#------------------------------------------------------------------------------
#$Date: 2016-02-20 22:30:07 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176789 $
#$URL: svn://www.crystallography.net/cod/cif/2/22/41/2224159.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2224159
loop_
_publ_author_name
'Sun, Qiaozhen'
'Xiao, Tao'
'Chen, Ping'
'Gan, Xiaoqiang'
'Bao, Lin'
_publ_section_title
;Bis[μ-1,2-diphenyl-N,N'-bis(di-2-pyridylmethyleneamino)ethane-1,2-diimine]disilver(I)
 bis(hexafluoridophosphate) acetonitrile disolvate
;
_journal_coeditor_code           CS2124
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1637
_journal_page_last               m1638
_journal_paper_doi               10.1107/S160053680904882X
_journal_volume                  65
_journal_year                    2009
_chemical_formula_iupac          '[Ag2 (C36 H26 N8)2] (P F6)2, 2C2 H3 N'
_chemical_formula_moiety         'C72 H52 Ag2 N16 2+, 2(F6 P -), 2(C2 H3 N)'
_chemical_formula_sum            'C76 H58 Ag2 F12 N18 P2'
_chemical_formula_weight         1729.08
_chemical_name_systematic
;
Bis[μ-1,2-diphenyl-N,N'-bis(di-2-
pyridylmethyleneamino)ethane-1,2-diimine]disilver(I)
bis(hexafluoridophosphate) acetonitrile disolvate
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                110.037(4)
_cell_angle_beta                 90.798(4)
_cell_angle_gamma                101.192(4)
_cell_formula_units_Z            1
_cell_length_a                   11.595(2)
_cell_length_b                   12.544(3)
_cell_length_c                   13.893(3)
_cell_measurement_reflns_used    1917
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      19.78
_cell_measurement_theta_min      2.28
_cell_volume                     1855.2(7)
_computing_cell_refinement       'SAINT (Bruker, 2000)'
_computing_data_collection       'SMART (Bruker, 2000)'
_computing_data_reduction        'SAINT (Bruker, 2000)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXTL (Sheldrick, 2008)'
_computing_structure_solution    'SHELXTL (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker SMART CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0584
_diffrn_reflns_av_sigmaI/netI    0.1017
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            9153
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.80
_exptl_absorpt_coefficient_mu    0.659
_exptl_absorpt_correction_T_max  0.8130
_exptl_absorpt_correction_T_min  0.7664
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 2000)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.548
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             872
_exptl_crystal_size_max          0.36
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.30
_refine_diff_density_max         0.939
_refine_diff_density_min         -0.434
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.999
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     496
_refine_ls_number_reflns         6299
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.069
_refine_ls_R_factor_all          0.1037
_refine_ls_R_factor_gt           0.0616
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0420P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1207
_refine_ls_wR_factor_ref         0.1320
_reflns_number_gt                3860
_reflns_number_total             6299
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            cs2124.cif
_cod_data_source_block           I
_cod_original_cell_volume        1855.1(7)
_cod_database_code               2224159
_cod_database_fobs_code          2224159
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag Ag1 0.12500(5) 0.95781(4) 0.12566(4) 0.0597(2) Uani d . 1 . .
N N1 0.0264(4) 0.6675(4) 0.0581(4) 0.0477(12) Uani d . 1 . .
N N2 -0.0614(4) 0.7111(4) 0.1186(4) 0.0484(12) Uani d . 1 . .
N N3 0.1775(5) 0.8631(4) 0.2274(4) 0.0518(13) Uani d . 1 . .
N N4 -0.0751(5) 0.8984(5) 0.3691(4) 0.0589(14) Uani d . 1 . .
N N6 0.2588(5) 1.0100(4) 0.0189(4) 0.0550(13) Uani d . 1 . .
N N7 0.0420(4) 0.8746(4) -0.0466(3) 0.0439(12) Uani d . 1 . .
N N8 -0.0692(4) 0.8050(4) -0.0812(3) 0.0481(12) Uani d . 1 . .
