#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/2/30/01/2300196.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2300196
loop_
_publ_author_name
'Fan, Jiandong'
'Zhang, Huaijin'
'Yu, Wentao'
'Yu, Haohai'
'Wang, Jiyang'
'Jiang, Minhua'
_publ_section_title
;
 A Yb³⁺-doped NaY(WO₄)₂ crystal grown by the Czochralski
 technique
;
_journal_coeditor_code           AJ5103
_journal_issue                   3
_journal_name_full               'Journal of Applied Crystallography'
_journal_page_first              584
_journal_page_last               591
_journal_paper_doi               10.1107/S0021889808008649
_journal_volume                  41
_journal_year                    2008
_chemical_formula_moiety         'Na O8 W2 Y0.95 Yb0.05'
_chemical_formula_sum            'Na O8 W2 Y0.95 Yb0.05'
_chemical_formula_weight         611.81
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           88
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-I 4ad'
_symmetry_space_group_name_H-M   'I 41/a :2'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   5.2039(2)
_cell_length_b                   5.2039(2)
_cell_length_c                   11.2838(9)
_cell_measurement_reflns_used    995
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      33.11
_cell_measurement_theta_min      4.31
_cell_volume                     305.57(3)
_computing_cell_refinement       'APEX2 Software Suite (Bruker,2005)'
_computing_data_collection       'APEX2 Software Suite (Bruker,2005)'
_computing_data_reduction        'APEX2 Software Suite (Bruker,2005)'
_computing_molecular_graphics    'SHELXTL (Bruker, 1997)'
_computing_publication_material  'WINGX (Farrugia,1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR97 (Altomare,1999)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type
'Bruker APEX2 CCD area-detector diffractometer'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0436
_diffrn_reflns_av_sigmaI/netI    0.0413
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            1208
_diffrn_reflns_theta_full        33.36
_diffrn_reflns_theta_max         33.36
_diffrn_reflns_theta_min         4.31
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    47.332
_exptl_absorpt_correction_T_max  0.3127
_exptl_absorpt_correction_T_min  0.0324
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'APEX2 Software Suite (Bruker,2005)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    6.649
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             527
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.03
_refine_diff_density_max         2.087
_refine_diff_density_min         -3.038
_refine_ls_extinction_coef       0.038(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.230
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     15
_refine_ls_number_reflns         292
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.230
_refine_ls_R_factor_all          0.0306
_refine_ls_R_factor_gt           0.0279
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0221P)²+2.0193P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0636
_refine_ls_wR_factor_ref         0.0645
_reflns_number_gt                257
_reflns_number_total             292
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            aj5103.cif
_cod_data_source_block           fanjd02
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Tetragonal' changed to 'tetragonal'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Tetragonal' changed to 'tetragonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_Hall     '-I 4ad '
_cod_original_sg_symbol_H-M      'I4(1)/a  '
_cod_database_code               2300196
_cod_database_fobs_code          2300196
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-y+3/4, x+1/4, z+1/4'
'y+3/4, -x+3/4, z+3/4'
'x+1/2, y+1/2, z+1/2'
'-x+1, -y+1/2, z+1'
'-y+5/4, x+3/4, z+3/4'
'y+5/4, -x+5/4, z+5/4'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'y-3/4, -x-1/4, -z-1/4'
'-y-3/4, x-3/4, -z-3/4'
'-x+1/2, -y+1/2, -z+1/2'
'x, y+1/2, -z'
'y-1/4, -x+1/4, -z+1/4'
'-y-1/4, x-1/4, -z-1/4'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W W1 0.5000 1.2500 0.8750 0.0111(2) Uani d S 1 . .
Y Y1 0.0000 0.7500 0.8750 0.0090(4) Uani d SP 0.475 . .
Na Na1 0.0000 0.7500 0.8750 0.0090(4) Uani d SP 0.50 . .
Yb Yb1 0.0000 0.7500 0.8750 0.0090(4) Uani d SP 0.025 . .
O O1 0.3443(7) 1.0072(7) 0.7891(4) 0.0195(7) Uani d . 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 W1 O1 . 16_767 107.10(13) ?
