#------------------------------------------------------------------------------
#$Date: 2016-02-21 02:03:34 +0200 (Sun, 21 Feb 2016) $
#$Revision: 176798 $
#$URL: svn://www.crystallography.net/cod/cif/2/23/52/2235281.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2235281
loop_
_publ_author_name
'Jerbi, Hasna'
'Hidouri, Mourad'
'Mongi, Ben Amara'
_publ_section_title
;
 Na₇Mg₁₃Nd(PO₄)₁₂
;
_journal_coeditor_code           WM2593
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i44
_journal_paper_doi               10.1107/S1600536812017850
_journal_volume                  68
_journal_year                    2012
_chemical_formula_iupac          'Na7 Mg13 Nd (P O4)12'
_chemical_formula_moiety         'Mg13 Na7 Nd O48 P12'
_chemical_formula_sum            'Mg13 Na7 Nd O48 P12'
_chemical_formula_weight         1760.84
_chemical_melting_point          1007
_chemical_name_systematic
;
heptasodium tridecamagnesium neodymium dodecakisphosphate
;
_space_group_IT_number           36
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.301(3)
_cell_length_b                   15.461(4)
_cell_length_c                   23.384(6)
_cell_measurement_reflns_used    44599
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      40
_cell_measurement_theta_min      2.38
_cell_volume                     3724.2(17)
_computing_cell_refinement       'SCALEPACK (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Nonius, 1998)'
_computing_data_reduction
'SCALEPACK and DENZO (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'DIAMOND (Brandenburg, 1998)'
_computing_publication_material  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SIR92 (Altomare et al., 1993)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker--Nonius KappaCCD'
_diffrn_measurement_method       'non-profiled ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.1034
_diffrn_reflns_av_sigmaI/netI    0.1081
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_number            44522
_diffrn_reflns_theta_full        40.00
_diffrn_reflns_theta_max         39.99
_diffrn_reflns_theta_min         3.16
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.378
_exptl_absorpt_correction_T_max  0.878
_exptl_absorpt_correction_T_min  0.716
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   '(Alcock, 1970)'
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    3.140
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       parallelepiped
_exptl_crystal_F_000             3428
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.17
_refine_diff_density_max         2.366
_refine_diff_density_min         -2.231
_refine_ls_abs_structure_details 'Flack (1983), 5847 Friedel pairs'
_refine_ls_abs_structure_Flack   0.257(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.050
_refine_ls_matrix_type           full
_refine_ls_number_parameters     424
_refine_ls_number_reflns         11948
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.050
_refine_ls_R_factor_all          0.1149
_refine_ls_R_factor_gt           0.0568
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0124P)²+42.9558P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0883
_refine_ls_wR_factor_ref         0.1074
_reflns_number_gt                8244
_reflns_number_total             11948
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            wm2593.cif
_cod_data_source_block           I
_cod_database_code               2235281