N N9 0.1326(7) 0.5150(7) 0.4160(6) 0.103(2) Uani d . 1 . .
C C1 0.2128(6) 0.6376(6) -0.0729(5) 0.0656(19) Uani d . 1 . .
H H1B 0.2364 0.6752 -0.0032 0.079 Uiso calc R 1 . .
C C2 0.2942(6) 0.6007(7) -0.1391(6) 0.089(2) Uani d . 1 . .
H H2B 0.3725 0.6139 -0.1142 0.107 Uiso calc R 1 . .
C C3 0.2617(7) 0.5442(6) -0.2420(7) 0.081(2) Uani d . 1 . .
H H3A 0.3173 0.5194 -0.2874 0.098 Uiso calc R 1 . .
C C4 0.1464(7) 0.5249(6) -0.2767(5) 0.070(2) Uani d . 1 . .
H H4B 0.1228 0.4852 -0.3462 0.083 Uiso calc R 1 . .
C C5 0.0646(6) 0.5635(5) -0.2103(5) 0.0576(17) Uani d . 1 . .
H H5A -0.0135 0.5510 -0.2355 0.069 Uiso calc R 1 . .
C C6 0.0966(5) 0.6205(5) -0.1069(4) 0.0449(15) Uani d . 1 . .
C C7 0.0102(5) 0.6614(4) -0.0354(4) 0.0418(14) Uani d . 1 . .
C C8 -0.0267(5) 0.7660(5) 0.2139(4) 0.0456(15) Uani d . 1 . .
C C9 0.0976(5) 0.7900(5) 0.2574(4) 0.0449(14) Uani d . 1 . .
C C10 0.1285(6) 0.7424(6) 0.3259(5) 0.0615(18) Uani d . 1 . .
H H10A 0.0710 0.6931 0.3458 0.074 Uiso calc R 1 . .
C C11 0.2428(7) 0.7662(6) 0.3658(5) 0.072(2) Uani d . 1 . .
H H11A 0.2642 0.7314 0.4107 0.086 Uiso calc R 1 . .
C C12 0.3251(6) 0.8425(6) 0.3385(5) 0.0665(19) Uani d . 1 . .
H H12A 0.4030 0.8641 0.3665 0.080 Uiso calc R 1 . .
C C13 0.2877(6) 0.8860(6) 0.2675(5) 0.0673(19) Uani d . 1 . .
H H13A 0.3440 0.9350 0.2463 0.081 Uiso calc R 1 . .
C C14 -0.1161(6) 0.8080(5) 0.2831(4) 0.0479(15) Uani d . 1 . .
C C15 -0.2335(6) 0.7572(6) 0.2609(5) 0.074(2) Uani d . 1 . .
H H15A -0.2594 0.6933 0.2012 0.089 Uiso calc R 1 . .
C C16 -0.3131(7) 0.8019(7) 0.3282(6) 0.086(2) Uani d . 1 . .
H H16A -0.3933 0.7685 0.3146 0.104 Uiso calc R 1 . .
C C17 -0.2723(7) 0.8959(7) 0.4149(6) 0.077(2) Uani d . 1 . .
H H17A -0.3236 0.9282 0.4617 0.092 Uiso calc R 1 . .
C C18 -0.1534(7) 0.9410(6) 0.4309(5) 0.072(2) Uani d . 1 . .
H H18A -0.1259 1.0062 0.4894 0.086 Uiso calc R 1 . .
C C24 0.0996(5) 0.9089(5) -0.1129(4) 0.0431(14) Uani d . 1 . .
C C25 0.2171(5) 0.9865(5) -0.0784(5) 0.0495(15) Uani d . 1 . .
C C26 0.2823(6) 1.0298(6) -0.1438(5) 0.068(2) Uani d . 1 . .
H H26A 0.2528 1.0123 -0.2113 0.082 Uiso calc R 1 . .
C C27 0.3915(8) 1.0991(7) -0.1073(7) 0.094(3) Uani d . 1 . .
