#------------------------------------------------------------------------------
#$Date: 2016-02-20 22:30:07 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176789 $
#$URL: svn://www.crystallography.net/cod/cif/2/22/49/2224980.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2224980
loop_
_publ_author_name
'Abo-Amer, Anwar'
_publ_section_title
;
 cis-Dimethylbis(triphenylarsine)platinum(II)
;
_journal_coeditor_code           HB5294
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m172
_journal_paper_doi               10.1107/S1600536809055470
_journal_volume                  66
_journal_year                    2010
_chemical_formula_iupac          '[Pt (C H3)2 (C18 H15 As)2]'
_chemical_formula_moiety         'C38 H36 As2 Pt'
_chemical_formula_sum            'C38 H36 As2 Pt'
_chemical_formula_weight         837.60
_chemical_name_systematic
;
cis-Dimethylbis(triphenylarsine)platinum(II)
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                91.106(2)
_cell_angle_beta                 99.588(2)
_cell_angle_gamma                115.227(2)
_cell_formula_units_Z            2
_cell_length_a                   10.1033(9)
_cell_length_b                   10.3937(8)
_cell_length_c                   17.2452(13)
_cell_measurement_reflns_used    9885
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      30.16
_cell_measurement_theta_min      2.27
_cell_volume                     1607.0(2)
_computing_cell_refinement       'SAINT (Bruker, 2001)'
_computing_data_collection       'APEX2 (Bruker, 2001)'
_computing_data_reduction        'SAINT (Bruker, 2001)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Bruker APEXII CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0192
_diffrn_reflns_av_sigmaI/netI    0.0292
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            19166
_diffrn_reflns_theta_full        30.16
_diffrn_reflns_theta_max         30.16
_diffrn_reflns_theta_min         1.20
_exptl_absorpt_coefficient_mu    6.434
_exptl_absorpt_correction_T_max  0.374
_exptl_absorpt_correction_T_min  0.332
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 2001)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.731
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             816
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.19
_refine_diff_density_max         0.559
_refine_diff_density_min         -1.070
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.642
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     372
_refine_ls_number_reflns         9358
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.642
_refine_ls_R_factor_all          0.0240
_refine_ls_R_factor_gt           0.0203
_refine_ls_shift/su_max          0.066
_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0702
_refine_ls_wR_factor_ref         0.0774
_reflns_number_gt                8543
_reflns_number_total             9358
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            hb5294.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_database_code               2224980
_cod_database_fobs_code          2224980
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt Pt1 1.029195(9) 0.072490(9) 0.271372(5) 0.01642(4) Uani d . 1 . .
As As1 1.04466(3) 0.25078(3) 0.367248(15) 0.01542(6) Uani d . 1 . .
As As2 0.85760(3) 0.10672(3) 0.168572(15) 0.01719(6) Uani d . 1 . .
C C1 0.8543(3) 0.2235(3) 0.39079(15) 0.0188(4) Uani d . 1 . .
C C2 0.8076(3) 0.3307(3) 0.39670(16) 0.0236(5) Uani d . 1 . .
H H2 0.8707 0.4259 0.3885 0.028 Uiso calc R 1 . .
C C3 0.6679(3) 0.2982(4) 0.41463(17) 0.0311(6) Uani d . 1 . .
H H3 0.6352 0.3710 0.4180 0.037 Uiso calc R 1 . .
C C4 0.5768(3) 0.1597(4) 0.42758(19) 0.0357(7) Uani d . 1 . .
H H4 0.4829 0.1382 0.4412 0.043 Uiso calc R 1 . .
C C5 0.6223(3) 0.0536(4) 0.42067(19) 0.0336(7) Uani d . 1 . .
H H5 0.5586 -0.0414 0.4288 0.040 Uiso calc R 1 . .
C C6 0.7605(3) 0.0839(3) 0.40192(17) 0.0248(5) Uani d . 1 . .
H H6 0.7908 0.0098 0.3967 0.030 Uiso calc R 1 . .
C C7 1.1385(2) 0.4450(3) 0.33885(15) 0.0176(4) Uani d . 1 . .
C C8 1.1859(3) 0.4651(3) 0.26647(16) 0.0241(5) Uani d . 1 . .
