#------------------------------------------------------------------------------
#$Date: 2016-02-14 16:26:36 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176435 $
#$URL: svn://www.crystallography.net/cod/cif/2/23/36/2233615.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2233615
loop_
_publ_author_name
'Zhao, Dan'
'Zhu, Jing'
'Liang, Peng'
'Chang, Huan'
'He, Rong'
_publ_section_title
;
 Lithium europium(III) molybdate(VI), Li~3.5~Eu~1.5~(MoO₄)₄
;
_journal_coeditor_code           RU2018
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i14
_journal_paper_doi               10.1107/S1600536812000268
_journal_volume                  68
_journal_year                    2012
_chemical_formula_iupac          'Li3.5 Eu1.5 (Mo O4)4'
_chemical_formula_moiety         'Eu1.50 Li3.50 Mo4 O16'
_chemical_formula_sum            'Eu1.5 Li3.5 Mo4 O16'
_chemical_formula_weight         891.99
_chemical_name_systematic
;
Lithium europium(III) molybdate(VI)
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                100.09(2)
_cell_angle_beta                 100.341(15)
_cell_angle_gamma                111.891(15)
_cell_formula_units_Z            1
_cell_length_a                   5.2182(11)
_cell_length_b                   6.7008(12)
_cell_length_c                   10.3167(5)
_cell_measurement_reflns_used    791
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      2.0801
_cell_volume                     317.49(11)
_computing_cell_refinement       'CrystalClear (Rigaku, 2004)'
_computing_data_collection       'CrystalClear (Rigaku, 2004)'
_computing_data_reduction        'CrystalClear (Rigaku, 2004)'
_computing_molecular_graphics    'DIAMOND (Brandenburg, 2004)'
_computing_publication_material
'SHELXTL (Sheldrick, 2008) and PLATON (Spek, 2009)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean 14.6306
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device_type  'Rigaku Mercury70 CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0143
_diffrn_reflns_av_sigmaI/netI    0.0214
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            2478
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.40
_exptl_absorpt_coefficient_mu    11.222
_exptl_absorpt_correction_T_max  0.6038