H H27A 0.4360 1.1297 -0.1506 0.113 Uiso calc R 1 . .
C C28 0.4358(7) 1.1240(7) -0.0110(7) 0.087(2) Uani d . 1 . .
H H28A 0.5105 1.1705 0.0135 0.105 Uiso calc R 1 . .
C C29 0.3656(6) 1.0772(6) 0.0511(6) 0.073(2) Uani d . 1 . .
H H29A 0.3948 1.0939 0.1185 0.087 Uiso calc R 1 . .
C C30 -0.0869(5) 0.7038(5) -0.0724(4) 0.0443(14) Uani d . 1 . .
C C31 -0.2037(5) 0.6277(5) -0.1080(4) 0.0472(15) Uani d . 1 . .
C C32 -0.2863(6) 0.6554(6) -0.1619(5) 0.0625(18) Uani d . 1 . .
H H32A -0.2682 0.7240 -0.1757 0.075 Uiso calc R 1 . .
C C33 -0.3952(6) 0.5833(8) -0.1957(6) 0.085(2) Uani d . 1 . .
H H33A -0.4502 0.6031 -0.2322 0.102 Uiso calc R 1 . .
C C34 -0.4231(7) 0.4823(7) -0.1759(6) 0.092(3) Uani d . 1 . .
H H34A -0.4975 0.4342 -0.1971 0.110 Uiso calc R 1 . .
C C35 -0.3411(8) 0.4533(7) -0.1249(7) 0.106(3) Uani d . 1 . .
H H35A -0.3593 0.3840 -0.1124 0.127 Uiso calc R 1 . .
C C36 -0.2317(6) 0.5243(6) -0.0915(6) 0.078(2) Uani d . 1 . .
H H36A -0.1761 0.5022 -0.0575 0.094 Uiso calc R 1 . .
C C37 0.3081(8) 0.4417(8) 0.4581(7) 0.117(3) Uani d . 1 . .
H H37B 0.3621 0.4377 0.4058 0.140 Uiso calc R 1 . .
H H37A 0.2809 0.3657 0.4612 0.140 Uiso calc R 1 . .
H H37C 0.3474 0.4933 0.5234 0.140 Uiso calc R 1 . .
C C38 0.2105(9) 0.4837(7) 0.4343(6) 0.083(3) Uani d . 1 . .
P P1 0.47556(19) 0.79693(19) 0.62145(17) 0.0765(6) Uani d . 1 . .
F F1 0.3401(4) 0.7611(5) 0.5937(3) 0.1205(17) Uani d . 1 . .
F F2 0.6120(4) 0.8324(5) 0.6505(5) 0.150(2) Uani d . 1 . .
F F3 0.4756(5) 0.6863(5) 0.6438(5) 0.171(3) Uani d . 1 . .
F F4 0.4932(5) 0.7295(6) 0.5091(4) 0.169(2) Uani d . 1 . .
F F5 0.4802(6) 0.9025(6) 0.5900(7) 0.205(3) Uani d U 1 . .
F F6 0.4586(6) 0.8673(7) 0.7292(5) 0.199(3) Uani d U 1 . .
N N5 -0.0396(5) 0.9091(4) -0.2430(3) 0.0515(13) Uani d . 1 . .
C C19 -0.0838(6) 0.8697(5) -0.3419(5) 0.0620(18) Uani d . 1 . .
H H19A -0.1478 0.8967 -0.3585 0.074 Uiso calc R 1 . .
C C20 -0.0392(7) 0.7925(6) -0.4184(5) 0.069(2) Uani d . 1 . .
H H20A -0.0736 0.7658 -0.4856 0.082 Uiso calc R 1 . .
C C21 0.0560(7) 0.7547(6) -0.3959(5) 0.071(2) Uani d . 1 . .
H H21A 0.0881 0.7024 -0.4477 0.085 Uiso calc R 1 . .