_cod_database_fobs_code          2235281
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_symmetry_multiplicity
Nd Nd 0.0000 0.54408(2) 0.000015(13) 0.00904(5) Uani d S 1 2
P P1 0.21976(9) 0.43115(7) 0.05989(4) 0.00612(16) Uani d . 1 1
O O11 0.1824(3) 0.3576(2) 0.09995(13) 0.0116(6) Uani d . 1 1
O O12 0.3671(3) 0.4462(2) 0.05621(14) 0.0129(6) Uani d . 1 1
O O13 0.1558(3) 0.41806(18) 0.00077(17) 0.0125(5) Uani d . 1 1
O O14 0.1526(3) 0.5162(2) 0.08102(14) 0.0112(5) Uani d . 1 1
P P2 0.74694(10) 0.46442(7) 0.22216(5) 0.00978(18) Uani d . 1 1
O O21 0.7715(4) 0.5517(2) 0.19519(16) 0.0232(8) Uani d . 1 1
O O22 0.7106(3) 0.4816(2) 0.28494(15) 0.0191(7) Uani d . 1 1
O O23 0.6391(3) 0.4113(2) 0.19233(14) 0.0125(6) Uani d . 1 1
O O24 0.8668(3) 0.4038(2) 0.21746(13) 0.0107(5) Uani d . 1 1
P P3 0.24602(11) 0.70154(7) 0.98592(4) 0.00913(18) Uani d . 1 1
O O31 0.2995(3) 0.6688(2) 0.04252(14) 0.0168(7) Uani d . 1 1
O O32 0.1777(4) 0.6272(2) 0.95352(15) 0.0170(7) Uani d . 1 1
O O33 0.3605(3) 0.7387(2) 0.95155(16) 0.0153(6) Uani d . 1 1
O O34 0.1511(3) 0.7784(2) 0.98766(14) 0.0160(7) Uani d . 1 1
P P4 0.23934(11) 0.72710(8) 0.81954(5) 0.0116(2) Uani d . 1 1
O O41 0.3634(4) 0.6820(3) 0.8390(2) 0.0337(12) Uani d . 1 1
O O42 0.2489(5) 0.7603(3) 0.75815(16) 0.0286(9) Uani d . 1 1
O O43 0.1310(3) 0.6600(2) 0.82915(14) 0.0143(6) Uani d . 1 1
O O44 0.2043(4) 0.8076(2) 0.85537(15) 0.0210(8) Uani d . 1 1
P P5 0.0000 0.72322(10) 0.11586(7) 0.0069(3) Uani d S 1 2
O O51 0.0000 0.6619(3) 0.0654(2) 0.0144(8) Uani d S 1 2
O O52 0.0000 0.8177(3) 0.09809(19) 0.0105(8) Uani d S 1 2
O O53 0.1213(3) 0.7066(2) 0.15281(15) 0.0132(6) Uani d . 1 1
P P6 0.5000 0.64818(10) 0.16991(6) 0.0060(2) Uani d S 1 2
O O61 0.6206(3) 0.7003(2) 0.15437(17) 0.0180(7) Uani d . 1 1
O O62 0.5000 0.5682(3) 0.1316(2) 0.0294(14) Uani d S 1 2
O O63 0.5000 0.6231(4) 0.2330(2) 0.0169(10) Uani d S 1 2
P P7 0.02504(19) 0.55827(15) 0.36368(10) 0.0078(5) Uani d P 0.50 1
O O71 0.0000 0.5300(3) 0.3018(2) 0.0166(9) Uani d S 1 2
O O72X -0.020(3) 0.6490(5) 0.3742(4) 0.037(6) Uani d P 0.50 1
O O73X 0.0621(7) 0.4980(6) 0.3999(3) 0.0252(18) Uani d P 0.50 1
O O74X 0.1652(7) 0.5446(5) 0.3848(3) 0.0177(12) Uiso d P 0.50 1
P P8 0.5147(8) 0.53079(15) 0.39974(9) 0.0120(12) Uani d P 0.50 1
O O81 0.5000 0.5645(4) 0.3388(2) 0.0255(13) Uani d S 1 2
O O82X 0.4470(6) 0.5929(4) 0.4417(3) 0.0130(12) Uani d P 0.50 1
O O83X 0.3373(6) 0.5306(4) 0.4107(3) 0.0141(12) Uani d P 0.50 1
O O84X 0.5429(8) 0.4411(6) 0.4069(4) 0.037(2) Uiso d P 0.50 1
Mg Mg1 0.0000 0.40172(15) 0.28024(9) 0.0100(4) Uani d S 1 2
Mg Mg2 0.5000 0.43819(13) 0.13099(9) 0.0072(4) Uani d S 1 2
Mg Mg3 0.0000 0.85120(14) 0.01707(9) 0.0082(4) Uani d S 1 2
Mg Mg4 0.0000 0.78245(17) 0.39476(10) 0.0115(4) Uani d S 1 2
Mg Mg5 0.76130(15) 0.29805(10) 0.17575(7) 0.0091(3) Uani d . 1 1
Mg Mg6 0.2319(3) 0.63904(12) 0.43096(8) 0.0284(5) Uani d . 1 1
Mg Mg7 0.34561(18) 0.60958(11) 0.28670(8) 0.0187(4) Uani d . 1 1
Mg Mg8 0.24440(18) 0.61726(10) 0.11851(7) 0.0155(3) Uani d . 1 1
Mg Mg 0.2460(2) 0.56877(13) 0.87518(8) 0.0254(5) Uani d P 0.50 1
Na Na 0.2460(2) 0.56877(13) 0.87518(8) 0.0254(5) Uani d P 0.50 1
Na Na1 0.0000 0.0937(2) 0.78091(13) 0.0195(6) Uani d S 1 2
Na Na2 0.0000 0.2634(2) 0.40137(14) 0.0226(7) Uani d S 1 2
Na Na3 0.0000 0.4531(3) 0.14512(14) 0.0235(8) Uani d S 1 2
Na Na4 0.5000 0.4330(2) 0.52265(14) 0.0230(6) Uani d S 1 2
Na Na5 0.5000 0.7765(2) 0.05347(18) 0.0352(9) Uani d S 1 2
