#------------------------------------------------------------------------------
#$Date: 2019-12-26 21:25:21 +0200 (Thu, 26 Dec 2019) $
#$Revision: 246105 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/31/17/2311788.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2311788
loop_
_publ_author_name
'Hejny, C.'
'Bindi, L.'
_publ_section_title
;
 Low-temperature behaviour of
 K₂Sc[Si₂O₆]F: determination of the
 lock-in phase and its relationships with fresnoite- and melilite-type
 compounds.
;
_journal_coeditor_code           DK5057SUP1
_journal_issue                   'Pt 5'
_journal_name_full
'Acta crystallographica Section B, Structural science, crystal engineering and materials'
_journal_page_first              923
_journal_page_last               930
_journal_paper_doi               10.1107/S2052520617010241
_journal_volume                  73
_journal_year                    2017
_chemical_formula_moiety         'F18 K O108 Sc18 Si36, 35(K)'
_chemical_formula_sum            'F18 K36 O108 Sc18 Si36'
_chemical_formula_weight         5298.12
_space_group_crystal_system      monoclinic
_space_group_IT_number           10
_space_group_name_Hall           '-P 2y'
_space_group_name_H-M_alt        'P 1 2/m 1'
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2017-08-09 # Formatted by IUCr publCIF

;
_cell_angle_alpha                90
_cell_angle_beta                 90.000(10)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   26.785(3)
_cell_length_b                   8.2451(16)
_cell_length_c                   26.824(3)
_cell_measurement_reflns_used    589
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      15.4
_cell_measurement_theta_min      4.2
_cell_volume                     5923.9(15)
_computing_cell_refinement       'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_collection       'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction        'CrysAlis (Oxford Diffraction, 2006)'
_computing_molecular_graphics    'DIAMOND (Brandenburg, 2001)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_computing_structure_solution    'SHELXS-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.960
_diffrn_measurement_device_type  'Oxford Xcalibur 3'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.032
_diffrn_reflns_av_unetI/netI     0.0114
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.960
_diffrn_reflns_number            28536
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.960
_diffrn_reflns_theta_full        25.240
_diffrn_reflns_theta_max         27.996
_diffrn_reflns_theta_min         3.042
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    2.751
_exptl_absorpt_correction_T_max  0.995
_exptl_absorpt_correction_T_min  0.994
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(ABSPACK; Oxford Diffraction, 2006)'
_exptl_crystal_colour            white
_exptl_crystal_density_diffrn    2.970
_exptl_crystal_description       block
_exptl_crystal_F_000             5184.0
_exptl_crystal_size_max          0.090
_exptl_crystal_size_mid          0.070
_exptl_crystal_size_min          0.060
_exptl_transmission_factor_max   0.945
_exptl_transmission_factor_min   0.815
_refine_diff_density_max         0.560
_refine_diff_density_min         -0.936
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.281
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1087
_refine_ls_number_reflns         14668
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.281
_refine_ls_R_factor_all          0.0327
_refine_ls_R_factor_gt           0.0312
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0561P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1010
_refine_ls_wR_factor_ref         0.1011
_reflns_Friedel_coverage         0.000
_reflns_number_gt                11412
_reflns_number_total             14668
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            dk5057sup1.cif
_cod_data_source_block           I
_cod_original_cell_volume        5924.1(15)
_cod_original_sg_symbol_H-M      'P 2/m'
_cod_database_code               2311788
_publcif_datablock.id            {9c7527d8-f9a1-4280-9998-e33738fbf57e}
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number           2013-4
_publcif_info_exptl_table_max_cols 4
_publcif_info_exptl_table_use_headnotes n
_publcif_funding_html
;
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'-x, -y, -z'
'x, -y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Sc1 Sc 0.33276(2) 0.24314(7) 0.33406(2) 0.04954(14) Uani 1 1 d . . .
Sc2 Sc 0.33193(2) 0.24652(6) -0.00604(2) 0.04962(13) Uani 1 1 d . . .
Sc3 Sc 0.5000 0.25304(8) 0.5000 0.04947(17) Uani 1 2 d S T P
Sc4 Sc 0.16716(2) 0.24547(7) 0.16561(2) 0.04933(14) Uani 1 1 d . . .
Sc5 Sc -0.00318(2) 0.24673(6) 0.33600(2) 0.04951(13) Uani 1 1 d . . .
Sc6 Sc 0.83156(2) 0.25250(7) 0.16747(2) 0.04943(14) Uani 1 1 d . . .
Sc7 Sc 0.66248(2) 0.24847(7) 0.33258(2) 0.04968(13) Uani 1 1 d . . .
Sc8 Sc 0.49267(2) 0.24808(6) 0.16556(2) 0.04941(13) Uani 1 1 d . . .
Sc9 Sc 0.16771(2) 0.25108(6) 0.50030(2) 0.04947(13) Uani 1 1 d . . .
Sc10 Sc 0.0000 0.24541(8) 0.0000 0.04983(17) Uani 1 2 d S T P
K01 K 0.24789(3) 0.5000 0.07340(3) 0.04923(16) Uani 1 2 d S T P
K02 K 0.12996(3) 0.0000 0.26687(3) 0.04952(16) Uani 1 2 d S T P
K03 K 0.26043(3) 0.0000 0.23265(3) 0.04954(17) Uani 1 2 d S T P
K04 K 0.54706(3) 0.0000 0.37154(3) 0.04931(16) Uani 1 2 d S T P
K05 K 0.55811(3) 0.5000 0.41030(3) 0.04929(16) Uani 1 2 d S T P
K06 K 0.41317(3) 0.0000 0.43913(3) 0.04940(17) Uani 1 2 d S T P
K07 K 0.45529(3) 0.0000 -0.06128(3) 0.04960(16) Uani 1 2 d S T P
K08 K 0.76533(3) 0.0000 0.29798(3) 0.04926(16) Uani 1 2 d S T P
K09 K 0.43597(3) 0.5000 0.27689(3) 0.04931(16) Uani 1 2 d S T P
K10 K 0.07838(3) 0.0000 0.11027(3) 0.04931(16) Uani 1 2 d S T P
K11 K 0.76090(3) 0.5000 0.24768(3) 0.04935(16) Uani 1 2 d S T P
K12 K 0.27077(3) 0.0000 -0.11030(3) 0.04920(16) Uani 1 2 d S T P
K13 K -0.06312(3) 0.0000 0.22527(3) 0.04953(16) Uani 1 2 d S T P
K14 K 0.26497(3) 0.5000 0.20257(3) 0.04952(16) Uani 1 2 d S T P
K15 K 0.06046(3) 0.5000 0.45600(3) 0.04951(16) Uani 1 2 d S T P
K16 K 0.63640(3) 0.5000 0.22019(3) 0.04940(16) Uani 1 2 d S T P
K17 K 0.72552(3) 0.5000 0.10066(3) 0.04919(16) Uani 1 2 d S T P
K18 K 0.40960(3) 0.0000 0.09913(3) 0.04948(17) Uani 1 2 d S T P
K19 K 0.26342(3) 0.5000 0.53422(3) 0.04914(16) Uani 1 2 d S T P
K20 K 0.11950(3) 0.0000 -0.05812(3) 0.04964(16) Uani 1 2 d S T P
K21 K 0.23756(3) 0.0000 0.04343(3) 0.04937(16) Uani 1 2 d S T P
K22 K 0.91452(3) 0.5000 0.08105(3) 0.04939(16) Uani 1 2 d S T P
K23 K 0.10698(3) 0.5000 0.26965(3) 0.04944(16) Uani 1 2 d S T P
K24 K 0.36979(3) 0.5000 0.11832(3) 0.04926(16) Uani 1 2 d S T P
K25 K 0.22813(3) 0.0000 0.37833(3) 0.04927(16) Uani 1 2 d S T P
K26 K 0.08621(3) 0.0000 0.43810(3) 0.04970(16) Uani 1 2 d S T P
K27 K 0.87691(3) 0.5000 0.41728(3) 0.04941(16) Uani 1 2 d S T P
K28 K 0.93857(3) 0.5000 0.21068(3) 0.04949(16) Uani 1 2 d S T P
K29 K 0.60637(3) 0.0000 0.24196(3) 0.04935(16) Uani 1 2 d S T P
K30 K 0.38101(3) 0.5000 0.44235(3) 0.04922(16) Uani 1 2 d S T P
K31 K 0.07198(3) 0.5000 0.13528(3) 0.04937(16) Uani 1 2 d S T P
K32 K 0.74829(3) 0.0000 0.42704(3) 0.04923(16) Uani 1 2 d S T P
K33 K 0.23211(3) 0.5000 0.41080(3) 0.04944(16) Uani 1 2 d S T P
K34 K 0.91118(3) 0.0000 0.37055(3) 0.04977(16) Uani 1 2 d S T P
K35 K 0.45719(3) 0.0000 0.27167(3) 0.04946(16) Uani 1 2 d S T P
K36 K 0.55407(3) 0.5000 0.08534(3) 0.04911(16) Uani 1 2 d S T P
Si1 Si 0.45732(3) 0.30153(8) 0.03888(3) 0.04930(16) Uani 1 1 d . . .
Si2 Si 0.12483(3) 0.30568(8) 0.04663(3) 0.04927(16) Uani 1 1 d . . .
Si3 Si 0.20610(3) 0.30173(8) -0.03991(3) 0.04944(16) Uani 1 1 d . . .
Si4 Si 0.62629(3) 0.19519(8) 0.12657(3) 0.04923(16) Uani 1 1 d . . .
Si5 Si 0.29109(3) 0.19236(8) 0.12440(3) 0.04932(16) Uani 1 1 d . . .
Si6 Si -0.03530(3) 0.20007(8) 0.12629(3) 0.04958(16) Uani 1 1 d . . .
Si7 Si 0.12665(3) 0.30511(8) 0.37291(3) 0.04927(16) Uani 1 1 d . . .
Si8 Si 0.79110(3) 0.30222(8) 0.37661(3) 0.04946(16) Uani 1 1 d . . .
Si9 Si 0.46050(3) 0.30158(8) 0.37548(3) 0.04950(16) Uani 1 1 d . . .
Si10 Si 0.54107(3) 0.31193(8) 0.28697(3) 0.04932(16) Uani 1 1 d . . .
Si11 Si -0.12380(3) 0.30866(8) 0.29442(3) 0.04947(16) Uani 1 1 d . . .
Si12 Si 0.21102(3) 0.30549(8) 0.29238(3) 0.04937(16) Uani 1 1 d . . .
Si13 Si 0.04309(3) 0.19064(8) 0.53547(3) 0.04923(16) Uani 1 1 d . . .
Si14 Si 0.29237(3) 0.19284(8) 0.45638(3) 0.04936(16) Uani 1 1 d . . .
Si15 Si 0.62668(3) 0.20009(8) 0.45422(3) 0.04946(16) Uani 1 1 d . . .
Si16 Si 0.04270(3) 0.19451(8) 0.21352(3) 0.04912(16) Uani 1 1 d . . .
Si17 Si 0.37250(3) 0.18998(8) 0.20660(3) 0.04929(16) Uani 1 1 d . . .
Si18 Si 0.70988(3) 0.19213(8) 0.21019(3) 0.04956(16) Uani 1 1 d . . .
F1 F 0.65234(7) 0.0000 0.32755(7) 0.0494(4) Uani 1 2 d S T P
F2 F 0.17298(7) 0.0000 0.17175(7) 0.0487(5) Uani 1 2 d S T P
F3 F 0.16661(6) 0.5000 0.17349(7) 0.0494(5) Uani 1 2 d S T P
F4 F 0.5000 0.0000 0.5000 0.0486(6) Uani 1 4 d S T P
F5 F -0.01325(7) 0.5000 0.33701(7) 0.0491(4) Uani 1 2 d S T P
F6 F 0.33386(7) 0.5000 0.00561(7) 0.0491(5) Uani 1 2 d S T P
F7 F 0.66791(6) 0.5000 0.33522(6) 0.0488(5) Uani 1 2 d S T P
F8 F 0.32962(7) 0.0000 -0.00962(7) 0.0494(4) Uani 1 2 d S T P
F9 F 0.0000 0.0000 0.0000 0.0487(6) Uani 1 4 d S T P
F10 F 0.48979(7) 0.0000 0.16501(7) 0.0494(4) Uani 1 2 d S T P
F11 F 0.50156(6) 0.5000 0.16966(7) 0.0490(5) Uani 1 2 d S T P
F12 F 0.17119(7) 0.5000 0.49139(7) 0.0488(4) Uani 1 2 d S T P
F13 F 0.33471(6) 0.0000 0.33744(7) 0.0494(5) Uani 1 2 d S T P
F14 F 0.83867(7) 0.0000 0.17161(7) 0.0492(5) Uani 1 2 d S T P
F15 F 0.5000 0.5000 0.5000 0.0497(6) Uani 1 4 d S T P
F16 F 0.00406(7) 0.0000 0.33614(7) 0.0496(5) Uani 1 2 d S T P
F17 F 0.83362(6) 0.5000 0.16359(6) 0.0495(5) Uani 1 2 d S T P
F18 F 0.0000 0.5000 0.0000 0.0487(6) Uani 1 4 d S T P
F19 F 0.33843(7) 0.5000 0.33373(6) 0.0488(5) Uani 1 2 d S T P
F20 F 0.17245(7) 0.0000 0.50214(7) 0.0486(5) Uani 1 2 d S T P
O1 O 0.37182(9) 0.0000 0.20490(9) 0.0490(5) Uani 1 2 d S T P
O2 O -0.12578(9) 0.5000 0.30103(9) 0.0506(6) Uani 1 2 d S T P
O3 O 0.66061(6) 0.2627(2) 0.17228(6) 0.0493(4) Uani 1 1 d . . .
O4 O 0.57023(7) 0.24113(18) 0.14451(7) 0.0491(4) Uani 1 1 d . . .
O5 O 0.28582(9) 0.0000 0.13342(9) 0.0497(5) Uani 1 2 d S T P
O6 O -0.03165(7) 0.25906(18) 0.40765(7) 0.0488(4) Uani 1 1 d . . .
O7 O 0.5000 0.2291(3) 0.0000 0.0500(6) Uani 1 2 d S T P
O8 O 0.63403(9) 0.0000 0.12470(9) 0.0494(5) Uani 1 2 d S T P
O9 O 0.47163(7) 0.23975(18) 0.42811(7) 0.0493(4) Uani 1 1 d . . .
O10 O 0.83302(6) 0.2350(2) 0.33760(6) 0.0500(5) Uani 1 1 d . . .
O11 O 0.13632(9) 0.5000 0.37915(8) 0.0487(5) Uani 1 2 d S T P
O12 O 0.33142(6) 0.2681(2) 0.50591(6) 0.0499(4) Uani 1 1 d . . .
O13 O 0.00718(6) 0.2442(2) 0.16547(6) 0.0501(4) Uani 1 1 d . . .
O14 O 0.80169(9) 0.5000 0.04371(9) 0.0497(5) Uani 1 2 d S T P
O15 O 0.81988(6) 0.23900(18) 0.09039(6) 0.0492(4) Uani 1 1 d . . .
O16 O 0.21410(9) 0.5000 0.63299(9) 0.0490(5) Uani 1 2 d S T P
O17 O 0.50981(7) 0.2401(2) 0.33789(6) 0.0489(4) Uani 1 1 d . . .
O18 O 0.10052(6) 0.24108(18) 0.20107(6) 0.0492(4) Uani 1 1 d . . .
O19 O 0.03974(9) 0.0000 0.21241(9) 0.0492(5) Uani 1 2 d S T P
O20 O 0.46379(9) 0.5000 0.37064(9) 0.0495(5) Uani 1 2 d S T P
O21 O -0.07687(7) 0.22912(18) 0.30972(6) 0.0489(4) Uani 1 1 d . . .
O22 O 0.0000 0.2446(3) 0.5000 0.0483(6) Uani 1 2 d S T P
O23 O 0.70031(7) 0.24814(18) 0.26138(7) 0.0496(4) Uani 1 1 d . . .
O24 O 0.85232(6) 0.27095(17) 0.24244(7) 0.0490(4) Uani 1 1 d . . .
O25 O 0.35094(6) 0.23807(18) 0.26008(6) 0.0484(4) Uani 1 1 d . . .
O26 O 0.16177(6) 0.2340(2) 0.32890(6) 0.0495(4) Uani 1 1 d . . .
O27 O 0.17026(6) 0.2209(2) 0.00873(6) 0.0495(4) Uani 1 1 d . . .
O28 O 0.53196(9) 0.5000 0.28817(9) 0.0497(5) Uani 1 2 d S T P
O29 O 0.45609(9) 0.5000 0.03018(9) 0.0496(5) Uani 1 2 d S T P
O30 O -0.03646(9) 0.0000 0.13172(9) 0.0499(6) Uani 1 2 d S T P
O31 O 0.26215(6) 0.23221(18) -0.03059(6) 0.0488(4) Uani 1 1 d . . .
O32 O 0.41109(6) 0.23917(18) 0.34806(6) 0.0488(4) Uani 1 1 d . . .
O33 O 0.04614(8) 0.0000 0.53484(9) 0.0497(5) Uani 1 2 d S T P
O34 O 0.75862(7) 0.24906(18) 0.18039(6) 0.0493(4) Uani 1 1 d . . .
O35 O 0.09639(7) 0.26608(18) 0.51899(6) 0.0487(4) Uani 1 1 d . . .
O36 O 0.30795(6) 0.23709(18) 0.06985(7) 0.0487(4) Uani 1 1 d . . .
O37 O 0.40519(6) 0.22317(18) 0.01963(6) 0.0495(4) Uani 1 1 d . . .
O38 O 0.14446(6) 0.22112(18) 0.42305(7) 0.0490(4) Uani 1 1 d . . .
O39 O 0.63530(7) 0.24507(18) 0.40110(7) 0.0492(4) Uani 1 1 d . . .
O40 O 0.13595(6) 0.23899(18) 0.10017(7) 0.0489(4) Uani 1 1 d . . .
O41 O 0.23944(7) 0.27586(18) 0.14034(6) 0.0484(4) Uani 1 1 d . . .
O42 O 0.20342(6) 0.23810(18) 0.24021(7) 0.0486(4) Uani 1 1 d . . .
O43 O 0.30367(9) 0.0000 0.45849(9) 0.0492(5) Uani 1 2 d S T P
O44 O 0.20962(9) 0.5000 0.29673(9) 0.0504(6) Uani 1 2 d S T P
O45 O 0.59747(7) 0.24383(18) 0.29930(6) 0.0490(4) Uani 1 1 d . . .
O46 O 0.25954(6) 0.21600(17) 0.32197(6) 0.0490(4) Uani 1 1 d . . .
O47 O 0.73792(7) 0.23208(18) 0.36232(7) 0.0489(4) Uani 1 1 d . . .
O48 O 0.47250(7) 0.25702(18) 0.09387(7) 0.0487(4) Uani 1 1 d . . .
O49 O 0.07476(7) 0.23402(18) 0.02121(6) 0.0491(4) Uani 1 1 d . . .
O50 O 0.33178(6) 0.2643(2) 0.16366(6) 0.0496(5) Uani 1 1 d . . .
O51 O 0.70536(9) 0.0000 0.20692(9) 0.0501(6) Uani 1 2 d S T P
O52 O -0.08933(6) 0.27594(18) 0.15068(6) 0.0495(4) Uani 1 1 d . . .
O53 O 0.24347(6) 0.23112(18) 0.47165(6) 0.0492(4) Uani 1 1 d . . .
O54 O 0.57157(7) 0.26705(18) 0.47694(6) 0.0486(4) Uani 1 1 d . . .
O55 O 0.12564(9) 0.5000 0.03704(9) 0.0498(5) Uani 1 2 d S T P
O57 O 0.32084(6) 0.26823(18) 0.40997(7) 0.0501(4) Uani 1 1 d . . .
O58 O 0.06942(6) 0.26880(17) 0.36179(6) 0.0489(4) Uani 1 1 d . . .
O59 O 0.02163(6) 0.27077(18) 0.26306(7) 0.0490(4) Uani 1 1 d . . .
O60 O 0.64105(6) 0.27398(18) 0.07643(7) 0.0488(4) Uani 1 1 d . . .
O61 O 0.52008(6) 0.22641(18) 0.24008(7) 0.0493(4) Uani 1 1 d . . .
O62 O -0.02386(6) 0.26710(18) 0.07267(7) 0.0494(4) Uani 1 1 d . . .
O63 O 0.80691(6) 0.26891(18) 0.43153(6) 0.0489(4) Uani 1 1 d . . .
O64 O 0.62484(9) 0.0000 0.46178(9) 0.0488(5) Uani 1 2 d S T P
O65 O 0.42541(7) 0.27393(18) 0.19176(6) 0.0488(4) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sc Sc 0.2519 0.3716 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O46 Sc1 F13 85.47(7) . .
O46 Sc1 O25 94.24(7) . .
F13 Sc1 O25 90.99(7) . .
O46 Sc1 O57 91.10(7) . .
F13 Sc1 O57 93.39(7) . .
O25 Sc1 O57 173.34(7) . .
O46 Sc1 F19 100.43(7) . .
F13 Sc1 F19 173.93(7) . .
O25 Sc1 F19 89.97(6) . .
O57 Sc1 F19 85.15(6) . .
O46 Sc1 O32 172.65(7) . .
F13 Sc1 O32 87.20(6) . .
O25 Sc1 O32 86.35(7) . .
O57 Sc1 O32 88.86(7) . .
F19 Sc1 O32 86.89(6) . .
O46 Sc1 K25 40.30(5) . .
F13 Sc1 K25 57.04(5) . .
O25 Sc1 K25 119.23(5) . .
O57 Sc1 K25 67.42(5) . .
F19 Sc1 K25 127.22(5) . .
O32 Sc1 K25 133.70(5) . .
O46 Sc1 K09 135.18(5) . .
F13 Sc1 K09 123.72(5) . .
O25 Sc1 K09 56.43(5) . .
O57 Sc1 K09 116.91(5) . .
F19 Sc1 K09 52.50(5) . .
O32 Sc1 K09 50.54(5) . .
K25 Sc1 K09 174.94(2) . .
O46 Sc1 K30 121.12(5) . .
F13 Sc1 K30 120.69(5) . .
O25 Sc1 K30 132.00(5) . .
O57 Sc1 K30 41.35(5) . .
F19 Sc1 K30 54.97(5) . .
O32 Sc1 K30 62.71(5) . .
K25 Sc1 K30 108.50(2) . .
K09 Sc1 K30 75.648(19) . .
O46 Sc1 K03 48.82(5) . .
F13 Sc1 K03 62.00(5) . .
O25 Sc1 K03 55.24(5) . .
O57 Sc1 K03 131.38(5) . .
F19 Sc1 K03 123.10(5) . .
O32 Sc1 K03 127.21(5) . .
K25 Sc1 K03 64.022(19) . .
K09 Sc1 K03 111.50(2) . .
K30 Sc1 K03 169.94(2) . .
O46 Sc1 K33 58.78(5) . .
F13 Sc1 K33 121.54(5) . .
O25 Sc1 K33 132.17(5) . .
O57 Sc1 K33 48.48(5) . .
F19 Sc1 K33 61.45(5) . .
O32 Sc1 K33 125.52(5) . .
K25 Sc1 K33 66.741(17) . .
K09 Sc1 K33 113.74(2) . .
K30 Sc1 K33 62.808(18) . .
K03 Sc1 K33 107.259(19) . .
O46 Sc1 K06 125.12(5) . .
F13 Sc1 K06 57.56(5) . .
O25 Sc1 K06 122.39(5) . .
O57 Sc1 K06 56.68(5) . .
F19 Sc1 K06 117.11(5) . .
O32 Sc1 K06 49.48(5) . .
K25 Sc1 K06 84.860(19) . .
K09 Sc1 K06 99.706(19) . .
K30 Sc1 K06 64.403(16) . .
K03 Sc1 K06 119.52(2) . .
K33 Sc1 K06 105.119(19) . .
O31 Sc2 O60 91.92(7) . 2_655
O31 Sc2 F8 84.05(7) . .
O60 Sc2 F8 94.48(7) 2_655 .
O31 Sc2 O37 171.30(7) . .
O60 Sc2 O37 88.97(7) 2_655 .
F8 Sc2 O37 87.26(7) . .
O31 Sc2 F6 97.52(7) . .
O60 Sc2 F6 91.06(7) 2_655 .
F8 Sc2 F6 174.19(8) . .
O37 Sc2 F6 91.11(7) . .
O31 Sc2 O36 91.77(7) . .
O60 Sc2 O36 174.49(7) 2_655 .
F8 Sc2 O36 89.97(7) . .
O37 Sc2 O36 88.00(7) . .
F6 Sc2 O36 84.40(7) . .
O31 Sc2 K21 53.99(5) . .
O60 Sc2 K21 132.25(5) 2_655 .
F8 Sc2 K21 54.33(5) . .
O37 Sc2 K21 119.96(5) . .
F6 Sc2 K21 122.35(5) . .
O36 Sc2 K21 53.21(5) . .
O31 Sc2 K17 53.35(5) . 3_665
O60 Sc2 K17 55.80(5) 2_655 3_665
F8 Sc2 K17 121.93(6) . 3_665
O37 Sc2 K17 132.99(5) . 3_665
F6 Sc2 K17 62.91(5) . 3_665
O36 Sc2 K17 124.04(5) . 3_665
K21 Sc2 K17 107.03(2) . 3_665
O31 Sc2 K01 69.84(5) . .
O60 Sc2 K01 132.91(5) 2_655 .
F8 Sc2 K01 124.52(6) . .
O37 Sc2 K01 115.43(5) . .
F6 Sc2 K01 51.52(5) . .
O36 Sc2 K01 45.26(4) . .
K21 Sc2 K01 70.980(18) . .
K17 Sc2 K01 79.711(19) 3_665 .
O31 Sc2 K12 47.37(5) . .
O60 Sc2 K12 62.16(5) 2_655 .
F8 Sc2 K12 54.69(6) . .
O37 Sc2 K12 126.47(5) . .
F6 Sc2 K12 130.08(5) . .
O36 Sc2 K12 123.27(5) . .
K21 Sc2 K12 70.111(19) . .
K17 Sc2 K12 67.246(17) 3_665 .
K01 Sc2 K12 117.12(2) . .
O31 Sc2 K18 133.20(5) . .
O60 Sc2 K18 121.29(5) 2_655 .
F8 Sc2 K18 63.11(6) . .
O37 Sc2 K18 40.69(5) . .
F6 Sc2 K18 112.36(5) . .
O36 Sc2 K18 58.17(5) . .
K21 Sc2 K18 79.39(2) . .
K17 Sc2 K18 173.336(19) 3_665 .
K01 Sc2 K18 101.12(2) . .
K12 Sc2 K18 117.536(19) . .
O31 Sc2 K24 122.53(5) . .
O60 Sc2 K24 128.00(5) 2_655 .
F8 Sc2 K24 124.03(6) . .
O37 Sc2 K24 62.77(5) . .
F6 Sc2 K24 50.52(5) . .
O36 Sc2 K24 46.50(4) . .
K21 Sc2 K24 99.64(2) . .
K17 Sc2 K24 112.551(19) 3_665 .
K01 Sc2 K24 52.775(18) . .
K12 Sc2 K24 168.48(2) . .
K18 Sc2 K24 63.800(16) . .
O54 Sc3 O54 173.44(9) . 2_656
O54 Sc3 F15 86.72(5) . .
O54 Sc3 F15 86.72(5) 2_656 .
O54 Sc3 O9 86.56(7) . 2_656
O54 Sc3 O9 93.79(7) 2_656 2_656
F15 Sc3 O9 93.03(5) . 2_656
O54 Sc3 O9 93.79(7) . .
O54 Sc3 O9 86.56(7) 2_656 .
F15 Sc3 O9 93.03(5) . .
O9 Sc3 O9 173.95(9) 2_656 .
O54 Sc3 F4 93.28(5) . .
O54 Sc3 F4 93.28(5) 2_656 .
F15 Sc3 F4 180.0 . .
O9 Sc3 F4 86.97(5) 2_656 .
O9 Sc3 F4 86.97(5) . .
O54 Sc3 K05 126.68(5) . 3_666
O54 Sc3 K05 48.42(5) 2_656 3_666
F15 Sc3 K05 54.603(13) . 3_666
O9 Sc3 K05 63.69(5) 2_656 3_666
O9 Sc3 K05 120.29(5) . 3_666
F4 Sc3 K05 125.397(13) . 3_666
O54 Sc3 K05 48.42(5) . .
O54 Sc3 K05 126.68(5) 2_656 .
F15 Sc3 K05 54.604(13) . .
O9 Sc3 K05 120.29(5) 2_656 .
O9 Sc3 K05 63.69(5) . .
F4 Sc3 K05 125.396(13) . .
K05 Sc3 K05 109.21(3) 3_666 .
O54 Sc3 K06 121.25(5) . .
O54 Sc3 K06 63.19(5) 2_656 .
F15 Sc3 K06 126.285(13) . .
O9 Sc3 K06 129.84(5) 2_656 .