C C22 0.1044(6) 0.7941(6) -0.2965(5) 0.0628(18) Uani d . 1 . .
H H22A 0.1706 0.7702 -0.2797 0.075 Uiso calc R 1 . .
C C23 0.0535(5) 0.8690(5) -0.2228(4) 0.0473(15) Uani d . 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N3 Ag1 N5 . 2_575 99.33(17) ?
N3 Ag1 N6 . . 119.34(18) ?
N5 Ag1 N6 2_575 . 122.00(16) ?
N3 Ag1 N7 . . 127.26(16) ?
N5 Ag1 N7 2_575 . 119.22(17) ?
N6 Ag1 N7 . . 70.27(17) ?
C7 N1 N2 . . 112.5(5) ?
C8 N2 N1 . . 114.4(5) ?
C13 N3 C9 . . 116.7(5) ?
C13 N3 Ag1 . . 120.8(4) ?
C9 N3 Ag1 . . 122.2(4) ?
C18 N4 C14 . . 117.2(6) ?
C29 N6 C25 . . 118.1(6) ?
C29 N6 Ag1 . . 124.5(5) ?
C25 N6 Ag1 . . 116.4(4) ?
C24 N7 N8 . . 116.3(5) ?
C24 N7 Ag1 . . 116.6(4) ?
N8 N7 Ag1 . . 126.5(3) ?
C30 N8 N7 . . 116.2(5) ?
C2 C1 C6 . . 121.4(6) ?
C2 C1 H1B . . 119.3 ?
C6 C1 H1B . . 119.3 ?
C1 C2 C3 . . 120.5(7) ?
C1 C2 H2B . . 119.7 ?
C3 C2 H2B . . 119.7 ?
C4 C3 C2 . . 118.7(7) ?
C4 C3 H3A . . 120.6 ?
C2 C3 H3A . . 120.6 ?
C3 C4 C5 . . 120.7(7) ?
C3 C4 H4B . . 119.6 ?
C5 C4 H4B . . 119.6 ?
C4 C5 C6 . . 120.8(6) ?
C4 C5 H5A . . 119.6 ?
C6 C5 H5A . . 119.6 ?
C1 C6 C5 . . 117.7(6) ?
C1 C6 C7 . . 121.0(5) ?
C5 C6 C7 . . 121.3(6) ?
N1 C7 C6 . . 118.6(5) ?
N1 C7 C30 . . 123.0(5) ?
C6 C7 C30 . . 118.1(5) ?
N2 C8 C14 . . 117.2(5) ?
N2 C8 C9 . . 123.8(5) ?
C14 C8 C9 . . 118.9(5) ?
N3 C9 C10 . . 121.7(6) ?
N3 C9 C8 . . 116.8(5) ?
C10 C9 C8 . . 121.5(6) ?
C9 C10 C11 . . 120.8(6) ?
C9 C10 H10A . . 119.6 ?
C11 C10 H10A . . 119.6 ?
C10 C11 C12 . . 118.6(6) ?
C10 C11 H11A . . 120.7 ?
C12 C11 H11A . . 120.7 ?
C11 C12 C13 . . 117.3(6) ?
C11 C12 H12A . . 121.3 ?
C13 C12 H12A . . 121.3 ?
N3 C13 C12 . . 124.8(6) ?
N3 C13 H13A . . 117.6 ?
C12 C13 H13A . . 117.6 ?
N4 C14 C15 . . 122.2(6) ?
N4 C14 C8 . . 115.7(6) ?
C15 C14 C8 . . 122.0(6) ?
C14 C15 C16 . . 119.2(6) ?
C14 C15 H15A . . 120.4 ?
C16 C15 H15A . . 120.4 ?
C17 C16 C15 . . 118.9(7) ?
C17 C16 H16A . . 120.6 ?
C15 C16 H16A . . 120.6 ?
C16 C17 C18 . . 117.9(7) ?
C16 C17 H17A . . 121.0 ?
C18 C17 H17A . . 121.0 ?
N4 C18 C17 . . 124.4(7) ?