O1 W1 O1 . 11_577 107.10(13) ?
O1 W1 O1 16_767 11_577 114.3(3) ?
O1 W1 O1 . 6_574 114.3(3) ?
O1 W1 O1 16_767 6_574 107.10(13) ?
O1 W1 O1 11_577 6_574 107.10(13) ?
O1 W1 Yb1 . 1_665 145.17(13) ?
O1 W1 Yb1 16_767 1_665 79.66(12) ?
O1 W1 Yb1 11_577 1_665 100.34(12) ?
O1 W1 Yb1 6_574 1_665 34.83(13) ?
O1 W1 Na1 . 1_665 145.17(13) ?
O1 W1 Na1 16_767 1_665 79.66(12) ?
O1 W1 Na1 11_577 1_665 100.34(12) ?
O1 W1 Na1 6_574 1_665 34.83(13) ?
Yb1 W1 Na1 1_665 1_665 0.0 ?
O1 W1 Na1 . 1_655 79.66(12) ?
O1 W1 Na1 16_767 1_655 34.83(13) ?
O1 W1 Na1 11_577 1_655 145.17(13) ?
O1 W1 Na1 6_574 1_655 100.34(12) ?
Yb1 W1 Na1 1_665 1_655 90.0 ?
Na1 W1 Na1 1_665 1_655 90.0 ?
O1 W1 Yb1 . 1_655 79.66(12) ?
O1 W1 Yb1 16_767 1_655 34.83(13) ?
O1 W1 Yb1 11_577 1_655 145.17(13) ?
O1 W1 Yb1 6_574 1_655 100.34(12) ?
Yb1 W1 Yb1 1_665 1_655 90.0 ?
Na1 W1 Yb1 1_665 1_655 90.0 ?
Na1 W1 Yb1 1_655 1_655 0.0 ?
O1 W1 Yb1 . 1_565 100.34(12) ?
O1 W1 Yb1 16_767 1_565 145.17(13) ?
O1 W1 Yb1 11_577 1_565 34.83(13) ?
O1 W1 Yb1 6_574 1_565 79.66(12) ?
Yb1 W1 Yb1 1_665 1_565 90.0 ?
Na1 W1 Yb1 1_665 1_565 90.0 ?
Na1 W1 Yb1 1_655 1_565 180.0 ?
Yb1 W1 Yb1 1_655 1_565 180.0 ?
O1 W1 Na1 . 1_565 100.34(12) ?
O1 W1 Na1 16_767 1_565 145.17(13) ?
O1 W1 Na1 11_577 1_565 34.83(13) ?
O1 W1 Na1 6_574 1_565 79.66(12) ?
Yb1 W1 Na1 1_665 1_565 90.0 ?
Na1 W1 Na1 1_665 1_565 90.0 ?
Na1 W1 Na1 1_655 1_565 180.0 ?
Yb1 W1 Na1 1_655 1_565 180.0 ?
Yb1 W1 Na1 1_565 1_565 0.0 ?
O1 Y1 O1 8_354 13_566 125.70(12) ?
O1 Y1 O1 8_354 10_557 125.70(12) ?
O1 Y1 O1 13_566 10_557 80.4(2) ?
O1 Y1 O1 8_354 3 80.4(2) ?
O1 Y1 O1 13_566 3 125.70(12) ?
O1 Y1 O1 10_557 3 125.70(12) ?
O1 Y1 O1 8_354 6_464 153.25(18) ?
O1 Y1 O1 13_566 6_464 68.83(9) ?
O1 Y1 O1 10_557 6_464 75.74(14) ?
O1 Y1 O1 3 6_464 73.40(8) ?
O1 Y1 O1 8_354 . 73.40(8) ?
O1 Y1 O1 13_566 . 75.74(14) ?
O1 Y1 O1 10_557 . 68.83(9) ?
O1 Y1 O1 3 . 153.25(18) ?
O1 Y1 O1 6_464 . 133.2(2) ?
O1 Y1 O1 8_354 11_567 68.83(9) ?