O9 Sc3 K06 45.32(5) . .
F4 Sc3 K06 53.715(13) . .
K05 Sc3 K06 111.574(18) 3_666 .
K05 Sc3 K06 108.534(18) . .
O54 Sc3 K06 63.19(5) . 3_656
O54 Sc3 K06 121.25(5) 2_656 3_656
F15 Sc3 K06 126.285(13) . 3_656
O9 Sc3 K06 45.32(5) 2_656 3_656
O9 Sc3 K06 129.84(5) . 3_656
F4 Sc3 K06 53.715(13) . 3_656
K05 Sc3 K06 108.534(18) 3_666 3_656
K05 Sc3 K06 111.576(18) . 3_656
K06 Sc3 K06 107.43(3) . 3_656
O54 Sc3 K30 126.63(5) . .
O54 Sc3 K30 49.18(5) 2_656 .
F15 Sc3 K30 60.111(11) . .
O9 Sc3 K30 131.57(5) 2_656 .
O9 Sc3 K30 52.35(5) . .
F4 Sc3 K30 119.889(11) . .
K05 Sc3 K30 67.977(18) 3_666 .
K05 Sc3 K30 78.326(19) . .
K06 Sc3 K30 66.735(15) . .
K06 Sc3 K30 170.000(17) 3_656 .
O54 Sc3 K30 49.18(5) . 3_666
O54 Sc3 K30 126.63(5) 2_656 3_666
F15 Sc3 K30 60.111(11) . 3_666
O9 Sc3 K30 52.35(5) 2_656 3_666
O9 Sc3 K30 131.57(5) . 3_666
F4 Sc3 K30 119.889(11) . 3_666
K05 Sc3 K30 78.327(19) 3_666 3_666
K05 Sc3 K30 67.980(18) . 3_666
K06 Sc3 K30 170.001(17) . 3_666
K06 Sc3 K30 66.734(15) 3_656 3_666
K30 Sc3 K30 120.22(2) . 3_666
O40 Sc4 O18 92.56(7) . .
O40 Sc4 F2 94.50(7) . .
O18 Sc4 F2 90.67(7) . .
O40 Sc4 O41 96.31(7) . .
O18 Sc4 O41 169.44(7) . .
F2 Sc4 O41 94.32(7) . .
O40 Sc4 F3 96.59(7) . .
O18 Sc4 F3 87.97(7) . .
F2 Sc4 F3 168.87(8) . .
O41 Sc4 F3 85.34(6) . .
O40 Sc4 O42 176.83(7) . .
O18 Sc4 O42 87.82(7) . .
F2 Sc4 O42 82.34(7) . .
O41 Sc4 O42 83.64(7) . .
F3 Sc4 O42 86.57(6) . .
O40 Sc4 K31 58.59(5) . .
O18 Sc4 K31 57.46(5) . .
F2 Sc4 K31 133.63(5) . .
O41 Sc4 K31 123.30(5) . .
F3 Sc4 K31 53.47(5) . .
O42 Sc4 K31 124.01(5) . .
O40 Sc4 K10 45.64(5) . .
O18 Sc4 K10 65.45(5) . .
F2 Sc4 K10 60.37(5) . .
O41 Sc4 K10 125.06(5) . .
F3 Sc4 K10 128.36(5) . .
O42 Sc4 K10 132.10(5) . .
K31 Sc4 K10 75.104(19) . .
O40 Sc4 K14 126.43(5) . .
O18 Sc4 K14 122.55(5) . .
F2 Sc4 K14 121.04(6) . .
O41 Sc4 K14 47.08(5) . .
F3 Sc4 K14 51.70(5) . .
O42 Sc4 K14 55.59(4) . .
K31 Sc4 K14 105.00(2) . .
K10 Sc4 K14 170.89(2) . .
O40 Sc4 K02 123.87(5) . .
O18 Sc4 K02 51.62(5) . .
F2 Sc4 K02 52.39(5) . .
O41 Sc4 K02 125.89(5) . .
F3 Sc4 K02 119.43(6) . .
O42 Sc4 K02 54.25(4) . .
K31 Sc4 K02 109.04(2) . .
K10 Sc4 K02 78.50(2) . .
K14 Sc4 K02 109.69(2) . .
O40 Sc4 K03 135.80(5) . .
O18 Sc4 K03 111.04(5) . .
F2 Sc4 K03 50.41(5) . .
O41 Sc4 K03 65.88(5) . .
F3 Sc4 K03 120.16(5) . .
O42 Sc4 K03 41.41(4) . .
K31 Sc4 K03 164.62(2) . .
K10 Sc4 K03 110.76(2) . .
K14 Sc4 K03 71.549(18) . .
K02 Sc4 K03 60.061(19) . .
O40 Sc4 K23 119.33(5) . .
O18 Sc4 K23 45.48(5) . .
F2 Sc4 K23 121.05(5) . .
O41 Sc4 K23 124.37(5) . .
F3 Sc4 K23 51.79(5) . .
O42 Sc4 K23 62.95(5) . .
K31 Sc4 K23 61.492(19) . .
K10 Sc4 K23 110.05(2) . .
K14 Sc4 K23 77.35(2) . .
K02 Sc4 K23 68.675(17) . .
K03 Sc4 K23 103.28(2) . .
F16 Sc5 O6 94.71(7) . .
F16 Sc5 O58 89.87(7) . .
O6 Sc5 O58 91.80(7) . .
F16 Sc5 O59 93.81(7) . .
O6 Sc5 O59 171.22(7) . .
O58 Sc5 O59 90.34(7) . .
F16 Sc5 O21 91.20(7) . .
O6 Sc5 O21 88.21(7) . .
O58 Sc5 O21 178.93(7) . .
O59 Sc5 O21 89.50(7) . .
F16 Sc5 F5 177.91(8) . .
O6 Sc5 F5 83.81(7) . .
O58 Sc5 F5 91.65(7) . .
O59 Sc5 F5 87.62(7) . .
O21 Sc5 F5 87.28(7) . .
F16 Sc5 K34 55.61(5) . 1_455
O6 Sc5 K34 59.91(5) . 1_455
O58 Sc5 K34 129.14(5) . 1_455
O59 Sc5 K34 124.24(5) . 1_455
O21 Sc5 K34 51.71(5) . 1_455
F5 Sc5 K34 122.30(6) . 1_455
F16 Sc5 K13 61.73(5) . .
O6 Sc5 K13 125.09(5) . .
O58 Sc5 K13 132.78(5) . .
O59 Sc5 K13 57.96(5) . .
O21 Sc5 K13 47.85(5) . .
F5 Sc5 K13 117.99(5) . .
K34 Sc5 K13 66.33(2) 1_455 .
F16 Sc5 K23 116.57(6) . .
O6 Sc5 K23 130.87(5) . .
O58 Sc5 K23 54.18(5) . .
O59 Sc5 K23 45.55(5) . .
O21 Sc5 K23 125.15(5) . .
F5 Sc5 K23 65.52(6) . .
K34 Sc5 K23 168.94(2) 1_455 .
K13 Sc5 K23 103.47(2) . .
F16 Sc5 K26 57.21(5) . .
O6 Sc5 K26 68.00(5) . .
O58 Sc5 K26 44.30(5) . .
O59 Sc5 K26 118.82(5) . .
O21 Sc5 K26 136.58(5) . .
F5 Sc5 K26 123.31(5) . .
K34 Sc5 K26 84.90(2) 1_455 .
K13 Sc5 K26 118.504(19) . .
K23 Sc5 K26 97.038(19) . .
F16 Sc5 K15 117.07(5) . .
O6 Sc5 K15 54.08(5) . .
O58 Sc5 K15 47.10(5) . .
O59 Sc5 K15 123.04(5) . .
O21 Sc5 K15 132.30(5) . .
F5 Sc5 K15 63.18(5) . .
K34 Sc5 K15 112.63(2) 1_455 .
K13 Sc5 K15 178.685(17) . .
K23 Sc5 K15 77.500(18) . .
K26 Sc5 K15 60.378(15) . .
F16 Sc5 K28 121.67(5) . 1_455
O6 Sc5 K28 125.06(5) . 1_455
O58 Sc5 K28 124.40(5) . 1_455
O59 Sc5 K28 47.60(5) . 1_455
O21 Sc5 K28 54.85(5) . 1_455
F5 Sc5 K28 58.43(5) . 1_455
K34 Sc5 K28 106.13(2) 1_455 1_455
K13 Sc5 K28 60.561(15) . 1_455
K23 Sc5 K28 70.438(18) . 1_455
K26 Sc5 K28 165.83(2) . 1_455
K15 Sc5 K28 120.706(18) . 1_455
O34 Sc6 F17 92.85(7) . .
O34 Sc6 O24 95.44(7) . .
F17 Sc6 O24 88.24(6) . .
O34 Sc6 F14 93.78(7) . .
F17 Sc6 F14 173.24(7) . .
O24 Sc6 F14 89.84(7) . .
O34 Sc6 O15 91.41(7) . .
F17 Sc6 O15 90.39(6) . .
O24 Sc6 O15 173.07(7) . .
F14 Sc6 O15 90.74(7) . .
O34 Sc6 O52 175.30(7) . 1_655
F17 Sc6 O52 82.79(6) . 1_655
O24 Sc6 O52 86.20(7) . 1_655
F14 Sc6 O52 90.62(6) . 1_655
O15 Sc6 O52 86.89(7) . 1_655
O34 Sc6 K11 51.08(5) . .
F17 Sc6 K11 57.76(5) . .
O24 Sc6 K11 60.85(5) . .
F14 Sc6 K11 126.40(5) . .
O15 Sc6 K11 123.66(5) . .
O52 Sc6 K11 126.82(5) 1_655 .
O34 Sc6 K28 135.65(5) . .
F17 Sc6 K28 56.30(5) . .
O24 Sc6 K28 56.88(5) . .
F14 Sc6 K28 117.45(5) . .
O15 Sc6 K28 116.99(5) . .
O52 Sc6 K28 42.44(4) 1_655 .
K11 Sc6 K28 84.57(2) . .
O34 Sc6 K12 49.23(5) . 3_655
F17 Sc6 K12 123.40(5) . 3_655
O24 Sc6 K12 128.66(5) . 3_655
F14 Sc6 K12 62.50(5) . 3_655
O15 Sc6 K12 57.33(5) . 3_655
O52 Sc6 K12 132.34(5) 1_655 3_655
K11 Sc6 K12 100.25(2) . 3_655
K28 Sc6 K12 173.99(2) . 3_655
O34 Sc6 K22 133.55(5) . .
F17 Sc6 K22 54.39(5) . .
O24 Sc6 K22 113.05(5) . .
F14 Sc6 K22 120.83(5) . .
O15 Sc6 K22 60.93(5) . .
O52 Sc6 K22 42.03(4) 1_655 .
K11 Sc6 K22 112.07(2) . .
K28 Sc6 K22 56.171(19) . .
K12 Sc6 K22 118.24(2) 3_655 .
O34 Sc6 K20 117.59(5) . 3_655
F17 Sc6 K20 119.64(5) . 3_655
O24 Sc6 K20 133.24(5) . 3_655
F14 Sc6 K20 57.90(5) . 3_655
O15 Sc6 K20 42.75(5) . 3_655
O52 Sc6 K20 63.64(5) 1_655 3_655
K11 Sc6 K20 165.52(2) . 3_655
K28 Sc6 K20 105.92(2) . 3_655
K12 Sc6 K20 68.703(19) 3_655 3_655
K22 Sc6 K20 67.967(17) . 3_655
O34 Sc6 K13 130.25(5) . 1_655
F17 Sc6 K13 122.89(5) . 1_655
O24 Sc6 K13 56.99(5) . 1_655
F14 Sc6 K13 51.07(5) . 1_655
O15 Sc6 K13 118.71(5) . 1_655
O52 Sc6 K13 54.20(5) 1_655 1_655
K11 Sc6 K13 117.62(2) . 1_655
K28 Sc6 K13 66.629(17) . 1_655
K12 Sc6 K13 113.56(2) 3_655 1_655
K22 Sc6 K13 96.20(2) . 1_655
K20 Sc6 K13 76.265(19) 3_655 1_655
O45 Sc7 O39 95.51(8) . .
O45 Sc7 F1 80.46(7) . .
O39 Sc7 F1 89.90(7) . .
O45 Sc7 F7 95.58(7) . .
O39 Sc7 F7 90.48(7) . .
F1 Sc7 F7 176.04(7) . .
O45 Sc7 O23 90.81(7) . .
O39 Sc7 O23 173.60(6) . .
F1 Sc7 O23 90.15(7) . .
F7 Sc7 O23 89.91(6) . .
O45 Sc7 O47 172.71(7) . .
O39 Sc7 O47 90.02(7) . .
F1 Sc7 O47 94.83(7) . .
F7 Sc7 O47 89.11(6) . .
O23 Sc7 O47 83.60(7) . .
O45 Sc7 K29 45.01(5) . .
O39 Sc7 K29 118.49(5) . .
F1 Sc7 K29 47.36(5) . .
F7 Sc7 K29 129.36(5) . .
O23 Sc7 K29 65.73(5) . .
O47 Sc7 K29 127.88(5) . .
O45 Sc7 K08 123.98(5) . .
O39 Sc7 K08 121.32(5) . .
F1 Sc7 K08 60.97(6) . .
F7 Sc7 K08 121.94(5) . .
O23 Sc7 K08 53.53(5) . .
O47 Sc7 K08 48.76(5) . .
K29 Sc7 K08 79.34(2) . .
O45 Sc7 K16 58.33(5) . .
O39 Sc7 K16 133.72(5) . .
F1 Sc7 K16 118.25(6) . .
F7 Sc7 K16 59.04(5) . .
O23 Sc7 K16 51.22(4) . .
O47 Sc7 K16 120.35(5) . .
K29 Sc7 K16 71.622(17) . .
K08 Sc7 K16 104.76(2) . .
O45 Sc7 K04 53.09(5) . .
O39 Sc7 K04 56.28(5) . .
F1 Sc7 K04 52.16(5) . .
F7 Sc7 K04 125.24(5) . .
O23 Sc7 K04 127.95(5) . .
O47 Sc7 K04 127.77(5) . .
K29 Sc7 K04 62.277(19) . .
K08 Sc7 K04 112.71(2) . .
K16 Sc7 K04 111.41(2) . .
O45 Sc7 K32 142.43(5) . .
O39 Sc7 K32 67.31(5) . .
F1 Sc7 K32 66.97(6) . .
F7 Sc7 K32 116.76(5) . .
O23 Sc7 K32 106.89(5) . .
O47 Sc7 K32 36.88(4) . .
K29 Sc7 K32 112.72(2) . .
K08 Sc7 K32 54.789(18) . .
K16 Sc7 K32 155.28(2) . .
K04 Sc7 K32 90.97(2) . .
O45 Sc7 K11 109.41(5) . .
O39 Sc7 K11 140.26(5) . .
F1 Sc7 K11 123.69(5) . .
F7 Sc7 K11 57.56(5) . .
O23 Sc7 K11 36.84(4) . .
O47 Sc7 K11 68.53(5) . .
K29 Sc7 K11 100.81(2) . .
K08 Sc7 K11 69.168(17) . .
K16 Sc7 K11 51.871(18) . .
K04 Sc7 K11 161.09(2) . .
K32 Sc7 K11 104.18(2) . .
O65 Sc8 O48 95.35(8) . .
O65 Sc8 F10 94.43(7) . .
O48 Sc8 F10 91.13(7) . .
O65 Sc8 F11 88.72(7) . .
O48 Sc8 F11 92.56(7) . .
F10 Sc8 F11 174.91(8) . .
O65 Sc8 O61 89.40(7) . .
O48 Sc8 O61 174.79(7) . .
F10 Sc8 O61 86.34(7) . .
F11 Sc8 O61 89.70(7) . .
O65 Sc8 O4 172.27(7) . .
O48 Sc8 O4 90.54(7) . .
F10 Sc8 O4 90.45(7) . .
F11 Sc8 O4 86.01(6) . .
O61 Sc8 O4 84.93(7) . .
O65 Sc8 K36 127.39(5) . .
O48 Sc8 K36 60.08(5) . .
F10 Sc8 K36 128.44(6) . .
F11 Sc8 K36 51.28(5) . .
O61 Sc8 K36 118.36(5) . .
O4 Sc8 K36 52.12(5) . .
O65 Sc8 K18 70.13(5) . .
O48 Sc8 K18 50.32(5) . .
F10 Sc8 K18 52.40(5) . .
F11 Sc8 K18 132.63(5) . .
O61 Sc8 K18 130.11(5) . .
O4 Sc8 K18 117.58(5) . .
K36 Sc8 K18 109.88(2) . .
O65 Sc8 K35 62.37(5) . .
O48 Sc8 K35 134.76(5) . .
F10 Sc8 K35 55.46(5) . .
F11 Sc8 K35 123.19(5) . .
O61 Sc8 K35 46.35(5) . .
O4 Sc8 K35 116.30(5) . .
K36 Sc8 K35 164.36(2) . .
K18 Sc8 K35 84.48(2) . .
O65 Sc8 K07 132.54(5) . 3_655
O48 Sc8 K07 53.17(5) . 3_655
F10 Sc8 K07 57.41(6) . 3_655
F11 Sc8 K07 122.69(5) . 3_655
O61 Sc8 K07 121.77(5) . 3_655
O4 Sc8 K07 55.18(5) . 3_655
K36 Sc8 K07 71.414(18) . 3_655
K18 Sc8 K07 62.423(19) . 3_655
K35 Sc8 K07 112.10(2) . 3_655
O65 Sc8 K09 46.52(5) . .
O48 Sc8 K09 127.25(5) . .
F10 Sc8 K09 121.17(6) . .
F11 Sc8 K09 58.75(5) . .
O61 Sc8 K09 57.85(5) . .
O4 Sc8 K09 125.75(5) . .
K36 Sc8 K09 110.03(2) . .
K18 Sc8 K09 116.59(2) . .
K35 Sc8 K09 66.561(17) . .
K07 Sc8 K09 178.542(18) 3_655 .
O65 Sc8 K24 46.49(5) . .
O48 Sc8 K24 57.73(5) . .
F10 Sc8 K24 118.33(6) . .
F11 Sc8 K24 66.69(5) . .
O61 Sc8 K24 127.47(5) . .
O4 Sc8 K24 135.07(5) . .
K36 Sc8 K24 83.31(2) . .
K18 Sc8 K24 68.201(17) . .
K35 Sc8 K24 108.54(2) . .
K07 Sc8 K24 110.25(2) 3_655 .
K09 Sc8 K24 69.963(18) . .
O63 Sc9 O35 95.39(7) 2_656 .
O63 Sc9 F12 91.02(7) 2_656 .
O35 Sc9 F12 90.62(7) . .
O63 Sc9 F20 91.81(7) 2_656 .
O35 Sc9 F20 96.63(7) . .
F12 Sc9 F20 171.94(8) . .
O63 Sc9 O53 90.67(7) 2_656 .
O35 Sc9 O53 173.93(7) . .
F12 Sc9 O53 89.55(7) . .
F20 Sc9 O53 82.86(7) . .
O63 Sc9 O38 175.73(7) 2_656 .
O35 Sc9 O38 88.41(7) . .
F12 Sc9 O38 90.89(7) . .
F20 Sc9 O38 85.81(6) . .
O53 Sc9 O38 85.53(7) . .
O63 Sc9 K27 56.20(5) 2_656 3_666
O35 Sc9 K27 55.41(5) . 3_666
F12 Sc9 K27 57.84(6) . 3_666
F20 Sc9 K27 129.61(6) . 3_666
O53 Sc9 K27 129.19(5) . 3_666
O38 Sc9 K27 127.94(5) . 3_666
O63 Sc9 K19 56.20(5) 2_656 .
O35 Sc9 K19 128.39(5) . .
F12 Sc9 K19 53.08(5) . .
F20 Sc9 K19 123.27(6) . .
O53 Sc9 K19 55.83(4) . .
O38 Sc9 K19 122.51(5) . .
K27 Sc9 K19 73.40(2) 3_666 .
O63 Sc9 K26 135.97(5) 2_656 .
O35 Sc9 K26 63.12(5) . .
F12 Sc9 K26 124.73(5) . .
F20 Sc9 K26 56.63(5) . .
O53 Sc9 K26 112.02(5) . .
O38 Sc9 K26 44.67(4) . .
K27 Sc9 K26 118.51(2) 3_666 .
K19 Sc9 K26 165.77(2) . .
O63 Sc9 K33 114.46(5) 2_656 .
O35 Sc9 K33 126.59(5) . .
F12 Sc9 K33 48.35(6) . .
F20 Sc9 K33 123.75(6) . .
O53 Sc9 K33 50.25(4) . .
O38 Sc9 K33 64.34(5) . .
K27 Sc9 K33 105.68(2) 3_666 .
K19 Sc9 K33 58.268(19) . .
K26 Sc9 K33 108.89(2) . .
O63 Sc9 K32 47.54(5) 2_656 3_656
O35 Sc9 K32 119.91(5) . 3_656
F12 Sc9 K32 126.92(5) . 3_656
F20 Sc9 K32 51.65(5) . 3_656
O53 Sc9 K32 64.40(5) . 3_656
O38 Sc9 K32 128.62(5) . 3_656
K27 Sc9 K32 102.91(2) 3_666 3_656
K19 Sc9 K32 74.542(19) . 3_656
K26 Sc9 K32 108.11(2) . 3_656
K33 Sc9 K32 112.75(2) . 3_656
O63 Sc9 K15 121.65(5) 2_656 .
O35 Sc9 K15 45.73(5) . .
F12 Sc9 K15 56.72(5) . .
F20 Sc9 K15 127.20(5) . .
O53 Sc9 K15 130.40(5) . .
O38 Sc9 K15 62.52(5) . .
K27 Sc9 K15 65.47(2) 3_666 .
K19 Sc9 K15 109.48(2) . .
K26 Sc9 K15 71.789(18) . .
K33 Sc9 K15 80.95(2) . .
K32 Sc9 K15 164.71(2) 3_656 .
F9 Sc10 O62 94.98(5) . .
F9 Sc10 O62 94.98(5) . 2
O62 Sc10 O62 170.03(9) . 2
F9 Sc10 O49 87.42(5) . 2
O62 Sc10 O49 87.94(7) . 2
O62 Sc10 O49 92.51(7) 2 2
F9 Sc10 O49 87.42(5) . .
O62 Sc10 O49 92.51(7) . .
O62 Sc10 O49 87.94(7) 2 .
O49 Sc10 O49 174.83(9) 2 .
F9 Sc10 F18 180.0 . .
O62 Sc10 F18 85.02(5) . .
O62 Sc10 F18 85.02(5) 2 .
O49 Sc10 F18 92.58(5) 2 .
O49 Sc10 F18 92.58(5) . .
F9 Sc10 K22 123.615(12) . 1_455
O62 Sc10 K22 38.89(5) . 1_455
O62 Sc10 K22 133.01(5) 2 1_455
O49 Sc10 K22 66.50(5) 2 1_455
O49 Sc10 K22 116.66(5) . 1_455
F18 Sc10 K22 56.385(12) . 1_455
F9 Sc10 K22 123.615(12) . 3_665
O62 Sc10 K22 133.02(5) . 3_665
O62 Sc10 K22 38.89(5) 2 3_665
O49 Sc10 K22 116.66(5) 2 3_665
O49 Sc10 K22 66.50(5) . 3_665
F18 Sc10 K22 56.385(12) . 3_665
K22 Sc10 K22 112.77(2) 1_455 3_665
F9 Sc10 K20 60.389(11) . 3
O62 Sc10 K20 55.94(5) . 3
O62 Sc10 K20 130.23(5) 2 3
O49 Sc10 K20 47.98(5) 2 3
O49 Sc10 K20 128.67(5) . 3
F18 Sc10 K20 119.611(11) . 3
K22 Sc10 K20 65.370(14) 1_455 3
K22 Sc10 K20 164.549(15) 3_665 3
F9 Sc10 K20 60.389(11) . .
O62 Sc10 K20 130.23(5) . .
O62 Sc10 K20 55.94(5) 2 .
O49 Sc10 K20 128.67(5) 2 .
O49 Sc10 K20 47.98(5) . .
F18 Sc10 K20 119.611(11) . .
K22 Sc10 K20 164.549(15) 1_455 .
K22 Sc10 K20 65.370(14) 3_665 .
K20 Sc10 K20 120.78(2) 3 .
F9 Sc10 K10 60.844(11) . 3
O62 Sc10 K10 124.02(5) . 3
O62 Sc10 K10 61.65(5) 2 3
O49 Sc10 K10 45.40(5) 2 3
O49 Sc10 K10 131.16(5) . 3
F18 Sc10 K10 119.156(11) . 3
K22 Sc10 K10 111.890(16) 1_455 3
K22 Sc10 K10 99.590(16) 3_665 3
K20 Sc10 K10 68.610(17) 3 3
K20 Sc10 K10 83.296(18) . 3
F9 Sc10 K10 60.845(11) . .
O62 Sc10 K10 61.65(5) . .
O62 Sc10 K10 124.02(5) 2 .
O49 Sc10 K10 131.17(5) 2 .
O49 Sc10 K10 45.40(5) . .
F18 Sc10 K10 119.155(11) . .
K22 Sc10 K10 99.590(16) 1_455 .
K22 Sc10 K10 111.890(16) 3_665 .
K20 Sc10 K10 83.297(18) 3 .
K20 Sc10 K10 68.610(17) . .
K10 Sc10 K10 121.69(2) 3 .
O41 K01 O41 91.20(7) 4_565 .
O41 K01 O36 60.21(5) 4_565 4_565
O41 K01 O36 130.53(6) . 4_565
O41 K01 O36 130.53(6) 4_565 .
O41 K01 O36 60.21(5) . .
O36 K01 O36 106.74(8) 4_565 .
O41 K01 F6 119.92(5) 4_565 .
O41 K01 F6 119.92(5) . .
O36 K01 F6 60.71(4) 4_565 .
O36 K01 F6 60.71(4) . .
O41 K01 Si5 108.08(5) 4_565 .
O41 K01 Si5 31.04(4) . .
O36 K01 Si5 116.68(5) 4_565 .
O36 K01 Si5 30.47(4) . .
F6 K01 Si5 88.88(3) . .
O41 K01 Si5 31.04(4) 4_565 4_565
O41 K01 Si5 108.08(5) . 4_565
O36 K01 Si5 30.47(4) 4_565 4_565
O36 K01 Si5 116.68(5) . 4_565
F6 K01 Si5 88.88(3) . 4_565
Si5 K01 Si5 109.52(4) . 4_565
O41 K01 O14 127.25(4) 4_565 3_665
O41 K01 O14 127.25(4) . 3_665
O36 K01 O14 101.51(5) 4_565 3_665
O36 K01 O14 101.51(5) . 3_665
F6 K01 O14 74.62(6) . 3_665
Si5 K01 O14 123.43(2) . 3_665
Si5 K01 O14 123.43(2) 4_565 3_665
O41 K01 O55 96.57(5) 4_565 .
O41 K01 O55 96.57(5) . .
O36 K01 O55 124.11(4) 4_565 .
O36 K01 O55 124.11(4) . .
F6 K01 O55 125.12(6) . .
Si5 K01 O55 118.87(2) . .
Si5 K01 O55 118.87(2) 4_565 .
O14 K01 O55 50.50(6) 3_665 .
O41 K01 K24 80.89(4) 4_565 .
O41 K01 K24 80.89(4) . .
O36 K01 K24 56.87(4) 4_565 .
O36 K01 K24 56.87(4) . .
F6 K01 K24 58.55(4) . .
Si5 K01 K24 59.861(19) . .
Si5 K01 K24 59.860(19) 4_565 .
O14 K01 K24 133.17(5) 3_665 .
O55 K01 K24 176.33(5) . .
O41 K01 K14 47.41(4) 4_565 .
O41 K01 K14 47.41(4) . .
O36 K01 K14 87.53(4) 4_565 .
O36 K01 K14 87.53(4) . .
F6 K01 K14 120.77(4) . .
Si5 K01 K14 60.952(19) . .
Si5 K01 K14 60.952(19) 4_565 .
O14 K01 K14 164.61(5) 3_665 .
O55 K01 K14 114.11(5) . .
K24 K01 K14 62.22(2) . .
O41 K01 Si3 103.45(4) 4_565 4_565
O41 K01 Si3 151.22(4) . 4_565
O36 K01 Si3 78.03(4) 4_565 4_565
O36 K01 Si3 121.05(5) . 4_565
F6 K01 Si3 73.92(4) . 4_565
Si5 K01 Si3 148.43(3) . 4_565
Si5 K01 Si3 96.66(2) 4_565 4_565
O14 K01 Si3 26.908(14) 3_665 4_565
O55 K01 Si3 57.67(4) . 4_565
K24 K01 Si3 125.41(2) . 4_565
K14 K01 Si3 150.564(17) . 4_565
O26 K02 O26 91.82(8) . 4
O26 K02 O18 177.88(6) . 4
O26 K02 O18 88.26(5) 4 4
O26 K02 O18 88.26(5) . .