N4 C18 H18A . . 117.8 ?
C17 C18 H18A . . 117.8 ?
N7 C24 C25 . . 118.1(5) ?
N7 C24 C23 . . 122.1(5) ?
C25 C24 C23 . . 119.7(5) ?
N6 C25 C26 . . 121.5(6) ?
N6 C25 C24 . . 116.9(5) ?
C26 C25 C24 . . 121.5(6) ?
C27 C26 C25 . . 118.4(7) ?
C27 C26 H26A . . 120.8 ?
C25 C26 H26A . . 120.8 ?
C28 C27 C26 . . 121.6(8) ?
C28 C27 H27A . . 119.2 ?
C26 C27 H27A . . 119.2 ?
C27 C28 C29 . . 117.1(7) ?
C27 C28 H28A . . 121.5 ?
C29 C28 H28A . . 121.5 ?
N6 C29 C28 . . 123.3(7) ?
N6 C29 H29A . . 118.3 ?
C28 C29 H29A . . 118.3 ?
N8 C30 C31 . . 117.7(5) ?
N8 C30 C7 . . 121.5(5) ?
C31 C30 C7 . . 120.5(5) ?
C36 C31 C32 . . 118.2(6) ?
C36 C31 C30 . . 120.5(6) ?
C32 C31 C30 . . 121.3(6) ?
C33 C32 C31 . . 120.9(7) ?
C33 C32 H32A . . 119.5 ?
C31 C32 H32A . . 119.5 ?
C34 C33 C32 . . 120.1(7) ?
C34 C33 H33A . . 119.9 ?
C32 C33 H33A . . 119.9 ?
C35 C34 C33 . . 119.2(8) ?
C35 C34 H34A . . 120.4 ?
C33 C34 H34A . . 120.4 ?
C34 C35 C36 . . 121.2(8) ?
C34 C35 H35A . . 119.4 ?
C36 C35 H35A . . 119.4 ?
C35 C36 C31 . . 120.3(7) ?
C35 C36 H36A . . 119.8 ?
C31 C36 H36A . . 119.8 ?
C38 C37 H37B . . 109.5 ?
C38 C37 H37A . . 109.5 ?
H37B C37 H37A . . 109.5 ?
C38 C37 H37C . . 109.5 ?
H37B C37 H37C . . 109.5 ?
H37A C37 H37C . . 109.5 ?
N9 C38 C37 . . 178.7(11) ?
F6 P1 F3 . . 94.9(4) ?
F6 P1 F5 . . 90.1(4) ?
F3 P1 F5 . . 174.8(5) ?
F6 P1 F4 . . 177.3(5) ?
F3 P1 F4 . . 87.8(4) ?
F5 P1 F4 . . 87.2(4) ?
F6 P1 F1 . . 90.8(3) ?
F3 P1 F1 . . 91.2(3) ?
F5 P1 F1 . . 90.1(3) ?
F4 P1 F1 . . 89.2(3) ?
F6 P1 F2 . . 88.8(3) ?
F3 P1 F2 . . 88.2(3) ?
F5 P1 F2 . . 90.5(3) ?
F4 P1 F2 . . 91.2(4) ?
F1 P1 F2 . . 179.3(4) ?
C23 N5 C19 . . 116.5(5) ?
C23 N5 Ag1 . 2_575 125.8(4) ?
C19 N5 Ag1 . 2_575 117.7(4) ?
N5 C19 C20 . . 123.0(6) ?
N5 C19 H19A . . 118.5 ?
C20 C19 H19A . . 118.5 ?
C21 C20 C19 . . 119.2(6) ?
C21 C20 H20A . . 120.4 ?
C19 C20 H20A . . 120.4 ?
C20 C21 C22 . . 119.5(7) ?
C20 C21 H21A . . 120.3 ?
C22 C21 H21A . . 120.3 ?
C23 C22 C21 . . 118.4(7) ?
C23 C22 H22A . . 120.8 ?