H H8 1.1696 0.3849 0.2322 0.029 Uiso calc R 1 . .
C C9 1.2570(3) 0.6023(3) 0.2447(2) 0.0322(6) Uani d . 1 . .
H H9 1.2887 0.6161 0.1954 0.039 Uiso calc R 1 . .
C C10 1.2818(3) 0.7199(3) 0.2954(2) 0.0330(7) Uani d . 1 . .
H H10 1.3291 0.8139 0.2803 0.040 Uiso calc R 1 . .
C C11 1.2374(3) 0.6997(3) 0.3677(2) 0.0295(6) Uani d . 1 . .
H H11 1.2559 0.7800 0.4026 0.035 Uiso calc R 1 . .
C C12 1.1659(3) 0.5623(3) 0.38953(16) 0.0227(5) Uani d . 1 . .
H H12 1.1358 0.5489 0.4393 0.027 Uiso calc R 1 . .
C C13 1.1613(3) 0.2778(3) 0.47356(15) 0.0180(4) Uani d . 1 . .
C C14 1.3155(3) 0.3227(3) 0.48190(17) 0.0246(5) Uani d . 1 . .
H H14 1.3604 0.3403 0.4366 0.029 Uiso calc R 1 . .
C C15 1.4027(3) 0.3414(3) 0.55628(19) 0.0299(6) Uani d . 1 . .
H H15 1.5072 0.3723 0.5617 0.036 Uiso calc R 1 . .
C C16 1.3385(3) 0.3152(3) 0.62213(18) 0.0303(6) Uani d . 1 . .
H H16 1.3988 0.3279 0.6728 0.036 Uiso calc R 1 . .
C C17 1.1872(4) 0.2707(4) 0.61499(18) 0.0340(7) Uani d . 1 . .
H H17 1.1434 0.2533 0.6607 0.041 Uiso calc R 1 . .
C C18 1.0979(3) 0.2513(3) 0.54014(17) 0.0264(5) Uani d . 1 . .
H H18 0.9934 0.2198 0.5352 0.032 Uiso calc R 1 . .
C C19 1.0329(3) -0.0808(3) 0.19328(19) 0.0294(6) Uani d . 1 . .
H H19A 1.1365 -0.0600 0.1916 0.044 Uiso calc R 1 . .
H H19B 0.9808 -0.0790 0.1403 0.044 Uiso calc R 1 . .
H H19C 0.9833 -0.1757 0.2112 0.044 Uiso calc R 1 . .
C C20 1.1755(3) 0.0233(3) 0.34881(18) 0.0297(6) Uani d . 1 . .
H H20A 1.1554 -0.0765 0.3362 0.045 Uiso calc R 1 . .
H H20B 1.1627 0.0367 0.4030 0.045 Uiso calc R 1 . .
H H20C 1.2780 0.0862 0.3440 0.045 Uiso calc R 1 . .
C C21 0.7011(3) -0.0729(3) 0.11442(15) 0.0190(4) Uani d . 1 . .
C C22 0.6602(3) -0.1928(3) 0.15666(18) 0.0266(5) Uani d . 1 . .
H H22 0.7092 -0.1856 0.2097 0.032 Uiso calc R 1 . .
C C23 0.5468(3) -0.3232(3) 0.1202(2) 0.0320(6) Uani d . 1 . .
H H23 0.5195 -0.4051 0.1486 0.038 Uiso calc R 1 . .
C C24 0.4745(3) -0.3344(3) 0.0442(2) 0.0314(6) Uani d . 1 . .
H H24 0.3960 -0.4234 0.0206 0.038 Uiso calc R 1 . .
C C25 0.5153(3) -0.2165(3) 0.00144(18) 0.0286(6) Uani d . 1 . .
H H25 0.4660 -0.2248 -0.0517 0.034 Uiso calc R 1 . .
C C26 0.6292(3) -0.0855(3) 0.03672(16) 0.0231(5) Uani d . 1 . .
H H26 0.6577 -0.0046 0.0075 0.028 Uiso calc R 1 . .
C C27 0.9495(3) 0.2048(3) 0.08340(16) 0.0208(5) Uani d . 1 . .
