#------------------------------------------------------------------------------
#$Date: 2015-06-14 05:19:47 +0300 (Sun, 14 Jun 2015) $
#$Revision: 139190 $
#$URL: svn://www.crystallography.net/cod/cif/2/24/08/2240822.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2240822
loop_
_publ_author_name
'Gougeon, Patrick'
'Gall, Philippe'
'Salloum, Diala'
_publ_section_title
;
 Crystal structure of Sc~1.91~In~1.39~Mo₁₅Se₁₉, containing Mo₆ and
 Mo₉ clusters
;
_journal_coeditor_code           WM5164
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              760
_journal_page_last               762
_journal_paper_doi               10.1107/S2056989015010634
_journal_volume                  71
_journal_year                    2015
_chemical_formula_iupac          'Sc1.91 In1.39 Mo15 Se19'
_chemical_formula_moiety         'In1.39 Mo15 Sc1.91 Se19'
_chemical_formula_sum            'In1.39 Mo15 Sc1.91 Se19'
_chemical_formula_weight         3185.04
_chemical_name_systematic
;
Scandium indium pentadecamolybdenum nonadecaselenide
;
_space_group_crystal_system      hexagonal
_space_group_IT_number           176
_space_group_name_Hall           '-P 6c'
_space_group_name_H-M_alt        'P 63/m'
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_audit_creation_method           SHELXL-2014/6
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            2
_cell_length_a                   9.7530(2)
_cell_length_b                   9.7530(2)
_cell_length_c                   19.3977(2)
_cell_measurement_temperature    293(2)
_cell_volume                     1597.93(5)
_computing_cell_refinement
;
COLLECT (Nonius, 1998)
;
_computing_data_collection
;
COLLECT (Nonius, 1998)
;
_computing_data_reduction
;
EvalCCD (Duisenberg et al., 2003)
;
_computing_molecular_graphics
;
DIAMOND (Bergerhoff, 1996)
;
_computing_publication_material
;
SHELXL-2014/6 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL-2014/6 (Sheldrick, 2015)
;
_computing_structure_solution
;
SIR97 (Altomare et al., 1999)
;
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       'φ scans (κ = 0) + additional ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0732
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            31413
_diffrn_reflns_theta_full        25.240
_diffrn_reflns_theta_max         34.986
_diffrn_reflns_theta_min         2.411
_exptl_absorpt_coefficient_mu    28.650
_exptl_absorpt_correction_T_max  0.4240
_exptl_absorpt_correction_T_min  0.2788
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
(de Meulenaar & Tompa, 1965)
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    6.620
_exptl_crystal_description       'irregular block'
_exptl_crystal_F_000             2769
_exptl_crystal_size_max          0.063
_exptl_crystal_size_mid          0.054
_exptl_crystal_size_min          0.038