O1 Y1 O1 13_566 11_567 73.40(8) ?
O1 Y1 O1 10_557 11_567 153.25(18) ?
O1 Y1 O1 3 11_567 75.74(14) ?
O1 Y1 O1 6_464 11_567 99.09(7) ?
O1 Y1 O1 . 11_567 99.09(7) ?
O1 Y1 O1 8_354 16_667 75.74(14) ?
O1 Y1 O1 13_566 16_667 153.25(18) ?
O1 Y1 O1 10_557 16_667 73.40(8) ?
O1 Y1 O1 3 16_667 68.83(9) ?
O1 Y1 O1 6_464 16_667 99.09(7) ?
O1 Y1 O1 . 16_667 99.09(7) ?
O1 Y1 O1 11_567 16_667 133.2(2) ?
O1 Y1 Na1 8_354 13_466 159.36(8) ?
O1 Y1 Na1 13_566 13_466 70.43(9) ?
O1 Y1 Na1 10_557 13_466 37.99(9) ?
O1 Y1 Na1 3 13_466 100.80(10) ?
O1 Y1 Na1 6_464 13_466 37.75(9) ?
O1 Y1 Na1 . 13_466 101.90(10) ?
O1 Y1 Na1 11_567 13_466 131.64(10) ?
O1 Y1 Na1 16_667 13_466 85.41(9) ?
O1 Y1 Na1 8_354 9_577 37.99(9) ?
O1 Y1 Na1 13_566 9_577 159.36(8) ?
O1 Y1 Na1 10_557 9_577 100.80(10) ?
O1 Y1 Na1 3 9_577 70.43(9) ?
O1 Y1 Na1 6_464 9_577 131.64(10) ?
O1 Y1 Na1 . 9_577 85.41(9) ?
O1 Y1 Na1 11_567 9_577 101.90(10) ?
O1 Y1 Na1 16_667 9_577 37.75(9) ?
Na1 Y1 Na1 13_466 9_577 122.705(3) ?
O1 Y1 Y1 8_354 13_466 159.36(8) ?
O1 Y1 Y1 13_566 13_466 70.43(9) ?
O1 Y1 Y1 10_557 13_466 37.99(9) ?
O1 Y1 Y1 3 13_466 100.80(10) ?
O1 Y1 Y1 6_464 13_466 37.75(9) ?
O1 Y1 Y1 . 13_466 101.90(10) ?
O1 Y1 Y1 11_567 13_466 131.64(10) ?
O1 Y1 Y1 16_667 13_466 85.41(9) ?
Na1 Y1 Y1 13_466 13_466 0.0 ?
Na1 Y1 Y1 9_577 13_466 122.705(3) ?
O1 Y1 Yb1 8_354 9_577 37.99(9) ?
O1 Y1 Yb1 13_566 9_577 159.36(8) ?
O1 Y1 Yb1 10_557 9_577 100.80(10) ?
O1 Y1 Yb1 3 9_577 70.43(9) ?
O1 Y1 Yb1 6_464 9_577 131.64(10) ?
O1 Y1 Yb1 . 9_577 85.41(9) ?
O1 Y1 Yb1 11_567 9_577 101.90(10) ?
O1 Y1 Yb1 16_667 9_577 37.75(9) ?
Na1 Y1 Yb1 13_466 9_577 122.705(3) ?
Na1 Y1 Yb1 9_577 9_577 0.0 ?
Y1 Y1 Yb1 13_466 9_577 122.705(3) ?
W1 O1 Yb1 . 13_566 130.77(18) ?
W1 O1 Na1 . 13_566 130.77(18) ?
Yb1 O1 Na1 13_566 13_566 0.0 ?
W1 O1 Y1 . 13_566 130.77(18) ?
Yb1 O1 Y1 13_566 13_566 0.0 ?
Na1 O1 Y1 13_566 13_566 0.0 ?
W1 O1 Y1 . . 120.4(2) ?
Yb1 O1 Y1 13_566 . 104.26(14) ?
Na1 O1 Y1 13_566 . 104.26(14) ?
