3 . . 120.0 ?
C2 C3 H3 . . 120.0 ?
C3 C4 C5 . . 121.5(3) ?
C3 C4 Cl1 . . 119.1(2) ?
C5 C4 Cl1 . . 119.4(2) ?
C4 C5 C6 . . 117.2(3) ?
C4 C5 C7 . . 125.7(3) ?
C6 C5 C7 . . 117.0(3) ?
N1 C6 C5 . . 121.5(3) ?
N1 C6 C1 . . 116.0(3) ?
C5 C6 C1 . . 122.5(3) ?
C8 C7 C5 . . 119.9(3) ?
C8 C7 H7 . . 120.0 ?
C5 C7 H7 . . 120.0 ?
C7 C8 C9 . . 119.4(3) ?
C7 C8 H8 . . 120.3 ?
C9 C8 H8 . . 120.3 ?
N1 C9 C8 . . 122.0(3) ?
N1 C9 H9 . . 119.0 ?
C8 C9 H9 . . 119.0 ?
O2 C10 C11 . . 124.0(3) ?
O2 C10 C15 . . 120.0(3) ?
C11 C10 C15 . . 116.0(3) ?
C10 C11 C12 . . 122.2(3) ?
C10 C11 Cl4 . . 119.5(2) ?
C12 C11 Cl4 . . 118.3(2) ?
C13 C12 C11 . . 120.4(3) ?
C13 C12 H12 . . 119.8 ?
C11 C12 H12 . . 119.8 ?
C12 C13 C14 . . 121.5(3) ?
C12 C13 Cl3 . . 119.0(3) ?
C14 C13 Cl3 . . 119.5(3) ?
C15 C14 C13 . . 116.7(3) ?
C15 C14 C16 . . 117.0(3) ?
C13 C14 C16 . . 126.3(3) ?
N2 C15 C14 . . 121.6(3) ?
N2 C15 C10 . . 115.3(3) ?
C14 C15 C10 . . 123.2(3) ?
C17 C16 C14 . . 119.8(3) ?
C17 C16 H16 . . 120.1 ?
C14 C16 H16 . . 120.1 ?
C16 C17 C18 . . 120.1(3) ?
C16 C17 H17 . . 119.9 ?
C18 C17 H17 . . 119.9 ?
N2 C18 C17 . . 121.4(3) ?
N2 C18 H18 . . 119.3 ?
C17 C18 H18 . . 119.3 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sn1 O1 . 2.055(2) ?
Sn1 O2 . 2.061(2) ?
Sn1 N1 . 2.222(2) ?
Sn1 N2 . 2.244(2) ?
Sn1 Cl6 . 2.3122(9) ?
Sn1 Cl5 . 2.3561(8) ?
Cl1 C4 . 1.737(3) ?
Cl2 C2 . 1.726(3) ?
Cl3 C13 . 1.735(3) ?
Cl4 C11 . 1.726(3) ?
O1 C1 . 1.332(3) ?
O2 C10 . 1.321(4) ?
N1 C9 . 1.316(4) ?
N1 C6 . 1.369(4) ?
N2 C18 . 1.323(4) ?
N2 C15 . 1.365(4) ?
C1 C2 . 1.378(4) ?
C1 C6 . 1.425(4) ?
C2 C3 . 1.411(4) ?
C3 C4 . 1.362(4) ?
C3 H3 . 0.9500 ?
C4 C5 . 1.405(4) ?
C5 C6 . 1.413(4) ?
C5 C7 . 1.419(4) ?
C7 C8 . 1.374(5) ?
C7 H7 . 0.9500 ?
C8 C9 . 1.400(4) ?
C8 H8 . 0.9500 ?
C9 H9 . 0.9500 ?
C10 C11 . 1.383(4) ?
C10 C15 . 1.432(4) ?
C11 C12 . 1.401(4) ?
C12 C13 . 1.366(5) ?
C12 H12 . 0.9500 ?
C13 C14 . 1.411(5) ?
C14 C15 . 1.412(4) ?
C14 C16 . 1.418(5) ?
C16 C17 . 1.361(5) ?
C16 H16 . 0.9500 ?
C17 C18 . 1.400(5) ?
C17 H17 . 0.9500 ?
C18 H18 . 0.9500 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
O2 Sn1 O1 C1 . . . . -49.4(3) ?
N1 Sn1 O1 C1 . . . . -1.69(19) ?
N2 Sn1 O1 C1 . . . . -86.08(19) ?
Cl6 Sn1 O1 C1 . . . . 85.96(19) ?
Cl5 Sn1 O1 C1 . . . . -173.99(18) ?
O1 Sn1 O2 C10 . . . . -45.4(4) ?
N1 Sn1 O2 C10 . . . . -91.7(2) ?
N2 Sn1 O2 C10 . . . . -7.57(19) ?
Cl6 Sn1 O2 C10 . . . . 178.82(19) ?
Cl5 Sn1 O2 C10 . . . . 78.7(2) ?
O1 Sn1 N1 C9 . . . . -179.7(3) ?
O2 Sn1 N1 C9 . . . . -13.9(2) ?
N2 Sn1 N1 C9 . . . . -90.7(3) ?
Cl6 Sn1 N1 C9 . . . . 81.3(2) ?
Cl5 Sn1 N1 C9 . . . . -136.4(3) ?