_exptl_absorpt_correction_T_min  0.2125
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(ABSCOR; Higashi, 1995)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    4.665
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             401
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.951
_refine_diff_density_min         -1.615
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.102
_refine_ls_matrix_type           full
_refine_ls_number_parameters     105
_refine_ls_number_reflns         1437
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.102
_refine_ls_R_factor_all          0.0339
_refine_ls_R_factor_gt           0.0286
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0380P)²+1.5273P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0755
_refine_ls_wR_factor_ref         0.0787
_reflns_number_gt                1224
_reflns_number_total             1437
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            ru2018.cif
_cod_data_source_block           I
_cod_original_cell_volume        317.49(9)
_cod_original_formula_sum        'Eu1.50 Li3.50 Mo4 O16'
_cod_database_code               2233615
_cod_database_fobs_code          2233615
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_symmetry_multiplicity
Li Li1 0.62034(7) 0.77190(5) 0.43965(3) 0.00542(13) Uani d P 0.25 1
Eu Eu1 0.62034(7) 0.77190(5) 0.43965(3) 0.00542(13) Uani d P 0.75 1
Mo Mo1 0.16529(10) 0.70023(7) 0.68099(5) 0.00873(15) Uani d . 1 1
Mo Mo2 1.08254(11) 0.84541(8) 0.19822(5) 0.01044(15) Uani d . 1 1
O O1 0.3065(9) 0.5032(7) 0.7078(4) 0.0141(9) Uani d . 1 1
O O2 0.8045(9) 0.5637(7) 0.5724(4) 0.0145(9) Uani d . 1 1
O O3 0.7317(9) 0.3263(7) 0.7745(4) 0.0175(9) Uani d . 1 1
O O4 0.7691(10) 0.6882(7) 0.0693(5) 0.0213(10) Uani d . 1 1
O O5 0.3812(8) 0.8834(6) 0.5948(4) 0.0099(8) Uani d . 1 1
O O6 1.0161(9) 0.9568(7) 0.3572(4) 0.0141(9) Uani d . 1 1
O O7 1.1437(9) 0.8249(7) 0.8386(4) 0.0175(9) Uani d . 1 1
O O8 1.3010(9) 1.0575(7) 0.1374(4) 0.0167(9) Uani d . 1 1
Li Li2 0.669(4) 0.593(3) 0.869(2) 0.060(5) Uiso d . 1 1
Li Li3 1.5000 1.0000 0.0000 0.049(6) Uiso d S 1 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
O1 Li1 O6 2_666 . 72.17(14)
O1 Li1 O5 2_666 . 152.17(14)