Na Na6 0.9685(5) 0.6495(4) 0.2386(2) 0.0455(19) Uani d P 0.50 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nd Nd -0.1943 3.0179 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
O51 Nd O32 . 3_554 83.43(11)
O51 Nd O32 . 1_554 83.43(11)
O32 Nd O32 3_554 1_554 94.83(17)
O51 Nd O14 . 3 69.20(11)
O32 Nd O14 3_554 3 87.56(11)
O32 Nd O14 1_554 3 152.10(10)
O51 Nd O14 . . 69.20(11)
O32 Nd O14 3_554 . 152.10(10)
O32 Nd O14 1_554 . 87.56(11)
O14 Nd O14 3 . 77.97(14)
O51 Nd O73X . 2_564 142.9(2)
O32 Nd O73X 3_554 2_564 62.54(18)
O32 Nd O73X 1_554 2_564 85.0(2)
O14 Nd O73X 3 2_564 120.1(2)
O14 Nd O73X . 2_564 145.25(18)
O51 Nd O73X . 4_564 142.9(2)
O32 Nd O73X 3_554 4_564 85.0(2)
O32 Nd O73X 1_554 4_564 62.54(18)
O14 Nd O73X 3 4_564 145.25(18)
O14 Nd O73X . 4_564 120.1(2)
O51 Nd O13 . 3 125.91(10)
O32 Nd O13 3_554 3 86.19(11)
O32 Nd O13 1_554 3 150.44(11)
O14 Nd O13 3 3 57.41(11)
O14 Nd O13 . 3 105.15(11)
O73X Nd O13 2_564 3 69.2(2)
O73X Nd O13 4_564 3 88.21(19)
O51 Nd O13 . . 125.91(10)
O32 Nd O13 3_554 . 150.44(11)
O32 Nd O13 1_554 . 86.19(11)
O14 Nd O13 3 . 105.15(11)
O14 Nd O13 . . 57.41(11)
O73X Nd O13 2_564 . 88.21(19)
O73X Nd O13 4_564 . 69.2(2)
O13 Nd O13 3 . 78.96(13)
O11 P1 O12 . . 113.35(18)
O11 P1 O13 . . 110.18(18)
O12 P1 O13 . . 112.99(18)
O11 P1 O14 . . 108.76(18)
O12 P1 O14 . . 109.08(18)
O13 P1 O14 . . 101.78(16)
O21 P2 O22 . . 106.5(2)
O21 P2 O23 . . 113.9(2)
O22 P2 O23 . . 110.3(2)
O21 P2 O24 . . 112.1(2)
O22 P2 O24 . . 111.42(19)
O23 P2 O24 . . 102.61(18)
O31 P3 O33 1_556 . 107.5(2)
O31 P3 O34 1_556 . 117.7(2)
O33 P3 O34 . . 102.28(19)
O31 P3 O32 1_556 . 110.1(2)
O33 P3 O32 . . 111.7(2)
O34 P3 O32 . . 107.3(2)
O41 P4 O42 . . 112.4(3)
O41 P4 O43 . . 104.8(2)
O42 P4 O43 . . 114.2(2)
O41 P4 O44 . . 113.7(2)
O42 P4 O44 . . 104.7(2)
O43 P4 O44 . . 107.1(2)
O51 P5 O52 . . 112.9(3)
O51 P5 O53 . 3 109.44(18)
O52 P5 O53 . 3 108.27(17)
O51 P5 O53 . . 109.44(18)
O52 P5 O53 . . 108.27(17)
O53 P5 O53 3 . 108.4(3)
O61 P6 O61 3_655 . 109.1(3)
O61 P6 O62 3_655 . 106.7(2)
O61 P6 O62 . . 106.7(2)
O61 P6 O63 3_655 . 111.39(19)
O61 P6 O63 . . 111.39(19)
O62 P6 O63 . . 111.2(3)
O73X P7 O72X . 3 126.7(7)
O73X P7 O72X . . 130.4(5)
O73X P7 O71 . . 117.0(4)
O72X P7 O71 3 . 115.9(5)
O72X P7 O71 . . 111.7(5)
O72X P7 O74X 3 . 96.5(11)
O72X P7 O74X . . 111.4(10)
O71 P7 O74X . . 114.9(3)
O72X P7 O73X 3 3 118.5(9)
O72X P7 O73X . 3 107.2(9)
O71 P7 O73X . 3 104.3(3)
O74X P7 O73X . 3 106.6(4)
O73X P7 O74X . 3 92.9(4)
O72X P7 O74X 3 3 91.4(11)
O72X P7 O74X . 3 76.0(10)
O71 P7 O74X . 3 92.1(2)
O74X P7 O74X . 3 144.3(5)
O84X P8 O82X . 3_655 121.1(5)
P8 P8 O84X 3_655 3_655 66.9(4)
O82X P8 O84X 3_655 3_655 130.2(5)
O84X P8 O81 . . 117.6(5)
O82X P8 O81 3_655 . 116.1(4)
O84X P8 O81 3_655 . 112.1(5)
O84X P8 O82X . . 128.5(5)
O84X P8 O82X 3_655 . 108.8(6)
O81 P8 O82X . . 109.7(4)
O84X P8 O83X . 3_655 77.2(5)
O82X P8 O83X 3_655 3_655 67.4(4)
O84X P8 O83X 3_655 3_655 111.5(5)
O81 P8 O83X . 3_655 104.7(4)
O82X P8 O83X . 3_655 110.0(4)
O84X P8 O83X . . 100.6(5)
O82X P8 O83X 3_655 . 100.3(4)
O84X P8 O83X 3_655 . 66.1(5)
O81 P8 O83X . . 91.8(4)
O82X P8 O83X . . 57.6(4)
O83X P8 O83X 3_655 . 162.4(5)
O24 Mg1 O24 1_455 3_655 86.12(19)
O24 Mg1 O43 1_455 2_564 87.97(13)
O24 Mg1 O43 3_655 2_564 151.84(19)
O24 Mg1 O43 1_455 4_564 151.84(19)
O24 Mg1 O43 3_655 4_564 87.97(13)
O43 Mg1 O43 2_564 4_564 84.4(2)
O24 Mg1 O71 1_455 . 99.48(16)
O24 Mg1 O71 3_655 . 99.48(16)
O43 Mg1 O71 2_564 . 108.65(16)
O43 Mg1 O71 4_564 . 108.65(16)