C C28 1.0904(3) 0.2177(3) 0.07933(18) 0.0256(5) Uani d . 1 . .
H H28 1.1393 0.1803 0.1179 0.031 Uiso calc R 1 . .
C C29 1.1602(3) 0.2855(3) 0.0186(2) 0.0338(7) Uani d . 1 . .
H H29 1.2560 0.2925 0.0155 0.041 Uiso calc R 1 . .
C C30 1.0929(4) 0.3417(3) -0.03621(19) 0.0326(7) Uani d . 1 . .
H H30 1.1421 0.3888 -0.0770 0.039 Uiso calc R 1 . .
C C31 0.9532(4) 0.3303(3) -0.03262(18) 0.0317(6) Uani d . 1 . .
H H31 0.9059 0.3689 -0.0713 0.038 Uiso calc R 1 . .
C C32 0.8815(3) 0.2632(3) 0.02676(17) 0.0260(5) Uani d . 1 . .
H H32 0.7856 0.2566 0.0291 0.031 Uiso calc R 1 . .
C C33 0.7360(3) 0.2037(3) 0.18684(15) 0.0196(5) Uani d . 1 . .
C C34 0.7918(3) 0.3515(3) 0.18978(17) 0.0236(5) Uani d . 1 . .
H H34 0.8900 0.4068 0.1812 0.028 Uiso calc R 1 . .
C C35 0.7047(3) 0.4193(3) 0.20524(18) 0.0297(6) Uani d . 1 . .
H H35 0.7431 0.5203 0.2063 0.036 Uiso calc R 1 . .
C C36 0.5628(4) 0.3401(4) 0.2190(2) 0.0328(6) Uani d . 1 . .
H H36 0.5037 0.3866 0.2297 0.039 Uiso calc R 1 . .
C C37 0.5064(3) 0.1928(4) 0.21732(19) 0.0322(6) Uani d . 1 . .
H H37 0.4089 0.1383 0.2270 0.039 Uiso calc R 1 . .
C C38 0.5923(3) 0.1251(3) 0.20146(17) 0.0261(5) Uani d . 1 . .
H H38 0.5532 0.0241 0.2005 0.031 Uiso calc R 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C20 Pt1 C19 . . 84.17(12) ?
C20 Pt1 As1 . . 91.34(8) ?
C19 Pt1 As1 . . 175.17(8) ?
C20 Pt1 As2 . . 172.47(8) ?
C19 Pt1 As2 . . 88.30(9) ?
As1 Pt1 As2 . . 96.184(10) ?
C1 As1 C7 . . 106.44(10) ?
C1 As1 C13 . . 100.90(10) ?
C7 As1 C13 . . 99.16(10) ?
C1 As1 Pt1 . . 114.16(8) ?
C7 As1 Pt1 . . 114.10(7) ?
C13 As1 Pt1 . . 120.02(7) ?
C27 As2 C21 . . 103.04(11) ?
C27 As2 C33 . . 101.73(11) ?
C21 As2 C33 . . 99.24(11) ?
C27 As2 Pt1 . . 113.51(8) ?
C21 As2 Pt1 . . 112.60(8) ?
C33 As2 Pt1 . . 123.96(7) ?
C2 C1 C6 . . 119.8(2) ?
C2 C1 As1 . . 125.07(19) ?
C6 C1 As1 . . 115.17(19) ?
C1 C2 C3 . . 119.9(3) ?
C1 C2 H2 . . 120.1 ?
C3 C2 H2 . . 120.1 ?
C4 C3 C2 . . 120.0(3) ?
C4 C3 H3 . . 120.0 ?
C2 C3 H3 . . 120.0 ?
C5 C4 C3 . . 120.1(3) ?
C5 C4 H4 . . 120.0 ?
C3 C4 H4 . . 120.0 ?
C4 C5 C6 . . 120.6(3) ?
C4 C5 H5 . . 119.7 ?
C6 C5 H5 . . 119.7 ?
C5 C6 C1 . . 119.6(3) ?
C5 C6 H6 . . 120.2 ?
C1 C6 H6 . . 120.2 ?
C12 C7 C8 . . 119.8(2) ?
C12 C7 As1 . . 122.02(19) ?