O26 K02 O18 177.88(6) 4 .
O18 K02 O18 91.59(7) 4 .
O26 K02 F2 115.72(5) . .
O26 K02 F2 115.72(5) 4 .
O18 K02 F2 62.41(4) 4 .
O18 K02 F2 62.41(4) . .
O26 K02 O19 126.28(5) . .
O26 K02 O19 126.28(5) 4 .
O18 K02 O19 55.06(4) 4 .
O18 K02 O19 55.06(4) . .
F2 K02 O19 83.15(7) . .
O26 K02 O42 115.35(5) . 4
O26 K02 O42 56.33(5) 4 4
O18 K02 O42 63.00(5) 4 4
O18 K02 O42 121.79(6) . 4
F2 K02 O42 59.39(4) . 4
O19 K02 O42 117.25(5) . 4
O26 K02 O42 56.33(5) . .
O26 K02 O42 115.35(5) 4 .
O18 K02 O42 121.79(6) 4 .
O18 K02 O42 63.00(5) . .
F2 K02 O42 59.39(4) . .
O19 K02 O42 117.25(5) . .
O42 K02 O42 86.32(7) 4 .
O26 K02 Si16 151.08(4) . 4
O26 K02 Si16 98.61(4) 4 4
O18 K02 Si16 30.88(4) 4 4
O18 K02 Si16 82.29(4) . 4
F2 K02 Si16 83.81(4) . 4
O19 K02 Si16 30.337(15) . 4
O42 K02 Si16 92.69(4) 4 4
O42 K02 Si16 137.55(5) . 4
O26 K02 Si16 98.61(4) . .
O26 K02 Si16 151.08(4) 4 .
O18 K02 Si16 82.29(4) 4 .
O18 K02 Si16 30.88(4) . .
F2 K02 Si16 83.81(4) . .
O19 K02 Si16 30.337(15) . .
O42 K02 Si16 137.55(5) 4 .
O42 K02 Si16 92.69(4) . .
Si16 K02 Si16 60.67(3) 4 .
O26 K02 Si12 101.84(4) . 4
O26 K02 Si12 30.63(4) 4 4
O18 K02 Si12 77.19(4) 4 4
O18 K02 Si12 147.36(5) . 4
F2 K02 Si12 85.44(3) . 4
O19 K02 Si12 130.66(2) . 4
O42 K02 Si12 26.40(4) 4 4
O42 K02 Si12 96.85(4) . 4
Si16 K02 Si12 100.77(2) 4 4
Si16 K02 Si12 159.43(3) . 4
O26 K02 Si12 30.62(4) . .
O26 K02 Si12 101.84(4) 4 .
O18 K02 Si12 147.36(5) 4 .
O18 K02 Si12 77.19(4) . .
F2 K02 Si12 85.44(3) . .
O19 K02 Si12 130.66(2) . .
O42 K02 Si12 96.85(4) 4 .
O42 K02 Si12 26.40(4) . .
Si16 K02 Si12 159.44(3) 4 .
Si16 K02 Si12 100.77(2) . .
Si12 K02 Si12 95.79(3) 4 .
O42 K03 O42 103.76(8) 4 .
O42 K03 O5 103.31(5) 4 .
O42 K03 O5 103.31(5) . .
O42 K03 F2 62.91(5) 4 .
O42 K03 F2 62.91(5) . .
O5 K03 F2 69.44(6) . .
O42 K03 O46 57.36(5) 4 4
O42 K03 O46 113.53(6) . 4
O5 K03 O46 141.22(4) . 4
F2 K03 O46 116.91(5) . 4
O42 K03 O46 113.53(6) 4 .
O42 K03 O46 57.36(5) . .
O5 K03 O46 141.22(4) . .
F2 K03 O46 116.91(5) . .
O46 K03 O46 73.25(6) 4 .
O42 K03 O1 127.84(4) 4 .
O42 K03 O1 127.84(4) . .
O5 K03 O1 61.66(7) . .
F2 K03 O1 131.09(6) . .
O46 K03 O1 101.66(5) 4 .
O46 K03 O1 101.66(5) . .
O42 K03 O25 157.83(6) 4 .
O42 K03 O25 87.84(5) . .
O5 K03 O25 92.02(5) . .
F2 K03 O25 138.74(3) . .
O46 K03 O25 100.79(5) 4 .
O46 K03 O25 57.08(5) . .
O1 K03 O25 47.29(4) . .
O42 K03 O25 87.84(5) 4 4
O42 K03 O25 157.83(6) . 4
O5 K03 O25 92.02(5) . 4
F2 K03 O25 138.74(3) . 4
O46 K03 O25 57.07(5) 4 4
O46 K03 O25 100.79(5) . 4
O1 K03 O25 47.29(4) . 4
O25 K03 O25 75.54(6) . 4
O42 K03 Si12 26.52(4) 4 4
O42 K03 Si12 108.60(5) . 4
O5 K03 Si12 125.15(2) . 4
F2 K03 Si12 87.03(3) . 4
O46 K03 Si12 31.01(3) 4 4
O46 K03 Si12 93.62(4) . 4
O1 K03 Si12 120.80(3) . 4
O25 K03 Si12 131.79(4) . 4
O25 K03 Si12 73.83(3) 4 4
O42 K03 Si12 108.60(5) 4 .
O42 K03 Si12 26.53(4) . .
O5 K03 Si12 125.15(2) . .
F2 K03 Si12 87.03(3) . .
O46 K03 Si12 93.62(4) 4 .
O46 K03 Si12 31.00(3) . .
O1 K03 Si12 120.80(3) . .
O25 K03 Si12 73.83(3) . .
O25 K03 Si12 131.79(4) 4 .
Si12 K03 Si12 100.95(3) 4 .
O42 K03 Si5 125.64(5) 4 .
O42 K03 Si5 81.41(4) . .
O5 K03 Si5 27.761(14) . .
F2 K03 Si5 73.16(4) . .
O46 K03 Si5 164.37(4) 4 .
O46 K03 Si5 114.08(3) . .
O1 K03 Si5 63.90(4) . .
O25 K03 Si5 74.24(4) . .
O25 K03 Si5 107.35(4) 4 .
Si12 K03 Si5 150.97(3) 4 .
Si12 K03 Si5 99.02(2) . .
O17 K04 O17 111.60(8) . 4
O17 K04 F1 103.82(5) . .
O17 K04 F1 103.82(5) 4 .
O17 K04 O45 118.81(6) . 4
O17 K04 O45 53.82(5) 4 4
F1 K04 O45 50.00(4) . 4
O17 K04 O45 53.82(5) . .
O17 K04 O45 118.81(6) 4 .
F1 K04 O45 50.00(4) . .
O45 K04 O45 80.81(6) 4 .
O17 K04 O64 123.90(4) . .
O17 K04 O64 123.90(4) 4 .
F1 K04 O64 71.99(6) . .
O45 K04 O64 100.92(5) 4 .
O45 K04 O64 100.92(5) . .
O17 K04 O9 115.18(6) . 4
O17 K04 O9 53.58(5) 4 4
F1 K04 O9 139.78(3) . 4
O45 K04 O9 99.80(4) 4 4
O45 K04 O9 165.71(5) . 4
O64 K04 O9 93.00(5) . 4
O17 K04 O9 53.58(5) . .
O17 K04 O9 115.18(6) 4 .
F1 K04 O9 139.78(3) . .
O45 K04 O9 165.71(5) 4 .
O45 K04 O9 99.80(4) . .
O64 K04 O9 93.00(5) . .
O9 K04 O9 76.08(6) 4 .
O17 K04 O39 157.06(6) . 4
O17 K04 O39 83.07(5) 4 4
F1 K04 O39 54.26(4) . 4
O45 K04 O39 54.94(5) 4 4
O45 K04 O39 104.00(5) . 4
O64 K04 O39 48.11(4) . 4
O9 K04 O39 87.65(4) 4 4
O9 K04 O39 137.31(5) . 4
O17 K04 O39 83.07(5) . .
O17 K04 O39 157.06(6) 4 .
F1 K04 O39 54.26(4) . .
O45 K04 O39 104.00(5) 4 .
O45 K04 O39 54.94(5) . .
O64 K04 O39 48.11(4) . .
O9 K04 O39 137.31(5) 4 .
O9 K04 O39 87.65(4) . .
O39 K04 O39 78.05(6) 4 .
O17 K04 Si9 28.71(4) . .
O17 K04 Si9 109.40(5) 4 .
F1 K04 Si9 129.85(2) . .
O45 K04 Si9 142.18(4) 4 .
O45 K04 Si9 80.92(4) . .
O64 K04 Si9 114.91(3) . .
O9 K04 Si9 90.37(4) 4 .
O9 K04 Si9 26.57(3) . .
O39 K04 Si9 162.69(4) 4 .
O39 K04 Si9 91.95(3) . .
O17 K04 Si9 109.40(5) . 4
O17 K04 Si9 28.72(4) 4 4
F1 K04 Si9 129.85(2) . 4
O45 K04 Si9 80.92(4) 4 4
O45 K04 Si9 142.18(4) . 4
O64 K04 Si9 114.91(3) . 4
O9 K04 Si9 26.57(3) 4 4
O9 K04 Si9 90.37(4) . 4
O39 K04 Si9 91.95(3) 4 4
O39 K04 Si9 162.69(4) . 4
Si9 K04 Si9 93.94(3) . 4
O54 K05 O54 92.97(7) . 4_565
O54 K05 O20 112.80(5) . .
O54 K05 O20 112.80(5) 4_565 .
O54 K05 F15 60.48(4) . .
O54 K05 F15 60.48(4) 4_565 .
O20 K05 F15 79.94(6) . .
O54 K05 O39 118.45(6) . 4_565
O54 K05 O39 56.35(5) 4_565 4_565
O20 K05 O39 127.71(4) . 4_565
F15 K05 O39 116.72(4) . 4_565
O54 K05 O39 56.35(5) . .
O54 K05 O39 118.44(6) 4_565 .
O20 K05 O39 127.71(4) . .
F15 K05 O39 116.72(4) . .
O39 K05 O39 90.54(7) 4_565 .
O54 K05 O17 88.80(5) . .
O54 K05 O17 163.71(6) 4_565 .
O20 K05 O17 52.10(4) . .
F15 K05 O17 107.04(4) . .
O39 K05 O17 135.61(5) 4_565 .
O39 K05 O17 75.75(5) . .
O54 K05 O17 163.71(6) . 4_565
O54 K05 O17 88.80(5) 4_565 4_565
O20 K05 O17 52.10(4) . 4_565
F15 K05 O17 107.04(4) . 4_565
O39 K05 O17 75.75(5) 4_565 4_565
O39 K05 O17 135.61(5) . 4_565
O17 K05 O17 85.10(6) . 4_565
O54 K05 O9 119.02(5) . 4_565
O54 K05 O9 60.69(5) 4_565 4_565
O20 K05 O9 52.38(4) . 4_565
F15 K05 O9 58.70(3) . 4_565
O39 K05 O9 92.41(4) 4_565 4_565
O39 K05 O9 175.36(5) . 4_565
O17 K05 O9 104.47(5) . 4_565
O17 K05 O9 48.79(4) 4_565 4_565
O54 K05 O9 60.69(5) . .
O54 K05 O9 119.02(5) 4_565 .
O20 K05 O9 52.38(4) . .
F15 K05 O9 58.70(3) . .
O39 K05 O9 175.36(5) 4_565 .
O39 K05 O9 92.41(4) . .
O17 K05 O9 48.78(4) . .
O17 K05 O9 104.47(5) 4_565 .
O9 K05 O9 84.44(6) 4_565 .
O54 K05 Si9 86.44(4) . .
O54 K05 Si9 132.40(5) 4_565 .
O20 K05 Si9 30.657(16) . .
F15 K05 Si9 78.62(2) . .
O39 K05 Si9 154.61(4) 4_565 .
O39 K05 Si9 100.49(4) . .
O17 K05 Si9 31.53(3) . .
O17 K05 Si9 80.46(4) 4_565 .
O9 K05 Si9 78.23(4) 4_565 .
O9 K05 Si9 27.60(3) . .
O54 K05 Si9 132.40(5) . 4_565
O54 K05 Si9 86.45(4) 4_565 4_565
O20 K05 Si9 30.656(16) . 4_565
F15 K05 Si9 78.62(2) . 4_565
O39 K05 Si9 100.49(4) 4_565 4_565
O39 K05 Si9 154.61(4) . 4_565
O17 K05 Si9 80.46(4) . 4_565
O17 K05 Si9 31.53(3) 4_565 4_565
O9 K05 Si9 27.60(3) 4_565 4_565
O9 K05 Si9 78.23(4) . 4_565
Si9 K05 Si9 61.02(3) . 4_565
O9 K06 O9 102.25(8) . 4
O9 K06 F4 64.03(4) . .
O9 K06 F4 64.03(4) 4 .
O9 K06 O64 109.23(5) . 3_656
O9 K06 O64 109.23(5) 4 3_656
F4 K06 O64 75.89(5) . 3_656
O9 K06 O43 128.87(4) . .
O9 K06 O43 128.87(4) 4 .
F4 K06 O43 134.89(5) . .
O64 K06 O43 59.00(7) 3_656 .
O9 K06 O32 114.16(6) . 4
O9 K06 O32 55.35(5) 4 4
F4 K06 O32 117.49(4) . 4
O64 K06 O32 136.07(4) 3_656 4
O43 K06 O32 96.79(5) . 4
O9 K06 O32 55.35(5) . .
O9 K06 O32 114.16(6) 4 .
F4 K06 O32 117.49(4) . .
O64 K06 O32 136.07(4) 3_656 .
O43 K06 O32 96.79(5) . .
O32 K06 O32 77.81(6) 4 .
O9 K06 O54 57.54(5) . 2_656
O9 K06 O54 122.89(6) 4 2_656
F4 K06 O54 59.16(3) . 2_656
O64 K06 O54 51.97(4) 3_656 2_656
O43 K06 O54 90.18(5) . 2_656
O32 K06 O54 171.62(5) 4 2_656
O32 K06 O54 96.80(4) . 2_656
O9 K06 O54 122.89(6) . 3_656
O9 K06 O54 57.54(5) 4 3_656
F4 K06 O54 59.16(3) . 3_656
O64 K06 O54 51.97(4) 3_656 3_656
O43 K06 O54 90.18(5) . 3_656
O32 K06 O54 96.80(4) 4 3_656
O32 K06 O54 171.62(5) . 3_656
O54 K06 O54 87.80(6) 2_656 3_656
O9 K06 Si9 26.96(4) . .
O9 K06 Si9 106.97(5) 4 .
F4 K06 Si9 89.01(2) . .
O64 K06 Si9 128.75(2) 3_656 .
O43 K06 Si9 118.20(3) . .
O32 K06 Si9 94.48(4) 4 .
O32 K06 Si9 28.79(3) . .
O54 K06 Si9 78.06(4) 2_656 .
O54 K06 Si9 147.89(4) 3_656 .
O9 K06 Si9 106.98(5) . 4
O9 K06 Si9 26.96(4) 4 4
F4 K06 Si9 89.01(2) . 4
O64 K06 Si9 128.75(2) 3_656 4
O43 K06 Si9 118.20(3) . 4
O32 K06 Si9 28.79(3) 4 4
O32 K06 Si9 94.48(4) . 4
O54 K06 Si9 147.90(4) 2_656 4
O54 K06 Si9 78.06(3) 3_656 4
Si9 K06 Si9 98.92(3) . 4
O9 K06 O57 85.16(5) . .
O9 K06 O57 157.80(6) 4 .
F4 K06 O57 136.52(3) . .
O64 K06 O57 87.41(5) 3_656 .
O43 K06 O57 47.59(4) . .
O32 K06 O57 102.48(5) 4 .
O32 K06 O57 53.21(4) . .
O54 K06 O57 78.82(4) 2_656 .
O54 K06 O57 134.90(5) 3_656 .
Si9 K06 O57 70.63(3) . .
Si9 K06 O57 130.88(4) 4 .
O7 K07 O7 85.76(7) 3_655 .
O7 K07 O8 134.02(4) 3_655 3_655
O7 K07 O8 134.02(4) . 3_655
O7 K07 O48 112.03(5) 3_655 2_655
O7 K07 O48 54.09(4) . 2_655
O8 K07 O48 110.89(5) 3_655 2_655
O7 K07 O48 54.09(4) 3_655 3_655
O7 K07 O48 112.03(5) . 3_655
O8 K07 O48 110.89(5) 3_655 3_655
O48 K07 O48 89.91(7) 2_655 3_655
O7 K07 O4 94.94(5) 3_655 3_655
O7 K07 O4 165.58(4) . 3_655
O8 K07 O4 52.88(4) 3_655 3_655
O48 K07 O4 112.93(5) 2_655 3_655
O48 K07 O4 58.23(5) 3_655 3_655
O7 K07 O4 165.58(4) 3_655 2_655
O7 K07 O4 94.94(5) . 2_655
O8 K07 O4 52.88(4) 3_655 2_655
O48 K07 O4 58.23(5) 2_655 2_655
O48 K07 O4 112.93(5) 3_655 2_655
O4 K07 O4 80.83(6) 3_655 2_655
O7 K07 O37 99.99(4) 3_655 .
O7 K07 O37 51.50(3) . .
O8 K07 O37 92.99(5) 3_655 .
O48 K07 O37 93.61(5) 2_655 .
O48 K07 O37 152.80(5) 3_655 .
O4 K07 O37 141.85(5) 3_655 .
O4 K07 O37 91.60(4) 2_655 .
O7 K07 O37 51.50(3) 3_655 4
O7 K07 O37 99.99(4) . 4
O8 K07 O37 92.99(5) 3_655 4
O48 K07 O37 152.80(5) 2_655 4
O48 K07 O37 93.61(5) 3_655 4
O4 K07 O37 91.60(4) 3_655 4
O4 K07 O37 141.85(5) 2_655 4
O37 K07 O37 71.59(6) . 4
O7 K07 F10 108.78(3) 3_655 3_655
O7 K07 F10 108.78(3) . 3_655
O8 K07 F10 82.45(6) 3_655 3_655
O48 K07 F10 56.01(4) 2_655 3_655
O48 K07 F10 56.01(4) 3_655 3_655
O4 K07 F10 57.36(4) 3_655 3_655
O4 K07 F10 57.36(4) 2_655 3_655
O37 K07 F10 144.02(3) . 3_655
O37 K07 F10 144.02(3) 4 3_655
O7 K07 Si4 105.90(4) 3_655 3_655
O7 K07 Si4 162.20(3) . 3_655
O8 K07 Si4 30.051(16) 3_655 3_655
O48 K07 Si4 129.07(4) 2_655 3_655
O48 K07 Si4 85.77(4) 3_655 3_655
O4 K07 Si4 29.70(4) 3_655 3_655
O4 K07 Si4 77.14(4) 2_655 3_655
O37 K07 Si4 112.15(4) . 3_655
O37 K07 Si4 78.12(4) 4 3_655
F10 K07 Si4 80.61(4) 3_655 3_655
O7 K07 Si4 162.20(3) 3_655 2_655
O7 K07 Si4 105.90(4) . 2_655
O8 K07 Si4 30.051(16) 3_655 2_655
O48 K07 Si4 85.77(4) 2_655 2_655
O48 K07 Si4 129.07(4) 3_655 2_655
O4 K07 Si4 77.14(4) 3_655 2_655
O4 K07 Si4 29.70(4) 2_655 2_655
O37 K07 Si4 78.12(4) . 2_655
O37 K07 Si4 112.14(4) 4 2_655
F10 K07 Si4 80.61(4) 3_655 2_655
Si4 K07 Si4 59.77(3) 3_655 2_655
O47 K08 O47 91.14(8) 4 .
O47 K08 O10 114.73(6) 4 .
O47 K08 O10 56.65(5) . .
O47 K08 O10 56.65(5) 4 4
O47 K08 O10 114.73(6) . 4
O10 K08 O10 85.35(7) . 4
O47 K08 O23 62.84(5) 4 4
O47 K08 O23 124.41(6) . 4
O10 K08 O23 176.93(5) . 4
O10 K08 O23 91.65(5) 4 4
O47 K08 O23 124.41(6) 4 .
O47 K08 O23 62.84(5) . .
O10 K08 O23 91.65(5) . .
O10 K08 O23 176.93(5) 4 .
O23 K08 O23 91.33(7) 4 .
O47 K08 O51 112.81(5) 4 .
O47 K08 O51 112.81(5) . .
O10 K08 O51 131.23(4) . .
O10 K08 O51 131.24(4) 4 .
O23 K08 O51 51.59(4) 4 .
O23 K08 O51 51.59(4) . .
O47 K08 F1 64.64(5) 4 .
O47 K08 F1 64.63(5) . .
O10 K08 F1 121.28(4) . .
O10 K08 F1 121.28(4) 4 .
O23 K08 F1 59.88(4) 4 .
O23 K08 F1 59.88(4) . .
O51 K08 F1 71.36(6) . .
O47 K08 Si18 134.40(5) 4 .
O47 K08 Si18 89.62(4) . .
O10 K08 Si18 103.42(4) . .
O10 K08 Si18 154.51(4) 4 .
O23 K08 Si18 79.58(4) 4 .
O23 K08 Si18 27.34(4) . .
O51 K08 Si18 29.659(15) . .
F1 K08 Si18 74.80(4) . .
O47 K08 Si18 89.62(4) 4 4
O47 K08 Si18 134.40(5) . 4
O10 K08 Si18 154.51(4) . 4
O10 K08 Si18 103.42(4) 4 4
O23 K08 Si18 27.34(4) 4 4
O23 K08 Si18 79.58(4) . 4
O51 K08 Si18 29.659(15) . 4
F1 K08 Si18 74.80(4) . 4
Si18 K08 Si18 59.28(3) . 4
O47 K08 Si8 27.90(4) 4 4
O47 K08 Si8 100.53(4) . 4
O10 K08 Si8 98.05(4) . 4
O10 K08 Si8 29.26(3) 4 4
O23 K08 Si8 78.97(4) 4 4
O23 K08 Si8 151.28(5) . 4
O51 K08 Si8 129.93(2) . 4
F1 K08 Si8 92.28(3) . 4
Si18 K08 Si8 158.42(3) . 4
Si18 K08 Si8 101.03(2) 4 4
O47 K08 Si8 100.53(4) 4 .
O47 K08 Si8 27.90(4) . .
O10 K08 Si8 29.26(3) . .
O10 K08 Si8 98.04(4) 4 .
O23 K08 Si8 151.28(5) 4 .
O23 K08 Si8 78.98(4) . .
O51 K08 Si8 129.93(2) . .
F1 K08 Si8 92.28(3) . .
Si18 K08 Si8 101.03(2) . .
Si18 K08 Si8 158.42(3) 4 .
Si8 K08 Si8 96.62(3) 4 .
O28 K09 O20 66.78(8) . .
O28 K09 O32 98.54(5) . .
O20 K09 O32 56.22(4) . .
O28 K09 O32 98.54(5) . 4_565
O20 K09 O32 56.22(4) . 4_565
O32 K09 O32 93.53(7) . 4_565
O28 K09 O65 100.66(6) . 4_565
O20 K09 O65 140.04(3) . 4_565
O32 K09 O65 159.35(5) . 4_565
O32 K09 O65 91.06(4) 4_565 4_565
O28 K09 O65 100.66(6) . .
O20 K09 O65 140.04(3) . .
O32 K09 O65 91.07(4) . .
O32 K09 O65 159.35(5) 4_565 .
O65 K09 O65 78.02(7) 4_565 .
O28 K09 F19 143.02(7) . .
O20 K09 F19 76.24(6) . .
O32 K09 F19 58.60(4) . .
O32 K09 F19 58.60(4) 4_565 .
O65 K09 F19 107.83(5) 4_565 .
O65 K09 F19 107.83(5) . .
O28 K09 O25 136.89(3) . 4_565
O20 K09 O25 109.90(5) . 4_565
O32 K09 O25 115.21(5) . 4_565
O32 K09 O25 55.50(4) 4_565 4_565
O65 K09 O25 52.63(5) 4_565 4_565
O65 K09 O25 104.50(5) . 4_565
F19 K09 O25 56.72(4) . 4_565
O28 K09 O25 136.89(3) . .
O20 K09 O25 109.90(5) . .
O32 K09 O25 55.50(4) . .
O32 K09 O25 115.21(5) 4_565 .
O65 K09 O25 104.50(5) 4_565 .
O65 K09 O25 52.63(5) . .
F19 K09 O25 56.72(4) . .
O25 K09 O25 85.85(6) 4_565 .
O28 K09 Si9 72.39(5) . 4_565
O20 K09 Si9 31.075(16) . 4_565
O32 K09 Si9 83.31(4) . 4_565
O32 K09 Si9 29.95(4) 4_565 4_565
O65 K09 Si9 109.72(4) 4_565 4_565
O65 K09 Si9 170.19(4) . 4_565
F19 K09 Si9 76.06(4) . 4_565
O25 K09 Si9 85.19(4) 4_565 4_565
O25 K09 Si9 128.12(4) . 4_565
O28 K09 Si9 72.39(5) . .
O20 K09 Si9 31.075(16) . .
O32 K09 Si9 29.95(4) . .
O32 K09 Si9 83.31(4) 4_565 .
O65 K09 Si9 170.19(4) 4_565 .
O65 K09 Si9 109.72(4) . .
F19 K09 Si9 76.06(4) . .
O25 K09 Si9 128.12(4) 4_565 .
O25 K09 Si9 85.19(4) . .
Si9 K09 Si9 61.96(3) 4_565 .
O28 K09 Si10 28.761(15) . 4_565
O20 K09 Si10 70.83(5) . 4_565
O32 K09 Si10 119.54(4) . 4_565
O32 K09 Si10 78.03(4) 4_565 4_565
O65 K09 Si10 81.11(4) 4_565 4_565
O65 K09 Si10 116.79(4) . 4_565
F19 K09 Si10 135.36(3) . 4_565
O25 K09 Si10 108.14(3) 4_565 4_565
O25 K09 Si10 165.08(4) . 4_565
Si9 K09 Si10 60.16(2) 4_565 4_565
Si9 K09 Si10 89.85(3) . 4_565
O40 K10 O40 103.06(8) 4 .
O40 K10 O19 108.49(5) 4 .
O40 K10 O19 108.49(5) . .
O40 K10 F2 62.95(4) 4 .
O40 K10 F2 62.95(4) . .
O19 K10 F2 77.64(6) . .
O40 K10 O49 115.30(6) 4 .
O40 K10 O49 56.22(5) . .
O19 K10 O49 135.74(4) . .
F2 K10 O49 116.78(5) . .
O40 K10 O49 56.22(5) 4 4
O40 K10 O49 115.30(6) . 4
O19 K10 O49 135.74(4) . 4
F2 K10 O49 116.78(5) . 4
O49 K10 O49 77.81(6) . 4
O40 K10 O30 128.46(4) 4 .
O40 K10 O30 128.47(4) . .
O19 K10 O30 58.71(7) . .
F2 K10 O30 136.35(6) . .
O49 K10 O30 96.43(5) . .
O49 K10 O30 96.43(5) 4 .
O40 K10 O13 157.49(6) 4 .
O40 K10 O13 85.47(5) . .
O19 K10 O13 49.08(4) . .
F2 K10 O13 104.57(4) . .
O49 K10 O13 86.84(5) . .
O49 K10 O13 138.53(5) 4 .
O30 K10 O13 46.93(4) . .
O40 K10 O13 85.47(5) 4 4
O40 K10 O13 157.49(6) . 4
O19 K10 O13 49.08(4) . 4
F2 K10 O13 104.57(4) . 4
O49 K10 O13 138.53(5) . 4
O49 K10 O13 86.84(5) 4 4
O30 K10 O13 46.93(4) . 4
O13 K10 O13 79.65(7) . 4
O40 K10 O18 117.05(6) 4 .
O40 K10 O18 58.80(5) . .
O19 K10 O18 49.71(4) . .
F2 K10 O18 55.20(4) . .
O49 K10 O18 101.98(4) . .
O49 K10 O18 171.12(5) 4 .
O30 K10 O18 92.42(5) . .
O13 K10 O18 49.91(4) . .
O13 K10 O18 98.73(5) 4 .
O40 K10 O18 58.79(5) 4 4
O40 K10 O18 117.05(6) . 4
O19 K10 O18 49.71(4) . 4
F2 K10 O18 55.20(4) . 4
O49 K10 O18 171.12(5) . 4
O49 K10 O18 101.98(4) 4 4
O30 K10 O18 92.42(5) . 4
O13 K10 O18 98.73(5) . 4
O13 K10 O18 49.91(4) 4 4
O18 K10 O18 76.82(6) . 4
O40 K10 Si2 27.41(4) 4 4
O40 K10 Si2 108.20(5) . 4
O19 K10 Si2 128.26(2) . 4
F2 K10 Si2 88.05(3) . 4
O49 K10 Si2 95.15(4) . 4
O49 K10 Si2 29.19(3) 4 4
O30 K10 Si2 117.86(3) . 4
O13 K10 Si2 164.77(4) . 4
O13 K10 Si2 89.04(4) 4 4
O18 K10 Si2 143.25(4) . 4
O18 K10 Si2 81.31(3) 4 4
O23 K11 O23 102.59(8) 4_565 .