O6 Li1 O5 . . 135.59(14)
O1 Li1 O5 2_666 2_676 128.42(13)
O6 Li1 O5 . 2_676 70.23(13)
O5 Li1 O5 . 2_676 74.09(15)
O1 Li1 O3 2_666 2_666 75.14(14)
O6 Li1 O3 . 2_666 94.56(15)
O5 Li1 O3 . 2_666 100.26(14)
O5 Li1 O3 2_676 2_666 74.05(14)
O1 Li1 O2 2_666 . 70.22(14)
O6 Li1 O2 . . 101.42(14)
O5 Li1 O2 . . 97.18(13)
O5 Li1 O2 2_676 . 151.16(14)
O3 Li1 O2 2_666 . 134.77(14)
O1 Li1 O6 2_666 2_776 124.00(14)
O6 Li1 O6 . 2_776 75.58(15)
O5 Li1 O6 . 2_776 71.94(13)
O5 Li1 O6 2_676 2_776 78.18(14)
O3 Li1 O6 2_666 2_776 152.23(14)
O2 Li1 O6 . 2_776 72.99(14)
O1 Li1 O2 2_666 2_666 79.65(14)
O6 Li1 O2 . 2_666 150.92(14)
O5 Li1 O2 . 2_666 73.02(13)
O5 Li1 O2 2_676 2_666 125.81(14)
O3 Li1 O2 2_666 2_666 70.98(15)
O2 Li1 O2 . 2_666 74.91(16)
O6 Li1 O2 2_776 2_666 128.19(14)
O1 Li1 Li2 2_666 2_666 38.4(4)
O6 Li1 Li2 . 2_666 87.0(3)
O5 Li1 Li2 . 2_666 128.2(4)
O5 Li1 Li2 2_676 2_666 105.7(4)
O3 Li1 Li2 2_666 2_666 37.4(4)
O2 Li1 Li2 . 2_666 101.2(4)
O6 Li1 Li2 2_776 2_666 159.8(3)
O2 Li1 Li2 2_666 2_666 66.1(3)
O1 Li1 Eu1 2_666 2_776 99.68(11)
O6 Li1 Eu1 . 2_776 38.45(10)
O5 Li1 Eu1 . 2_776 104.25(10)
O5 Li1 Eu1 2_676 2_776 69.98(10)
O3 Li1 Eu1 2_666 2_776 128.14(11)
O2 Li1 Eu1 . 2_776 86.31(10)
O6 Li1 Eu1 2_776 2_776 37.13(9)
O2 Li1 Eu1 2_666 2_776 160.33(10)
Li2 Li1 Eu1 2_666 2_776 124.7(3)
O1 Li1 Eu1 2_666 2_676 160.49(10)
O6 Li1 Eu1 . 2_676 103.47(10)
O5 Li1 Eu1 . 2_676 37.21(9)
O5 Li1 Eu1 2_676 2_676 36.87(9)
O3 Li1 Eu1 2_666 2_676 86.47(10)
O2 Li1 Eu1 . 2_676 128.97(10)
O6 Li1 Eu1 2_776 2_676 71.20(10)
O2 Li1 Eu1 2_666 2_676 100.71(10)
Li2 Li1 Eu1 2_666 2_676 123.8(3)
Eu1 Li1 Eu1 2_776 2_676 86.46(2)
O1 Li1 Eu1 2_666 2_666 70.99(10)
O6 Li1 Eu1 . 2_666 132.65(10)
O5 Li1 Eu1 . 2_666 83.87(9)
O5 Li1 Eu1 2_676 2_666 156.82(9)
O3 Li1 Eu1 2_666 2_666 103.58(11)
O2 Li1 Eu1 . 2_666 37.69(10)
O6 Li1 Eu1 2_776 2_666 102.02(10)
O2 Li1 Eu1 2_666 2_666 37.21(10)
Li2 Li1 Eu1 2_666 2_666 82.2(3)
Eu1 Li1 Eu1 2_776 2_666 123.78(2)
Eu1 Li1 Eu1 2_676 2_666 120.77(2)
O7 Mo1 O1 1_455 . 106.9(2)
O7 Mo1 O2 1_455 1_455 106.3(2)
O1 Mo1 O2 . 1_455 110.91(19)
O7 Mo1 O5 1_455 . 116.72(19)
O1 Mo1 O5 . . 108.58(18)
O2 Mo1 O5 1_455 . 107.45(19)
O7 Mo1 Li3 1_455 1_456 31.81(14)
O1 Mo1 Li3 . 1_456 90.06(14)