C8 C7 As1 . . 118.05(19) ?
C9 C8 C7 . . 120.0(3) ?
C9 C8 H8 . . 120.0 ?
C7 C8 H8 . . 120.0 ?
C8 C9 C10 . . 119.8(3) ?
C8 C9 H9 . . 120.1 ?
C10 C9 H9 . . 120.1 ?
C11 C10 C9 . . 120.0(3) ?
C11 C10 H10 . . 120.0 ?
C9 C10 H10 . . 120.0 ?
C10 C11 C12 . . 120.2(3) ?
C10 C11 H11 . . 119.9 ?
C12 C11 H11 . . 119.9 ?
C7 C12 C11 . . 120.1(3) ?
C7 C12 H12 . . 120.0 ?
C11 C12 H12 . . 120.0 ?
C18 C13 C14 . . 119.1(2) ?
C18 C13 As1 . . 122.79(19) ?
C14 C13 As1 . . 118.08(19) ?
C15 C14 C13 . . 120.1(3) ?
C15 C14 H14 . . 119.9 ?
C13 C14 H14 . . 119.9 ?
C16 C15 C14 . . 120.3(3) ?
C16 C15 H15 . . 119.9 ?
C14 C15 H15 . . 119.9 ?
C15 C16 C17 . . 120.4(3) ?
C15 C16 H16 . . 119.8 ?
C17 C16 H16 . . 119.8 ?
C16 C17 C18 . . 119.9(3) ?
C16 C17 H17 . . 120.1 ?
C18 C17 H17 . . 120.1 ?
C13 C18 C17 . . 120.2(3) ?
C13 C18 H18 . . 119.9 ?
C17 C18 H18 . . 119.9 ?
Pt1 C19 H19A . . 109.5 ?
Pt1 C19 H19B . . 109.5 ?
H19A C19 H19B . . 109.5 ?
Pt1 C19 H19C . . 109.5 ?
H19A C19 H19C . . 109.5 ?
H19B C19 H19C . . 109.5 ?
Pt1 C20 H20A . . 109.5 ?
Pt1 C20 H20B . . 109.5 ?
H20A C20 H20B . . 109.5 ?
Pt1 C20 H20C . . 109.5 ?
H20A C20 H20C . . 109.5 ?
H20B C20 H20C . . 109.5 ?
C26 C21 C22 . . 119.6(2) ?
C26 C21 As2 . . 122.77(19) ?
C22 C21 As2 . . 117.67(19) ?
C23 C22 C21 . . 119.4(3) ?
C23 C22 H22 . . 120.3 ?
C21 C22 H22 . . 120.3 ?
C24 C23 C22 . . 120.8(3) ?
C24 C23 H23 . . 119.6 ?
C22 C23 H23 . . 119.6 ?
C23 C24 C25 . . 120.2(3) ?
C23 C24 H24 . . 119.9 ?
C25 C24 H24 . . 119.9 ?
C24 C25 C26 . . 119.7(3) ?
C24 C25 H25 . . 120.1 ?
C26 C25 H25 . . 120.1 ?
C21 C26 C25 . . 120.3(3) ?
C21 C26 H26 . . 119.9 ?
C25 C26 H26 . . 119.9 ?
C28 C27 C32 . . 118.8(3) ?
C28 C27 As2 . . 117.8(2) ?
C32 C27 As2 . . 123.44(19) ?
C27 C28 C29 . . 119.9(3) ?
C27 C28 H28 . . 120.0 ?
C29 C28 H28 . . 120.0 ?
C30 C29 C28 . . 120.8(3) ?
C30 C29 H29 . . 119.6 ?
C28 C29 H29 . . 119.6 ?
C29 C30 C31 . . 119.9(3) ?
C29 C30 H30 . . 120.1 ?
C31 C30 H30 . . 120.1 ?
C30 C31 C32 . . 120.5(3) ?
C30 C31 H31 . . 119.8 ?
C32 C31 H31 . . 119.8 ?
C31 C32 C27 . . 120.2(3) ?
C31 C32 H32 . . 119.9 ?
C27 C32 H32 . . 119.9 ?
C34 C33 C38 . . 118.6(2) ?
C34 C33 As2 . . 121.24(19) ?