O1 Sn1 N1 C6 . . . . 0.71(18) ?
O2 Sn1 N1 C6 . . . . 166.44(19) ?
N2 Sn1 N1 C6 . . . . 89.65(19) ?
Cl6 Sn1 N1 C6 . . . . -98.36(18) ?
Cl5 Sn1 N1 C6 . . . . 43.9(4) ?
O1 Sn1 N2 C18 . . . . -8.2(3) ?
O2 Sn1 N2 C18 . . . . -176.5(3) ?
N1 Sn1 N2 C18 . . . . -86.3(3) ?
Cl6 Sn1 N2 C18 . . . . -137.9(3) ?
Cl5 Sn1 N2 C18 . . . . 85.6(3) ?
O1 Sn1 N2 C15 . . . . 174.68(19) ?
O2 Sn1 N2 C15 . . . . 6.47(18) ?
N1 Sn1 N2 C15 . . . . 96.60(19) ?
Cl6 Sn1 N2 C15 . . . . 45.0(5) ?
Cl5 Sn1 N2 C15 . . . . -91.45(18) ?
Sn1 O1 C1 C2 . . . . -178.4(2) ?
Sn1 O1 C1 C6 . . . . 2.5(3) ?
O1 C1 C2 C3 . . . . -177.7(3) ?
C6 C1 C2 C3 . . . . 1.3(4) ?
O1 C1 C2 Cl2 . . . . 0.8(4) ?
C6 C1 C2 Cl2 . . . . 179.9(2) ?
C1 C2 C3 C4 . . . . 0.1(4) ?
Cl2 C2 C3 C4 . . . . -178.4(2) ?
C2 C3 C4 C5 . . . . -1.7(4) ?
C2 C3 C4 Cl1 . . . . 176.8(2) ?
C3 C4 C5 C6 . . . . 1.6(4) ?
Cl1 C4 C5 C6 . . . . -176.9(2) ?
C3 C4 C5 C7 . . . . -179.0(3) ?
Cl1 C4 C5 C7 . . . . 2.5(4) ?
C9 N1 C6 C5 . . . . 1.0(4) ?
Sn1 N1 C6 C5 . . . . -179.3(2) ?
C9 N1 C6 C1 . . . . -179.4(3) ?
Sn1 N1 C6 C1 . . . . 0.3(3) ?
C4 C5 C6 N1 . . . . 179.5(3) ?
C7 C5 C6 N1 . . . . 0.1(4) ?
C4 C5 C6 C1 . . . . -0.1(4) ?
C7 C5 C6 C1 . . . . -179.5(3) ?
O1 C1 C6 N1 . . . . -1.9(4) ?
C2 C1 C6 N1 . . . . 179.0(2) ?
O1 C1 C6 C5 . . . . 177.8(3) ?
C2 C1 C6 C5 . . . . -1.3(4) ?
C4 C5 C7 C8 . . . . 179.9(3) ?
C6 C5 C7 C8 . . . . -0.7(4) ?
C5 C7 C8 C9 . . . . 0.2(4) ?
C6 N1 C9 C8 . . . . -1.5(4) ?
Sn1 N1 C9 C8 . . . . 178.9(2) ?
C7 C8 C9 N1 . . . . 0.9(5) ?
Sn1 O2 C10 C11 . . . . -173.6(2) ?
Sn1 O2 C10 C15 . . . . 7.9(3) ?
O2 C10 C11 C12 . . . . -178.9(3) ?
C15 C10 C11 C12 . . . . -0.3(4) ?
O2 C10 C11 Cl4 . . . . 0.0(4) ?
C15 C10 C11 Cl4 . . . . 178.6(2) ?
C10 C11 C12 C13 . . . . 0.6(5) ?
Cl4 C11 C12 C13 . . . . -178.3(2) ?
C11 C12 C13 C14 . . . . -0.1(5) ?
C11 C12 C13 Cl3 . . . . 179.6(2) ?
C12 C13 C14 C15 . . . . -0.7(4) ?
Cl3 C13 C14 C15 . . . . 179.6(2) ?
C12 C13 C14 C16 . . . . 178.4(3) ?
Cl3 C13 C14 C16 . . . . -1.3(4) ?
C18 N2 C15 C14 . . . . -1.8(4) ?
Sn1 N2 C15 C14 . . . . 175.6(2) ?
C18 N2 C15 C10 . . . . 178.0(3) ?
Sn1 N2 C15 C10 . . . . -4.6(3) ?
C13 C14 C15 N2 . . . . -179.2(3) ?
C16 C14 C15 N2 . . . . 1.6(4) ?
C13 C14 C15 C10 . . . . 1.1(4) ?
C16 C14 C15 C10 . . . . -178.1(3) ?
O2 C10 C15 N2 . . . . -1.7(4) ?
C11 C10 C15 N2 . . . . 179.7(3) ?
O2 C10 C15 C14 . . . . 178.1(3) ?
C11 C10 C15 C14 . . . . -0.6(4) ?
C15 C14 C16 C17 . . . . 0.1(4) ?
C13 C14 C16 C17 . . . . -179.1(3) ?
C14 C16 C17 C18 . . . . -1.5(5) ?
C15 N2 C18 C17 . . . . 0.2(4) ?
Sn1 N2 C18 C17 . . . . -176.6(2) ?
C16 C17 C18 N2 . . . . 1.5(5) ?