O23 K11 O34 131.69(6) 4_565 .
O23 K11 O34 59.29(5) . .
O23 K11 O34 59.29(5) 4_565 4_565
O23 K11 O34 131.69(6) . 4_565
O34 K11 O34 97.77(7) . 4_565
O23 K11 F17 120.21(4) 4_565 .
O23 K11 F17 120.21(4) . .
O34 K11 F17 61.13(4) . .
O34 K11 F17 61.13(4) 4_565 .
O23 K11 Si18 114.92(5) 4_565 .
O23 K11 Si18 28.80(4) . .
O34 K11 Si18 31.49(4) . .
O34 K11 Si18 113.58(4) 4_565 .
F17 K11 Si18 92.48(3) . .
O23 K11 Si18 28.80(4) 4_565 4_565
O23 K11 Si18 114.92(5) . 4_565
O34 K11 Si18 113.58(4) . 4_565
O34 K11 Si18 31.49(4) 4_565 4_565
F17 K11 Si18 92.48(3) . 4_565
Si18 K11 Si18 112.48(4) . 4_565
O23 K11 O24 164.75(5) 4_565 .
O23 K11 O24 90.72(5) . .
O34 K11 O24 61.85(5) . .
O34 K11 O24 116.58(5) 4_565 .
F17 K11 O24 56.54(4) . .
Si18 K11 O24 80.33(3) . .
Si18 K11 O24 147.82(4) 4_565 .
O23 K11 O24 90.72(5) 4_565 4_565
O23 K11 O24 164.75(5) . 4_565
O34 K11 O24 116.58(5) . 4_565
O34 K11 O24 61.85(5) 4_565 4_565
F17 K11 O24 56.54(4) . 4_565
Si18 K11 O24 147.82(4) . 4_565
Si18 K11 O24 80.33(3) 4_565 4_565
O24 K11 O24 75.19(6) . 4_565
O23 K11 O16 89.41(5) 4_565 3_666
O23 K11 O16 89.41(5) . 3_666
O34 K11 O16 130.38(4) . 3_666
O34 K11 O16 130.38(4) 4_565 3_666
F17 K11 O16 127.37(6) . 3_666
Si18 K11 O16 114.45(3) . 3_666
Si18 K11 O16 114.45(3) 4_565 3_666
O24 K11 O16 83.25(5) . 3_666
O24 K11 O16 83.25(5) 4_565 3_666
O23 K11 O2 119.52(4) 4_565 1_655
O23 K11 O2 119.52(4) . 1_655
O34 K11 O2 107.48(5) . 1_655
O34 K11 O2 107.48(5) 4_565 1_655
F17 K11 O2 74.43(6) . 1_655
Si18 K11 O2 123.05(2) . 1_655
Si18 K11 O2 123.05(2) 4_565 1_655
O24 K11 O2 45.88(4) . 1_655
O24 K11 O2 45.88(4) 4_565 1_655
O16 K11 O2 52.94(6) 3_666 1_655
O23 K11 K16 55.55(4) 4_565 .
O23 K11 K16 55.55(4) . .
O34 K11 K16 80.58(4) . .
O34 K11 K16 80.58(4) 4_565 .
F17 K11 K16 118.34(4) . .
Si18 K11 K16 59.459(19) . .
Si18 K11 K16 59.458(19) 4_565 .
O24 K11 K16 139.69(3) . .
O24 K11 K16 139.70(3) 4_565 .
O16 K11 K16 114.28(5) 3_666 .
O2 K11 K16 167.22(5) 1_655 .
O8 K12 O51 67.52(8) 3_655 3_655
O8 K12 O31 100.98(6) 3_655 .
O51 K12 O31 137.75(3) 3_655 .
O8 K12 O31 100.98(6) 3_655 4
O51 K12 O31 137.75(3) 3_655 4
O31 K12 O31 83.35(7) . 4
O8 K12 O34 99.88(6) 3_655 3_655
O51 K12 O34 55.55(4) 3_655 3_655
O31 K12 O34 158.85(6) . 3_655
O31 K12 O34 89.36(5) 4 3_655
O8 K12 O34 99.88(6) 3_655 2_655
O51 K12 O34 55.55(4) 3_655 2_655
O31 K12 O34 89.36(5) . 2_655
O31 K12 O34 158.85(6) 4 2_655
O34 K12 O34 90.43(7) 3_655 2_655
O8 K12 F8 68.34(7) 3_655 .
O51 K12 F8 135.87(7) 3_655 .
O31 K12 F8 53.06(4) . .
O31 K12 F8 53.06(4) 4 .
O34 K12 F8 134.29(3) 3_655 .
O34 K12 F8 134.29(3) 2_655 .
O8 K12 Si18 73.17(5) 3_655 3_655
O51 K12 Si18 30.260(16) 3_655 3_655
O31 K12 Si18 167.83(4) . 3_655
O31 K12 Si18 108.05(4) 4 3_655
O34 K12 Si18 30.30(4) 3_655 3_655
O34 K12 Si18 81.33(4) 2_655 3_655
F8 K12 Si18 130.58(4) . 3_655
O8 K12 Si18 73.17(5) 3_655 2_655
O51 K12 Si18 30.260(16) 3_655 2_655
O31 K12 Si18 108.05(4) . 2_655
O31 K12 Si18 167.83(4) 4 2_655
O34 K12 Si18 81.33(4) 3_655 2_655
O34 K12 Si18 30.30(4) 2_655 2_655
F8 K12 Si18 130.58(4) . 2_655
Si18 K12 Si18 60.27(3) 3_655 2_655
O8 K12 O15 141.44(3) 3_655 3_655
O51 K12 O15 110.29(5) 3_655 3_655
O31 K12 O15 103.10(5) . 3_655
O31 K12 O15 53.17(5) 4 3_655
O34 K12 O15 57.33(5) 3_655 3_655
O34 K12 O15 110.00(5) 2_655 3_655
F8 K12 O15 103.91(4) . 3_655
Si18 K12 O15 87.53(4) 3_655 3_655
Si18 K12 O15 125.49(4) 2_655 3_655
O8 K12 O15 141.44(3) 3_655 2_655
O51 K12 O15 110.29(5) 3_655 2_655
O31 K12 O15 53.17(5) . 2_655
O31 K12 O15 103.10(5) 4 2_655
O34 K12 O15 110.00(5) 3_655 2_655
O34 K12 O15 57.33(5) 2_655 2_655
F8 K12 O15 103.91(4) . 2_655
Si18 K12 O15 125.49(4) 3_655 2_655
Si18 K12 O15 87.53(4) 2_655 2_655
O15 K12 O15 76.80(6) 3_655 2_655
O8 K12 Si4 29.965(15) 3_655 2_655
O51 K12 Si4 70.34(5) 3_655 2_655
O31 K12 Si4 80.62(4) . 2_655
O31 K12 Si4 120.08(4) 4 2_655
O34 K12 Si4 119.95(4) 3_655 2_655
O34 K12 Si4 77.90(4) 2_655 2_655
F8 K12 Si4 71.68(4) . 2_655
Si18 K12 Si4 89.72(3) 3_655 2_655
Si18 K12 Si4 59.58(2) 2_655 2_655
O15 K12 Si4 171.10(4) 3_655 2_655
O15 K12 Si4 111.56(3) 2_655 2_655
O30 K13 O19 66.97(7) . .
O30 K13 O21 140.08(3) . .
O19 K13 O21 102.57(5) . .
O30 K13 O21 140.08(3) . 4
O19 K13 O21 102.57(5) . 4
O21 K13 O21 78.91(7) . 4
O30 K13 F14 77.20(6) . 1_455
O19 K13 F14 144.18(7) . 1_455
O21 K13 F14 104.90(5) . 1_455
O21 K13 F14 104.90(5) 4 1_455
O30 K13 O52 56.16(4) . 4
O19 K13 O52 98.28(5) . 4
O21 K13 O52 158.00(5) . 4
O21 K13 O52 89.85(4) 4 4
F14 K13 O52 59.55(4) 1_455 4
O30 K13 O52 56.16(4) . .
O19 K13 O52 98.28(5) . .
O21 K13 O52 89.85(4) . .
O21 K13 O52 158.00(5) 4 .
F14 K13 O52 59.55(4) 1_455 .
O52 K13 O52 94.04(6) 4 .
O30 K13 O13 49.81(4) . 4
O19 K13 O13 49.59(4) . 4
O21 K13 O13 149.05(5) . 4
O21 K13 O13 93.17(4) 4 4
F14 K13 O13 106.05(4) 1_455 4
O52 K13 O13 49.30(4) 4 4
O52 K13 O13 105.76(5) . 4
O30 K13 O13 49.81(4) . .
O19 K13 O13 49.58(4) . .
O21 K13 O13 93.17(5) . .
O21 K13 O13 149.05(5) 4 .
F14 K13 O13 106.05(4) 1_455 .
O52 K13 O13 105.76(5) 4 .
O52 K13 O13 49.30(4) . .
O13 K13 O13 78.29(6) 4 .
O30 K13 Si6 30.890(15) . 4
O19 K13 Si6 70.56(5) . 4
O21 K13 Si6 169.95(4) . 4
O21 K13 Si6 109.40(4) 4 4
F14 K13 Si6 78.86(4) 1_455 4
O52 K13 Si6 31.27(3) 4 4
O52 K13 Si6 84.05(4) . 4
O13 K13 Si6 28.78(3) 4 4
O13 K13 Si6 76.80(4) . 4
O30 K13 Si6 30.889(15) . .
O19 K13 Si6 70.56(5) . .
O21 K13 Si6 109.40(4) . .
O21 K13 Si6 169.95(4) 4 .
F14 K13 Si6 78.86(4) 1_455 .
O52 K13 Si6 84.05(4) 4 .
O52 K13 Si6 31.27(3) . .
O13 K13 Si6 76.80(4) 4 .
O13 K13 Si6 28.78(3) . .
Si6 K13 Si6 61.78(3) 4 .
O30 K13 O24 109.31(5) . 4_455
O19 K13 O24 135.80(3) . 4_455
O21 K13 O24 104.19(5) . 4_455
O21 K13 O24 50.34(5) 4 4_455
F14 K13 O24 56.68(4) 1_455 4_455
O52 K13 O24 54.88(4) 4 4_455
O52 K13 O24 116.21(5) . 4_455
O13 K13 O24 92.83(4) 4 4_455
O13 K13 O24 157.94(5) . 4_455
Si6 K13 O24 85.70(4) 4 4_455
Si6 K13 O24 129.69(4) . 4_455
O41 K14 O41 91.38(8) . 4_565
O41 K14 F3 64.06(5) . .
O41 K14 F3 64.06(5) 4_565 .
O41 K14 O50 55.92(5) . .
O41 K14 O50 114.76(6) 4_565 .
F3 K14 O50 119.99(4) . .
O41 K14 O50 114.76(6) . 4_565
O41 K14 O50 55.92(5) 4_565 4_565
F3 K14 O50 119.99(4) . 4_565
O50 K14 O50 86.33(7) . 4_565
O41 K14 O42 62.71(5) . .
O41 K14 O42 127.43(6) 4_565 .
F3 K14 O42 63.48(4) . .
O50 K14 O42 88.66(5) . .
O50 K14 O42 174.93(5) 4_565 .
O41 K14 O42 127.43(6) . 4_565
O41 K14 O42 62.71(5) 4_565 4_565
F3 K14 O42 63.48(4) . 4_565
O50 K14 O42 174.93(5) . 4_565
O50 K14 O42 88.66(5) 4_565 4_565
O42 K14 O42 96.33(7) . 4_565
O41 K14 O44 115.05(5) . .
O41 K14 O44 115.06(5) 4_565 .
F3 K14 O44 76.08(6) . .
O50 K14 O44 129.48(4) . .
O50 K14 O44 129.48(4) 4_565 .
O42 K14 O44 53.96(4) . .
O42 K14 O44 53.96(4) 4_565 .
O41 K14 Si12 135.88(5) . 4_565
O41 K14 Si12 90.48(4) 4_565 4_565
F3 K14 Si12 77.47(4) . 4_565
O50 K14 Si12 153.42(4) . 4_565
O50 K14 Si12 102.47(4) 4_565 4_565
O42 K14 Si12 81.71(4) . 4_565
O42 K14 Si12 28.00(4) 4_565 4_565
O44 K14 Si12 29.726(15) . 4_565
O41 K14 Si12 90.48(4) . .
O41 K14 Si12 135.89(5) 4_565 .
F3 K14 Si12 77.47(4) . .
O50 K14 Si12 102.47(4) . .
O50 K14 Si12 153.42(4) 4_565 .
O42 K14 Si12 28.00(4) . .
O42 K14 Si12 81.71(4) 4_565 .
O44 K14 Si12 29.726(15) . .
Si12 K14 Si12 59.44(3) 4_565 .
O41 K14 Si5 101.05(5) . 4_565
O41 K14 Si5 27.47(4) 4_565 4_565
F3 K14 Si5 91.29(3) . 4_565
O50 K14 Si5 98.96(4) . 4_565
O50 K14 Si5 28.86(3) 4_565 4_565
O42 K14 Si5 153.78(4) . 4_565
O42 K14 Si5 76.92(4) 4_565 4_565
O44 K14 Si5 129.996(19) . 4_565
Si12 K14 Si5 100.56(2) 4_565 4_565
Si12 K14 Si5 158.56(3) . 4_565
O41 K14 Si5 27.47(4) . .
O41 K14 Si5 101.05(5) 4_565 .
F3 K14 Si5 91.29(3) . .
O50 K14 Si5 28.86(3) . .
O50 K14 Si5 98.96(4) 4_565 .
O42 K14 Si5 76.92(4) . .
O42 K14 Si5 153.78(4) 4_565 .
O44 K14 Si5 129.996(19) . .
Si12 K14 Si5 158.56(3) 4_565 .
Si12 K14 Si5 100.56(2) . .
Si5 K14 Si5 97.86(3) 4_565 .
O35 K15 O35 89.53(7) 4_565 .
O35 K15 O11 101.11(5) 4_565 .
O35 K15 O11 101.11(5) . .
O35 K15 O22 55.61(4) 4_565 3_566
O35 K15 O22 117.09(5) . 3_566
O11 K15 O22 132.86(3) . 3_566
O35 K15 O22 117.09(5) 4_565 .
O35 K15 O22 55.61(4) . .
O11 K15 O22 132.86(3) . .
O22 K15 O22 92.85(6) 3_566 .
O35 K15 F12 58.48(4) 4_565 .
O35 K15 F12 58.48(4) . .
O11 K15 F12 63.16(6) . .
O22 K15 F12 114.00(3) 3_566 .
O22 K15 F12 114.00(3) . .
O35 K15 O58 152.55(6) 4_565 .
O35 K15 O58 92.39(5) . .
O11 K15 O58 51.68(4) . .
O22 K15 O58 143.16(4) 3_566 .
O22 K15 O58 86.00(4) . .
F12 K15 O58 99.83(5) . .
O35 K15 O58 92.39(5) 4_565 4_565
O35 K15 O58 152.55(6) . 4_565
O11 K15 O58 51.68(4) . 4_565
O22 K15 O58 86.00(4) 3_566 4_565
O22 K15 O58 143.16(4) . 4_565
F12 K15 O58 99.83(5) . 4_565
O58 K15 O58 73.81(6) . 4_565
O35 K15 Si7 83.33(4) 4_565 4_565
O35 K15 Si7 125.17(5) . 4_565
O11 K15 Si7 30.001(17) . 4_565
O22 K15 Si7 102.87(3) 3_566 4_565
O22 K15 Si7 159.19(3) . 4_565
F12 K15 Si7 72.03(4) . 4_565
O58 K15 Si7 73.23(4) . 4_565
O58 K15 Si7 28.52(3) 4_565 4_565
O35 K15 Si7 125.17(5) 4_565 .
O35 K15 Si7 83.33(4) . .
O11 K15 Si7 30.001(17) . .
O22 K15 Si7 159.19(3) 3_566 .
O22 K15 Si7 102.87(3) . .
F12 K15 Si7 72.03(4) . .
O58 K15 Si7 28.52(3) . .
O58 K15 Si7 73.23(4) 4_565 .
Si7 K15 Si7 58.87(3) 4_565 .
O35 K15 O38 114.31(5) 4_565 .
O35 K15 O38 56.02(5) . .
O11 K15 O38 48.54(4) . .
O22 K15 O38 169.28(4) 3_566 .
O22 K15 O38 89.08(4) . .
F12 K15 O38 55.84(4) . .
O58 K15 O38 47.49(4) . .
O58 K15 O38 98.74(5) 4_565 .
Si7 K15 O38 78.02(4) 4_565 .
Si7 K15 O38 27.76(3) . .
O35 K15 O38 56.02(5) 4_565 4_565
O35 K15 O38 114.31(5) . 4_565
O11 K15 O38 48.54(4) . 4_565
O22 K15 O38 89.08(4) 3_566 4_565
O22 K15 O38 169.28(4) . 4_565
F12 K15 O38 55.84(4) . 4_565
O58 K15 O38 98.74(5) . 4_565
O58 K15 O38 47.49(4) 4_565 4_565
Si7 K15 O38 27.76(3) 4_565 4_565
Si7 K15 O38 78.02(4) . 4_565
O38 K15 O38 87.13(6) . 4_565
O3 K16 O3 107.30(9) . 4_565
O3 K16 O23 57.92(5) . .
O3 K16 O23 128.22(6) 4_565 .
O3 K16 O23 128.22(6) . 4_565
O3 K16 O23 57.92(5) 4_565 4_565
O23 K16 O23 91.08(7) . 4_565
O3 K16 O45 84.57(5) . .
O3 K16 O45 168.11(5) 4_565 .
O23 K16 O45 57.58(5) . .
O23 K16 O45 114.51(5) 4_565 .
O3 K16 O45 168.11(5) . 4_565
O3 K16 O45 84.58(5) 4_565 4_565
O23 K16 O45 114.51(5) . 4_565
O23 K16 O45 57.58(5) 4_565 4_565
O45 K16 O45 83.54(6) . 4_565
O3 K16 F7 116.10(4) . .
O3 K16 F7 116.10(4) 4_565 .
O23 K16 F7 58.56(4) . .
O23 K16 F7 58.56(4) 4_565 .
O45 K16 F7 56.02(4) . .
O45 K16 F7 56.02(4) 4_565 .
O3 K16 Si18 115.29(5) . 4_565
O3 K16 Si18 32.72(4) 4_565 4_565
O23 K16 Si18 103.55(4) . 4_565
O23 K16 Si18 27.14(4) 4_565 4_565
O45 K16 Si18 141.36(4) . 4_565
O45 K16 Si18 74.45(4) 4_565 4_565
F7 K16 Si18 85.36(3) . 4_565
O3 K16 Si18 32.72(4) . .
O3 K16 Si18 115.29(5) 4_565 .
O23 K16 Si18 27.14(4) . .
O23 K16 Si18 103.55(4) 4_565 .
O45 K16 Si18 74.45(4) . .
O45 K16 Si18 141.36(4) 4_565 .
F7 K16 Si18 85.36(3) . .
Si18 K16 Si18 103.91(3) 4_565 .
O3 K16 O28 120.84(5) . .
O3 K16 O28 120.84(5) 4_565 .
O23 K16 O28 106.59(5) . .
O23 K16 O28 106.59(5) 4_565 .
O45 K16 O28 50.13(4) . .
O45 K16 O28 50.13(4) 4_565 .
F7 K16 O28 72.20(5) . .
Si18 K16 O28 123.84(2) 4_565 .
Si18 K16 O28 123.85(2) . .
O3 K16 K11 81.58(4) . .
O3 K16 K11 81.58(4) 4_565 .
O23 K16 K11 48.96(4) . .
O23 K16 K11 48.96(4) 4_565 .
O45 K16 K11 100.17(4) . .
O45 K16 K11 100.17(4) 4_565 .
F7 K16 K11 62.23(4) . .
Si18 K16 K11 54.670(18) 4_565 .
Si18 K16 K11 54.670(18) . .
O28 K16 K11 134.43(5) . .
O3 K16 Si10 96.27(4) . .
O3 K16 Si10 145.73(5) 4_565 .
O23 K16 Si10 85.31(4) . .
O23 K16 Si10 123.63(4) 4_565 .
O45 K16 Si10 28.13(3) . .
O45 K16 Si10 73.22(4) 4_565 .
F7 K16 Si10 72.39(3) . .
Si18 K16 Si10 147.24(3) 4_565 .
Si18 K16 Si10 98.04(2) . .
O28 K16 Si10 26.502(14) . .
K11 K16 Si10 127.21(2) . .
O14 K17 O31 61.54(4) . 2_655
O14 K17 O31 61.54(4) . 3_665
O31 K17 O31 98.33(7) 2_655 3_665
O14 K17 Si3 34.002(18) . 2_655
O31 K17 Si3 32.19(4) 2_655 2_655
O31 K17 Si3 89.61(4) 3_665 2_655
O14 K17 Si3 34.002(18) . 3_665
O31 K17 Si3 89.61(4) 2_655 3_665
O31 K17 Si3 32.19(4) 3_665 3_665
Si3 K17 Si3 67.39(3) 2_655 3_665
O14 K17 O60 118.26(5) . 4_565
O31 K17 O60 114.55(5) 2_655 4_565
O31 K17 O60 58.41(5) 3_665 4_565
Si3 K17 O60 133.87(5) 2_655 4_565
Si3 K17 O60 90.24(4) 3_665 4_565
O14 K17 O60 118.26(5) . .
O31 K17 O60 58.41(5) 2_655 .
O31 K17 O60 114.55(5) 3_665 .
Si3 K17 O60 90.25(4) 2_655 .
Si3 K17 O60 133.87(5) 3_665 .
O60 K17 O60 76.73(6) 4_565 .
O14 K17 O34 100.62(5) . 4_565
O31 K17 O34 156.27(5) 2_655 4_565
O31 K17 O34 84.67(4) 3_665 4_565
Si3 K17 O34 124.97(4) 2_655 4_565
Si3 K17 O34 80.43(4) 3_665 4_565
O60 K17 O34 87.17(5) 4_565 4_565
O60 K17 O34 141.07(5) . 4_565
O14 K17 O34 100.62(5) . .
O31 K17 O34 84.67(4) 2_655 .
O31 K17 O34 156.27(5) 3_665 .
Si3 K17 O34 80.43(4) 2_655 .
Si3 K17 O34 124.97(4) 3_665 .
O60 K17 O34 141.07(5) 4_565 .
O60 K17 O34 87.17(5) . .
O34 K17 O34 83.58(6) 4_565 .
O14 K17 O3 141.57(4) . 4_565
O31 K17 O3 153.84(5) 2_655 4_565
O31 K17 O3 89.18(5) 3_665 4_565
Si3 K17 O3 173.94(4) 2_655 4_565
Si3 K17 O3 109.01(4) 3_665 4_565
O60 K17 O3 49.50(4) 4_565 4_565
O60 K17 O3 95.65(5) . 4_565
O34 K17 O3 48.99(4) 4_565 4_565
O34 K17 O3 98.45(5) . 4_565
O14 K17 O3 141.57(4) . .
O31 K17 O3 89.19(5) 2_655 .
O31 K17 O3 153.84(5) 3_665 .
Si3 K17 O3 109.01(4) 2_655 .
Si3 K17 O3 173.94(4) 3_665 .
O60 K17 O3 95.65(5) 4_565 .
O60 K17 O3 49.50(4) . .
O34 K17 O3 98.45(5) 4_565 .
O34 K17 O3 48.99(4) . .
O3 K17 O3 74.11(7) 4_565 .
O14 K17 F6 82.34(6) . 3_665
O31 K17 F6 59.52(4) 2_655 3_665
O31 K17 F6 59.52(4) 3_665 3_665
Si3 K17 F6 79.63(3) 2_655 3_665
Si3 K17 F6 79.63(3) 3_665 3_665
O60 K17 F6 56.20(4) 4_565 3_665
O60 K17 F6 56.20(4) . 3_665
O34 K17 F6 137.78(3) 4_565 3_665
O34 K17 F6 137.78(3) . 3_665
O3 K17 F6 104.82(4) 4_565 3_665
O3 K17 F6 104.82(4) . 3_665
O48 K18 O48 102.83(8) . 4
O48 K18 F10 63.46(4) . .
O48 K18 F10 63.46(4) 4 .
O48 K18 O37 58.43(5) . .
O48 K18 O37 119.80(6) 4 .
F10 K18 O37 120.86(5) . .
O48 K18 O37 119.80(6) . 4
O48 K18 O37 58.43(5) 4 4
F10 K18 O37 120.87(5) . 4
O37 K18 O37 81.49(7) . 4
O48 K18 O1 104.94(5) . .
O48 K18 O1 104.94(5) 4 .
F10 K18 O1 70.19(6) . .
O37 K18 O1 134.30(4) . .
O37 K18 O1 134.30(4) 4 .
O48 K18 Si1 109.26(5) . 4
O48 K18 Si1 29.08(4) 4 4
F10 K18 Si1 90.71(3) . 4
O37 K18 Si1 98.08(4) . 4
O37 K18 Si1 30.17(4) 4 4
O1 K18 Si1 127.18(2) . 4
O48 K18 Si1 29.08(4) . .
O48 K18 Si1 109.26(5) 4 .
F10 K18 Si1 90.71(3) . .
O37 K18 Si1 30.17(4) . .
O37 K18 Si1 98.08(4) 4 .
O1 K18 Si1 127.19(2) . .
Si1 K18 Si1 100.70(4) 4 .
O48 K18 O65 55.86(5) . .
O48 K18 O65 118.82(5) 4 .
F10 K18 O65 55.73(4) . .
O37 K18 O65 97.18(4) . .
O37 K18 O65 175.00(5) 4 .
O1 K18 O65 49.50(4) . .
Si1 K18 O65 146.28(4) 4 .
Si1 K18 O65 78.70(3) . .
O48 K18 O65 118.83(5) . 4
O48 K18 O65 55.86(5) 4 4
F10 K18 O65 55.73(4) . 4
O37 K18 O65 175.00(5) . 4
O37 K18 O65 97.18(4) 4 4
O1 K18 O65 49.50(4) . 4
Si1 K18 O65 78.70(3) 4 4
Si1 K18 O65 146.28(4) . 4
O65 K18 O65 83.73(6) . 4
O48 K18 Si17 125.53(5) . 4
O48 K18 Si17 82.34(4) 4 4
F10 K18 Si17 71.92(4) . 4
O37 K18 Si17 157.25(4) . 4
O37 K18 Si17 109.01(4) 4 4
O1 K18 Si17 27.197(14) . 4
Si1 K18 Si17 100.59(2) 4 4
Si1 K18 Si17 152.56(3) . 4
O65 K18 Si17 73.97(4) . 4
O65 K18 Si17 27.62(3) 4 4
O48 K18 Si17 82.34(4) . .
O48 K18 Si17 125.53(5) 4 .
F10 K18 Si17 71.92(4) . .
O37 K18 Si17 109.01(4) . .
O37 K18 Si17 157.25(4) 4 .
O1 K18 Si17 27.197(14) . .
Si1 K18 Si17 152.56(3) 4 .
Si1 K18 Si17 100.59(2) . .
O65 K18 Si17 27.62(3) . .
O65 K18 Si17 73.97(4) 4 .
Si17 K18 Si17 54.38(3) 4 .
F12 K19 O12 118.98(5) . .
F12 K19 O12 118.98(5) . 4_565
O12 K19 O12 88.18(8) . 4_565
F12 K19 O53 65.10(4) . 4_565
O12 K19 O53 120.40(6) . 4_565
O12 K19 O53 54.30(5) 4_565 4_565
F12 K19 O53 65.10(4) . .
O12 K19 O53 54.30(5) . .
O12 K19 O53 120.40(6) 4_565 .
O53 K19 O53 103.06(7) 4_565 .
F12 K19 O63 62.20(5) . 2_656
O12 K19 O63 93.58(5) . 2_656
O12 K19 O63 176.95(6) 4_565 2_656
O53 K19 O63 126.40(5) 4_565 2_656
O53 K19 O63 62.62(5) . 2_656
F12 K19 O63 62.20(5) . 3_666
O12 K19 O63 176.95(6) . 3_666
O12 K19 O63 93.58(5) 4_565 3_666
O53 K19 O63 62.62(5) 4_565 3_666
O53 K19 O63 126.40(5) . 3_666
O63 K19 O63 84.55(7) 2_656 3_666
F12 K19 O16 88.44(6) . .
O12 K19 O16 122.90(5) . .
O12 K19 O16 122.90(5) 4_565 .
O53 K19 O16 116.50(4) 4_565 .
O53 K19 O16 116.50(4) . .
O63 K19 O16 54.05(4) 2_656 .
O63 K19 O16 54.05(4) 3_666 .