O2 Mo1 Li3 1_455 1_456 138.06(13)
O5 Mo1 Li3 . 1_456 98.83(13)
O7 Mo1 Li2 1_455 . 84.1(4)
O1 Mo1 Li2 . . 32.6(4)
O2 Mo1 Li2 1_455 . 141.4(4)
O5 Mo1 Li2 . . 100.0(4)
Li3 Mo1 Li2 1_456 . 59.6(3)
O7 Mo1 Eu1 1_455 1_455 102.85(14)
O1 Mo1 Eu1 . 1_455 141.46(14)
O2 Mo1 Eu1 1_455 1_455 35.65(13)
O5 Mo1 Eu1 . 1_455 78.16(13)
Li3 Mo1 Eu1 1_456 1_455 127.214(19)
Li2 Mo1 Eu1 . 1_455 173.0(3)
O7 Mo1 Eu1 1_455 2_676 94.98(15)
O1 Mo1 Eu1 . 2_676 137.51(14)
O2 Mo1 Eu1 1_455 2_676 96.59(14)
O5 Mo1 Eu1 . 2_676 29.83(12)
Li3 Mo1 Eu1 1_456 2_676 90.23(2)
Li2 Mo1 Eu1 . 2_676 119.9(3)
Eu1 Mo1 Eu1 1_455 2_676 61.28(2)
O7 Mo1 Eu1 1_455 2_666 133.27(15)
O1 Mo1 Eu1 . 2_666 26.58(13)
O2 Mo1 Eu1 1_455 2_666 95.63(13)
O5 Mo1 Eu1 . 2_666 94.11(12)
Li3 Mo1 Eu1 1_456 2_666 114.76(2)
Li2 Mo1 Eu1 . 2_666 55.2(3)
Eu1 Mo1 Eu1 1_455 2_666 118.02(2)
Eu1 Mo1 Eu1 2_676 2_666 123.353(18)
O4 Mo2 O8 . . 107.4(2)
O4 Mo2 O3 . 2_766 108.3(2)
O8 Mo2 O3 . 2_766 106.3(2)
O4 Mo2 O6 . . 112.4(2)
O8 Mo2 O6 . . 111.97(19)
O3 Mo2 O6 2_766 . 110.20(19)
O4 Mo2 Li3 . . 96.73(15)
O8 Mo2 Li3 . . 30.53(14)
O3 Mo2 Li3 2_766 . 83.23(14)
O6 Mo2 Li3 . . 140.59(13)
O4 Mo2 Eu1 . 1_655 140.06(16)
O8 Mo2 Eu1 . 1_655 100.92(14)
O3 Mo2 Eu1 2_766 1_655 35.15(14)
O6 Mo2 Eu1 . 1_655 80.96(13)
Li3 Mo2 Eu1 . 1_655 93.60(2)
O4 Mo2 Eu1 . 2_776 143.13(16)
O8 Mo2 Eu1 . 2_776 90.70(14)
O3 Mo2 Eu1 2_766 2_776 96.42(14)
O6 Mo2 Eu1 . 2_776 31.22(13)
Li3 Mo2 Eu1 . 2_776 113.38(2)
Eu1 Mo2 Eu1 1_655 2_776 61.522(18)
Mo1 O1 Li2 . . 120.3(6)
Mo1 O1 Eu1 . 2_666 133.9(2)
Li2 O1 Eu1 . 2_666 97.0(5)
Mo1 O1 Li1 . 2_666 133.9(2)
Li2 O1 Li1 . 2_666 97.0(5)
Eu1 O1 Li1 2_666 2_666 0.000(12)
Mo1 O2 Li1 1_655 . 118.9(2)
Mo1 O2 Li1 1_655 2_666 134.1(2)
Li1 O2 Li1 . 2_666 105.10(16)
Mo1 O2 Eu1 1_655 2_666 134.1(2)
Li1 O2 Eu1 . 2_666 105.10(16)
Li1 O2 Eu1 2_666 2_666 0.00(2)
Mo2 O3 Li2 2_766 . 143.2(6)
Mo2 O3 Li1 2_766 2_666 119.6(2)
Li2 O3 Li1 . 2_666 96.9(6)
Mo2 O3 Eu1 2_766 2_666 119.6(2)
Li2 O3 Eu1 . 2_666 96.9(6)
Li1 O3 Eu1 2_666 2_666 0.00(3)
Mo2 O4 Li2 . 1_554 135.4(6)
Mo2 O4 Li2 . 2_666 118.2(5)
Li2 O4 Li2 1_554 2_666 103.7(6)
Mo1 O5 Li1 . . 123.90(18)
Mo1 O5 Eu1 . 2_676 128.12(19)
Li1 O5 Eu1 . 2_676 105.91(15)
Mo1 O5 Li1 . 2_676 128.12(19)
Li1 O5 Li1 . 2_676 105.91(15)