_refine_diff_density_max         2.221
_refine_diff_density_min         -1.965
_refine_ls_extinction_coef       0.00065(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.083
_refine_ls_matrix_type           full
_refine_ls_number_parameters     67
_refine_ls_number_reflns         2414
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.083
_refine_ls_R_factor_all          0.0498
_refine_ls_R_factor_gt           0.0309
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0228P)²+7.5263P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0583
_refine_ls_wR_factor_ref         0.0633
_reflns_number_gt                1847
_reflns_number_total             2414
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            wm5164sup1.cf
_cod_data_source_block           I
_cod_original_cell_volume        1597.93(7)
_cod_database_code               2240822
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number           2014/6
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'-y, x-y, z'
'-x+y, -x, z'
'x-y, x, z+1/2'
'y, -x+y, z+1/2'
'-x, -y, -z'
'x, y, -z-1/2'
'y, -x+y, -z'
'x-y, x, -z'
'-x+y, -x, -z-1/2'
'-y, x-y, -z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
Mo Mo1 0.16732(4) 0.01628(4) 0.55740(2) 0.00813(7) Uani d 1
Mo Mo2 0.68442(4) 0.18633(4) 0.63321(2) 0.00769(7) Uani d 1
Mo Mo3 0.51261(5) 0.16694(5) 0.7500 0.00748(8) Uani d 1
Se Se1 0.03573(5) -0.28735(5) 0.55124(2) 0.01007(8) Uani d 1
Se Se2 0.37937(5) 0.00705(5) 0.64001(2) 0.01114(9) Uani d 1
Se Se3 0.34923(7) 0.30997(7) 0.7500 0.01107(11) Uani d 1
Se Se4 0.0000 0.0000 0.66131(3) 0.01933(16) Uani d 1
Se Se5 0.6667 0.3333 0.52931(3) 0.01116(13) Uani d 1
In In 0.6667 0.3333 0.37124(6) 0.0358(4) Uani d 0.695(3)
Sc Sc -0.2115(2) -0.1745(2) 0.7500 0.0143(5) Uani d 0.638(6)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Sc Sc 0.2519 0.3716 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
In In -0.7276 1.3100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
Se4 Mo1 Se1 . 10_556 176.406(19)
Se4 Mo1 Se1 . . 91.698(13)
Se1 Mo1 Se1 10_556 . 89.030(13)
Se4 Mo1 Se1 . 3 90.788(13)
Se1 Mo1 Se1 10_556 3 88.161(13)
Se1 Mo1 Se1 . 3 174.05(2)
Se4 Mo1 Se2 . . 90.338(16)
Se1 Mo1 Se2 10_556 . 93.220(16)
Se1 Mo1 Se2 . . 86.430(16)
Se1 Mo1 Se2 3 . 98.964(16)
Se4 Mo1 Mo1 . 3 58.012(9)
Se1 Mo1 Mo1 10_556 3 118.654(14)
Se1 Mo1 Mo1 . 3 119.304(17)
Se1 Mo1 Mo1 3 3 57.940(16)
Se2 Mo1 Mo1 . 3 137.271(14)
Se4 Mo1 Mo1 . 4 58.012(9)
Se1 Mo1 Mo1 10_556 4 119.634(13)
Se1 Mo1 Mo1 . 4 59.376(17)
Se1 Mo1 Mo1 3 4 117.870(16)
Se2 Mo1 Mo1 . 4 129.426(16)
Mo1 Mo1 Mo1 3 4 60.0
Se4 Mo1 Mo1 . 10_556 118.212(12)
Se1 Mo1 Mo1 10_556 10_556 58.430(15)
Se1 Mo1 Mo1 . 10_556 117.048(15)
Se1 Mo1 Mo1 3 10_556 57.068(11)
Se2 Mo1 Mo1 . 10_556 140.439(16)
Mo1 Mo1 Mo1 3 10_556 60.224(8)
Mo1 Mo1 Mo1 4 10_556 90.0
Se4 Mo1 Mo1 . 9_556 118.212(12)