F12 K19 Si8 84.41(4) . 3_666
O12 K19 Si8 148.48(4) . 3_666
O12 K19 Si8 98.78(4) 4_565 3_666
O53 K19 Si8 87.62(4) 4_565 3_666
O53 K19 Si8 138.25(5) . 3_666
O63 K19 Si8 78.43(4) 2_656 3_666
O63 K19 Si8 28.70(4) 3_666 3_666
O16 K19 Si8 30.553(16) . 3_666
F12 K19 Si8 84.41(4) . 2_656
O12 K19 Si8 98.78(4) . 2_656
O12 K19 Si8 148.48(4) 4_565 2_656
O53 K19 Si8 138.25(5) 4_565 2_656
O53 K19 Si8 87.62(4) . 2_656
O63 K19 Si8 28.70(4) 2_656 2_656
O63 K19 Si8 78.43(4) 3_666 2_656
O16 K19 Si8 30.553(17) . 2_656
Si8 K19 Si8 60.39(3) 3_666 2_656
F12 K19 Si14 86.99(3) . .
O12 K19 Si14 32.22(4) . .
O12 K19 Si14 101.48(4) 4_565 .
O53 K19 Si14 105.33(4) 4_565 .
O53 K19 Si14 24.28(4) . .
O63 K19 Si14 81.29(4) 2_656 .
O63 K19 Si14 149.18(4) 3_666 .
O16 K19 Si14 131.043(17) . .
Si8 K19 Si14 159.70(3) 3_666 .
Si8 K19 Si14 100.52(2) 2_656 .
F12 K19 Si14 86.99(3) . 4_565
O12 K19 Si14 101.47(4) . 4_565
O12 K19 Si14 32.22(4) 4_565 4_565
O53 K19 Si14 24.28(4) 4_565 4_565
O53 K19 Si14 105.33(4) . 4_565
O63 K19 Si14 149.18(4) 2_656 4_565
O63 K19 Si14 81.29(4) 3_666 4_565
O16 K19 Si14 131.044(17) . 4_565
Si8 K19 Si14 100.52(2) 3_666 4_565
Si8 K19 Si14 159.70(3) 2_656 4_565
Si14 K19 Si14 97.34(3) . 4_565
O15 K20 O15 93.92(7) 2_655 3_655
O15 K20 O27 57.06(5) 2_655 .
O15 K20 O27 112.08(5) 3_655 .
O15 K20 O27 112.08(5) 2_655 4
O15 K20 O27 57.06(5) 3_655 4
O27 K20 O27 77.97(7) . 4
O15 K20 O30 103.72(5) 2_655 3
O15 K20 O30 103.72(5) 3_655 3
O27 K20 O30 139.68(4) . 3
O27 K20 O30 139.68(4) 4 3
O15 K20 O49 89.90(5) 2_655 .
O15 K20 O49 154.76(5) 3_655 .
O27 K20 O49 50.75(5) . .
O27 K20 O49 98.48(5) 4 .
O30 K20 O49 99.55(5) 3 .
O15 K20 O49 154.76(5) 2_655 4
O15 K20 O49 89.91(5) 3_655 4
O27 K20 O49 98.48(5) . 4
O27 K20 O49 50.76(5) 4 4
O30 K20 O49 99.55(5) 3 4
O49 K20 O49 76.63(6) . 4
O15 K20 F14 59.38(4) 2_655 3_655
O15 K20 F14 59.38(4) 3_655 3_655
O27 K20 F14 114.77(5) . 3_655
O27 K20 F14 114.77(5) 4 3_655
O30 K20 F14 68.61(6) 3 3_655
O49 K20 F14 140.77(3) . 3_655
O49 K20 F14 140.77(3) 4 3_655
O15 K20 Si6 126.29(5) 2_655 3
O15 K20 Si6 82.52(4) 3_655 3
O27 K20 Si6 165.27(4) . 3
O27 K20 Si6 110.22(4) 4 3
O30 K20 Si6 29.704(15) 3 3
O49 K20 Si6 114.87(4) . 3
O49 K20 Si6 78.94(4) 4 3
F14 K20 Si6 73.70(3) 3_655 3
O15 K20 Si6 82.52(4) 2_655 2
O15 K20 Si6 126.29(5) 3_655 2
O27 K20 Si6 110.21(4) . 2
O27 K20 Si6 165.27(4) 4 2
O30 K20 Si6 29.704(15) 3 2
O49 K20 Si6 78.94(4) . 2
O49 K20 Si6 114.87(4) 4 2
F14 K20 Si6 73.70(3) 3_655 2
Si6 K20 Si6 59.21(3) 3 2
O15 K20 O62 152.89(5) 2_655 3
O15 K20 O62 86.76(5) 3_655 3
O27 K20 O62 146.33(5) . 3
O27 K20 O62 91.00(5) 4 3
O30 K20 O62 50.24(4) 3 3
O49 K20 O62 100.95(5) . 3
O49 K20 O62 52.19(4) 4 3
F14 K20 O62 98.77(4) 3_655 3
Si6 K20 O62 26.94(3) 3 3
Si6 K20 O62 75.42(4) 2 3
O15 K20 O62 86.76(5) 2_655 2
O15 K20 O62 152.89(5) 3_655 2
O27 K20 O62 91.00(5) . 2
O27 K20 O62 146.33(5) 4 2
O30 K20 O62 50.24(4) 3 2
O49 K20 O62 52.19(4) . 2
O49 K20 O62 100.95(5) 4 2
F14 K20 O62 98.77(4) 3_655 2
Si6 K20 O62 75.42(4) 3 2
Si6 K20 O62 26.94(3) 2 2
O62 K20 O62 80.72(6) 3 2
O27 K21 O27 83.84(7) 4 .
O27 K21 O5 127.81(5) 4 .
O27 K21 O5 127.81(5) . .
O27 K21 O36 174.62(6) 4 .
O27 K21 O36 93.73(5) . .
O5 K21 O36 57.34(5) . .
O27 K21 O36 93.73(5) 4 4
O27 K21 O36 174.62(6) . 4
O5 K21 O36 57.33(5) . 4
O36 K21 O36 88.28(7) . 4
O27 K21 O31 111.45(5) 4 .
O27 K21 O31 57.56(5) . .
O5 K21 O31 120.50(5) . .
O36 K21 O31 63.29(5) . .
O36 K21 O31 119.40(6) 4 .
O27 K21 O31 57.56(5) 4 4
O27 K21 O31 111.45(5) . 4
O5 K21 O31 120.50(5) . 4
O36 K21 O31 119.40(6) . 4
O36 K21 O31 63.29(5) 4 4
O31 K21 O31 84.93(7) . 4
O27 K21 F8 113.71(5) 4 .
O27 K21 F8 113.71(5) . .
O5 K21 F8 91.82(7) . .
O36 K21 F8 62.90(5) . .
O36 K21 F8 62.90(5) 4 .
O31 K21 F8 56.55(4) . .
O31 K21 F8 56.55(4) 4 .
O27 K21 Si5 154.42(5) 4 .
O27 K21 Si5 101.93(4) . .
O5 K21 Si5 31.751(18) . .
O36 K21 Si5 30.86(4) . .
O36 K21 Si5 82.32(4) 4 .
O31 K21 Si5 92.20(4) . .
O31 K21 Si5 137.82(5) 4 .
F8 K21 Si5 87.06(4) . .
O27 K21 Si5 101.93(4) 4 4
O27 K21 Si5 154.42(5) . 4
O5 K21 Si5 31.751(18) . 4
O36 K21 Si5 82.32(4) . 4
O36 K21 Si5 30.86(4) 4 4
O31 K21 Si5 137.81(5) . 4
O31 K21 Si5 92.20(4) 4 4
F8 K21 Si5 87.06(4) . 4
Si5 K21 Si5 62.71(3) . 4
O27 K21 Si3 30.16(4) 4 4
O27 K21 Si3 95.69(4) . 4
O5 K21 Si3 133.368(17) . 4
O36 K21 Si3 146.11(5) . 4
O36 K21 Si3 79.95(4) 4 4
O31 K21 Si3 95.16(4) . 4
O31 K21 Si3 27.87(4) 4 4
F8 K21 Si3 83.55(3) . 4
Si5 K21 Si3 162.20(3) . 4
Si5 K21 Si3 101.62(2) 4 4
O27 K21 Si3 95.69(4) 4 .
O27 K21 Si3 30.16(4) . .
O5 K21 Si3 133.368(17) . .
O36 K21 Si3 79.95(4) . .
O36 K21 Si3 146.11(5) 4 .
O31 K21 Si3 27.87(4) . .
O31 K21 Si3 95.16(4) 4 .
F8 K21 Si3 83.55(3) . .
Si5 K21 Si3 101.62(2) . .
Si5 K21 Si3 162.20(3) 4 .
Si3 K21 Si3 92.32(3) 4 .
O62 K22 O62 98.12(8) 4_665 1_655
O62 K22 O52 63.74(6) 4_665 4_665
O62 K22 O52 128.25(6) 1_655 4_665
O62 K22 O52 128.25(6) 4_665 1_655
O62 K22 O52 63.74(6) 1_655 1_655
O52 K22 O52 89.28(7) 4_665 1_655
O62 K22 Si6 30.78(4) 4_665 4_665
O62 K22 Si6 111.08(5) 1_655 4_665
O52 K22 Si6 33.80(4) 4_665 4_665
O52 K22 Si6 107.63(5) 1_655 4_665
O62 K22 Si6 111.08(5) 4_665 1_655
O62 K22 Si6 30.78(4) 1_655 1_655
O52 K22 Si6 107.63(5) 4_665 1_655
O52 K22 Si6 33.80(4) 1_655 1_655
Si6 K22 Si6 107.57(4) 4_665 1_655
O62 K22 F17 121.16(5) 4_665 .
O62 K22 F17 121.16(5) 1_655 .
O52 K22 F17 57.65(4) 4_665 .
O52 K22 F17 57.65(4) 1_655 .
Si6 K22 F17 91.36(3) 4_665 .
Si6 K22 F17 91.36(3) 1_655 .
O62 K22 F18 57.87(4) 4_665 1_655
O62 K22 F18 57.87(4) 1_655 1_655
O52 K22 F18 121.17(4) 4_665 1_655
O52 K22 F18 121.17(4) 1_655 1_655
Si6 K22 F18 87.40(2) 4_665 1_655
Si6 K22 F18 87.40(2) 1_655 1_655
F17 K22 F18 177.90(4) . 1_655
O62 K22 O14 126.05(4) 4_665 .
O62 K22 O14 126.05(4) 1_655 .
O52 K22 O14 100.74(5) 4_665 .
O52 K22 O14 100.74(5) 1_655 .
Si6 K22 O14 122.74(2) 4_665 .
Si6 K22 O14 122.74(2) 1_655 .
F17 K22 O14 63.95(6) . .
F18 K22 O14 118.15(5) 1_655 .
O62 K22 O15 171.01(5) 4_665 .
O62 K22 O15 90.73(5) 1_655 .
O52 K22 O15 111.73(5) 4_665 .
O52 K22 O15 57.54(5) 1_655 .
Si6 K22 O15 145.52(4) 4_665 .
Si6 K22 O15 77.46(3) 1_655 .
F17 K22 O15 54.17(4) . .
F18 K22 O15 127.08(3) 1_655 .
O14 K22 O15 45.74(3) . .
O62 K22 O15 90.73(5) 4_665 4_565
O62 K22 O15 171.01(5) 1_655 4_565
O52 K22 O15 57.54(5) 4_665 4_565
O52 K22 O15 111.73(5) 1_655 4_565
Si6 K22 O15 77.46(3) 4_665 4_565
Si6 K22 O15 145.52(4) 1_655 4_565
F17 K22 O15 54.17(4) . 4_565
F18 K22 O15 127.09(3) 1_655 4_565
O14 K22 O15 45.74(3) . 4_565
O15 K22 O15 80.38(6) . 4_565
O62 K22 O55 97.18(5) 4_665 3_665
O62 K22 O55 97.18(5) 1_655 3_665
O52 K22 O55 131.31(4) 4_665 3_665
O52 K22 O55 131.31(4) 1_655 3_665
Si6 K22 O55 121.06(2) 4_665 3_665
Si6 K22 O55 121.06(2) 1_655 3_665
F17 K22 O55 116.86(6) . 3_665
F18 K22 O55 65.24(4) 1_655 3_665
O14 K22 O55 52.91(6) . 3_665
O15 K22 O55 80.02(5) . 3_665
O15 K22 O55 80.02(5) 4_565 3_665
O18 K23 O18 98.25(7) 4_565 .
O18 K23 O44 103.05(5) 4_565 .
O18 K23 O44 103.05(5) . .
O18 K23 O59 113.26(5) 4_565 .
O18 K23 O59 55.47(5) . .
O44 K23 O59 139.38(3) . .
O18 K23 O59 55.47(5) 4_565 4_565
O18 K23 O59 113.26(5) . 4_565
O44 K23 O59 139.38(3) . 4_565
O59 K23 O59 78.99(6) . 4_565
O18 K23 F3 58.56(4) 4_565 .
O18 K23 F3 58.55(4) . .
O44 K23 F3 73.04(6) . .
O59 K23 F3 110.76(5) . .
O59 K23 F3 110.76(5) 4_565 .
O18 K23 O11 130.19(4) 4_565 .
O18 K23 O11 130.19(4) . .
O44 K23 O11 60.22(7) . .
O59 K23 O11 104.85(5) . .
O59 K23 O11 104.85(5) 4_565 .
F3 K23 O11 133.26(6) . .
O18 K23 O26 154.65(5) 4_565 .
O18 K23 O26 80.05(5) . .
O44 K23 O26 53.67(4) . .
O59 K23 O26 86.82(5) . .
O59 K23 O26 148.22(5) 4_565 .
F3 K23 O26 100.83(4) . .
O11 K23 O26 51.57(4) . .
O18 K23 O26 80.05(5) 4_565 4_565
O18 K23 O26 154.65(5) . 4_565
O44 K23 O26 53.67(4) . 4_565
O59 K23 O26 148.21(5) . 4_565
O59 K23 O26 86.82(5) 4_565 4_565
F3 K23 O26 100.83(4) . 4_565
O11 K23 O26 51.57(4) . 4_565
O26 K23 O26 90.78(7) . 4_565
O18 K23 Si7 101.05(4) 4_565 4_565
O18 K23 Si7 160.13(4) . 4_565
O44 K23 Si7 67.98(5) . 4_565
O59 K23 Si7 119.38(4) . 4_565
O59 K23 Si7 81.99(4) 4_565 4_565
F3 K23 Si7 129.81(3) . 4_565
O11 K23 Si7 29.948(16) . 4_565
O26 K23 Si7 80.49(4) . 4_565
O26 K23 Si7 29.52(3) 4_565 4_565
O18 K23 Si7 160.13(4) 4_565 .
O18 K23 Si7 101.05(4) . .
O44 K23 Si7 67.98(5) . .
O59 K23 Si7 81.99(4) . .
O59 K23 Si7 119.38(4) 4_565 .
F3 K23 Si7 129.81(3) . .
O11 K23 Si7 29.948(16) . .
O26 K23 Si7 29.52(3) . .
O26 K23 Si7 80.49(4) 4_565 .
Si7 K23 Si7 59.36(3) 4_565 .
O18 K23 Si12 78.64(4) 4_565 4_565
O18 K23 Si12 122.97(4) . 4_565
O44 K23 Si12 29.440(15) . 4_565
O59 K23 Si12 167.94(4) . 4_565
O59 K23 Si12 110.76(4) 4_565 4_565
F3 K23 Si12 73.15(4) . 4_565
O11 K23 Si12 66.42(4) . 4_565
O26 K23 Si12 81.20(4) . 4_565
O26 K23 Si12 31.71(3) 4_565 4_565
Si7 K23 Si12 57.32(2) 4_565 4_565
Si7 K23 Si12 86.87(3) . 4_565
O50 K24 O50 101.56(8) 4_565 .
O50 K24 O36 55.28(5) 4_565 4_565
O50 K24 O36 122.81(6) . 4_565
O50 K24 O36 122.81(6) 4_565 .
O50 K24 O36 55.28(5) . .
O36 K24 O36 91.67(6) 4_565 .
O50 K24 O65 110.69(5) 4_565 .
O50 K24 O65 54.55(5) . .
O36 K24 O65 165.90(5) 4_565 .
O36 K24 O65 96.07(4) . .
O50 K24 O65 54.55(5) 4_565 4_565
O50 K24 O65 110.69(5) . 4_565
O36 K24 O65 96.07(4) 4_565 4_565
O36 K24 O65 165.90(5) . 4_565
O65 K24 O65 74.08(6) . 4_565
O50 K24 F6 109.81(4) 4_565 .
O50 K24 F6 109.81(4) . .
O36 K24 F6 54.82(4) 4_565 .
O36 K24 F6 54.82(4) . .
O65 K24 F6 138.82(4) . .
O65 K24 F6 138.82(4) 4_565 .
O50 K24 Si5 28.58(4) 4_565 4_565
O50 K24 Si5 108.18(5) . 4_565
O36 K24 Si5 28.40(4) 4_565 4_565
O36 K24 Si5 102.85(4) . 4_565
O65 K24 Si5 137.61(4) . 4_565
O65 K24 Si5 79.23(4) 4_565 4_565
F6 K24 Si5 81.58(3) . 4_565
O50 K24 Si5 108.18(5) 4_565 .
O50 K24 Si5 28.58(4) . .
O36 K24 Si5 102.85(4) 4_565 .
O36 K24 Si5 28.40(4) . .
O65 K24 Si5 79.23(4) . .
O65 K24 Si5 137.61(4) 4_565 .
F6 K24 Si5 81.58(3) . .
Si5 K24 Si5 100.38(3) 4_565 .
O50 K24 O29 129.08(4) 4_565 .
O50 K24 O29 129.08(4) . .
O36 K24 O29 94.34(5) 4_565 .
O36 K24 O29 94.34(5) . .
O65 K24 O29 96.81(5) . .
O65 K24 O29 96.81(5) 4_565 .
F6 K24 O29 62.01(5) . .
Si5 K24 O29 118.79(3) 4_565 .
Si5 K24 O29 118.79(3) . .
O50 K24 K01 77.71(4) 4_565 .
O50 K24 K01 77.71(4) . .
O36 K24 K01 48.46(3) 4_565 .
O36 K24 K01 48.46(3) . .
O65 K24 K01 132.23(4) . .
O65 K24 K01 132.23(4) 4_565 .
F6 K24 K01 52.09(4) . .
Si5 K24 K01 54.426(18) 4_565 .
Si5 K24 K01 54.425(18) . .
O29 K24 K01 114.10(5) . .
O50 K24 Si17 27.23(4) 4_565 4_565
O50 K24 Si17 104.31(5) . 4_565
O36 K24 Si17 77.15(4) 4_565 4_565
O36 K24 Si17 146.08(4) . 4_565
O65 K24 Si17 89.95(4) . 4_565
O65 K24 Si17 27.82(3) 4_565 4_565
F6 K24 Si17 130.826(18) . 4_565
Si5 K24 Si17 54.29(2) 4_565 4_565
Si5 K24 Si17 122.89(3) . 4_565
O29 K24 Si17 118.12(3) . 4_565
K01 K24 Si17 104.76(2) . 4_565
O46 K25 O46 91.66(8) . 4
O46 K25 O26 113.65(5) . 4
O46 K25 O26 57.28(5) 4 4
O46 K25 O26 57.27(5) . .
O46 K25 O26 113.65(5) 4 .
O26 K25 O26 82.06(7) 4 .
O46 K25 O43 102.19(5) . .
O46 K25 O43 102.19(5) 4 .
O26 K25 O43 137.98(4) 4 .
O26 K25 O43 137.98(4) . .
O46 K25 F13 57.68(4) . .
O46 K25 F13 57.68(4) 4 .
O26 K25 F13 113.75(4) 4 .
O26 K25 F13 113.74(4) . .
O43 K25 F13 67.76(6) . .
O46 K25 O38 153.41(6) . 4
O46 K25 O38 93.34(5) 4 4
O26 K25 O38 50.00(4) 4 4
O26 K25 O38 97.03(5) . 4
O43 K25 O38 102.22(5) . 4
F13 K25 O38 143.74(3) . 4
O46 K25 O38 93.33(5) . .
O46 K25 O38 153.42(6) 4 .
O26 K25 O38 97.03(5) 4 .
O26 K25 O38 50.00(4) . .
O43 K25 O38 102.22(5) . .
F13 K25 O38 143.74(3) . .
O38 K25 O38 71.30(6) 4 .
O46 K25 Si14 125.67(5) . 4
O46 K25 Si14 81.79(4) 4 4
O26 K25 Si14 107.43(4) 4 4
O26 K25 Si14 164.56(4) . 4
O43 K25 Si14 30.620(16) . 4
F13 K25 Si14 74.20(4) . 4
O38 K25 Si14 80.90(4) 4 4
O38 K25 Si14 115.58(4) . 4
O46 K25 Si14 81.79(4) . .
O46 K25 Si14 125.67(5) 4 .
O26 K25 Si14 164.56(4) 4 .
O26 K25 Si14 107.43(4) . .
O43 K25 Si14 30.619(16) . .
F13 K25 Si14 74.20(4) . .
O38 K25 Si14 115.58(4) 4 .
O38 K25 Si14 80.90(4) . .
Si14 K25 Si14 60.80(3) 4 .
O46 K25 O53 90.33(5) . .
O46 K25 O53 150.15(6) 4 .
O26 K25 O53 145.94(5) 4 .
O26 K25 O53 92.29(5) . .
O43 K25 O53 48.44(4) . .
F13 K25 O53 99.33(4) . .
O38 K25 O53 98.07(5) 4 .
O38 K25 O53 55.96(4) . .
Si14 K25 O53 72.98(4) 4 .
Si14 K25 O53 25.76(3) . .
O46 K25 O53 150.15(6) . 4
O46 K25 O53 90.33(5) 4 4
O26 K25 O53 92.29(5) 4 4
O26 K25 O53 145.94(5) . 4
O43 K25 O53 48.44(4) . 4
F13 K25 O53 99.33(4) . 4
O38 K25 O53 55.96(4) 4 4
O38 K25 O53 98.07(5) . 4
Si14 K25 O53 25.76(3) 4 4
Si14 K25 O53 72.98(4) . 4
O53 K25 O53 73.83(6) . 4
O38 K26 O38 97.04(8) . 4
O38 K26 O33 113.48(5) . .
O38 K26 O33 113.48(5) 4 .
O38 K26 F20 65.44(5) . .
O38 K26 F20 65.44(5) 4 .
O33 K26 F20 75.84(6) . .
O38 K26 O58 55.86(5) . .
O38 K26 O58 121.84(6) 4 .
O33 K26 O58 124.32(4) . .
F20 K26 O58 121.24(4) . .
O38 K26 O58 121.84(6) . 4
O38 K26 O58 55.86(5) 4 4
O33 K26 O58 124.32(4) . 4
F20 K26 O58 121.25(4) . 4
O58 K26 O58 93.20(6) . 4
O38 K26 O35 126.18(6) . 4
O38 K26 O35 61.91(5) 4 4
O33 K26 O35 52.15(4) . 4
F20 K26 O35 60.75(4) . 4
O58 K26 O35 176.07(5) . 4
O58 K26 O35 88.19(4) 4 4
O38 K26 O35 61.91(5) . .
O38 K26 O35 126.18(6) 4 .
O33 K26 O35 52.15(4) . .
F20 K26 O35 60.75(4) . .
O58 K26 O35 88.19(4) . .
O58 K26 O35 176.06(5) 4 .
O35 K26 O35 90.18(6) 4 .
O38 K26 Si7 27.99(4) . .
O38 K26 Si7 106.08(5) 4 .
O33 K26 Si7 128.657(19) . .
F20 K26 Si7 93.07(3) . .
O58 K26 Si7 29.02(3) . .
O58 K26 Si7 104.51(4) 4 .
O35 K26 Si7 153.62(4) 4 .
O35 K26 Si7 78.42(4) . .
O38 K26 Si7 106.08(5) . 4
O38 K26 Si7 27.99(4) 4 4
O33 K26 Si7 128.657(18) . 4
F20 K26 Si7 93.07(3) . 4
O58 K26 Si7 104.51(4) . 4
O58 K26 Si7 29.02(3) 4 4
O35 K26 Si7 78.42(4) 4 4
O35 K26 Si7 153.62(4) . 4
Si7 K26 Si7 101.46(3) . 4
O38 K26 Si13 89.94(4) . .
O38 K26 Si13 136.17(5) 4 .
O33 K26 Si13 28.860(15) . .
F20 K26 Si13 78.83(4) . .
O58 K26 Si13 97.76(4) . .
O58 K26 Si13 146.70(4) 4 .
O35 K26 Si13 79.14(4) 4 .
O35 K26 Si13 29.36(3) . .
Si7 K26 Si13 100.13(2) . .
Si7 K26 Si13 157.30(2) 4 .
O38 K26 Si13 136.17(5) . 4
O38 K26 Si13 89.94(4) 4 4
O33 K26 Si13 28.860(15) . 4
F20 K26 Si13 78.83(4) . 4
O58 K26 Si13 146.70(4) . 4
O58 K26 Si13 97.76(4) 4 4
O35 K26 Si13 29.37(3) 4 4
O35 K26 Si13 79.14(4) . 4
Si7 K26 Si13 157.30(2) . 4
Si7 K26 Si13 100.13(2) 4 4
Si13 K26 Si13 57.66(3) . 4
O35 K27 O35 92.29(7) 3_666 2_656
O35 K27 O63 127.15(6) 3_666 .
O35 K27 O63 65.56(5) 2_656 .
O35 K27 O63 65.56(5) 3_666 4_565
O35 K27 O63 127.15(6) 2_656 4_565
O63 K27 O63 89.75(7) . 4_565
O35 K27 F12 63.81(5) 3_666 3_666
O35 K27 F12 63.81(5) 2_656 3_666
O63 K27 F12 63.35(5) . 3_666
O63 K27 F12 63.35(5) 4_565 3_666
O35 K27 O16 122.91(5) 3_666 3_666
O35 K27 O16 122.91(5) 2_656 3_666
O63 K27 O16 57.38(5) . 3_666
O63 K27 O16 57.38(5) 4_565 3_666
F12 K27 O16 91.21(7) 3_666 3_666
O35 K27 Si8 145.40(5) 3_666 .
O35 K27 Si8 92.57(4) 2_656 .
O63 K27 Si8 30.93(4) . .
O63 K27 Si8 84.48(4) 4_565 .
F12 K27 Si8 88.02(4) 3_666 .
O16 K27 Si8 32.830(17) 3_666 .
O35 K27 Si8 92.58(4) 3_666 4_565
O35 K27 Si8 145.40(5) 2_656 4_565
O63 K27 Si8 84.47(4) . 4_565
O63 K27 Si8 30.93(4) 4_565 4_565
F12 K27 Si8 88.02(4) 3_666 4_565
O16 K27 Si8 32.829(17) 3_666 4_565
Si8 K27 Si8 65.31(3) . 4_565
O35 K27 O2 130.18(4) 3_666 1_655
O35 K27 O2 130.18(4) 2_656 1_655
O63 K27 O2 97.21(5) . 1_655
O63 K27 O2 97.21(5) 4_565 1_655
F12 K27 O2 150.93(6) 3_666 1_655
O16 K27 O2 59.72(7) 3_666 1_655
Si8 K27 O2 67.76(4) . 1_655
Si8 K27 O2 67.76(4) 4_565 1_655
O35 K27 O6 52.59(5) 3_666 4_665
O35 K27 O6 107.34(5) 2_656 4_665
O63 K27 O6 172.75(5) . 4_665
O63 K27 O6 96.09(4) 4_565 4_665
F12 K27 O6 115.63(5) 3_666 4_665
O16 K27 O6 129.63(5) 3_666 4_665
Si8 K27 O6 153.91(4) . 4_665
Si8 K27 O6 102.74(4) 4_565 4_665
O2 K27 O6 86.35(5) 1_655 4_665
O35 K27 O6 107.34(5) 3_666 1_655
O35 K27 O6 52.59(5) 2_656 1_655
O63 K27 O6 96.09(4) . 1_655
O63 K27 O6 172.75(5) 4_565 1_655
F12 K27 O6 115.63(5) 3_666 1_655
O16 K27 O6 129.63(5) 3_666 1_655
Si8 K27 O6 102.74(4) . 1_655
Si8 K27 O6 153.91(4) 4_565 1_655
O2 K27 O6 86.35(5) 1_655 1_655
O6 K27 O6 77.78(6) 4_665 1_655
O35 K27 Sc9 37.52(4) 3_666 3_666
O35 K27 Sc9 96.84(4) 2_656 3_666
O63 K27 Sc9 95.40(4) . 3_666
O63 K27 Sc9 37.01(4) 4_565 3_666
F12 K27 Sc9 39.239(14) 3_666 3_666
O16 K27 Sc9 90.43(4) 3_666 3_666
Si8 K27 Sc9 107.88(3) . 3_666
Si8 K27 Sc9 67.94(2) 4_565 3_666
O2 K27 Sc9 132.27(3) 1_655 3_666
O6 K27 Sc9 86.77(4) 4_665 3_666
O6 K27 Sc9 137.55(4) 1_655 3_666
O52 K28 O52 92.31(8) 1_655 4_665
O52 K28 O2 110.05(5) 1_655 1_655
O52 K28 O2 110.05(5) 4_665 1_655
O52 K28 O13 115.15(6) 1_655 4_665
O52 K28 O13 55.05(5) 4_665 4_665
O2 K28 O13 132.33(4) 1_655 4_665
O52 K28 O13 55.05(5) 1_655 1_655
O52 K28 O13 115.15(6) 4_665 1_655
O2 K28 O13 132.33(4) 1_655 1_655
O13 K28 O13 87.54(7) 4_665 1_655
O52 K28 F17 58.43(4) 1_655 .