O62 Mg2 O52 . 5_545 158.0(2)
O62 Mg2 O23 . . 101.27(16)
O52 Mg2 O23 5_545 . 94.54(15)
O62 Mg2 O23 . 3_655 101.27(16)
O52 Mg2 O23 5_545 3_655 94.54(15)
O23 Mg2 O23 . 3_655 87.7(2)
O62 Mg2 O12 . . 87.15(16)
O52 Mg2 O12 5_545 . 75.59(14)
O23 Mg2 O12 . . 169.17(16)
O23 Mg2 O12 3_655 . 97.46(13)
O62 Mg2 O12 . 3_655 87.15(16)
O52 Mg2 O12 5_545 3_655 75.59(14)
O23 Mg2 O12 . 3_655 97.46(13)
O23 Mg2 O12 3_655 3_655 169.17(16)
O12 Mg2 O12 . 3_655 75.97(18)
O52 Mg3 O82X . 8_464 161.1(2)
O52 Mg3 O82X . 6_564 161.1(2)
O82X Mg3 O82X 8_464 6_564 31.1(4)
O52 Mg3 O34 . 3_554 100.35(15)
O82X Mg3 O34 8_464 3_554 74.8(2)
O82X Mg3 O34 6_564 3_554 98.4(2)
O52 Mg3 O34 . 1_554 100.35(15)
O82X Mg3 O34 8_464 1_554 98.4(2)
O82X Mg3 O34 6_564 1_554 74.8(2)
O34 Mg3 O34 3_554 1_554 99.4(2)
O52 Mg3 O12 . 7 77.01(14)
O82X Mg3 O12 8_464 7 104.0(2)
O82X Mg3 O12 6_564 7 84.9(2)
O34 Mg3 O12 3_554 7 168.63(15)
O34 Mg3 O12 1_554 7 91.93(13)
O52 Mg3 O12 . 5_455 77.01(14)
O82X Mg3 O12 8_464 5_455 84.9(2)
O82X Mg3 O12 6_564 5_455 104.0(2)
O34 Mg3 O12 3_554 5_455 91.93(13)
O34 Mg3 O12 1_554 5_455 168.63(15)
O12 Mg3 O12 7 5_455 76.70(17)
O33 Mg4 O33 8_464 6_564 92.9(2)
O33 Mg4 O41 8_464 8_464 88.36(17)
O33 Mg4 O41 6_564 8_464 173.5(2)
O33 Mg4 O41 8_464 6_564 173.5(2)
O33 Mg4 O41 6_564 6_564 88.36(17)
O41 Mg4 O41 8_464 6_564 89.7(3)
O33 Mg4 O72X 8_464 . 85.5(6)
O33 Mg4 O72X 6_564 . 93.5(6)
O41 Mg4 O72X 8_464 . 93.0(6)
O41 Mg4 O72X 6_564 . 100.8(6)
O33 Mg4 O72X 8_464 3 93.5(6)
O33 Mg4 O72X 6_564 3 85.5(6)
O41 Mg4 O72X 8_464 3 100.8(6)
O41 Mg4 O72X 6_564 3 93.0(6)
O72X Mg4 O72X . 3 11.1(15)
O33 Mg4 O84X 8_464 5_455 102.3(2)
O33 Mg4 O84X 6_564 5_455 87.6(2)
O41 Mg4 O84X 8_464 5_455 85.9(3)
O41 Mg4 O84X 6_564 5_455 71.3(3)
O72X Mg4 O84X . 5_455 172.1(5)
O72X Mg4 O84X 3 5_455 163.0(7)
O33 Mg4 O84X 8_464 7 87.6(2)
O33 Mg4 O84X 6_564 7 102.3(2)
O41 Mg4 O84X 8_464 7 71.3(3)
O41 Mg4 O84X 6_564 7 85.9(3)
O72X Mg4 O84X . 7 163.0(7)
O72X Mg4 O84X 3 7 172.1(5)
O84X Mg4 O84X 5_455 7 20.3(4)
O61 Mg5 O11 7_645 3_655 87.23(15)
O61 Mg5 O53 7_645 5_545 81.09(15)
O11 Mg5 O53 3_655 5_545 105.84(15)
O61 Mg5 O42 7_645 2_664 86.34(19)
O11 Mg5 O42 3_655 2_664 166.46(18)
O53 Mg5 O42 5_545 2_664 84.92(16)
O61 Mg5 O23 7_645 . 174.75(16)
O11 Mg5 O23 3_655 . 87.55(13)
O53 Mg5 O23 5_545 . 100.94(14)
O42 Mg5 O23 2_664 . 98.63(18)
O61 Mg5 O24 7_645 . 111.86(16)
O11 Mg5 O24 3_655 . 84.91(13)
O53 Mg5 O24 5_545 . 163.94(15)
O42 Mg5 O24 2_664 . 86.44(15)
O23 Mg5 O24 . . 67.04(12)
O74X Mg6 O13 . 4_565 89.1(2)
O74X Mg6 O83X . . 56.3(3)
O13 Mg6 O83X 4_565 . 92.0(2)
O74X Mg6 O44 . 6_564 86.4(2)
O13 Mg6 O44 4_565 6_564 174.7(2)
O83X Mg6 O44 . 6_564 87.8(2)
O74X Mg6 O33 . 6_564 128.5(3)
O13 Mg6 O33 4_565 6_564 91.79(15)
O83X Mg6 O33 . 6_564 173.9(2)
O44 Mg6 O33 6_564 6_564 88.92(16)
O74X Mg6 O34 . 6_564 164.9(3)
O13 Mg6 O34 4_565 6_564 88.80(15)
O83X Mg6 O34 . 6_564 108.8(2)
O44 Mg6 O34 6_564 6_564 96.32(17)
O33 Mg6 O34 6_564 6_564 66.49(13)
O74X Mg6 O82X . . 99.5(3)
O13 Mg6 O82X 4_565 . 98.5(2)
O83X Mg6 O82X . . 43.6(2)
O44 Mg6 O82X 6_564 . 85.0(2)
O33 Mg6 O82X 6_564 . 131.0(2)
O34 Mg6 O82X 6_564 . 66.03(19)
O74X Mg6 O72X . 3 57.0(3)
O13 Mg6 O72X 4_565 3 96.6(4)
O83X Mg6 O72X . 3 112.4(3)
O44 Mg6 O72X 6_564 3 78.6(4)
O33 Mg6 O72X 6_564 3 71.9(2)
O34 Mg6 O72X 6_564 3 138.2(2)
O82X Mg6 O72X . 3 151.8(3)
O63 Mg7 O22 . 3_655 107.8(2)
O63 Mg7 O44 . 6_564 126.5(2)
O22 Mg7 O44 3_655 6_564 121.83(17)
O63 Mg7 O81 . . 78.59(17)
O22 Mg7 O81 3_655 . 84.7(2)