Se1 Mo1 Mo1 10_556 9_556 59.423(15)
Se1 Mo1 Mo1 . 9_556 57.499(11)
Se1 Mo1 Mo1 3 9_556 116.606(15)
Se2 Mo1 Mo1 . 9_556 132.232(15)
Mo1 Mo1 Mo1 3 9_556 90.0
Mo1 Mo1 Mo1 4 9_556 60.224(8)
Mo1 Mo1 Mo1 10_556 9_556 59.550(15)
Se5 Mo2 Se2 . . 92.412(13)
Se5 Mo2 Se2 . 3_655 91.604(13)
Se2 Mo2 Se2 . 3_655 174.13(2)
Se5 Mo2 Mo2 . 4_665 58.457(9)
Se2 Mo2 Mo2 . 4_665 60.191(17)
Se2 Mo2 Mo2 3_655 4_665 118.823(16)
Se5 Mo2 Mo2 . 3_655 58.457(9)
Se2 Mo2 Mo2 . 3_655 120.106(17)
Se2 Mo2 Mo2 3_655 3_655 58.906(16)
Mo2 Mo2 Mo2 4_665 3_655 60.0
Se5 Mo2 Se1 . 4_655 90.196(15)
Se2 Mo2 Se1 . 4_655 85.764(16)
Se2 Mo2 Se1 3_655 4_655 98.510(16)
Mo2 Mo2 Se1 4_665 4_655 129.579(16)
Mo2 Mo2 Se1 3_655 4_655 137.688(14)
Se5 Mo2 Se3 . 3_655 175.172(19)
Se2 Mo2 Se3 . 3_655 85.424(18)
Se2 Mo2 Se3 3_655 3_655 90.244(18)
Mo2 Mo2 Se3 4_665 3_655 116.797(15)
Mo2 Mo2 Se3 3_655 3_655 119.114(14)
Se1 Mo2 Se3 4_655 3_655 93.942(17)
Se5 Mo2 Mo3 . 3_655 120.527(17)
Se2 Mo2 Mo3 . 3_655 116.554(16)
Se2 Mo2 Mo3 3_655 3_655 57.619(13)
Mo2 Mo2 Mo3 4_665 3_655 91.213(12)
Mo2 Mo2 Mo3 3_655 3_655 62.083(12)
Se1 Mo2 Mo3 4_655 3_655 138.895(18)
Se3 Mo2 Mo3 3_655 3_655 57.133(16)
Se5 Mo2 Mo3 . . 118.709(16)
Se2 Mo2 Mo3 . . 57.381(13)
Se2 Mo2 Mo3 3_655 . 116.832(16)
Mo2 Mo2 Mo3 4_665 . 60.264(12)
Mo2 Mo2 Mo3 3_655 . 90.162(12)
Se1 Mo2 Mo3 4_655 . 131.676(18)
Se3 Mo2 Mo3 3_655 . 56.533(15)
Mo3 Mo2 Mo3 3_655 . 59.250(17)
Se2 Mo3 Se2 8_557 . 111.71(3)
Se2 Mo3 Se3 8_557 3_655 87.997(16)
Se2 Mo3 Se3 . 3_655 87.997(16)
Se2 Mo3 Se3 8_557 . 93.784(17)
Se2 Mo3 Se3 . . 93.784(17)
Se3 Mo3 Se3 3_655 . 176.82(2)
Se2 Mo3 Mo3 8_557 3_655 117.324(17)
Se2 Mo3 Mo3 . 3_655 117.324(17)
Se3 Mo3 Mo3 3_655 3_655 58.44(2)
Se3 Mo3 Mo3 . 3_655 118.38(2)
Se2 Mo3 Mo3 8_557 4_665 120.613(15)
Se2 Mo3 Mo3 . 4_665 120.614(15)
Se3 Mo3 Mo3 3_655 4_665 118.44(2)
Se3 Mo3 Mo3 . 4_665 58.38(2)
Mo3 Mo3 Mo3 3_655 4_665 60.0
Se2 Mo3 Mo2 8_557 11_667 59.397(12)
Se2 Mo3 Mo2 . 11_667 150.43(2)
Se3 Mo3 Mo2 3_655 11_667 118.002(13)
Se3 Mo3 Mo2 . 11_667 60.986(12)
Mo3 Mo3 Mo2 3_655 11_667 89.795(12)
Mo3 Mo3 Mo2 4_665 11_667 61.256(13)
Se2 Mo3 Mo2 8_557 4_665 150.43(2)
Se2 Mo3 Mo2 . 4_665 59.397(12)
Se3 Mo3 Mo2 3_655 4_665 118.002(13)
Se3 Mo3 Mo2 . 4_665 60.986(12)
Mo3 Mo3 Mo2 3_655 4_665 89.795(12)
Mo3 Mo3 Mo2 4_665 4_665 61.256(13)
Mo2 Mo3 Mo2 11_667 4_665 112.82(2)
Se2 Mo3 Mo2 8_557 . 145.46(2)
Se2 Mo3 Mo2 . . 57.907(12)
Se3 Mo3 Mo2 3_655 . 60.350(12)
Se3 Mo3 Mo2 . . 118.538(13)
Mo3 Mo3 Mo2 3_655 . 59.495(13)
Mo3 Mo3 Mo2 4_665 . 88.794(12)
Mo2 Mo3 Mo2 11_667 . 145.97(2)
Mo2 Mo3 Mo2 4_665 . 57.653(13)
Se2 Mo3 Mo2 8_557 8_557 57.907(12)
Se2 Mo3 Mo2 . 8_557 145.46(2)
Se3 Mo3 Mo2 3_655 8_557 60.349(12)
Se3 Mo3 Mo2 . 8_557 118.538(13)
Mo3 Mo3 Mo2 3_655 8_557 59.495(13)
Mo3 Mo3 Mo2 4_665 8_557 88.794(12)
Mo2 Mo3 Mo2 11_667 8_557 57.654(13)
Mo2 Mo3 Mo2 4_665 8_557 145.97(2)