O52 K28 F17 58.43(4) 4_665 .
O2 K28 F17 78.78(6) 1_655 .
O13 K28 F17 112.76(4) 4_665 .
O13 K28 F17 112.76(4) 1_655 .
O52 K28 O24 113.22(5) 1_655 4_565
O52 K28 O24 61.08(5) 4_665 4_565
O2 K28 O24 49.06(4) 1_655 4_565
O13 K28 O24 97.87(4) 4_665 4_565
O13 K28 O24 168.22(5) 1_655 4_565
F17 K28 O24 55.49(4) . 4_565
O52 K28 O24 61.08(5) 1_655 .
O52 K28 O24 113.22(5) 4_665 .
O2 K28 O24 49.06(4) 1_655 .
O13 K28 O24 168.22(5) 4_665 .
O13 K28 O24 97.87(4) 1_655 .
F17 K28 O24 55.49(4) . .
O24 K28 O24 74.98(6) 4_565 .
O52 K28 Si11 129.91(5) 1_655 4_665
O52 K28 Si11 86.18(4) 4_665 4_665
O2 K28 Si11 29.427(15) 1_655 4_665
O13 K28 Si11 104.58(4) 4_665 4_665
O13 K28 Si11 158.59(4) 1_655 4_665
F17 K28 Si11 79.18(4) . 4_665
O24 K28 Si11 28.62(3) 4_565 4_665
O24 K28 Si11 73.73(4) . 4_665
O52 K28 Si11 86.18(4) 1_655 1_655
O52 K28 Si11 129.91(5) 4_665 1_655
O2 K28 Si11 29.427(15) 1_655 1_655
O13 K28 Si11 158.59(4) 4_665 1_655
O13 K28 Si11 104.58(4) 1_655 1_655
F17 K28 Si11 79.18(4) . 1_655
O24 K28 Si11 73.73(4) 4_565 1_655
O24 K28 Si11 28.62(3) . 1_655
Si11 K28 Si11 58.81(3) 4_665 1_655
O52 K28 O59 153.32(6) 1_655 4_665
O52 K28 O59 92.98(5) 4_665 4_665
O2 K28 O59 92.56(5) 1_655 4_665
O13 K28 O59 49.83(4) 4_665 4_665
O13 K28 O59 99.33(5) 1_655 4_665
F17 K28 O59 143.53(3) . 4_665
O24 K28 O59 92.13(4) 4_565 4_665
O24 K28 O59 138.35(5) . 4_665
Si11 K28 O59 76.55(4) 4_665 4_665
Si11 K28 O59 109.90(4) 1_655 4_665
O52 K28 O59 92.98(5) 1_655 1_655
O52 K28 O59 153.32(6) 4_665 1_655
O2 K28 O59 92.56(5) 1_655 1_655
O13 K28 O59 99.33(5) 4_665 1_655
O13 K28 O59 49.83(4) 1_655 1_655
F17 K28 O59 143.53(3) . 1_655
O24 K28 O59 138.35(5) 4_565 1_655
O24 K28 O59 92.13(4) . 1_655
Si11 K28 O59 109.90(4) 4_665 1_655
Si11 K28 O59 76.55(4) 1_655 1_655
O59 K28 O59 71.38(6) 4_665 1_655
O45 K29 O45 104.50(8) . 4
O45 K29 F1 60.74(4) . .
O45 K29 F1 60.74(4) 4 .
O45 K29 O51 106.89(5) . .
O45 K29 O51 106.89(5) 4 .
F1 K29 O51 81.32(7) . .
O45 K29 O61 55.99(5) . .
O45 K29 O61 115.72(6) 4 .
F1 K29 O61 112.50(5) . .
O51 K29 O61 136.67(4) . .
O45 K29 O61 115.72(6) . 4
O45 K29 O61 55.98(5) 4 4
F1 K29 O61 112.50(5) . 4
O51 K29 O61 136.68(4) . 4
O61 K29 O61 77.84(6) . 4
O45 K29 O3 82.02(5) . .
O45 K29 O3 158.23(6) 4 .
F1 K29 O3 107.42(5) . .
O51 K29 O3 51.59(4) . .
O61 K29 O3 85.31(5) . .
O61 K29 O3 140.02(5) 4 .
O45 K29 O3 158.23(6) . 4
O45 K29 O3 82.02(5) 4 4
F1 K29 O3 107.42(5) . 4
O51 K29 O3 51.59(4) . 4
O61 K29 O3 140.02(5) . 4
O61 K29 O3 85.31(5) 4 4
O3 K29 O3 84.92(7) . 4
O45 K29 O8 127.62(4) . .
O45 K29 O8 127.62(4) 4 .
F1 K29 O8 138.54(6) . .
O51 K29 O8 57.23(7) . .
O61 K29 O8 99.31(5) . .
O61 K29 O8 99.31(5) 4 .
O3 K29 O8 47.87(4) . .
O3 K29 O8 47.87(4) 4 .
O45 K29 O23 58.90(5) . .
O45 K29 O23 117.94(5) 4 .
F1 K29 O23 59.88(4) . .
O51 K29 O23 48.01(4) . .
O61 K29 O23 101.96(4) . .
O61 K29 O23 171.85(5) 4 .
O3 K29 O23 47.55(4) . .
O3 K29 O23 99.56(5) 4 .
O8 K29 O23 88.78(5) . .
O45 K29 O23 117.93(5) . 4
O45 K29 O23 58.90(5) 4 4
F1 K29 O23 59.88(4) . 4
O51 K29 O23 48.01(4) . 4
O61 K29 O23 171.85(5) . 4
O61 K29 O23 101.96(4) 4 4
O3 K29 O23 99.56(5) . 4
O3 K29 O23 47.55(4) 4 4
O8 K29 O23 88.78(5) . 4
O23 K29 O23 77.05(6) . 4
O45 K29 Si18 127.86(5) . 4
O45 K29 Si18 81.70(4) 4 4
F1 K29 Si18 80.26(4) . 4
O51 K29 Si18 28.737(15) . 4
O61 K29 Si18 161.67(4) . 4
O61 K29 Si18 110.31(4) 4 4
O3 K29 Si18 78.09(4) . 4
O3 K29 Si18 31.40(3) 4 4
O8 K29 Si18 63.69(4) . 4
O23 K29 Si18 72.35(4) . 4
O23 K29 Si18 25.80(3) 4 4
O57 K30 O57 92.45(7) . 4_565
O57 K30 O12 55.61(5) . .
O57 K30 O12 113.07(6) 4_565 .
O57 K30 O12 113.08(6) . 4_565
O57 K30 O12 55.61(5) 4_565 4_565
O12 K30 O12 82.98(7) . 4_565
O57 K30 O20 104.18(5) . .
O57 K30 O20 104.18(5) 4_565 .
O12 K30 O20 137.30(4) . .
O12 K30 O20 137.30(4) 4_565 .
O57 K30 F19 58.16(4) . .
O57 K30 F19 58.16(4) 4_565 .
O12 K30 F19 112.48(4) . .
O12 K30 F19 112.49(4) 4_565 .
O20 K30 F19 70.44(6) . .
O57 K30 O54 155.28(6) . 3_666
O57 K30 O54 91.76(5) 4_565 3_666
O12 K30 O54 100.54(5) . 3_666
O12 K30 O54 51.51(5) 4_565 3_666
O20 K30 O54 98.35(5) . 3_666
F19 K30 O54 141.66(3) . 3_666
O57 K30 O54 91.76(5) . 2_656
O57 K30 O54 155.28(6) 4_565 2_656
O12 K30 O54 51.51(5) . 2_656
O12 K30 O54 100.54(5) 4_565 2_656
O20 K30 O54 98.35(5) . 2_656
F19 K30 O54 141.66(3) . 2_656
O54 K30 O54 74.85(6) 3_666 2_656
O57 K30 Si9 125.81(5) . 4_565
O57 K30 Si9 81.57(4) 4_565 4_565
O12 K30 Si9 165.34(4) . 4_565
O12 K30 Si9 107.23(4) 4_565 4_565
O20 K30 Si9 30.449(15) . 4_565
F19 K30 Si9 73.92(3) . 4_565
O54 K30 Si9 78.91(4) 3_666 4_565
O54 K30 Si9 115.05(4) 2_656 4_565
O57 K30 Si9 81.57(4) . .
O57 K30 Si9 125.81(5) 4_565 .
O12 K30 Si9 107.23(4) . .
O12 K30 Si9 165.33(4) 4_565 .
O20 K30 Si9 30.449(15) . .
F19 K30 Si9 73.92(3) . .
O54 K30 Si9 115.05(4) 3_666 .
O54 K30 Si9 78.91(4) 2_656 .
Si9 K30 Si9 60.88(3) 4_565 .
O57 K30 O9 86.55(5) . .
O57 K30 O9 152.83(6) 4_565 .
O12 K30 O9 88.62(5) . .
O12 K30 O9 147.94(5) 4_565 .
O20 K30 O9 50.30(4) . .
F19 K30 O9 99.33(4) . .
O54 K30 O9 100.42(5) 3_666 .
O54 K30 O9 51.79(4) 2_656 .
Si9 K30 O9 77.15(4) 4_565 .
Si9 K30 O9 27.27(3) . .
O57 K30 O9 152.83(6) . 4_565
O57 K30 O9 86.55(5) 4_565 4_565
O12 K30 O9 147.94(5) . 4_565
O12 K30 O9 88.62(5) 4_565 4_565
O20 K30 O9 50.30(4) . 4_565
F19 K30 O9 99.33(4) . 4_565
O54 K30 O9 51.79(4) 3_666 4_565
O54 K30 O9 100.42(5) 2_656 4_565
Si9 K30 O9 27.27(3) 4_565 4_565
Si9 K30 O9 77.15(4) . 4_565
O9 K30 O9 82.26(6) . 4_565
F3 K31 O13 117.27(4) . .
F3 K31 O13 117.27(4) . 4_565
O13 K31 O13 95.52(7) . 4_565
F3 K31 O18 61.52(4) . .
O13 K31 O18 55.77(5) . .
O13 K31 O18 122.51(5) 4_565 .
F3 K31 O18 61.52(4) . 4_565
O13 K31 O18 122.51(5) . 4_565
O13 K31 O18 55.77(5) 4_565 4_565
O18 K31 O18 95.97(7) . 4_565
F3 K31 O40 64.85(4) . 4_565
O13 K31 O40 177.46(5) . 4_565
O13 K31 O40 84.44(5) 4_565 4_565
O18 K31 O40 126.30(5) . 4_565
O18 K31 O40 59.48(5) 4_565 4_565
F3 K31 O40 64.85(4) . .
O13 K31 O40 84.44(5) . .
O13 K31 O40 177.46(5) 4_565 .
O18 K31 O40 59.48(5) . .
O18 K31 O40 126.30(5) 4_565 .
O40 K31 O40 95.49(7) 4_565 .
F3 K31 O55 83.40(6) . .
O13 K31 O55 122.77(4) . .
O13 K31 O55 122.77(4) 4_565 .
O18 K31 O55 114.31(5) . .
O18 K31 O55 114.32(5) 4_565 .
O40 K31 O55 55.49(4) 4_565 .
O40 K31 O55 55.49(4) . .
F3 K31 Si2 82.43(4) . 4_565
O13 K31 Si2 148.44(4) . 4_565
O13 K31 Si2 96.33(4) 4_565 4_565
O18 K31 Si2 135.33(5) . 4_565
O18 K31 Si2 88.09(4) 4_565 4_565
O40 K31 Si2 29.24(4) 4_565 4_565
O40 K31 Si2 82.48(4) . 4_565
O55 K31 Si2 30.140(16) . 4_565
F3 K31 Si2 82.43(4) . .
O13 K31 Si2 96.33(4) . .
O13 K31 Si2 148.44(4) 4_565 .
O18 K31 Si2 88.09(4) . .
O18 K31 Si2 135.33(5) 4_565 .
O40 K31 Si2 82.48(4) 4_565 .
O40 K31 Si2 29.24(4) . .
O55 K31 Si2 30.140(16) . .
Si2 K31 Si2 60.14(3) 4_565 .
F3 K31 Si16 88.98(3) . 4_565
O13 K31 Si16 103.56(4) . 4_565
O13 K31 Si16 29.33(4) 4_565 4_565
O18 K31 Si16 103.57(4) . 4_565
O18 K31 Si16 28.88(4) 4_565 4_565
O40 K31 Si16 77.63(4) 4_565 4_565
O40 K31 Si16 153.09(4) . 4_565
O55 K31 Si16 131.145(18) . 4_565
Si2 K31 Si16 101.04(2) 4_565 4_565
Si2 K31 Si16 160.10(3) . 4_565
F3 K31 Si16 88.98(3) . .
O13 K31 Si16 29.33(4) . .
O13 K31 Si16 103.56(4) 4_565 .
O18 K31 Si16 28.88(4) . .
O18 K31 Si16 103.57(4) 4_565 .
O40 K31 Si16 153.09(4) 4_565 .
O40 K31 Si16 77.63(4) . .
O55 K31 Si16 131.145(18) . .
Si2 K31 Si16 160.11(3) 4_565 .
Si2 K31 Si16 101.05(2) . .
Si16 K31 Si16 96.69(3) 4_565 .
O47 K32 O47 94.85(8) . 4
O47 K32 O63 133.76(6) . 4
O47 K32 O63 59.40(5) 4 4
O47 K32 O63 59.40(5) . .
O47 K32 O63 133.76(6) 4 .
O63 K32 O63 109.23(7) 4 .
O47 K32 F20 121.68(5) . 3_656
O47 K32 F20 121.68(5) 4 3_656
O63 K32 F20 62.63(4) 4 3_656
O63 K32 F20 62.63(4) . 3_656
O47 K32 Si8 31.20(4) . .
O47 K32 Si8 110.15(5) 4 .
O63 K32 Si8 117.86(5) 4 .
O63 K32 Si8 30.55(4) . .
F20 K32 Si8 90.89(3) 3_656 .
O47 K32 Si8 110.15(5) . 4
O47 K32 Si8 31.20(4) 4 4
O63 K32 Si8 30.56(4) 4 4
O63 K32 Si8 117.86(5) . 4
F20 K32 Si8 90.89(3) 3_656 4
Si8 K32 Si8 109.12(4) . 4
O47 K32 O53 97.53(5) . 2_656
O47 K32 O53 167.09(5) 4 2_656
O63 K32 O53 113.12(5) 4 2_656
O63 K32 O53 57.22(5) . 2_656
F20 K32 O53 53.55(4) 3_656 2_656
Si8 K32 O53 82.51(3) . 2_656
Si8 K32 O53 143.44(4) 4 2_656
O47 K32 O53 167.09(5) . 3_656
O47 K32 O53 97.53(5) 4 3_656
O63 K32 O53 57.21(5) 4 3_656
O63 K32 O53 113.12(5) . 3_656
F20 K32 O53 53.55(4) 3_656 3_656
Si8 K32 O53 143.44(4) . 3_656
Si8 K32 O53 82.51(3) 4 3_656
O53 K32 O53 69.90(6) 2_656 3_656
O47 K32 O43 124.36(5) . 3_656
O47 K32 O43 124.36(5) 4 3_656
O63 K32 O43 101.42(5) 4 3_656
O63 K32 O43 101.43(5) . 3_656
F20 K32 O43 72.56(6) 3_656 3_656
Si8 K32 O43 123.89(2) . 3_656
Si8 K32 O43 123.89(2) 4 3_656
O53 K32 O43 44.22(4) 2_656 3_656
O53 K32 O43 44.22(4) 3_656 3_656
O47 K32 K08 49.58(4) . .
O47 K32 K08 49.58(4) 4 .
O63 K32 K08 88.19(4) 4 .
O63 K32 K08 88.19(4) . .
F20 K32 K08 124.31(5) 3_656 .
Si8 K32 K08 60.82(2) . .
Si8 K32 K08 60.82(2) 4 .
O53 K32 K08 143.25(3) 2_656 .
O53 K32 K08 143.25(3) 3_656 .
O43 K32 K08 163.12(5) 3_656 .
O47 K32 Sc9 90.29(4) . 2_656
O47 K32 Sc9 147.77(5) 4 2_656
O63 K32 Sc9 94.78(4) 4 2_656
O63 K32 Sc9 32.05(4) . 2_656
F20 K32 Sc9 34.827(12) 3_656 2_656
Si8 K32 Sc9 62.61(2) . 2_656
Si8 K32 Sc9 118.05(3) 4 2_656
O53 K32 Sc9 36.16(3) 2_656 2_656
O53 K32 Sc9 81.19(3) 3_656 2_656
O43 K32 Sc9 76.50(4) 3_656 2_656
K08 K32 Sc9 116.86(2) . 2_656
O11 K33 F12 71.26(7) . .
O11 K33 O53 106.83(5) . .
F12 K33 O53 66.17(4) . .
O11 K33 O53 106.83(5) . 4_565
F12 K33 O53 66.17(4) . 4_565
O53 K33 O53 106.34(7) . 4_565
O11 K33 O57 137.52(4) . 4_565
F12 K33 O57 118.38(5) . 4_565
O53 K33 O57 114.85(5) . 4_565
O53 K33 O57 54.35(5) 4_565 4_565
O11 K33 O57 137.52(4) . .
F12 K33 O57 118.38(5) . .
O53 K33 O57 54.35(5) . .
O53 K33 O57 114.85(5) 4_565 .
O57 K33 O57 77.60(6) 4_565 .
O11 K33 O44 60.55(7) . .
F12 K33 O44 131.82(6) . .
O53 K33 O44 126.83(4) . .
O53 K33 O44 126.83(4) 4_565 .
O57 K33 O44 98.24(5) 4_565 .
O57 K33 O44 98.24(5) . .
O11 K33 Si14 126.23(2) . 4_565
F12 K33 Si14 89.94(3) . 4_565
O53 K33 Si14 110.38(4) . 4_565
O53 K33 Si14 25.57(4) 4_565 4_565
O57 K33 Si14 29.00(4) 4_565 4_565
O57 K33 Si14 95.98(4) . 4_565
O44 K33 Si14 117.78(3) . 4_565
O11 K33 Si14 126.23(2) . .
F12 K33 Si14 89.94(3) . .
O53 K33 Si14 25.57(4) . .
O53 K33 Si14 110.38(4) 4_565 .
O57 K33 Si14 95.98(4) 4_565 .
O57 K33 Si14 29.00(4) . .
O44 K33 Si14 117.78(3) . .
Si14 K33 Si14 102.71(3) 4_565 .
O11 K33 O38 49.94(4) . 4_565
F12 K33 O38 59.49(4) . 4_565
O53 K33 O38 125.23(5) . 4_565
O53 K33 O38 57.47(5) 4_565 4_565
O57 K33 O38 96.80(4) 4_565 4_565
O57 K33 O38 172.30(5) . 4_565
O44 K33 O38 87.72(5) . 4_565
Si14 K33 O38 76.85(3) 4_565 4_565
Si14 K33 O38 149.34(4) . 4_565
O11 K33 O38 49.94(4) . .
F12 K33 O38 59.49(4) . .
O53 K33 O38 57.47(5) . .
O53 K33 O38 125.23(5) 4_565 .
O57 K33 O38 172.30(5) 4_565 .
O57 K33 O38 96.80(4) . .
O44 K33 O38 87.72(5) . .
Si14 K33 O38 149.34(4) 4_565 .
Si14 K33 O38 76.85(3) . .
O38 K33 O38 88.26(6) 4_565 .
O11 K33 Si7 28.194(14) . 4_565
F12 K33 Si7 74.84(4) . 4_565
O53 K33 Si7 130.15(5) . 4_565
O53 K33 Si7 83.65(4) 4_565 4_565
O57 K33 Si7 110.40(3) 4_565 4_565
O57 K33 Si7 160.05(4) . 4_565
O44 K33 Si7 63.06(4) . 4_565
Si14 K33 Si7 99.03(2) 4_565 4_565
Si14 K33 Si7 153.39(3) . 4_565
O38 K33 Si7 27.30(3) 4_565 4_565
O38 K33 Si7 76.62(4) . 4_565
O21 K34 O21 97.30(8) 4_655 1_655
O21 K34 F16 69.84(5) 4_655 1_655
O21 K34 F16 69.84(5) 1_655 1_655
O21 K34 O33 122.61(5) 4_655 3_656
O21 K34 O33 122.61(5) 1_655 3_656
F16 K34 O33 86.11(7) 1_655 3_656
O21 K34 O6 136.96(6) 4_655 1_655
O21 K34 O6 65.78(5) 1_655 1_655
F16 K34 O6 67.19(5) 1_655 1_655
O33 K34 O6 56.86(4) 3_656 1_655
O21 K34 O6 65.78(5) 4_655 4_655
O21 K34 O6 136.96(6) 1_655 4_655
F16 K34 O6 67.19(5) 1_655 4_655
O33 K34 O6 56.86(4) 3_656 4_655
O6 K34 O6 98.94(7) 1_655 4_655
O21 K34 O10 53.85(5) 4_655 4
O21 K34 O10 112.60(6) 1_655 4
F16 K34 O10 123.66(4) 1_655 4
O33 K34 O10 123.90(5) 3_656 4
O6 K34 O10 168.50(5) 1_655 4
O6 K34 O10 89.63(5) 4_655 4
O21 K34 O10 112.60(6) 4_655 .
O21 K34 O10 53.85(5) 1_655 .
F16 K34 O10 123.66(4) 1_655 .
O33 K34 O10 123.90(5) 3_656 .
O6 K34 O10 89.63(5) 1_655 .
O6 K34 O10 168.50(5) 4_655 .
O10 K34 O10 80.91(7) 4 .
O21 K34 Sc5 101.43(5) 4_655 1_655
O21 K34 Sc5 40.94(4) 1_655 1_655
F16 K34 Sc5 39.459(14) 1_655 1_655
O33 K34 Sc5 88.27(4) 3_656 1_655
O6 K34 Sc5 39.60(4) 1_655 1_655
O6 K34 Sc5 101.25(4) 4_655 1_655
O10 K34 Sc5 145.94(4) 4 1_655
O10 K34 Sc5 90.24(4) . 1_655
O21 K34 Sc5 40.94(4) 4_655 4_655
O21 K34 Sc5 101.43(5) 1_655 4_655
F16 K34 Sc5 39.459(14) 1_655 4_655
O33 K34 Sc5 88.27(4) 3_656 4_655
O6 K34 Sc5 101.25(4) 1_655 4_655
O6 K34 Sc5 39.60(4) 4_655 4_655
O10 K34 Sc5 90.24(4) 4 4_655
O10 K34 Sc5 145.94(4) . 4_655
Sc5 K34 Sc5 78.86(3) 1_655 4_655
O21 K34 Si13 145.83(5) 4_655 2_656
O21 K34 Si13 95.34(4) 1_655 2_656
F16 K34 Si13 85.16(4) 1_655 2_656
O33 K34 Si13 29.327(15) 3_656 2_656
O6 K34 Si13 30.99(4) 1_655 2_656
O6 K34 Si13 83.47(4) 4_655 2_656
O10 K34 Si13 144.76(4) 4 2_656
O10 K34 Si13 100.49(4) . 2_656
Sc5 K34 Si13 69.11(2) 1_655 2_656
Sc5 K34 Si13 105.35(3) 4_655 2_656
O21 K34 Si13 95.34(4) 4_655 3_656
O21 K34 Si13 145.83(5) 1_655 3_656
F16 K34 Si13 85.16(4) 1_655 3_656
O33 K34 Si13 29.327(15) 3_656 3_656
O6 K34 Si13 83.47(4) 1_655 3_656
O6 K34 Si13 30.99(4) 4_655 3_656
O10 K34 Si13 100.49(4) 4 3_656
O10 K34 Si13 144.76(4) . 3_656
Sc5 K34 Si13 105.35(3) 1_655 3_656
Sc5 K34 Si13 69.11(2) 4_655 3_656
Si13 K34 Si13 58.57(3) 2_656 3_656
O61 K35 O61 89.42(7) 4 .
O61 K35 O1 107.63(5) 4 .
O61 K35 O1 107.63(5) . .
O61 K35 F10 60.61(5) 4 .
O61 K35 F10 60.61(5) . .
O1 K35 F10 68.90(6) . .
O61 K35 O17 55.14(5) 4 4
O61 K35 O17 110.73(5) . 4
O1 K35 O17 137.09(4) . 4
F10 K35 O17 115.32(5) . 4
O61 K35 O17 110.73(5) 4 .
O61 K35 O17 55.14(5) . .
O1 K35 O17 137.09(4) . .
F10 K35 O17 115.32(5) . .
O17 K35 O17 82.26(7) 4 .
O61 K35 O32 90.94(5) 4 4
O61 K35 O32 155.70(6) . 4
O1 K35 O32 95.40(5) . 4
F10 K35 O32 138.45(3) . 4
O17 K35 O32 51.55(5) 4 4
O17 K35 O32 102.41(5) . 4
O61 K35 O32 155.70(6) 4 .
O61 K35 O32 90.94(5) . .
O1 K35 O32 95.40(5) . .
F10 K35 O32 138.45(3) . .
O17 K35 O32 102.41(5) 4 .
O17 K35 O32 51.55(5) . .
O32 K35 O32 79.00(6) 4 .
O61 K35 O65 57.53(5) 4 4
O61 K35 O65 116.59(5) . 4
O1 K35 O65 51.90(4) . 4
F10 K35 O65 56.07(4) . 4
O17 K35 O65 93.15(4) 4 4
O17 K35 O65 167.28(5) . 4
O32 K35 O65 83.62(4) 4 4
O32 K35 O65 141.16(5) . 4
O61 K35 O65 116.59(5) 4 .
O61 K35 O65 57.53(5) . .
O1 K35 O65 51.90(4) . .
F10 K35 O65 56.07(4) . .
O17 K35 O65 167.28(5) 4 .
O17 K35 O65 93.16(4) . .
O32 K35 O65 141.16(5) 4 .
O32 K35 O65 83.62(4) . .
O65 K35 O65 88.80(6) 4 .
O61 K35 Si17 127.47(5) 4 .
O61 K35 Si17 86.14(4) . .
O1 K35 Si17 28.695(15) . .
F10 K35 Si17 72.02(4) . .
O17 K35 Si17 163.12(4) 4 .
O17 K35 Si17 108.99(4) . .
O32 K35 Si17 112.46(4) 4 .
O32 K35 Si17 76.78(4) . .
O65 K35 Si17 78.31(4) 4 .
O65 K35 Si17 29.02(3) . .
O61 K35 Si17 86.14(4) 4 4
O61 K35 Si17 127.46(5) . 4
O1 K35 Si17 28.695(15) . 4
F10 K35 Si17 72.02(4) . 4
O17 K35 Si17 108.99(4) 4 4
O17 K35 Si17 163.12(4) . 4
O32 K35 Si17 76.78(4) 4 4
O32 K35 Si17 112.46(4) . 4
O65 K35 Si17 29.02(3) 4 4
O65 K35 Si17 78.31(4) . 4
Si17 K35 Si17 57.38(3) . 4
F11 K36 O4 65.46(4) . .
F11 K36 O4 65.46(4) . 4_565
O4 K36 O4 104.75(8) . 4_565
F11 K36 O48 63.04(4) . 4_565
O4 K36 O48 127.34(6) . 4_565
O4 K36 O48 62.55(5) 4_565 4_565
F11 K36 O48 63.04(4) . .
O4 K36 O48 62.55(5) . .
O4 K36 O48 127.33(6) 4_565 .
O48 K36 O48 84.73(7) 4_565 .
F11 K36 O60 118.61(5) . .
O4 K36 O60 55.17(5) . .
O4 K36 O60 114.53(5) 4_565 .
O48 K36 O60 176.14(5) 4_565 .
O48 K36 O60 99.13(4) . .
F11 K36 O60 118.61(5) . 4_565
O4 K36 O60 114.52(5) . 4_565
O4 K36 O60 55.17(5) 4_565 4_565
O48 K36 O60 99.13(4) 4_565 4_565
O48 K36 O60 176.14(5) . 4_565
O60 K36 O60 77.01(6) . 4_565
F11 K36 O29 87.54(6) . .
O4 K36 O29 115.42(5) . .
O4 K36 O29 115.42(5) 4_565 .
O48 K36 O29 52.96(4) 4_565 .
O48 K36 O29 52.96(4) . .
O60 K36 O29 129.71(5) . .