Y1 O1 Y1 13_566 . 104.26(14) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
W1 O1 . 1.787(4) ?
W1 O1 16_767 1.787(4) ?
W1 O1 11_577 1.787(4) ?
W1 O1 6_574 1.787(4) ?
W1 Yb1 1_665 3.67971(14) ?
W1 Na1 1_665 3.67971(14) ?
W1 Na1 1_655 3.67971(14) ?
W1 Yb1 1_655 3.67971(14) ?
W1 Yb1 1_565 3.67971(14) ?
W1 Na1 1_565 3.67971(14) ?
Y1 O1 8_354 2.424(4) ?
Y1 O1 13_566 2.424(4) ?
Y1 O1 10_557 2.424(4) ?
Y1 O1 3 2.424(4) ?
Y1 O1 6_464 2.437(4) ?
Y1 O1 . 2.437(4) ?
Y1 O1 11_567 2.437(4) ?
Y1 O1 16_667 2.437(4) ?
Y1 Na1 13_466 3.83770(17) ?
Y1 Na1 9_577 3.83769(19) ?
Y1 Y1 13_466 3.83770(17) ?
Y1 Yb1 9_577 3.83769(19) ?
O1 Yb1 13_566 2.424(4) ?
O1 Na1 13_566 2.424(4) ?
O1 Y1 13_566 2.424(4) ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
O1 W1 O1 Yb1 16_767 . . 13_566 -68.56(13) ?
O1 W1 O1 Yb1 11_577 . . 13_566 168.4(3) ?
O1 W1 O1 Yb1 6_574 . . 13_566 49.9(2) ?
Yb1 W1 O1 Yb1 1_665 . . 13_566 27.9(4) ?
Na1 W1 O1 Yb1 1_665 . . 13_566 27.9(4) ?
Na1 W1 O1 Yb1 1_655 . . 13_566 -46.9(2) ?
Yb1 W1 O1 Yb1 1_655 . . 13_566 -46.9(2) ?
Yb1 W1 O1 Yb1 1_565 . . 13_566 133.1(2) ?
Na1 W1 O1 Yb1 1_565 . . 13_566 133.1(2) ?
O1 W1 O1 Na1 16_767 . . 13_566 -68.56(13) ?
O1 W1 O1 Na1 11_577 . . 13_566 168.4(3) ?
O1 W1 O1 Na1 6_574 . . 13_566 49.9(2) ?
Yb1 W1 O1 Na1 1_665 . . 13_566 27.9(4) ?
Na1 W1 O1 Na1 1_665 . . 13_566 27.9(4) ?
Na1 W1 O1 Na1 1_655 . . 13_566 -46.9(2) ?
Yb1 W1 O1 Na1 1_655 . . 13_566 -46.9(2) ?
Yb1 W1 O1 Na1 1_565 . . 13_566 133.1(2) ?
Na1 W1 O1 Na1 1_565 . . 13_566 133.1(2) ?
O1 W1 O1 Y1 16_767 . . 13_566 -68.56(13) ?
O1 W1 O1 Y1 11_577 . . 13_566 168.4(3) ?
O1 W1 O1 Y1 6_574 . . 13_566 49.9(2) ?
Yb1 W1 O1 Y1 1_665 . . 13_566 27.9(4) ?
Na1 W1 O1 Y1 1_665 . . 13_566 27.9(4) ?
Na1 W1 O1 Y1 1_655 . . 13_566 -46.9(2) ?
Yb1 W1 O1 Y1 1_655 . . 13_566 -46.9(2) ?
Yb1 W1 O1 Y1 1_565 . . 13_566 133.1(2) ?
Na1 W1 O1 Y1 1_565 . . 13_566 133.1(2) ?
O1 W1 O1 Y1 16_767 . . . 83.5(3) ?
O1 W1 O1 Y1 11_577 . . . -39.6(2) ?
O1 W1 O1 Y1 6_574 . . . -158.0(3) ?
Yb1 W1 O1 Y1 1_665 . . . 180.0 ?
Na1 W1 O1 Y1 1_665 . . . 180.0 ?