Mo2 Mo3 Mo2 . 8_557 109.89(2)
Se2 Mo3 Sc 8_557 3 61.629(19)
Se2 Mo3 Sc . 3 61.629(19)
Se3 Mo3 Sc 3_655 3 118.59(5)
Se3 Mo3 Sc . 3 64.60(4)
Mo3 Mo3 Sc 3_655 3 177.02(5)
Mo3 Mo3 Sc 4_665 3 122.98(5)
Mo2 Mo3 Sc 11_667 3 91.85(3)
Mo2 Mo3 Sc 4_665 3 91.85(3)
Mo2 Mo3 Sc . 3 119.536(18)
Mo2 Mo3 Sc 8_557 3 119.536(18)
Mo1 Se1 Mo1 9_556 . 64.071(16)
Mo1 Se1 Mo1 9_556 4 63.509(16)
Mo1 Se1 Mo1 . 4 62.685(17)
Mo1 Se1 Mo2 9_556 3_545 131.401(19)
Mo1 Se1 Mo2 . 3_545 128.246(18)
Mo1 Se1 Mo2 4 3_545 81.335(15)
Mo3 Se2 Mo2 . . 64.712(15)
Mo3 Se2 Mo2 . 4_665 62.984(14)
Mo2 Se2 Mo2 . 4_665 60.903(17)
Mo3 Se2 Mo1 . . 130.17(2)
Mo2 Se2 Mo1 . . 126.687(18)
Mo2 Se2 Mo1 4_665 . 81.187(15)
Mo3 Se2 Sc . 3 64.42(3)
Mo2 Se2 Sc . 3 129.13(3)
Mo2 Se2 Sc 4_665 3 95.44(4)
Mo1 Se2 Sc . 3 87.53(3)
Mo3 Se3 Mo3 4_665 . 63.18(2)
Mo3 Se3 Mo2 4_665 11_667 63.118(13)
Mo3 Se3 Mo2 . 11_667 61.881(13)
Mo3 Se3 Mo2 4_665 4_665 63.118(13)
Mo3 Se3 Mo2 . 4_665 61.881(14)
Mo2 Se3 Mo2 11_667 4_665 114.31(2)
Mo3 Se3 Sc 4_665 4 162.59(5)
Mo3 Se3 Sc . 4 134.23(5)
Mo2 Se3 Sc 11_667 4 121.404(15)
Mo2 Se3 Sc 4_665 4 121.404(15)
Mo3 Se3 Sc 4_665 3 125.62(4)
Mo3 Se3 Sc . 3 62.43(4)
Mo2 Se3 Sc 11_667 3 91.14(2)
Mo2 Se3 Sc 4_665 3 91.14(2)
Sc Se3 Sc 4 3 71.79(8)
Mo1 Se4 Mo1 4 3 63.974(19)
Mo1 Se4 Mo1 4 . 63.975(19)
Mo1 Se4 Mo1 3 . 63.974(19)
Mo1 Se4 Sc 4 4 148.00(4)
Mo1 Se4 Sc 3 4 95.16(3)
Mo1 Se4 Sc . 4 130.64(4)
Mo1 Se4 Sc 4 3 130.64(4)
Mo1 Se4 Sc 3 3 148.00(4)
Mo1 Se4 Sc . 3 95.16(3)
Sc Se4 Sc 4 3 80.06(5)
Mo1 Se4 Sc 4 . 95.16(3)
Mo1 Se4 Sc 3 . 130.64(4)
Mo1 Se4 Sc . . 148.00(4)
Sc Se4 Sc 4 . 80.06(5)
Sc Se4 Sc 3 . 80.06(5)
Mo2 Se5 Mo2 3_655 . 63.086(18)
Mo2 Se5 Mo2 3_655 4_665 63.086(18)
Mo2 Se5 Mo2 . 4_665 63.086(18)
Se4 Sc Se4 8_557 . 84.08(6)
Se4 Sc Se3 8_557 3 88.06(5)
Se4 Sc Se3 . 3 88.06(5)
Se4 Sc Se2 8_557 4 163.50(8)
Se4 Sc Se2 . 4 86.578(17)
Se3 Sc Se2 3 4 105.20(5)
Se4 Sc Se2 8_557 11_557 86.579(17)
Se4 Sc Se2 . 11_557 163.51(8)
Se3 Sc Se2 3 11_557 105.20(5)
Se2 Sc Se2 4 11_557 99.02(6)
Se4 Sc Mo3 8_557 4 120.92(5)
Se4 Sc Mo3 . 4 120.92(5)
Se3 Sc Mo3 3 4 138.83(8)
Se2 Sc Mo3 4 4 53.95(3)
Se2 Sc Mo3 11_557 4 53.95(3)
Se4 Sc Se3 8_557 4 83.19(5)
Se4 Sc Se3 . 4 83.19(5)
Se3 Sc Se3 3 4 168.21(8)
Se2 Sc Se3 4 4 82.23(4)
Se2 Sc Se3 11_557 4 82.23(4)
Mo3 Sc Se3 4 4 52.97(3)
Se4 Sc Sc 8_557 4 49.97(2)
Se4 Sc Sc . 4 49.97(2)
Se3 Sc Sc 3 4 57.39(6)
Se2 Sc Sc 4 4 129.92(3)
Se2 Sc Sc 11_557 4 129.92(3)
Mo3 Sc Sc 4 4 163.78(9)
Se3 Sc Sc 4 4 110.81(7)
Se4 Sc Sc 8_557 3 49.97(2)
Se4 Sc Sc . 3 49.97(2)
Se3 Sc Sc 3 3 117.39(6)
Se2 Sc Sc 4 3 114.00(7)
Se2 Sc Sc 11_557 3 114.00(7)
Mo3 Sc Sc 4 3 103.78(9)
Se3 Sc Sc 4 3 50.81(7)
Sc Sc Sc 4 3 60.0
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Mo1 Se4 . 2.5480(6) y
Mo1 Se1 10_556 2.5488(5) y
Mo1 Se1 . 2.5749(5) y
Mo1 Se1 3 2.6145(5) y
Mo1 Se2 . 2.6531(5) y
Mo1 Mo1 3 2.6995(6) y
Mo1 Mo1 4 2.6995(6) ?