Eu1 O5 Li1 2_676 2_676 0.00(2)
Mo2 O6 Li1 . . 125.4(2)
Mo2 O6 Eu1 . 2_776 126.0(2)
Li1 O6 Eu1 . 2_776 104.42(15)
Mo2 O6 Li1 . 2_776 126.0(2)
Li1 O6 Li1 . 2_776 104.42(15)
Eu1 O6 Li1 2_776 2_776 0.000(17)
Mo1 O7 Li3 1_655 1_556 121.6(2)
Mo1 O7 Li2 1_655 . 107.8(5)
Li3 O7 Li2 1_556 . 122.2(5)
Mo2 O8 Li3 . . 122.5(2)
Mo2 O8 Li2 . 2_776 133.5(5)
Li3 O8 Li2 . 2_776 101.5(5)
O4 Li2 O3 1_556 . 119.8(10)
O4 Li2 O1 1_556 . 136.5(10)
O3 Li2 O1 . . 89.5(8)
O4 Li2 O8 1_556 2_776 89.3(8)
O3 Li2 O8 . 2_776 144.5(10)
O1 Li2 O8 . 2_776 80.4(7)
O4 Li2 O7 1_556 . 97.9(8)
O3 Li2 O7 . . 85.3(7)
O1 Li2 O7 . . 117.2(9)
O8 Li2 O7 2_776 . 69.8(5)
O4 Li2 O4 1_556 2_666 76.3(6)
O3 Li2 O4 . 2_666 88.5(7)
O1 Li2 O4 . 2_666 73.0(6)
O8 Li2 O4 2_776 2_666 120.0(8)
O7 Li2 O4 . 2_666 168.0(9)
O4 Li2 Li3 1_556 1_456 64.3(5)
O3 Li2 Li3 . 1_456 174.0(9)
O1 Li2 Li3 . 1_456 84.6(6)
O8 Li2 Li3 2_776 1_456 35.6(3)
O7 Li2 Li3 . 1_456 98.6(6)
O4 Li2 Li3 2_666 1_456 88.4(5)
O4 Li2 Li1 1_556 2_666 156.0(9)
O3 Li2 Li1 . 2_666 45.7(4)
O1 Li2 Li1 . 2_666 44.6(4)
O8 Li2 Li1 2_776 2_666 112.4(7)
O7 Li2 Li1 . 2_666 99.2(6)
O4 Li2 Li1 2_666 2_666 83.6(5)
Li3 Li2 Li1 1_456 2_666 128.7(6)
O4 Li2 Eu1 1_556 2_666 156.0(9)
O3 Li2 Eu1 . 2_666 45.7(4)
O1 Li2 Eu1 . 2_666 44.6(4)
O8 Li2 Eu1 2_776 2_666 112.4(7)
O7 Li2 Eu1 . 2_666 99.2(6)
O4 Li2 Eu1 2_666 2_666 83.6(5)
Li3 Li2 Eu1 1_456 2_666 128.7(6)
Li1 Li2 Eu1 2_666 2_666 0.00(2)
O4 Li2 Mo1 1_556 . 120.3(8)
O3 Li2 Mo1 . . 115.1(8)
O1 Li2 Mo1 . . 27.1(3)
O8 Li2 Mo1 2_776 . 54.5(4)
O7 Li2 Mo1 . . 108.3(6)
O4 Li2 Mo1 2_666 . 83.6(5)
Li3 Li2 Mo1 1_456 . 59.4(3)
Li1 Li2 Mo1 2_666 . 69.4(4)
Eu1 Li2 Mo1 2_666 . 69.4(4)
O8 Li3 O8 2_875 . 180.0000(10)
O8 Li3 O7 2_875 2_876 97.16(17)
O8 Li3 O7 . 2_876 82.84(17)
O8 Li3 O7 2_875 1_554 82.84(17)
O8 Li3 O7 . 1_554 97.16(17)
O7 Li3 O7 2_876 1_554 180.0000(10)
O8 Li3 Mo2 2_875 2_875 26.92(13)
O8 Li3 Mo2 . 2_875 153.08(13)
O7 Li3 Mo2 2_876 2_875 87.08(12)
O7 Li3 Mo2 1_554 2_875 92.92(12)
O8 Li3 Mo2 2_875 . 153.08(13)
O8 Li3 Mo2 . . 26.92(13)
O7 Li3 Mo2 2_876 . 92.92(12)
O7 Li3 Mo2 1_554 . 87.08(12)
Mo2 Li3 Mo2 2_875 . 180.0000(10)
O8 Li3 Mo1 2_875 2_776 123.62(13)
O8 Li3 Mo1 . 2_776 56.38(13)
O7 Li3 Mo1 2_876 2_776 26.59(12)
O7 Li3 Mo1 1_554 2_776 153.41(12)