C21 C22 H22A . . 120.8 ?
N5 C23 C22 . . 123.4(6) ?
N5 C23 C24 . . 116.5(5) ?
C22 C23 C24 . . 120.1(6) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ag1 N3 . 2.277(5) ?
Ag1 N5 2_575 2.291(5) ?
Ag1 N6 . 2.317(5) ?
Ag1 N7 . 2.361(5) ?
N1 C7 . 1.284(6) ?
N1 N2 . 1.402(6) ?
N2 C8 . 1.281(6) ?
N3 C13 . 1.324(7) ?
N3 C9 . 1.348(7) ?
N4 C18 . 1.321(8) ?
N4 C14 . 1.336(7) ?
N6 C29 . 1.328(7) ?
N6 C25 . 1.342(7) ?
N7 C24 . 1.287(6) ?
N7 N8 . 1.385(6) ?
N8 C30 . 1.294(7) ?
N9 C38 . 1.112(10) ?
C1 C2 . 1.361(9) ?
C1 C6 . 1.373(8) ?
C1 H1B . 0.93 ?
C2 C3 . 1.370(9) ?
C2 H2B . 0.93 ?
C3 C4 . 1.362(9) ?
C3 H3A . 0.93 ?
C4 C5 . 1.371(8) ?
C4 H4B . 0.93 ?
C5 C6 . 1.375(7) ?
C5 H5A . 0.93 ?
C6 C7 . 1.460(7) ?
C7 C30 . 1.489(8) ?
C8 C14 . 1.473(8) ?
C8 C9 . 1.488(8) ?
C9 C10 . 1.362(8) ?
C10 C11 . 1.366(8) ?
C10 H10A . 0.93 ?
C11 C12 . 1.369(9) ?
C11 H11A . 0.93 ?
C12 C13 . 1.381(8) ?
C12 H12A . 0.93 ?
C13 H13A . 0.93 ?
C14 C15 . 1.368(8) ?
C15 C16 . 1.381(9) ?
C15 H15A . 0.93 ?
C16 C17 . 1.363(9) ?
C16 H16A . 0.93 ?
C17 C18 . 1.368(9) ?
C17 H17A . 0.93 ?
C18 H18A . 0.93 ?
C24 C25 . 1.477(8) ?
C24 C23 . 1.490(8) ?
C25 C26 . 1.375(8) ?
C26 C27 . 1.367(9) ?
C26 H26A . 0.93 ?
C27 C28 . 1.336(10) ?
C27 H27A . 0.93 ?
C28 C29 . 1.389(10) ?
C28 H28A . 0.93 ?
C29 H29A . 0.93 ?
C30 C31 . 1.465(7) ?
C31 C36 . 1.372(8) ?
C31 C32 . 1.373(8) ?
C32 C33 . 1.372(8) ?
C32 H32A . 0.93 ?
C33 C34 . 1.366(10) ?
C33 H33A . 0.93 ?
C34 C35 . 1.352(10) ?
C34 H34A . 0.93 ?
C35 C36 . 1.371(9) ?
C35 H35A . 0.93 ?
C36 H36A . 0.93 ?
C37 C38 . 1.416(11) ?
C37 H37B . 0.96 ?
C37 H37A . 0.96 ?
C37 H37C . 0.96 ?
P1 F6 . 1.493(6) ?
P1 F3 . 1.522(6) ?
P1 F5 . 1.522(6) ?
P1 F4 . 1.537(6) ?
P1 F1 . 1.552(4) ?
P1 F2 . 1.565(5) ?
N5 C23 . 1.340(7) ?
N5 C19 . 1.345(7) ?
N5 Ag1 2_575 2.291(5) ?
C19 C20 . 1.356(8) ?
C19 H19A . 0.93 ?
C20 C21 . 1.355(9) ?
C20 H20A . 0.93 ?
C21 C22 . 1.367(9) ?
C21 H21A . 0.93 ?
C22 C23 . 1.362(8) ?
C22 H22A . 0.93 ?