O60 K36 O29 129.71(5) 4_565 .
F11 K36 O29 143.11(6) . 3_665
O4 K36 O29 126.92(4) . 3_665
O4 K36 O29 126.92(4) 4_565 3_665
O48 K36 O29 90.71(5) 4_565 3_665
O48 K36 O29 90.71(5) . 3_665
O60 K36 O29 89.34(5) . 3_665
O60 K36 O29 89.34(5) 4_565 3_665
O29 K36 O29 55.57(8) . 3_665
F11 K36 Si1 84.62(4) . .
O4 K36 Si1 87.48(4) . .
O4 K36 Si1 137.68(5) 4_565 .
O48 K36 Si1 77.68(4) 4_565 .
O48 K36 Si1 28.37(4) . .
O60 K36 Si1 105.77(4) . .
O60 K36 Si1 152.57(4) 4_565 .
O29 K36 Si1 29.855(16) . .
O29 K36 Si1 63.66(4) 3_665 .
F11 K36 Si1 84.62(4) . 4_565
O4 K36 Si1 137.68(5) . 4_565
O4 K36 Si1 87.48(4) 4_565 4_565
O48 K36 Si1 28.37(4) 4_565 4_565
O48 K36 Si1 77.68(4) . 4_565
O60 K36 Si1 152.57(4) . 4_565
O60 K36 Si1 105.77(4) 4_565 4_565
O29 K36 Si1 29.855(16) . 4_565
O29 K36 Si1 63.66(4) 3_665 4_565
Si1 K36 Si1 59.28(3) . 4_565
F11 K36 Si4 91.41(3) . .
O4 K36 Si4 28.47(4) . .
O4 K36 Si4 107.83(4) 4_565 .
O48 K36 Si4 154.44(4) 4_565 .
O48 K36 Si4 83.90(4) . .
O60 K36 Si4 27.39(4) . .
O60 K36 Si4 92.51(4) 4_565 .
O29 K36 Si4 131.561(16) . .
O29 K36 Si4 112.23(3) 3_665 .
Si1 K36 Si4 101.83(2) . .
Si1 K36 Si4 160.95(2) 4_565 .
O48 Si1 O37 115.33(10) . .
O48 Si1 O29 111.61(11) . .
O37 Si1 O29 109.39(10) . .
O48 Si1 O7 109.10(8) . .
O37 Si1 O7 104.45(8) . .
O29 Si1 O7 106.35(12) . .
O48 Si1 K18 56.87(6) . .
O37 Si1 K18 60.80(6) . .
O29 Si1 K18 145.57(9) . .
O7 Si1 K18 108.07(8) . .
O48 Si1 K36 63.88(7) . .
O37 Si1 K36 172.16(7) . .
O29 Si1 K36 65.12(8) . .
O7 Si1 K36 82.83(5) . .
K18 Si1 K36 120.15(3) . .
O48 Si1 K07 59.72(7) . 3_655
O37 Si1 K07 110.52(6) . 3_655
O29 Si1 K07 138.38(9) . 3_655
O7 Si1 K07 52.07(5) . 3_655
K18 Si1 K07 68.19(2) . 3_655
K36 Si1 K07 76.15(2) . 3_655
O48 Si1 K24 73.55(7) . .
O37 Si1 K24 78.88(6) . .
O29 Si1 K24 67.48(9) . .
O7 Si1 K24 173.79(8) . .
K18 Si1 K24 78.11(2) . .
K36 Si1 K24 93.61(2) . .
K07 Si1 K24 132.02(3) 3_655 .
O48 Si1 K07 122.23(6) . .
O37 Si1 K07 58.89(6) . .
O29 Si1 K07 124.63(9) . .
O7 Si1 K07 45.91(5) . .
K18 Si1 K07 80.71(2) . .
K36 Si1 K07 128.61(3) . .
K07 Si1 K07 69.53(2) 3_655 .
K24 Si1 K07 137.77(3) . .
O48 Si1 K36 164.21(7) . 3_665
O37 Si1 K36 79.62(7) . 3_665
O29 Si1 K36 55.76(8) . 3_665
O7 Si1 K36 69.65(5) . 3_665
K18 Si1 K36 138.90(3) . 3_665
K36 Si1 K36 100.59(3) . 3_665
K07 Si1 K36 121.69(3) 3_655 3_665
K24 Si1 K36 106.21(2) . 3_665
K07 Si1 K36 68.937(19) . 3_665
O40 Si2 O49 114.60(9) . .
O40 Si2 O55 119.30(11) . .
O49 Si2 O55 107.76(11) . .
O40 Si2 O27 105.24(9) . .
O49 Si2 O27 100.82(9) . .
O55 Si2 O27 107.20(11) . .
O40 Si2 K31 65.06(7) . .
O49 Si2 K31 97.44(7) . .
O55 Si2 K31 68.23(9) . .
O27 Si2 K31 161.67(7) . .
O40 Si2 K10 47.70(6) . .
O49 Si2 K10 67.97(6) . .
O55 Si2 K10 147.57(10) . .
O27 Si2 K10 105.14(6) . .
K31 Si2 K10 80.24(2) . .
O40 Si2 K01 78.85(7) . .
O49 Si2 K01 165.98(7) . .
O55 Si2 K01 66.12(8) . .
O27 Si2 K01 70.49(6) . .
K31 Si2 K01 91.88(2) . .
K10 Si2 K01 124.26(3) . .
O40 Si2 K20 117.06(6) . .
O49 Si2 K20 53.91(6) . .
O55 Si2 K20 122.77(9) . .
O27 Si2 K20 47.24(6) . .
K31 Si2 K20 150.54(3) . .
K10 Si2 K20 81.98(2) . .
K01 Si2 K20 117.56(3) . .
O40 Si2 K22 173.89(7) . 3_665
O49 Si2 K22 63.79(6) . 3_665
O55 Si2 K22 57.47(9) . 3_665
O27 Si2 K22 80.86(6) . 3_665
K31 Si2 K22 108.99(2) . 3_665
K10 Si2 K22 131.62(3) . 3_665
K01 Si2 K22 103.27(2) . 3_665
K20 Si2 K22 67.240(19) . 3_665
O40 Si2 K21 69.46(7) . .
O49 Si2 K21 113.17(6) . .
O55 Si2 K21 128.23(9) . .
O27 Si2 K21 35.89(6) . .
K31 Si2 K21 132.62(3) . .
K10 Si2 K21 79.09(2) . .
K01 Si2 K21 66.526(18) . .
K20 Si2 K21 65.50(2) . .
K22 Si2 K21 116.65(2) 3_665 .
O15 Si3 O31 114.56(9) 2_655 .
O15 Si3 O14 102.22(10) 2_655 3_665
O31 Si3 O14 118.36(10) . 3_665
O15 Si3 O27 105.54(9) 2_655 .
O31 Si3 O27 104.92(9) . .
O14 Si3 O27 110.69(11) 3_665 .
O15 Si3 K17 88.95(7) 2_655 3_665
O31 Si3 K17 72.95(6) . 3_665
O14 Si3 K17 59.67(9) 3_665 3_665
O27 Si3 K17 164.51(7) . 3_665
O15 Si3 K20 49.86(6) 2_655 .
O31 Si3 K20 112.95(6) . .
O14 Si3 K20 128.51(9) 3_665 .
O27 Si3 K20 57.35(6) . .
K17 Si3 K20 137.96(3) 3_665 .
O15 Si3 K21 114.81(6) 2_655 .
O31 Si3 K21 54.60(6) . .
O14 Si3 K21 141.72(9) 3_665 .
O27 Si3 K21 51.44(6) . .
K17 Si3 K21 127.36(3) 3_665 .
K20 Si3 K21 74.62(2) . .
O15 Si3 K12 62.65(6) 2_655 .
O31 Si3 K12 52.27(6) . .
O14 Si3 K12 135.91(9) 3_665 .
O27 Si3 K12 113.25(6) . .
K17 Si3 K12 78.03(2) 3_665 .
K20 Si3 K12 75.40(2) . .
K21 Si3 K12 73.84(2) . .
O15 Si3 K01 169.72(7) 2_655 .
O31 Si3 K01 75.24(6) . .
O14 Si3 K01 69.18(8) 3_665 .
O27 Si3 K01 73.53(6) . .
K17 Si3 K01 91.24(3) 3_665 .
K20 Si3 K01 130.81(3) . .
K21 Si3 K01 72.94(2) . .
K12 Si3 K01 127.38(3) . .
O15 Si3 K22 61.57(6) 2_655 3_665
O31 Si3 K22 170.03(7) . 3_665
O14 Si3 K22 56.40(8) 3_665 3_665
O27 Si3 K22 85.05(6) . 3_665
K17 Si3 K22 97.45(3) 3_665 3_665
K20 Si3 K22 72.25(2) . 3_665
K21 Si3 K22 135.15(3) . 3_665
K12 Si3 K22 124.10(3) . 3_665
K01 Si3 K22 108.24(2) . 3_665
O60 Si4 O4 113.40(10) . .
O60 Si4 O8 110.93(11) . .
O4 Si4 O8 111.04(11) . .
O60 Si4 O3 111.51(10) . .
O4 Si4 O3 102.66(9) . .
O8 Si4 O3 106.85(11) . .
O60 Si4 K12 82.71(7) . 3_655
O4 Si4 K12 161.66(7) . 3_655
O8 Si4 K12 52.52(8) . 3_655
O3 Si4 K12 77.87(7) . 3_655
O60 Si4 K07 84.87(7) . 3_655
O4 Si4 K07 69.57(6) . 3_655
O8 Si4 K07 64.89(8) . 3_655
O3 Si4 K07 163.61(7) . 3_655
K12 Si4 K07 104.87(3) 3_655 3_655
O60 Si4 K36 63.01(7) . .
O4 Si4 K36 52.38(6) . .
O8 Si4 K36 143.62(9) . .
O3 Si4 K36 108.47(7) . .
K12 Si4 K36 145.28(3) 3_655 .
K07 Si4 K36 78.73(2) 3_655 .
O60 Si4 K29 173.64(7) . .
O4 Si4 K29 72.92(7) . .
O8 Si4 K29 66.07(9) . .
O3 Si4 K29 65.26(7) . .
K12 Si4 K29 91.17(3) 3_655 .
K07 Si4 K29 98.40(3) 3_655 .
K36 Si4 K29 122.88(3) . .
O60 Si4 K16 107.31(7) . .
O4 Si4 K16 72.33(6) . .
O8 Si4 K16 135.34(9) . .
O3 Si4 K16 35.54(6) . .
K12 Si4 K16 112.50(3) 3_655 .
K07 Si4 K16 141.72(3) 3_655 .
K36 Si4 K16 75.41(2) . .
K29 Si4 K16 73.44(2) . .
O60 Si4 K17 51.03(7) . .
O4 Si4 K17 123.97(6) . .
O8 Si4 K17 124.90(9) . .
O3 Si4 K17 60.48(7) . .
K12 Si4 K17 72.60(2) 3_655 .
K07 Si4 K17 135.89(3) 3_655 .
K36 Si4 K17 81.06(2) . .
K29 Si4 K17 125.41(3) . .
K16 Si4 K17 66.50(2) . .
O36 Si5 O41 113.23(9) . .
O36 Si5 O5 113.28(11) . .
O41 Si5 O5 107.89(11) . .
O36 Si5 O50 108.89(9) . .
O41 Si5 O50 104.41(9) . .
O5 Si5 O50 108.70(11) . .
O36 Si5 K21 66.09(6) . .
O41 Si5 K21 90.43(7) . .
O5 Si5 K21 63.47(9) . .
O50 Si5 K21 164.98(7) . .
O36 Si5 K01 60.42(6) . .
O41 Si5 K01 56.30(6) . .
O5 Si5 K01 146.90(9) . .
O50 Si5 K01 103.70(7) . .
K21 Si5 K01 86.32(3) . .
O36 Si5 K24 65.87(6) . .
O41 Si5 K24 103.54(6) . .
O5 Si5 K24 145.07(9) . .
O50 Si5 K24 47.50(6) . .
K21 Si5 K24 131.67(3) . .
K01 Si5 K24 65.71(2) . .
O36 Si5 K14 117.52(6) . .
O41 Si5 K14 47.98(6) . .
O5 Si5 K14 129.10(9) . .
O50 Si5 K14 57.40(6) . .
K21 Si5 K14 137.61(3) . .
K01 Si5 K14 65.25(2) . .
K24 Si5 K14 65.45(2) . .
O36 Si5 K03 165.76(7) . .
O41 Si5 K03 76.40(7) . .
O5 Si5 K03 52.62(9) . .
O50 Si5 K03 77.28(6) . .
K21 Si5 K03 104.57(3) . .
K01 Si5 K03 131.72(3) . .
K24 Si5 K03 123.59(3) . .
K14 Si5 K03 76.69(2) . .
O36 Si5 K18 71.13(7) . .
O41 Si5 K18 175.35(7) . .
O5 Si5 K18 70.91(9) . .
O50 Si5 K18 72.12(6) . .
K21 Si5 K18 92.94(3) . .
K01 Si5 K18 127.11(3) . .
K24 Si5 K18 76.53(2) . .
K14 Si5 K18 129.10(3) . .
K03 Si5 K18 99.63(2) . .
O62 Si6 O13 112.63(10) . .
O62 Si6 O30 115.76(11) . .
O13 Si6 O30 100.54(11) . .
O62 Si6 O52 112.79(9) . .
O13 Si6 O52 105.63(9) . .
O30 Si6 O52 108.39(11) . .
O62 Si6 K22 55.89(7) . 1_455
O13 Si6 K22 113.00(7) . 1_455
O30 Si6 K22 146.12(9) . 1_455
O52 Si6 K22 58.96(6) . 1_455
O62 Si6 K13 169.20(7) . .
O13 Si6 K13 74.78(7) . .
O30 Si6 K13 53.96(9) . .
O52 Si6 K13 71.02(6) . .
K22 Si6 K13 129.76(3) 1_455 .
O62 Si6 K20 78.70(7) . 3
O13 Si6 K20 163.26(7) . 3
O30 Si6 K20 62.84(8) . 3
O52 Si6 K20 79.54(6) . 3
K22 Si6 K20 83.43(2) 1_455 3
K13 Si6 K20 92.42(3) . 3
O62 Si6 K28 113.02(7) . 1_455
O13 Si6 K28 62.91(7) . 1_455
O30 Si6 K28 131.08(9) . 1_455
O52 Si6 K28 46.27(6) . 1_455
K22 Si6 K28 65.76(2) 1_455 1_455
K13 Si6 K28 77.13(2) . 1_455
K20 Si6 K28 125.49(3) 3 1_455
O62 Si6 K10 83.30(7) . .
O13 Si6 K10 64.24(7) . .
O30 Si6 K10 63.66(9) . .
O52 Si6 K10 163.78(7) . .
K22 Si6 K10 135.67(3) 1_455 .
K13 Si6 K10 93.52(3) . .
K20 Si6 K10 106.76(3) 3 .
K28 Si6 K10 126.95(3) 1_455 .
O62 Si6 K31 71.43(7) . .
O13 Si6 K31 42.97(6) . .
O30 Si6 K31 131.06(9) . .
O52 Si6 K31 112.24(6) . .
K22 Si6 K31 80.31(2) 1_455 .
K13 Si6 K31 117.20(3) . .
K20 Si6 K31 150.13(3) 3 .
K28 Si6 K31 69.06(2) 1_455 .
K10 Si6 K31 69.85(2) . .
O38 Si7 O58 111.53(9) . .
O38 Si7 O26 106.58(9) . .
O58 Si7 O26 110.80(9) . .
O38 Si7 O11 107.13(10) . .
O58 Si7 O11 110.90(10) . .
O26 Si7 O11 109.75(12) . .
O38 Si7 K23 171.37(7) . .
O58 Si7 K23 77.09(7) . .
O26 Si7 K23 69.58(7) . .
O11 Si7 K23 68.08(8) . .
O38 Si7 K26 46.06(6) . .
O58 Si7 K26 68.52(6) . .
O26 Si7 K26 107.81(7) . .
O11 Si7 K26 139.29(9) . .
K23 Si7 K26 142.05(3) . .
O38 Si7 K15 78.45(7) . .
O58 Si7 K15 72.41(6) . .
O26 Si7 K15 171.78(7) . .
O11 Si7 K15 62.19(9) . .
K23 Si7 K15 104.50(3) . .
K26 Si7 K15 80.38(2) . .
O38 Si7 K33 72.74(7) . .
O58 Si7 K33 160.84(7) . .
O26 Si7 K33 84.63(7) . .
O11 Si7 K33 51.30(8) . .
K23 Si7 K33 98.96(3) . .
K26 Si7 K33 118.77(3) . .
K15 Si7 K33 90.83(3) . .
O38 Si7 K25 56.62(6) . .
O58 Si7 K25 125.91(6) . .
O26 Si7 K25 49.98(6) . .
O11 Si7 K25 123.12(9) . .
K23 Si7 K25 119.24(3) . .
K26 Si7 K25 72.42(2) . .
K15 Si7 K25 134.78(3) . .
K33 Si7 K25 72.55(2) . .
O38 Si7 K02 109.80(6) . .
O58 Si7 K02 75.95(6) . .
O26 Si7 K02 36.95(6) . .
O11 Si7 K02 136.32(9) . .
K23 Si7 K02 72.09(2) . .
K26 Si7 K02 84.15(2) . .
K15 Si7 K02 148.05(3) . .
K33 Si7 K02 121.11(3) . .
K25 Si7 K02 64.07(2) . .
O63 Si8 O47 114.14(10) . .
O63 Si8 O10 111.08(9) . .
O47 Si8 O10 109.85(9) . .
O63 Si8 O16 110.10(11) . 3_666
O47 Si8 O16 104.24(10) . 3_666
O10 Si8 O16 106.99(11) . 3_666
O63 Si8 K27 63.06(6) . .
O47 Si8 K27 165.49(7) . .
O10 Si8 K27 83.76(7) . .
O16 Si8 K27 65.73(8) 3_666 .
O63 Si8 K32 62.60(6) . .
O47 Si8 K32 58.17(6) . .
O10 Si8 K32 105.37(7) . .
O16 Si8 K32 147.05(9) 3_666 .
K27 Si8 K32 124.41(3) . .
O63 Si8 K19 60.89(7) . 3_666
O47 Si8 K19 87.54(7) . 3_666
O10 Si8 K19 162.51(7) . 3_666
O16 Si8 K19 65.28(9) 3_666 3_666
K27 Si8 K19 78.75(3) . 3_666
K32 Si8 K19 85.10(3) . 3_666
O63 Si8 K08 121.50(7) . .
O47 Si8 K08 52.30(6) . .
O10 Si8 K08 58.90(6) . .
O16 Si8 K08 128.26(9) 3_666 .
K27 Si8 K08 142.04(3) . .
K32 Si8 K08 66.02(2) . .
K19 Si8 K08 138.47(3) 3_666 .
O63 Si8 K11 165.25(7) . .
O47 Si8 K11 75.65(7) . .
O10 Si8 K11 73.53(6) . .
O16 Si8 K11 55.55(8) 3_666 .
K27 Si8 K11 104.58(3) . .
K32 Si8 K11 130.82(3) . .
K19 Si8 K11 110.47(2) 3_666 .
K08 Si8 K11 73.10(2) . .
O9 Si9 O32 118.57(10) . .
O9 Si9 O20 113.20(11) . .
O32 Si9 O20 109.18(11) . .
O9 Si9 O17 106.87(9) . .
O32 Si9 O17 105.57(9) . .
O20 Si9 O17 101.75(11) . .
O9 Si9 K09 168.34(7) . .
O32 Si9 K09 67.17(6) . .
O20 Si9 K09 55.46(9) . .
O17 Si9 K09 79.88(6) . .
O9 Si9 K05 75.14(7) . .
O32 Si9 K05 165.50(7) . .
O20 Si9 K05 58.26(8) . .
O17 Si9 K05 72.51(6) . .
K09 Si9 K05 98.49(3) . .
O9 Si9 K30 77.57(7) . .
O32 Si9 K30 82.69(7) . .
O20 Si9 K30 64.84(9) . .
O17 Si9 K30 166.28(7) . .
K09 Si9 K30 93.74(3) . .
K05 Si9 K30 96.70(3) . .
O9 Si9 K06 48.77(7) . .
O32 Si9 K06 71.02(6) . .
O20 Si9 K06 144.93(10) . .
O17 Si9 K06 112.08(6) . .
K09 Si9 K06 138.19(3) . .
K05 Si9 K06 123.29(3) . .
K30 Si9 K06 80.77(2) . .
O9 Si9 K04 69.65(7) . .
O32 Si9 K04 108.34(7) . .
O20 Si9 K04 133.52(9) . .
O17 Si9 K04 41.46(6) . .
K09 Si9 K04 119.43(3) . .
K05 Si9 K04 80.04(2) . .
K30 Si9 K04 146.83(3) . .
K06 Si9 K04 74.02(2) . .
O9 Si9 K35 118.08(7) . .
O32 Si9 K35 54.77(7) . .
O20 Si9 K35 127.25(9) . .
O17 Si9 K35 52.49(6) . .
K09 Si9 K35 73.58(2) . .
K05 Si9 K35 124.99(3) . .
K30 Si9 K35 137.38(3) . .
K06 Si9 K35 82.75(2) . .
K04 Si9 K35 60.42(2) . .
O61 Si10 O28 114.21(11) . .
O61 Si10 O45 109.97(9) . .
O28 Si10 O45 118.41(11) . .
O61 Si10 O17 108.29(9) . .
O28 Si10 O17 104.45(11) . .
O45 Si10 O17 99.85(9) . .
O61 Si10 K09 80.43(7) . .
O28 Si10 K09 52.49(9) . .
O45 Si10 K09 169.22(7) . .
O17 Si10 K09 78.79(6) . .
O61 Si10 K29 62.95(6) . .
O28 Si10 K29 148.24(10) . .
O45 Si10 K29 47.80(6) . .
O17 Si10 K29 106.22(6) . .
K09 Si10 K29 142.93(3) . .
O61 Si10 K04 102.28(7) . .
O28 Si10 K04 137.18(9) . .
O45 Si10 K04 64.44(6) . .
O17 Si10 K04 40.09(6) . .
K09 Si10 K04 117.15(3) . .
K29 Si10 K04 68.73(2) . .
O61 Si10 K35 47.55(7) . .
O28 Si10 K35 129.74(9) . .
O45 Si10 K35 111.63(6) . .
O17 Si10 K35 61.05(6) . .
K09 Si10 K35 77.25(2) . .
K29 Si10 K35 73.91(2) . .
K04 Si10 K35 63.21(2) . .
O61 Si10 K16 92.93(7) . .
O28 Si10 K16 71.63(9) . .
O45 Si10 K16 65.31(6) . .
O17 Si10 K16 157.66(7) . .
K09 Si10 K16 112.50(3) . .
K29 Si10 K16 76.87(2) . .
K04 Si10 K16 129.72(3) . .
K35 Si10 K16 138.62(3) . .
O61 Si10 K05 165.25(7) . .
O28 Si10 K05 65.47(9) . .
O45 Si10 K05 81.33(6) . .
O17 Si10 K05 59.22(6) . .
K09 Si10 K05 88.91(3) . .
K29 Si10 K05 125.79(3) . .
K04 Si10 K05 73.50(2) . .
K35 Si10 K05 120.20(3) . .
K16 Si10 K05 100.59(2) . .
O21 Si11 O24 120.50(10) . 1_455
O21 Si11 O2 116.02(11) . .
O24 Si11 O2 106.45(11) 1_455 .
O21 Si11 O10 103.01(9) . 1_455
O24 Si11 O10 104.55(9) 1_455 1_455
O2 Si11 O10 104.43(12) . 1_455
O21 Si11 K28 88.27(7) . 1_455
O24 Si11 K28 71.77(7) 1_455 1_455
O2 Si11 K28 66.91(9) . 1_455
O10 Si11 K28 168.22(7) 1_455 1_455
O21 Si11 K34 42.66(7) . 1_455
O24 Si11 K34 119.98(6) 1_455 1_455
O2 Si11 K34 133.36(10) . 1_455
O10 Si11 K34 61.51(6) 1_455 1_455
K28 Si11 K34 130.17(3) 1_455 1_455
O21 Si11 K13 55.66(7) . .
O24 Si11 K13 65.07(6) 1_455 .
O2 Si11 K13 141.90(10) . .
O10 Si11 K13 113.67(7) 1_455 .
K28 Si11 K13 75.42(2) 1_455 .
K34 Si11 K13 69.51(2) 1_455 .
O21 Si11 K27 86.36(7) . 1_455
O24 Si11 K27 153.05(7) 1_455 1_455
O2 Si11 K27 58.04(9) . 1_455
O10 Si11 K27 63.59(6) 1_455 1_455
K28 Si11 K27 114.57(3) 1_455 1_455
K34 Si11 K27 77.27(2) 1_455 1_455
K13 Si11 K27 141.24(3) . 1_455
O21 Si11 K11 176.24(8) . 1_455
O24 Si11 K11 55.93(6) 1_455 1_455
O2 Si11 K11 65.49(9) . 1_455
O10 Si11 K11 79.61(6) 1_455 1_455
K28 Si11 K11 89.29(2) 1_455 1_455
K34 Si11 K11 139.15(3) 1_455 1_455
K13 Si11 K11 120.89(3) . 1_455
K27 Si11 K11 97.26(2) 1_455 1_455
O21 Si11 K08 110.53(7) . 1_455
O24 Si11 K08 65.31(7) 1_455 1_455
O2 Si11 K08 128.17(9) . 1_455
O10 Si11 K08 41.82(6) 1_455 1_455
K28 Si11 K08 136.98(3) 1_455 1_455
K34 Si11 K08 72.98(2) 1_455 1_455
K13 Si11 K08 83.90(2) . 1_455
K27 Si11 K08 105.24(2) 1_455 1_455
K11 Si11 K08 69.567(19) 1_455 1_455
O42 Si12 O44 115.36(11) . .
O42 Si12 O46 112.05(9) . .
O44 Si12 O46 114.75(10) . .
O42 Si12 O26 107.00(9) . .
O44 Si12 O26 106.15(11) . .
O46 Si12 O26 99.79(8) . .
O42 Si12 K14 63.59(7) . .
O44 Si12 K14 64.54(9) . .
O46 Si12 K14 102.85(7) . .
O26 Si12 K14 157.35(7) . .
O42 Si12 K03 47.18(7) . .
O44 Si12 K03 144.50(10) . .
O46 Si12 K03 65.33(6) . .
O26 Si12 K03 108.75(7) . .
K14 Si12 K03 80.56(2) . .
O42 Si12 K23 83.89(7) . .
O44 Si12 K23 60.33(9) . .
O46 Si12 K23 162.76(7) . .
O26 Si12 K23 68.07(6) . .
K14 Si12 K23 89.92(3) . .
K03 Si12 K23 129.18(3) . .
O42 Si12 K02 57.14(7) . .
O44 Si12 K02 137.69(9) . .
O46 Si12 K02 105.20(6) . .
O26 Si12 K02 51.65(6) . .
K14 Si12 K02 120.22(3) . .
K03 Si12 K02 65.67(2) . .
K23 Si12 K02 77.38(2) . .
O42 Si12 K25 111.52(7) . .
O44 Si12 K25 133.12(10) . .
O46 Si12 K25 42.70(6) . .
O26 Si12 K25 58.55(6) . .
K14 Si12 K25 143.26(3) . .
K03 Si12 K25 73.17(2) . .
K23 Si12 K25 126.61(3) . .
K02 Si12 K25 71.19(2) . .
O42 Si12 K33 174.75(7) . .
O44 Si12 K33 59.73(9) . .
O46 Si12 K33 70.13(6) . .
O26 Si12 K33 76.93(6) . .
K14 Si12 K33 111.46(3) . .
K03 Si12 K33 135.43(3) . .
K23 Si12 K33 94.57(2) . .
K02 Si12 K33 127.46(3) . .
K25 Si12 K33 73.42(2) . .
O22 Si13 O33 108.45(12) . .
O22 Si13 O35 112.11(8) . .
O33 Si13 O35 109.57(11) . .
O22 Si13 O6 109.15(8) . 2_556
O33 Si13 O6 111.09(11) . 2_556
O35 Si13 O6 106.49(9) . 2_556
O22 Si13 K34 154.11(6) . 3_656
O33 Si13 K34 60.01(9) . 3_656
O35 Si13 K34 93.78(7) . 3_656
O6 Si13 K34 60.93(6) 2_556 3_656
O22 Si13 K26 84.89(5) . .
O33 Si13 K26 59.43(9) . .
O35 Si13 K26 69.76(6) . .
O6 Si13 K26 165.56(7) 2_556 .
K34 Si13 K26 104.93(3) 3_656 .
O22 Si13 K15 59.92(6) . .
O33 Si13 K15 138.15(10) . .
O35 Si13 K15 54.01(6) . .
O6 Si13 K15 110.61(6) 2_556 .
K34 Si13 K15 144.79(3) 3_656 .
K26 Si13 K15 78.96(2) . .