Mo1 Mo1 10_556 2.7179(5) y
Mo1 Mo1 9_556 2.7179(5) ?
Mo2 Se5 . 2.5290(6) y
Mo2 Se2 . 2.5931(5) y
Mo2 Se2 3_655 2.6275(5) y
Mo2 Mo2 4_665 2.6460(6) y
Mo2 Mo2 3_655 2.6460(6) ?
Mo2 Se1 4_655 2.6581(5) y
Mo2 Se3 3_655 2.6965(4) y
Mo2 Mo3 3_655 2.7196(4) y
Mo2 Mo3 . 2.7675(4) y
Mo3 Se2 8_557 2.5780(5) y
Mo3 Se2 . 2.5780(5) y
Mo3 Se3 3_655 2.5884(7) y
Mo3 Se3 . 2.5900(7) y
Mo3 Mo3 3_655 2.7127(8) y
Mo3 Mo3 4_665 2.7127(8) ?
Mo3 Mo2 11_667 2.7196(4) ?
Mo3 Mo2 4_665 2.7196(4) ?
Mo3 Mo2 8_557 2.7675(4) ?
Mo3 Sc 3 2.8760(18) ?
Se1 Mo1 9_556 2.5488(5) ?
Se1 Mo1 4 2.6145(5) ?
Se1 Mo2 3_545 2.6581(5) ?
Se2 Mo2 4_665 2.6275(5) ?
Se2 Sc 3 2.8056(12) ?
Se3 Mo3 4_665 2.5884(7) ?
Se3 Mo2 11_667 2.6966(4) ?
Se3 Mo2 4_665 2.6966(4) ?
Se3 Sc 4 2.696(2) ?
Se3 Sc 3 2.931(2) ?
Se4 Mo1 4 2.5479(6) ?
Se4 Mo1 3 2.5479(6) ?
Se4 Sc 4 2.5691(15) ?
Se4 Sc 3 2.5691(15) ?
Se4 Sc . 2.5691(15) ?
Se5 Mo2 3_655 2.5290(6) ?
Se5 Mo2 4_665 2.5290(6) ?
In Se5 . 3.0662(13) y
In Se2 7_656 3.1273(4) y
In Se2 9_666 3.1273(4) y
In Se2 10_556 3.1273(4) y
In Se1 7_656 3.4912(6) y
In Se1 10_556 3.4912(6) y
In Se1 9_666 3.4912(6) y
In Se3 9_556 4.2657(8) ?
In Se3 10_656 4.2657(8) ?
In Se3 7_666 4.2657(8) ?
In Sc 9_656 4.5565(18) ?
In Sc 7_556 4.5565(18) ?
In Sc 10_666 4.5565(18) ?
Sc Se4 8_557 2.5691(15) y
Sc Se3 3 2.696(2) y
Sc Se2 4 2.8056(12) y
Sc Se2 11_557 2.8056(12) y
Sc Mo3 4 2.8760(18) ?
Sc Se3 4 2.931(2) y
Sc Sc 4 3.305(3) ?
Sc Sc 3 3.305(3) ?
Sc Mo1 11_557 3.7775(4) ?
Sc Mo1 4 3.7775(4) ?
Sc Mo2 3_545 4.0216(15) ?
Sc Mo2 12_547 4.0216(15) ?
Sc Se1 11_557 4.3993(10) ?
Sc Se1 4 4.3993(10) ?
Sc In 7_556 4.5564(18) ?

_cod_database_fobs_code 2240822