O44 Mg7 O81 6_564 . 86.87(19)
O63 Mg7 O42 . 6_564 93.50(19)
O22 Mg7 O42 3_655 6_564 134.79(17)
O44 Mg7 O42 6_564 6_564 66.04(15)
O81 Mg7 O42 . 6_564 139.5(2)
O63 Mg7 O21 . 3_655 83.75(16)
O22 Mg7 O21 3_655 3_655 61.68(13)
O44 Mg7 O21 6_564 3_655 135.69(17)
O81 Mg7 O21 . 3_655 134.72(19)
O42 Mg7 O21 6_564 3_655 82.42(14)
O14 Mg8 O31 . . 93.14(15)
O14 Mg8 O53 . . 113.75(15)
O31 Mg8 O53 . . 104.63(16)
O14 Mg8 O21 . 3_655 87.71(16)
O31 Mg8 O21 . 3_655 167.17(18)
O53 Mg8 O21 . 3_655 86.66(16)
O14 Mg8 O61 . 3_655 165.25(16)
O31 Mg8 O61 . 3_655 85.58(16)
O53 Mg8 O61 . 3_655 80.71(14)
O21 Mg8 O61 3_655 3_655 90.34(17)
O14 Mg8 O62 . . 106.35(15)
O31 Mg8 O62 . . 86.43(16)
O53 Mg8 O62 . . 137.41(16)
O21 Mg8 O62 3_655 . 81.06(17)
O61 Mg8 O62 3_655 . 58.92(15)
O74X Mg O83X 4_565 4_565 57.2(3)
O74X Mg O43 4_565 . 114.5(2)
O83X Mg O43 4_565 . 170.6(3)
O74X Mg O32 4_565 . 98.0(2)
O83X Mg O32 4_565 . 97.0(2)
O43 Mg O32 . . 88.34(15)
O74X Mg O73X 4_565 4_565 36.3(3)
O83X Mg O73X 4_565 4_565 86.3(3)
O43 Mg O73X . 4_565 88.0(3)
O32 Mg O73X . 4_565 72.4(2)
O74X Mg O41 4_565 . 162.5(3)
O83X Mg O41 4_565 . 119.8(2)
O43 Mg O41 . . 66.51(14)
O32 Mg O41 . . 99.53(16)
O73X Mg O41 4_565 . 153.8(3)
O74X Mg O22 4_565 2_665 83.3(2)
O83X Mg O22 4_565 2_665 91.7(2)
O43 Mg O22 . 2_665 82.45(14)
O32 Mg O22 . 2_665 170.34(17)
O73X Mg O22 4_565 2_665 104.3(2)
O41 Mg O22 . 2_665 79.46(16)
O74X Mg O84X 4_565 2_665 107.8(3)
O83X Mg O84X 4_565 2_665 50.7(3)
O43 Mg O84X . 2_665 137.0(3)
O32 Mg O84X . 2_665 93.5(3)
O73X Mg O84X 4_565 2_665 133.4(3)
O41 Mg O84X . 2_665 70.8(3)
O22 Mg O84X 2_665 2_665 95.2(3)
O41 Na1 O41 7_545 5_445 72.3(2)
O41 Na1 O22 7_545 6 140.18(17)
O41 Na1 O22 5_445 6 74.28(14)
O41 Na1 O22 7_545 8_455 74.28(14)
O41 Na1 O22 5_445 8_455 140.18(17)
O22 Na1 O22 6 8_455 123.4(2)
O41 Na1 O23 7_545 6 145.3(2)
O41 Na1 O23 5_445 6 98.65(13)
O22 Na1 O23 6 6 61.06(12)
O22 Na1 O23 8_455 6 121.17(16)
O41 Na1 O23 7_545 8_455 98.65(14)
O41 Na1 O23 5_445 8_455 145.3(2)
O22 Na1 O23 6 8_455 121.17(16)
O22 Na1 O23 8_455 8_455 61.06(12)
O23 Na1 O23 6 8_455 69.34(17)
O41 Na1 O81 7_545 6 102.98(19)
O41 Na1 O81 5_445 6 102.98(19)
O22 Na1 O81 6 6 64.39(11)
O22 Na1 O81 8_455 6 64.39(11)
O23 Na1 O81 6 6 111.76(16)
O23 Na1 O81 8_455 6 111.76(16)
O43 Na2 O43 2_564 4_564 66.40(17)
O43 Na2 O44 2_564 2_564 58.49(12)
O43 Na2 O44 4_564 2_564 111.21(16)
O43 Na2 O44 2_564 4_564 111.21(16)
O43 Na2 O44 4_564 4_564 58.49(12)
O44 Na2 O44 2_564 4_564 107.7(2)
O43 Na2 O34 2_564 2_564 108.65(10)
O43 Na2 O34 4_564 2_564 165.5(2)
O44 Na2 O34 2_564 2_564 74.65(12)
O44 Na2 O34 4_564 2_564 133.75(17)
O43 Na2 O34 2_564 4_564 165.5(2)
O43 Na2 O34 4_564 4_564 108.65(10)
O44 Na2 O34 2_564 4_564 133.75(17)
O44 Na2 O34 4_564 4_564 74.65(12)
O34 Na2 O34 2_564 4_564 72.59(16)
O43 Na2 O32 2_564 4_564 111.67(17)
O43 Na2 O32 4_564 4_564 69.32(12)
O44 Na2 O32 2_564 4_564 166.14(17)
O44 Na2 O32 4_564 4_564 84.56(11)
O34 Na2 O32 2_564 4_564 101.72(15)
O34 Na2 O32 4_564 4_564 54.69(11)
O43 Na2 O32 2_564 2_564 69.32(12)
O43 Na2 O32 4_564 2_564 111.67(17)
O44 Na2 O32 2_564 2_564 84.56(11)
O44 Na2 O32 4_564 2_564 166.14(17)
O34 Na2 O32 2_564 2_564 54.69(11)
O34 Na2 O32 4_564 2_564 101.72(15)
O32 Na2 O32 4_564 2_564 82.55(18)
O43 Na2 O82X 2_564 5_445 124.47(17)
O43 Na2 O82X 4_564 5_445 140.8(2)
O44 Na2 O82X 2_564 5_445 65.98(16)
O44 Na2 O82X 4_564 5_445 84.37(18)
O34 Na2 O82X 2_564 5_445 53.55(16)
O34 Na2 O82X 4_564 5_445 68.42(16)
O32 Na2 O82X 4_564 5_445 122.98(17)