C38 C33 As2 . . 120.0(2) ?
C33 C34 C35 . . 120.4(3) ?
C33 C34 H34 . . 119.8 ?
C35 C34 H34 . . 119.8 ?
C36 C35 C34 . . 120.2(3) ?
C36 C35 H35 . . 119.9 ?
C34 C35 H35 . . 119.9 ?
C35 C36 C37 . . 120.0(3) ?
C35 C36 H36 . . 120.0 ?
C37 C36 H36 . . 120.0 ?
C38 C37 C36 . . 119.9(3) ?
C38 C37 H37 . . 120.0 ?
C36 C37 H37 . . 120.0 ?
C37 C38 C33 . . 120.8(3) ?
C37 C38 H38 . . 119.6 ?
C33 C38 H38 . . 119.6 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Pt1 C20 . 2.060(3) y
Pt1 C19 . 2.083(3) y
Pt1 As1 . 2.3960(3) y
Pt1 As2 . 2.4086(3) y
As1 C1 . 1.935(2) ?
As1 C7 . 1.943(2) ?
As1 C13 . 1.951(2) ?
As2 C27 . 1.940(3) ?
As2 C21 . 1.945(2) ?
As2 C33 . 1.949(2) ?
C1 C2 . 1.391(4) ?
C1 C6 . 1.393(4) ?
C2 C3 . 1.395(4) ?
C2 H2 . 0.9500 ?
C3 C4 . 1.386(5) ?
C3 H3 . 0.9500 ?
C4 C5 . 1.374(5) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.391(4) ?
C5 H5 . 0.9500 ?
C6 H6 . 0.9500 ?
C7 C12 . 1.384(3) ?
C7 C8 . 1.398(4) ?
C8 C9 . 1.388(4) ?
C8 H8 . 0.9500 ?
C9 C10 . 1.395(5) ?
C9 H9 . 0.9500 ?
C10 C11 . 1.384(5) ?
C10 H10 . 0.9500 ?
C11 C12 . 1.391(4) ?
C11 H11 . 0.9500 ?
C12 H12 . 0.9500 ?
C13 C18 . 1.383(4) ?
C13 C14 . 1.403(3) ?
C14 C15 . 1.388(4) ?
C14 H14 . 0.9500 ?
C15 C16 . 1.375(4) ?
C15 H15 . 0.9500 ?
C16 C17 . 1.378(4) ?
C16 H16 . 0.9500 ?
C17 C18 . 1.403(4) ?
C17 H17 . 0.9500 ?
C18 H18 . 0.9500 ?
C19 H19A . 0.9800 ?
C19 H19B . 0.9800 ?
C19 H19C . 0.9800 ?
C20 H20A . 0.9800 ?
C20 H20B . 0.9800 ?
C20 H20C . 0.9800 ?
C21 C26 . 1.388(4) ?
C21 C22 . 1.397(4) ?
C22 C23 . 1.396(4) ?
C22 H22 . 0.9500 ?
C23 C24 . 1.366(5) ?
C23 H23 . 0.9500 ?
C24 C25 . 1.387(4) ?
C24 H24 . 0.9500 ?
C25 C26 . 1.396(4) ?
C25 H25 . 0.9500 ?
C26 H26 . 0.9500 ?
C27 C28 . 1.385(3) ?
C27 C32 . 1.396(4) ?
C28 C29 . 1.395(4) ?
C28 H28 . 0.9500 ?
C29 C30 . 1.356(5) ?
C29 H29 . 0.9500 ?
C30 C31 . 1.377(5) ?
C30 H30 . 0.9500 ?
C31 C32 . 1.380(4) ?
C31 H31 . 0.9500 ?
C32 H32 . 0.9500 ?
C33 C34 . 1.389(4) ?
C33 C38 . 1.399(3) ?
C34 C35 . 1.393(4) ?
C34 H34 . 0.9500 ?
C35 C36 . 1.380(4) ?
C35 H35 . 0.9500 ?
C36 C37 . 1.385(5) ?
C36 H36 . 0.9500 ?
C37 C38 . 1.383(4) ?
C37 H37 . 0.9500 ?
C38 H38 . 0.9500 ?