Mo2 Li3 Mo1 2_875 2_776 109.910(19)
Mo2 Li3 Mo1 . 2_776 70.09(2)
O8 Li3 Mo1 2_875 1_654 56.38(13)
O8 Li3 Mo1 . 1_654 123.62(13)
O7 Li3 Mo1 2_876 1_654 153.41(12)
O7 Li3 Mo1 1_554 1_654 26.59(12)
Mo2 Li3 Mo1 2_875 1_654 70.090(19)
Mo2 Li3 Mo1 . 1_654 109.910(19)
Mo1 Li3 Mo1 2_776 1_654 180.0
O8 Li3 Li2 2_875 2_776 137.1(4)
O8 Li3 Li2 . 2_776 42.9(4)
O7 Li3 Li2 2_876 2_776 81.2(4)
O7 Li3 Li2 1_554 2_776 98.8(4)
Mo2 Li3 Li2 2_875 2_776 110.9(3)
Mo2 Li3 Li2 . 2_776 69.1(3)
Mo1 Li3 Li2 2_776 2_776 61.0(4)
Mo1 Li3 Li2 1_654 2_776 119.0(4)
O8 Li3 Li2 2_875 1_654 42.9(4)
O8 Li3 Li2 . 1_654 137.1(4)
O7 Li3 Li2 2_876 1_654 98.8(4)
O7 Li3 Li2 1_554 1_654 81.2(4)
Mo2 Li3 Li2 2_875 1_654 69.1(3)
Mo2 Li3 Li2 . 1_654 110.9(3)
Mo1 Li3 Li2 2_776 1_654 119.0(4)
Mo1 Li3 Li2 1_654 1_654 61.0(4)
Li2 Li3 Li2 2_776 1_654 180.0000(10)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Li1 O1 2_666 2.368(4)
Li1 O6 . 2.370(4)
Li1 O5 . 2.381(4)
Li1 O5 2_676 2.400(4)
Li1 O3 2_666 2.413(4)
Li1 O2 . 2.437(4)
Li1 O6 2_776 2.442(4)
Li1 O2 2_666 2.465(4)
Li1 Li2 2_666 3.35(2)
Li1 Eu1 2_776 3.8024(13)
Li1 Eu1 2_676 3.8162(9)
Li1 Eu1 2_666 3.8915(10)
Mo1 O7 1_455 1.737(4)
Mo1 O1 . 1.772(4)
Mo1 O2 1_455 1.799(4)
Mo1 O5 . 1.811(4)
Mo1 Li3 1_456 3.3047(10)
Mo1 Li2 . 3.36(2)
Mo1 Eu1 1_455 3.6622(9)
Mo1 Eu1 2_676 3.7953(9)
Mo1 Eu1 2_666 3.8168(8)
Mo2 O4 . 1.731(5)
Mo2 O8 . 1.753(4)
Mo2 O3 2_766 1.786(4)
Mo2 O6 . 1.827(4)
Mo2 Li3 . 3.2648(7)
Mo2 Eu1 1_655 3.6433(9)
Mo2 Eu1 2_776 3.8126(12)
O1 Li2 . 2.10(2)
O1 Eu1 2_666 2.368(4)
O1 Li1 2_666 2.368(4)
O2 Mo1 1_655 1.799(4)
O2 Li1 2_666 2.464(4)
O2 Eu1 2_666 2.464(4)
O3 Mo2 2_766 1.786(4)
O3 Li2 . 2.05(2)
O3 Li1 2_666 2.413(4)
O3 Eu1 2_666 2.413(4)
O4 Li2 1_554 1.96(2)
O4 Li2 2_666 2.63(2)
O5 Eu1 2_676 2.400(4)
O5 Li1 2_676 2.400(4)
O6 Eu1 2_776 2.442(4)
O6 Li1 2_776 2.442(4)
O7 Mo1 1_655 1.737(4)
O7 Li3 1_556 2.045(4)
O7 Li2 . 2.50(2)
O8 Li3 . 1.968(4)
O8 Li2 2_776 2.30(2)
Li2 O4 1_556 1.96(2)
Li2 O8 2_776 2.30(2)
Li2 O4 2_666 2.63(2)
Li2 Li3 1_456 3.314(19)
Li2 Li1 2_666 3.35(2)
Li2 Eu1 2_666 3.35(2)
Li3 O8 2_875 1.968(4)
Li3 O7 2_876 2.045(4)
Li3 O7 1_554 2.045(4)
Li3 Mo2 2_875 3.2648(7)
Li3 Mo1 2_776 3.3046(10)
Li3 Mo1 1_654 3.3046(10)
Li3 Li2 2_776 3.314(19)
Li3 Li2 1_654 3.314(19)