O32 Na2 O82X 2_564 5_445 106.98(16)
O43 Na2 O82X 2_564 7_545 140.8(2)
O43 Na2 O82X 4_564 7_545 124.47(17)
O44 Na2 O82X 2_564 7_545 84.37(18)
O44 Na2 O82X 4_564 7_545 65.98(16)
O34 Na2 O82X 2_564 7_545 68.42(16)
O34 Na2 O82X 4_564 7_545 53.55(16)
O32 Na2 O82X 4_564 7_545 106.98(16)
O32 Na2 O82X 2_564 7_545 122.98(17)
O82X Na2 O82X 5_445 7_545 22.1(3)
O24 Na3 O24 3_655 1_455 72.97(18)
O24 Na3 O14 3_655 3 171.6(2)
O24 Na3 O14 1_455 3 101.77(11)
O24 Na3 O14 3_655 . 101.77(11)
O24 Na3 O14 1_455 . 171.6(2)
O14 Na3 O14 3 . 82.65(18)
O24 Na3 O11 3_655 3 122.51(19)
O24 Na3 O11 1_455 3 71.46(12)
O14 Na3 O11 3 3 60.14(11)
O14 Na3 O11 . 3 116.87(17)
O24 Na3 O11 3_655 . 71.46(12)
O24 Na3 O11 1_455 . 122.51(19)
O14 Na3 O11 3 . 116.87(17)
O14 Na3 O11 . . 60.14(11)
O11 Na3 O11 3 . 91.98(18)
O12 Na4 O12 2_665 4_565 68.10(16)
O12 Na4 O62 2_665 2_665 71.64(14)
O12 Na4 O62 4_565 2_665 71.64(14)
O12 Na4 O31 2_665 4_565 146.90(16)
O12 Na4 O31 4_565 4_565 87.77(11)
O62 Na4 O31 2_665 4_565 79.58(13)
O12 Na4 O31 2_665 2_665 87.77(11)
O12 Na4 O31 4_565 2_665 146.90(16)
O62 Na4 O31 2_665 2_665 79.58(13)
O31 Na4 O31 4_565 2_665 103.03(19)
O12 Na4 O84X 2_665 . 101.0(2)
O12 Na4 O84X 4_565 . 111.8(2)
O62 Na4 O84X 2_665 . 170.47(19)
O31 Na4 O84X 4_565 . 109.1(2)
O31 Na4 O84X 2_665 . 94.3(2)
O12 Na4 O84X 2_665 3_655 111.8(2)
O12 Na4 O84X 4_565 3_655 101.0(2)
O62 Na4 O84X 2_665 3_655 170.47(18)
O31 Na4 O84X 4_565 3_655 94.3(2)
O31 Na4 O84X 2_665 3_655 109.1(2)
O84X Na4 O84X . 3_655 18.5(4)
O11 Na5 O11 5 7 97.14(19)
O11 Na5 O31 5 . 159.2(2)
O11 Na5 O31 7 . 76.89(11)
O11 Na5 O31 5 3_655 76.89(11)
O11 Na5 O31 7 3_655 159.2(2)
O31 Na5 O31 . 3_655 101.6(2)
O11 Na5 O33 5 1_554 147.69(19)
O11 Na5 O33 7 1_554 95.00(11)
O31 Na5 O33 . 1_554 53.08(11)
O31 Na5 O33 3_655 1_554 100.52(15)
O11 Na5 O33 5 3_654 95.00(11)
O11 Na5 O33 7 3_654 147.69(19)
O31 Na5 O33 . 3_654 100.52(15)
O31 Na5 O33 3_655 3_654 53.08(11)
O33 Na5 O33 1_554 3_654 60.72(15)
O11 Na5 O61 5 . 62.08(13)
O11 Na5 O61 7 . 99.82(18)
O31 Na5 O61 . . 98.93(17)
O31 Na5 O61 3_655 . 59.67(13)
O33 Na5 O61 1_554 . 144.13(18)
O33 Na5 O61 3_654 . 112.32(12)
O11 Na5 O61 5 3_655 99.82(18)
O11 Na5 O61 7 3_655 62.08(13)
O31 Na5 O61 . 3_655 59.67(13)
O31 Na5 O61 3_655 3_655 98.93(17)
O33 Na5 O61 1_554 3_655 112.32(12)
O33 Na5 O61 3_654 3_655 144.13(18)
O61 Na5 O61 . 3_655 50.43(16)
O11 Na5 O13 5 7 102.48(15)
O11 Na5 O13 7 7 53.73(12)
O31 Na5 O13 . 7 90.11(11)
O31 Na5 O13 3_655 7 146.76(19)
O33 Na5 O13 1_554 7 62.13(12)
O33 Na5 O13 3_654 7 94.41(16)
O61 Na5 O13 . 7 149.41(17)
O61 Na5 O13 3_655 7 113.70(11)
O11 Na5 O13 5 5 53.73(12)
O11 Na5 O13 7 5 102.48(15)
O31 Na5 O13 . 5 146.76(19)
O31 Na5 O13 3_655 5 90.11(11)
O33 Na5 O13 1_554 5 94.41(16)
O33 Na5 O13 3_654 5 62.13(12)
O61 Na5 O13 . 5 113.70(11)
O61 Na5 O13 3_655 5 149.41(17)
O13 Na5 O13 7 5 65.17(14)
Na6 Na6 O53 3_755 3_655 112.87(15)
Na6 Na6 O71 3_755 1_655 82.19(13)
O53 Na6 O71 3_655 1_655 149.5(3)
Na6 Na6 O42 3_755 8_564 147.02(18)
O53 Na6 O42 3_655 8_564 67.95(17)
O71 Na6 O42 1_655 8_564 114.2(2)
Na6 Na6 O53 3_755 1_655 54.33(13)
O53 Na6 O53 3_655 1_655 58.54(18)
O71 Na6 O53 1_655 1_655 129.4(3)
O42 Na6 O53 8_564 1_655 116.5(2)
Na6 Na6 O21 3_755 . 138.10(16)
O53 Na6 O21 3_655 . 66.58(18)
O71 Na6 O21 1_655 . 84.4(2)
O42 Na6 O21 8_564 . 74.1(2)
O53 Na6 O21 1_655 . 109.8(2)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Nd O51 . 2.379(5)
Nd O32 3_554 2.487(4)
Nd O32 1_554 2.487(4)
Nd O14 3 2.499(3)