Na1 W1 O1 Y1 1_655 . . . 105.20(19) ?
Yb1 W1 O1 Y1 1_655 . . . 105.20(19) ?
Yb1 W1 O1 Y1 1_565 . . . -74.80(19) ?
Na1 W1 O1 Y1 1_565 . . . -74.80(19) ?
O1 Y1 O1 W1 8_354 . . . -23.8(2) ?
O1 Y1 O1 W1 13_566 . . . -158.5(3) ?
O1 Y1 O1 W1 10_557 . . . 116.45(14) ?
O1 Y1 O1 W1 3 . . . -12.0(4) ?
O1 Y1 O1 W1 6_464 . . . 160.0(2) ?
O1 Y1 O1 W1 11_567 . . . -88.3(3) ?
O1 Y1 O1 W1 16_667 . . . 48.3(2) ?
Na1 Y1 O1 W1 13_466 . . . 135.48(19) ?
Na1 Y1 O1 W1 9_577 . . . 13.00(19) ?
Y1 Y1 O1 W1 13_466 . . . 135.48(19) ?
Yb1 Y1 O1 W1 9_577 . . . 13.00(19) ?
O1 Y1 O1 Yb1 8_354 . . 13_566 134.75(16) ?
O1 Y1 O1 Yb1 13_566 . . 13_566 0.0 ?
O1 Y1 O1 Yb1 10_557 . . 13_566 -85.0(2) ?
O1 Y1 O1 Yb1 3 . . 13_566 146.5(2) ?
O1 Y1 O1 Yb1 6_464 . . 13_566 -41.50(10) ?
O1 Y1 O1 Yb1 11_567 . . 13_566 70.18(5) ?
O1 Y1 O1 Yb1 16_667 . . 13_566 -153.18(17) ?
Na1 Y1 O1 Yb1 13_466 . . 13_566 -66.00(13) ?
Na1 Y1 O1 Yb1 9_577 . . 13_566 171.52(13) ?
Y1 Y1 O1 Yb1 13_466 . . 13_566 -66.00(13) ?
Yb1 Y1 O1 Yb1 9_577 . . 13_566 171.52(13) ?
O1 Y1 O1 Na1 8_354 . . 13_566 134.75(16) ?
O1 Y1 O1 Na1 13_566 . . 13_566 0.0 ?
O1 Y1 O1 Na1 10_557 . . 13_566 -85.0(2) ?
O1 Y1 O1 Na1 3 . . 13_566 146.5(2) ?
O1 Y1 O1 Na1 6_464 . . 13_566 -41.50(10) ?
O1 Y1 O1 Na1 11_567 . . 13_566 70.18(5) ?
O1 Y1 O1 Na1 16_667 . . 13_566 -153.18(17) ?
Na1 Y1 O1 Na1 13_466 . . 13_566 -66.00(13) ?
Na1 Y1 O1 Na1 9_577 . . 13_566 171.52(13) ?
Y1 Y1 O1 Na1 13_466 . . 13_566 -66.00(13) ?
Yb1 Y1 O1 Na1 9_577 . . 13_566 171.52(13) ?
O1 Y1 O1 Y1 8_354 . . 13_566 134.75(16) ?
O1 Y1 O1 Y1 13_566 . . 13_566 0.0 ?
O1 Y1 O1 Y1 10_557 . . 13_566 -85.0(2) ?
O1 Y1 O1 Y1 3 . . 13_566 146.5(2) ?
O1 Y1 O1 Y1 6_464 . . 13_566 -41.50(10) ?
O1 Y1 O1 Y1 11_567 . . 13_566 70.18(5) ?
O1 Y1 O1 Y1 16_667 . . 13_566 -153.18(17) ?
Na1 Y1 O1 Y1 13_466 . . 13_566 -66.00(13) ?
Na1 Y1 O1 Y1 9_577 . . 13_566 171.52(13) ?
Y1 Y1 O1 Y1 13_466 . . 13_566 -66.00(13) ?
Yb1 Y1 O1 Y1 9_577 . . 13_566 171.52(13) ?