Nd O14 . 2.499(3)
Nd O73X 2_564 2.513(7)
Nd O73X 4_564 2.513(7)
Nd O13 3 2.525(3)
Nd O13 . 2.525(3)
Nd P1 3 3.1834(12)
Nd P1 . 3.1834(12)
Nd Na3 . 3.673(3)
P1 O11 . 1.523(3)
P1 O12 . 1.538(3)
P1 O13 . 1.545(4)
P1 O14 . 1.565(3)
P1 Na3 . 3.035(3)
P1 Mg8 . 3.197(2)
P1 Na5 5_445 3.296(3)
O11 Mg5 3_655 2.079(3)
O11 Na5 5_445 2.507(4)
O11 Na3 . 2.613(4)
O12 Mg3 5_545 2.206(4)
O12 Mg2 . 2.224(3)
O12 Na4 2_664 2.445(4)
O13 Mg6 4_564 2.015(4)
O13 Na5 5_445 2.981(5)
O14 Mg8 . 2.026(3)
O14 Na3 . 2.381(4)
P2 O21 . 1.511(4)
P2 O22 . 1.538(4)
P2 O23 . 1.547(4)
P2 O24 . 1.554(3)
P2 Mg5 . 2.796(2)
P2 Mg7 3_655 2.868(2)
P2 Na1 6_554 3.027(2)
P2 Mg1 1_655 3.0952(17)
P2 Na3 1_655 3.174(2)
O21 Mg8 3_655 2.066(4)
O21 Mg7 3_655 2.614(5)
O21 Na6 . 2.727(7)
O22 Mg7 3_655 2.062(4)
O22 Na 2_664 2.293(4)
O22 Mg 2_664 2.293(4)
O22 Na1 6_554 2.464(4)
O23 Mg2 . 2.070(4)
O23 Mg5 . 2.191(4)
O23 Na1 6_554 2.520(4)
O24 Mg1 1_655 2.010(3)
O24 Mg5 . 2.192(4)
O24 Na3 1_655 2.308(4)
P3 O31 1_556 1.521(3)
P3 O33 . 1.538(3)
P3 O34 . 1.540(3)
P3 O32 . 1.546(4)
P3 Mg6 6_565 2.789(2)
P3 Na2 2_565 3.260(2)
P3 Na5 1_556 3.269(3)
P3 Na4 2_665 3.451(2)
O31 P3 1_554 1.521(3)
O31 Mg8 . 2.029(4)
O31 Na4 2_664 2.638(4)
O31 Na5 . 2.665(4)
O32 Mg . 2.160(4)
O32 Nd 1_556 2.487(4)
O32 Na2 2_565 2.775(5)
O33 Mg4 6_565 1.984(4)
O33 Mg6 6_565 2.171(4)
O33 Na5 1_556 2.844(5)
O34 Mg3 1_556 2.040(3)
O34 Mg6 6_565 2.200(4)
O34 Na2 2_565 2.629(4)
P4 O41 . 1.525(4)
P4 O42 . 1.528(4)
P4 O43 . 1.540(4)
P4 O44 . 1.543(4)
P4 Mg . 2.773(2)
P4 Mg7 6_565 2.780(2)
P4 Na2 2_565 3.124(2)
O41 Mg4 6_565 1.995(4)
O41 Mg . 2.289(6)
O41 Na1 5 2.386(5)
O42 Mg5 2_665 2.130(4)
O42 Mg7 6_565 2.332(5)
O42 Na6 8_465 2.696(7)
O43 Mg1 2_565 2.010(4)
O43 Mg . 2.133(4)
O43 Na2 2_565 2.465(4)
O44 Mg6 6_565 2.058(4)
O44 Mg7 6_565 2.117(4)
O44 Na2 2_565 2.606(5)
P5 O51 . 1.513(5)
P5 O52 . 1.519(5)
P5 O53 3 1.541(3)
P5 O53 . 1.541(3)
P5 Mg8 3 3.004(2)
P5 Mg8 . 3.004(2)
P5 Mg3 . 3.042(3)
P5 Na6 3_655 3.106(5)
P5 Na6 1_455 3.106(5)
O52 Mg3 . 1.964(5)
O52 Mg2 5_455 2.015(5)
O53 Mg8 . 2.040(4)
O53 Mg5 5_455 2.089(4)
O53 Na6 3_655 2.380(6)
O53 Na6 1_455 2.699(6)
P6 O61 3_655 1.524(4)
P6 O61 . 1.524(4)
P6 O62 . 1.526(5)
P6 O63 . 1.526(5)
P6 Mg8 . 2.934(2)
P6 Mg8 3_655 2.934(2)
P6 Na5 . 3.369(5)
O61 Mg5 7_655 2.004(4)
O61 Mg8 3_655 2.070(4)
O61 Na5 . 2.915(6)
O62 Mg2 . 2.011(6)
O62 Na4 2_664 2.548(6)
O62 Mg8 . 2.757(3)
O62 Mg8 3_655 2.757(3)
O63 Mg7 3_655 2.037(4)
O63 Mg7 . 2.037(4)
P7 P7 3 0.516(4)
P7 O73X . 1.316(8)
P7 O72X 3 1.424(7)
P7 O72X . 1.497(12)
P7 O71 . 1.534(5)
P7 O74X . 1.540(7)
P7 O73X 3 1.546(7)
P7 O74X 3 2.032(7)
P7 Mg6 . 2.929(3)
P7 Na 4_564 3.018(3)
P7 Mg 4_564 3.018(3)
P7 Mg1 . 3.119(3)
O71 P7 3 1.534(5)
O71 Mg1 . 2.046(5)
O71 Na6 1_455 2.387(7)
O71 Na6 3_655 2.387(7)
O72X O72X 3 0.41(6)
O72X P7 3 1.424(7)
O72X Mg4 . 2.129(8)
O72X Mg6 3 2.56(2)
O73X O73X 3 1.279(14)
O73X O74X . 1.332(11)
O73X P7 3 1.546(7)
O73X Na 4_564 2.233(7)
O73X Mg 4_564 2.233(7)
O73X Nd 2_565 2.513(7)
O74X Mg6 . 1.941(8)
O74X Na 4_564 1.954(8)
O74X Mg 4_564 1.954(8)
O74X P7 3 2.032(7)
P8 P8 3_655 0.304(16)
P8 O84X . 1.426(10)
P8 O82X 3_655 1.428(7)
P8 O84X 3_655 1.517(10)
P8 O81 . 1.525(6)
P8 O82X . 1.540(7)
P8 O83X 3_655 1.546(10)
P8 O83X . 1.846(10)
P8 Na 2_664 2.962(7)
P8 Mg 2_664 2.962(7)
P8 Mg6 3_655 3.185(7)
P8 Na 4_564 3.219(7)
O81 P8 3_655 1.525(6)
O81 Mg7 . 2.121(4)
O81 Mg7 3_655 2.121(4)
O81 Na1 6_554 2.796(7)
O82X O82X 3_655 1.091(13)
O82X P8 3_655 1.428(7)
O82X O83X . 1.652(9)
O82X Mg3 6_565 2.037(6)
O82X Mg6 . 2.342(7)
O82X Na2 5 2.853(8)
O83X P8 3_655 1.546(10)
O83X Na 4_564 1.984(7)
O83X Mg 4_564 1.984(7)
O83X Mg6 . 2.052(7)
O84X O84X 3_655 0.885(17)
O84X P8 3_655 1.517(10)
O84X Na 2_664 2.303(9)
O84X Mg 2_664 2.303(9)
O84X Mg4 5_545 2.509(10)
O84X Na4 . 2.745(10)
Mg1 O24 1_455 2.010(3)
Mg1 O24 3_655 2.010(3)
Mg1 O43 2_564 2.010(4)
Mg1 O43 4_564 2.010(4)
Mg1 P2 1_455 3.0952(17)
Mg1 P2 3_655 3.0952(17)
Mg1 P7 3 3.119(3)
Mg1 Na3 . 3.258(4)
Mg1 Na 4_564 3.400(3)
Mg1 Mg 4_564 3.400(3)
Mg2 O52 5_545 2.015(5)
Mg2 O23 3_655 2.070(4)
Mg2 O12 3_655 2.224(3)
Mg2 Mg3 5_545 2.984(3)
Mg2 Na4 2_664 3.222(4)
Mg2 Na1 6_554 3.540(4)
Mg2 Mg5 3_655 3.610(2)
Mg2 Mg5 . 3.610(2)
Mg3 O82X 8_464 2.037(6)
Mg3 O82X 6_564 2.037(6)
Mg3 O34 3_554 2.040(3)
Mg3 O34 1_554 2.040(3)
Mg3 O12 7 2.206(4)
Mg3 O12 5_455 2.206(4)
Mg3 Mg2 5_455 2.984(3)
Mg3 Na2 2_564 3.234(4)
Mg3 Na4 6_564 3.338(4)
Mg3 Mg6 8_464 3.421(3)
Mg4 O33 8_464 1.984(4)
Mg4 O33 6_564 1.984(4)
Mg4 O41 8_464 1.995(4)
Mg4 O41 6_564 1.995(4)
Mg4 O72X 3 2.129(8)
Mg4 O84X 5_455 2.509(10)
Mg4 O84X 7 2.509(10)
Mg4 Na1 2_564 3.279(4)
Mg4 Mg6 3 3.368(3)
Mg4 Mg6 . 3.368(3)
Mg4 Mg 6_564 3.514(3)
Mg5 O61 7_645 2.004(4)
Mg5 O11 3_655 2.079(3)
Mg5 O53 5_545 2.089(4)
Mg5 O42 2_664 2.130(4)
Mg5 Mg8 5_545 3.104(2)
Mg5 Na3 1_655 3.508(3)
Mg5 Na6 7_645 3.612(5)
Mg5 Na5 5_545 3.786(4)
Mg6 O13 4_565 2.015(4)
Mg6 O44 6_564 2.058(4)
Mg6 O33 6_564 2.171(4)
Mg6 O34 6_564 2.200(4)
Mg6 O72X 3 2.56(2)
Mg6 P3 6_564 2.789(2)
Mg6 P8 3_655 3.185(7)
Mg7 O22 3_655 2.062(4)
Mg7 O44 6_564 2.117(4)
Mg7 O42 6_564 2.332(5)
Mg7 O21 3_655 2.614(5)
Mg7 P4 6_564 2.780(2)
Mg7 P2 3_655 2.868(2)
Mg7 Mg7 3_655 3.181(4)
Mg7 Na6 3_655 3.481(6)
Mg7 Na1 6_554 3.525(4)
Mg7 Mg 4_564 3.597(3)
Mg8 O21 3_655 2.066(4)
Mg8 O61 3_655 2.070(4)
Mg8 Mg5 5_455 3.104(2)
Mg8 Na4 2_664 3.544(3)
Mg8 Na6 3_655 3.598(6)
Mg O74X 4_565 1.954(8)
Mg O83X 4_565 1.984(7)
Mg O73X 4_565 2.233(7)
Mg O22 2_665 2.293(4)
Mg O84X 2_665 2.303(9)
Mg P8 2_665 2.962(7)
Mg P7 4_565 3.018(3)
Mg Mg1 2_565 3.400(3)
Na1 O41 7_545 2.386(5)
Na1 O41 5_445 2.386(5)
Na1 O22 6 2.464(4)
Na1 O22 8_455 2.464(4)
Na1 O23 6 2.520(4)
Na1 O23 8_455 2.520(4)
Na1 O81 6 2.796(7)
Na1 P2 6 3.027(2)
Na1 P2 8_455 3.027(2)
Na1 Mg4 2_565 3.279(4)
Na1 P8 8_455 3.384(4)
Na1 P8 6 3.384(4)
Na2 O43 2_564 2.465(4)
Na2 O43 4_564 2.465(4)
Na2 O44 2_564 2.606(5)
Na2 O44 4_564 2.606(5)
Na2 O34 2_564 2.629(4)
Na2 O34 4_564 2.629(4)
Na2 O32 4_564 2.775(5)
Na2 O32 2_564 2.775(5)
Na2 O82X 5_445 2.853(8)
Na2 O82X 7_545 2.853(8)
Na2 P4 2_564 3.124(2)
Na2 P4 4_564 3.124(2)
Na3 O24 3_655 2.308(4)
Na3 O24 1_455 2.308(4)
Na3 O14 3 2.381(4)
Na3 O11 3 2.613(4)
Na3 P1 3 3.035(3)
Na3 P2 3_655 3.174(2)
Na3 P2 1_455 3.174(2)
Na3 Na5 5_445 3.470(5)
Na4 O12 2_665 2.445(4)
Na4 O12 4_565 2.445(4)
Na4 O62 2_665 2.548(6)
Na4 O31 4_565 2.638(4)
Na4 O31 2_665 2.638(4)
Na4 O84X 3_655 2.745(10)
Na4 Mg2 2_665 3.222(4)
Na4 P8 3_655 3.251(4)
Na4 Na5 2_665 3.319(5)
Na4 Mg3 6_565 3.338(4)
Na5 O11 5 2.507(4)
Na5 O11 7 2.507(4)
Na5 O31 3_655 2.665(4)
Na5 O33 1_554 2.844(5)
Na5 O33 3_654 2.844(5)
Na5 O61 3_655 2.915(6)
Na5 O13 7 2.981(5)
Na5 O13 5 2.981(5)
Na5 P3 1_554 3.269(3)
Na5 P3 3_654 3.269(3)
Na6 Na6 3_755 0.649(11)
Na6 O53 3_655 2.380(6)
Na6 O71 1_655 2.387(7)
Na6 O42 8_564 2.696(7)
Na6 O53 1_655 2.699(6)
Na6 P5 1_655 3.106(5)
Na6 P7 3_655 3.247(5)
Na6 P7 1_655 3.298(5)
Na6 Mg7 3_655 3.481(6)
Na6 Mg8 3_655 3.598(6)
Na6 Mg5 7_655 3.612(5)