O22 Si13 K27 117.23(8) . 3_666
O33 Si13 K27 133.40(9) . 3_666
O35 Si13 K27 44.92(6) . 3_666
O6 Si13 K27 62.59(6) 2_556 3_666
K34 Si13 K27 80.90(2) 3_656 3_666
K26 Si13 K27 114.64(3) . 3_666
K15 Si13 K27 66.34(2) . 3_666
O22 Si13 K15 45.66(6) . 3_566
O33 Si13 K15 135.53(9) . 3_566
O35 Si13 K15 113.89(6) . 3_566
O6 Si13 K15 65.03(6) 2_556 3_566
K34 Si13 K15 124.26(3) 3_656 3_566
K26 Si13 K15 129.40(3) . 3_566
K15 Si13 K15 68.09(3) . 3_566
K27 Si13 K15 86.36(2) 3_666 3_566
O22 Si13 K26 64.24(5) . 3_556
O33 Si13 K26 69.07(9) . 3_556
O35 Si13 K26 174.65(7) . 3_556
O6 Si13 K26 78.69(7) 2_556 3_556
K34 Si13 K26 89.93(2) 3_656 3_556
K26 Si13 K26 105.55(2) . 3_556
K15 Si13 K26 123.31(3) . 3_556
K27 Si13 K26 139.80(3) 3_666 3_556
K15 Si13 K26 66.780(19) 3_566 3_556
O53 Si14 O57 125.97(10) . .
O53 Si14 O43 112.56(11) . .
O57 Si14 O43 108.80(11) . .
O53 Si14 O12 104.38(10) . .
O57 Si14 O12 99.48(9) . .
O43 Si14 O12 101.78(10) . .
O53 Si14 K25 78.33(7) . .
O57 Si14 K25 86.48(7) . .
O43 Si14 K25 68.21(9) . .
O12 Si14 K25 169.71(6) . .
O53 Si14 K33 58.10(7) . .
O57 Si14 K33 68.74(6) . .
O43 Si14 K33 150.81(9) . .
O12 Si14 K33 107.33(6) . .
K25 Si14 K33 82.61(2) . .
O53 Si14 K19 55.79(7) . .
O57 Si14 K19 107.58(6) . .
O43 Si14 K19 139.34(9) . .
O12 Si14 K19 54.41(6) . .
K25 Si14 K19 131.81(3) . .
K33 Si14 K19 62.13(2) . .
O53 Si14 K30 120.08(7) . .
O57 Si14 K30 45.94(6) . .
O43 Si14 K30 126.07(9) . .
O12 Si14 K30 55.58(6) . .
K25 Si14 K30 131.88(3) . .
K33 Si14 K30 74.42(2) . .
K19 Si14 K30 71.24(2) . .
O53 Si14 K06 164.38(8) . .
O57 Si14 K06 69.13(6) . .
O43 Si14 K06 53.75(8) . .
O12 Si14 K06 74.21(6) . .
K25 Si14 K06 100.45(3) . .
K33 Si14 K06 137.46(3) . .
K19 Si14 K06 127.73(3) . .
K30 Si14 K06 72.44(2) . .
O53 Si14 K32 64.76(7) . 3_656
O57 Si14 K32 168.53(7) . 3_656
O43 Si14 K32 66.47(9) . 3_656
O12 Si14 K32 72.15(6) . 3_656
K25 Si14 K32 100.71(3) . 3_656
K33 Si14 K32 120.76(3) . 3_656
K19 Si14 K32 74.33(2) . 3_656
K30 Si14 K32 127.40(3) . 3_656
K06 Si14 K32 100.55(2) . 3_656
O39 Si15 O12 115.47(10) . 2_656
O39 Si15 O64 111.59(11) . .
O12 Si15 O64 106.19(11) 2_656 .
O39 Si15 O54 113.50(10) . .
O12 Si15 O54 104.45(9) 2_656 .
O64 Si15 O54 104.73(11) . .
O39 Si15 K05 63.78(7) . .
O12 Si15 K05 110.83(7) 2_656 .
O64 Si15 K05 140.43(9) . .
O54 Si15 K05 52.94(6) . .
O39 Si15 K06 162.55(7) . 3_656
O12 Si15 K06 80.59(7) 2_656 3_656
O64 Si15 K06 54.47(9) . 3_656
O54 Si15 K06 65.75(6) . 3_656
K05 Si15 K06 118.66(3) . 3_656
O39 Si15 K04 66.72(7) . .
O12 Si15 K04 171.39(7) 2_656 .
O64 Si15 K04 65.83(9) . .
O54 Si15 K04 81.36(6) . .
K05 Si15 K04 77.71(2) . .
K06 Si15 K04 96.38(2) 3_656 .
O39 Si15 K30 123.77(7) . 3_666
O12 Si15 K30 47.78(6) 2_656 3_666
O64 Si15 K30 124.51(9) . 3_666
O54 Si15 K30 57.71(6) . 3_666
K05 Si15 K30 74.77(2) . 3_666
K06 Si15 K30 71.60(2) 3_656 3_666
K04 Si15 K30 138.90(3) . 3_666
O39 Si15 K32 77.74(7) . .
O12 Si15 K32 71.48(7) 2_656 .
O64 Si15 K32 67.06(8) . .
O54 Si15 K32 168.42(7) . .
K05 Si15 K32 138.55(3) . .
K06 Si15 K32 102.70(2) 3_656 .
K04 Si15 K32 101.58(2) . .
K30 Si15 K32 119.26(3) 3_666 .
O39 Si15 K19 78.41(7) . 3_666
O12 Si15 K19 37.83(6) 2_656 3_666
O64 Si15 K19 130.46(9) . 3_666
O54 Si15 K19 115.36(6) . 3_666
K05 Si15 K19 88.46(2) . 3_666
K06 Si15 K19 118.25(3) 3_656 3_666
K04 Si15 K19 145.11(3) . 3_666
K30 Si15 K19 63.67(2) 3_666 3_666
K32 Si15 K19 68.417(19) . 3_666
O59 Si16 O19 113.38(11) . .
O59 Si16 O18 114.80(9) . .
O19 Si16 O18 106.15(11) . .
O59 Si16 O13 110.65(9) . .
O19 Si16 O13 101.80(11) . .
O18 Si16 O13 109.18(9) . .
O59 Si16 K02 94.89(7) . .
O19 Si16 K02 62.63(9) . .
O18 Si16 K02 60.79(6) . .
O13 Si16 K02 154.14(7) . .
O59 Si16 K13 78.70(7) . .
O19 Si16 K13 57.97(9) . .
O18 Si16 K13 163.37(7) . .
O13 Si16 K13 72.42(7) . .
K02 Si16 K13 110.29(3) . .
O59 Si16 K10 173.73(7) . .
O19 Si16 K10 61.26(9) . .
O18 Si16 K10 70.81(6) . .
O13 Si16 K10 68.73(7) . .
K02 Si16 K10 85.44(3) . .
K13 Si16 K10 95.30(3) . .
O59 Si16 K31 108.08(6) . .
O19 Si16 K31 138.25(9) . .
O18 Si16 K31 58.36(6) . .
O13 Si16 K31 57.55(6) . .
K02 Si16 K31 119.12(3) . .
K13 Si16 K31 128.88(3) . .
K10 Si16 K31 77.05(2) . .
O59 Si16 K23 60.82(6) . .
O19 Si16 K23 140.58(9) . .
O18 Si16 K23 55.64(6) . .
O13 Si16 K23 116.92(7) . .
K02 Si16 K23 78.58(2) . .
K13 Si16 K23 139.35(3) . .
K10 Si16 K23 125.28(3) . .
K31 Si16 K23 66.71(2) . .
O59 Si16 K28 58.91(6) . 1_455
O19 Si16 K28 129.21(9) . 1_455
O18 Si16 K28 122.89(6) . 1_455
O13 Si16 K28 52.50(6) . 1_455
K02 Si16 K28 153.35(3) . 1_455
K13 Si16 K28 71.79(2) . 1_455
K10 Si16 K28 121.14(3) . 1_455
K31 Si16 K28 70.08(2) . 1_455
K23 Si16 K28 83.60(2) . 1_455
O1 Si17 O25 105.67(11) . .
O1 Si17 O65 115.36(11) . .
O25 Si17 O65 115.43(9) . .
O1 Si17 O50 109.45(11) . .
O25 Si17 O50 106.69(9) . .
O65 Si17 O50 103.87(9) . .
O1 Si17 K35 62.86(9) . .
O25 Si17 K35 83.68(7) . .
O65 Si17 K35 74.31(6) . .
O50 Si17 K35 168.89(7) . .
O1 Si17 K18 61.46(9) . .
O25 Si17 K18 166.90(7) . .
O65 Si17 K18 74.70(6) . .
O50 Si17 K18 77.35(6) . .
K35 Si17 K18 91.66(3) . .
O1 Si17 K03 62.80(9) . .
O25 Si17 K03 67.47(6) . .
O65 Si17 K03 177.09(7) . .
O50 Si17 K03 75.13(6) . .
K35 Si17 K03 106.14(3) . .
K18 Si17 K03 102.40(3) . .
O1 Si17 K24 135.48(10) . .
O25 Si17 K24 114.89(6) . .
O65 Si17 K24 62.60(6) . .
O50 Si17 K24 42.45(6) . .
K35 Si17 K24 136.89(3) . .
K18 Si17 K24 76.69(2) . .
K03 Si17 K24 116.84(3) . .
O1 Si17 K09 136.88(10) . .
O25 Si17 K09 61.59(6) . .
O65 Si17 K09 54.20(6) . .
O50 Si17 K09 113.67(7) . .
K35 Si17 K09 74.49(2) . .
K18 Si17 K09 128.87(3) . .
K03 Si17 K09 128.71(3) . .
K24 Si17 K09 81.09(2) . .
O1 Si17 K14 130.81(9) . .
O25 Si17 K14 65.79(6) . .
O65 Si17 K14 111.24(6) . .
O50 Si17 K14 42.47(6) . .
K35 Si17 K14 148.57(3) . .
K18 Si17 K14 119.76(3) . .
K03 Si17 K14 69.95(2) . .
K24 Si17 K14 58.58(2) . .
K09 Si17 K14 84.07(2) . .
O23 Si18 O51 110.53(12) . .
O23 Si18 O34 121.06(10) . .
O51 Si18 O34 109.05(11) . .
O23 Si18 O3 107.71(10) . .
O51 Si18 O3 103.87(11) . .
O34 Si18 O3 103.02(9) . .
O23 Si18 K11 60.63(7) . .
O51 Si18 K11 151.64(9) . .
O34 Si18 K11 63.62(6) . .
O3 Si18 K11 104.49(6) . .
O23 Si18 K12 168.16(7) . 3_655
O51 Si18 K12 57.72(9) . 3_655
O34 Si18 K12 65.75(6) . 3_655
O3 Si18 K12 78.41(6) . 3_655
K11 Si18 K12 128.57(3) . 3_655
O23 Si18 K08 63.25(7) . .
O51 Si18 K08 65.38(9) . .
O34 Si18 K08 97.70(7) . .
O3 Si18 K08 158.98(7) . .
K11 Si18 K08 87.80(3) . .
K12 Si18 K08 107.44(3) 3_655 .
O23 Si18 K16 64.46(7) . .
O51 Si18 K16 137.91(10) . .
O34 Si18 K16 107.97(7) . .
O3 Si18 K16 48.05(6) . .
K11 Si18 K16 65.87(2) . .
K12 Si18 K16 124.49(3) 3_655 .
K08 Si18 K16 127.70(3) . .
O23 Si18 K29 76.33(7) . .
O51 Si18 K29 58.21(9) . .
O34 Si18 K29 162.41(7) . .
O3 Si18 K29 71.30(6) . .
K11 Si18 K29 133.56(3) . .
K12 Si18 K29 96.67(3) 3_655 .
K08 Si18 K29 87.84(3) . .
K16 Si18 K29 81.01(2) . .
O23 Si18 K17 121.12(7) . .
O51 Si18 K17 127.86(10) . .
O34 Si18 K17 49.18(6) . .
O3 Si18 K17 55.41(6) . .
K11 Si18 K17 70.08(2) . .
K12 Si18 K17 70.72(2) 3_655 .
K08 Si18 K17 145.56(3) . .
K16 Si18 K17 67.43(2) . .
K29 Si18 K17 126.55(3) . .
Sc7 F1 Sc7 163.15(11) 4 .
Sc7 F1 K29 96.86(5) 4 .
Sc7 F1 K29 96.86(5) . .
Sc7 F1 K04 95.50(5) 4 .
Sc7 F1 K04 95.50(5) . .
K29 F1 K04 84.50(6) . .
Sc7 F1 K08 83.66(5) 4 .
Sc7 F1 K08 83.66(5) . .
K29 F1 K08 103.51(6) . .
K04 F1 K08 171.98(7) . .
Sc4 F2 Sc4 167.22(11) 4 .
Sc4 F2 K02 92.42(5) 4 .
Sc4 F2 K02 92.42(5) . .
Sc4 F2 K03 96.26(5) 4 .
Sc4 F2 K03 96.26(5) . .
K02 F2 K03 79.41(5) . .
Sc4 F2 K10 83.79(5) 4 .
Sc4 F2 K10 83.79(5) . .
K02 F2 K10 98.76(6) . .
K03 F2 K10 178.16(7) . .
Sc4 F3 Sc4 168.48(11) . 4_565
Sc4 F3 K31 88.22(5) . .
Sc4 F3 K31 88.22(5) 4_565 .
Sc4 F3 K14 91.25(5) . .
Sc4 F3 K14 91.25(5) 4_565 .
K31 F3 K14 174.48(8) . .
Sc4 F3 K23 95.09(5) . .
Sc4 F3 K23 95.10(5) 4_565 .
K31 F3 K23 80.25(5) . .
K14 F3 K23 105.27(6) . .
Sc3 F4 Sc3 180.0 3_656 .
Sc3 F4 K06 90.000(1) 3_656 .
Sc3 F4 K06 90.0 . .
Sc3 F4 K06 90.0 3_656 3_656
Sc3 F4 K06 90.000(1) . 3_656
K06 F4 K06 180.0 . 3_656
Sc5 F5 Sc5 165.21(11) . 4_565
Sc2 F6 Sc2 162.76(10) . 4_565
Sc2 F6 K01 94.15(5) . .
Sc2 F6 K01 94.15(5) 4_565 .
Sc2 F6 K24 98.53(5) . .
Sc2 F6 K24 98.53(5) 4_565 .
K01 F6 K24 69.36(5) . .
Sc2 F6 K17 81.89(5) . 3_665
Sc2 F6 K17 81.89(5) 4_565 3_665
K01 F6 K17 99.13(6) . 3_665
K24 F6 K17 168.49(7) . 3_665
Sc7 F7 Sc7 171.08(9) . 4_565
Sc7 F7 K16 87.06(5) . .
Sc7 F7 K16 87.07(5) 4_565 .
Sc2 F8 Sc2 173.56(11) 4 .
Sc2 F8 K21 90.16(5) 4 .
Sc2 F8 K21 90.16(5) . .
Sc2 F8 K12 93.22(6) 4 .
Sc2 F8 K12 93.22(6) . .
K21 F8 K12 89.72(6) . .
Sc10 F9 Sc10 180.0 3 .
Sc8 F10 Sc8 175.60(11) 4 .
Sc8 F10 K18 91.93(5) 4 .
Sc8 F10 K18 91.93(5) . .
Sc8 F10 K35 90.23(5) 4 .
Sc8 F10 K35 90.23(5) . .
K18 F10 K35 112.47(7) . .
Sc8 F10 K07 89.36(6) 4 3_655
Sc8 F10 K07 89.36(6) . 3_655
K18 F10 K07 78.42(5) . 3_655
K35 F10 K07 169.11(7) . 3_655
Sc8 F11 Sc8 165.60(10) 4_565 .
Sc8 F11 K36 90.89(5) 4_565 .
Sc8 F11 K36 90.89(5) . .
Sc8 F11 K09 89.17(5) 4_565 .
Sc8 F11 K09 89.17(5) . .
K36 F11 K09 179.54(7) . .
Sc9 F12 Sc9 165.76(11) 4_565 .
Sc9 F12 K33 96.85(6) 4_565 .
Sc9 F12 K33 96.85(6) . .
Sc9 F12 K19 89.55(5) 4_565 .
Sc9 F12 K19 89.55(5) . .
K33 F12 K19 77.89(6) . .
Sc9 F12 K27 82.93(6) 4_565 3_666
Sc9 F12 K27 82.92(6) . 3_666
K33 F12 K27 170.69(8) . 3_666
K19 F12 K27 92.80(6) . 3_666
Sc9 F12 K15 89.56(5) 4_565 .
Sc9 F12 K15 89.56(5) . .
K33 F12 K15 109.30(6) . .
K19 F12 K15 172.81(8) . .
K27 F12 K15 80.01(5) 3_666 .
Sc1 F13 Sc1 174.01(10) . 4
Sc1 F13 K25 89.54(5) . .
Sc1 F13 K25 89.54(5) 4 .
Sc6 F14 Sc6 167.92(10) . 4
Sc6 F14 K13 96.03(5) . 1_655
Sc6 F14 K13 96.04(5) 4 1_655
Sc6 F14 K20 88.95(5) . 3_655
Sc6 F14 K20 88.95(5) 4 3_655
K13 F14 K20 98.48(5) 1_655 3_655
Sc6 F14 K12 83.96(5) . 3_655
Sc6 F14 K12 83.96(5) 4 3_655
K13 F14 K12 179.40(7) 1_655 3_655
K20 F14 K12 80.92(5) 3_655 3_655
Sc3 F15 Sc3 180.0 3_666 .
Sc3 F15 K05 90.0 3_666 3_666
Sc3 F15 K05 90.0 . 3_666
Sc3 F15 K05 90.0 3_666 .
Sc3 F15 K05 90.0 . .
K05 F15 K05 180.0 3_666 .
Sc5 F16 Sc5 169.11(10) 4 .
Sc5 F16 K34 84.93(5) 4 1_455
Sc5 F16 K34 84.93(5) . 1_455
Sc6 F17 Sc6 173.39(10) 4_565 .
Sc6 F17 K11 86.78(5) 4_565 .
Sc6 F17 K11 86.78(5) . .
Sc6 F17 K28 90.21(5) 4_565 .
Sc6 F17 K28 90.21(5) . .
K11 F17 K28 106.62(6) . .
Sc6 F17 K22 93.17(5) 4_565 .
Sc6 F17 K22 93.17(5) . .
K11 F17 K22 176.43(6) . .
K28 F17 K22 69.81(4) . .
Sc6 F17 K17 90.14(5) 4_565 .
Sc6 F17 K17 90.14(5) . .
K11 F17 K17 79.43(4) . .
K28 F17 K17 173.95(6) . .
K22 F17 K17 104.14(5) . .
Sc10 F18 Sc10 180.0 . 3_565
Sc10 F18 K22 90.0 . 3_665
Sc10 F18 K22 90.0 3_565 3_665
Sc10 F18 K22 90.0 . 1_455
Sc10 F18 K22 90.0 3_565 1_455
K22 F18 K22 180.00(3) 3_665 1_455
Sc1 F19 Sc1 171.78(10) 4_565 .
Sc1 F19 K09 93.66(5) 4_565 .
Sc1 F19 K09 93.66(5) . .
Sc1 F19 K30 91.28(5) 4_565 .
Sc1 F19 K30 91.28(5) . .
K09 F19 K30 98.89(5) . .
Sc9 F20 Sc9 172.47(11) . 4
Sc9 F20 K32 93.52(5) . 3_656
Sc9 F20 K32 93.52(5) 4 3_656
Sc9 F20 K26 86.37(5) . .
Sc9 F20 K26 86.37(5) 4 .
K32 F20 K26 174.81(8) 3_656 .
Si17 O1 Si17 176.41(19) . 4
Si17 O1 K35 88.45(9) . .
Si17 O1 K35 88.45(9) 4 .
Si17 O1 K18 91.34(9) . .
Si17 O1 K18 91.34(9) 4 .
K35 O1 K18 108.44(8) . .
Si17 O1 K03 90.25(9) . .
Si17 O1 K03 90.25(9) 4 .
K35 O1 K03 127.92(9) . .
K18 O1 K03 123.64(8) . .
Si11 O2 Si11 166.61(19) 4_565 .
Si11 O2 K28 83.66(9) 4_565 1_455
Si11 O2 K28 83.66(9) . 1_455
Si11 O2 K27 96.37(9) 4_565 1_455
Si11 O2 K27 96.37(9) . 1_455
K28 O2 K27 143.26(9) 1_455 1_455
Si11 O2 K11 89.00(9) 4_565 1_455
Si11 O2 K11 89.00(9) . 1_455
K28 O2 K11 100.17(7) 1_455 1_455
K27 O2 K11 116.57(8) 1_455 1_455
Si4 O3 Si18 137.93(12) . .
Si4 O3 K16 121.50(9) . .
Si18 O3 K16 99.23(8) . .
Si4 O3 K29 87.26(7) . .
Si18 O3 K29 77.30(6) . .
K16 O3 K29 96.58(6) . .
Si4 O3 K17 93.60(8) . .
Si18 O3 K17 98.01(7) . .
K16 O3 K17 88.32(5) . .
K29 O3 K17 173.67(6) . .
Si4 O3 K12 73.16(7) . 3_655
Si18 O3 K12 69.91(6) . 3_655
K16 O3 K12 161.16(7) . 3_655
K29 O3 K12 95.90(5) . 3_655
K17 O3 K12 78.39(4) . 3_655
Si4 O4 Sc8 167.75(10) . .
Si4 O4 K36 99.15(8) . .
Sc8 O4 K36 88.76(6) . .
Si4 O4 K07 80.73(7) . 3_655
Sc8 O4 K07 89.61(6) . 3_655
K36 O4 K07 92.80(5) . 3_655
Si4 O4 K29 80.16(7) . .
Sc8 O4 K29 95.05(6) . .
K36 O4 K29 162.74(6) . .
K07 O4 K29 104.03(5) 3_655 .
Si5 O5 Si5 159.97(18) . 4
Si5 O5 K21 84.78(9) . .
Si5 O5 K21 84.78(9) 4 .
Si5 O5 K03 99.62(9) . .
Si5 O5 K03 99.62(9) 4 .
K21 O5 K03 137.50(9) . .
Si13 O6 Sc5 155.12(10) 2_556 .
Si13 O6 K34 88.08(7) 2_556 1_455
Sc5 O6 K34 80.48(6) . 1_455
Si13 O6 K27 89.74(7) 2_556 1_455
Sc5 O6 K27 113.06(7) . 1_455
K34 O6 K27 94.84(5) 1_455 1_455
Si13 O6 K15 88.96(7) 2_556 .
Sc5 O6 K15 96.59(6) . .
K34 O6 K15 165.48(6) 1_455 .
K27 O6 K15 99.36(4) 1_455 .
Si1 O7 Si1 137.78(15) . 2_655
Si1 O7 K07 99.80(5) . 3_655
Si1 O7 K07 108.66(5) 2_655 3_655
Si1 O7 K07 108.67(5) . .
Si1 O7 K07 99.80(5) 2_655 .
K07 O7 K07 94.24(7) 3_655 .
Si4 O8 Si4 164.90(17) . 4
Si4 O8 K12 97.52(9) . 3_655
Si4 O8 K12 97.52(9) 4 3_655
Si4 O8 K07 85.06(9) . 3_655
Si4 O8 K07 85.06(9) 4 3_655
K12 O8 K07 135.97(10) 3_655 3_655
Si4 O8 K29 86.60(9) . .
Si4 O8 K29 86.59(9) 4 .
K12 O8 K29 111.86(8) 3_655 .
K07 O8 K29 112.17(8) 3_655 .
Si9 O9 Sc3 155.62(10) . .
Si9 O9 K06 104.28(9) . .
Sc3 O9 K06 99.13(7) . .
Si9 O9 K05 77.26(7) . .
Sc3 O9 K05 80.67(5) . .
K06 O9 K05 171.07(7) . .
Si9 O9 K04 83.78(8) . .
Sc3 O9 K04 103.97(6) . .
K06 O9 K04 87.92(5) . .
K05 O9 K04 83.48(5) . .
Si9 O9 K30 75.16(7) . .
Sc3 O9 K30 97.41(6) . .
K06 O9 K30 92.27(6) . .
K05 O9 K30 96.62(4) . .
K04 O9 K30 158.32(6) . .
Si8 O10 Si11 139.76(12) . 1_655
Si8 O10 K08 91.84(7) . .
Si11 O10 K08 114.16(8) 1_655 .
Si8 O10 K34 120.85(8) . .
Si11 O10 K34 87.57(7) 1_655 .
K08 O10 K34 96.59(6) . .
Si8 O10 K27 66.54(6) . .
Si11 O10 K27 87.89(7) 1_655 .
K08 O10 K27 157.31(6) . .
K34 O10 K27 89.31(4) . .
Si7 O11 Si7 158.28(16) 4_565 .
Si7 O11 K33 100.51(8) 4_565 .
Si7 O11 K33 100.51(8) . .
Si7 O11 K15 87.80(9) 4_565 .
Si7 O11 K15 87.80(9) . .
K33 O11 K15 116.28(8) . .
Si7 O11 K23 81.97(8) 4_565 .
Si7 O11 K23 81.97(8) . .
K33 O11 K23 123.29(8) . .
K15 O11 K23 120.44(8) . .
Si15 O12 Si14 139.14(11) 2_656 .
Si15 O12 K19 120.58(9) 2_656 .
Si14 O12 K19 93.38(7) . .
Si15 O12 K30 107.18(8) 2_656 .
Si14 O12 K30 93.43(7) . .
K19 O12 K30 90.43(5) . .
Si6 O13 Si16 150.43(12) . .
Si6 O13 K31 114.65(8) . .
Si16 O13 K31 93.12(8) . .
Si6 O13 K28 89.41(8) . 1_455
Si16 O13 K28 102.01(8) . 1_455
K31 O13 K28 88.17(5) . 1_455
Si6 O13 K10 88.64(7) . .
Si16 O13 K10 81.92(7) . .
K31 O13 K10 88.32(5) . .
K28 O13 K10 174.86(6) 1_455 .
Si6 O13 K13 76.45(7) . .
Si16 O13 K13 77.96(7) . .
K31 O13 K13 165.93(6) . .
K28 O13 K13 83.15(5) 1_455 .
K10 O13 K13 101.00(5) . .
Si3 O14 Si3 163.82(17) 2_655 3_665
Si3 O14 K17 86.32(9) 2_655 .
Si3 O14 K17 86.32(9) 3_665 .
Si3 O14 K22 98.02(8) 2_655 .
Si3 O14 K22 98.02(8) 3_665 .
K17 O14 K22 124.84(9) . .
Si3 O14 K01 83.90(8) 2_655 3_665
Si3 O14 K01 83.91(8) 3_665 3_665
K17 O14 K01 103.91(8) . 3_665
K22 O14 K01 131.25(8) . 3_665
Si3 O15 Sc6 151.53(10) 2_655 .
Si3 O15 K20 103.02(8) 2_655 3_655
Sc6 O15 K20 105.42(7) . 3_655
Si3 O15 K12 90.59(7) 2_655 3_655
Sc6 O15 K12 88.92(6) . 3_655
K20 O15 K12 93.50(5) 3_655 3_655
Si3 O15 K17 62.19(6) 2_655 .
Sc6 O15 K17 89.85(6) . .
K20 O15 K17 162.89(7) 3_655 .
K12 O15 K17 78.85(4) 3_655 .
Si3 O15 K22 93.34(7) 2_655 .
Sc6 O15 K22 85.77(6) . .
K20 O15 K22 89.41(5) 3_655 .
K12 O15 K22 174.47(6) 3_655 .
K17 O15 K22 99.56(4) . .
Si8 O16 Si8 159.63(16) 2_656 3_666
Si8 O16 K27 81.44(8) 2_656 3_666
Si8 O16 K27 81.44(8) 3_666 3_666
Si8 O16 K19 84.16(9) 2_656 .
Si8 O16 K19 84.16(9) 3_666 .
K27 O16 K19 87.55(7) 3_666 .
Si8 O16 K11 99.76(8) 2_656 3_666
Si8 O16 K11 99.76(8) 3_666 3_666
K27 O16 K11 130.76(9) 3_666 3_666
K19 O16 K11 141.68(8) . 3_666
Si10 O17 Si9 137.39(11) . .
Si10 O17 K04 112.57(9) . .
Si9 O17 K04 109.83(8) . .
Si10 O17 K35 89.18(7) . .
Si9 O17 K35 100.27(8) . .
K04 O17 K35 82.74(5) . .
Si10 O17 K05 93.19(7) . .
Si9 O17 K05 75.96(6) . .
K04 O17 K05 99.08(6) . .
K35 O17 K05 176.17(7) . .
Si10 O17 K09 71.14(6) . .
Si9 O17 K09 69.36(6) . .
K04 O17 K09 163.97(7) . .
K35 O17 K09 81.71(4) . .
K05 O17 K09 96.21(5) . .
Si16 O18 Sc4 159.86(11) . .
Si16 O18 K02 88.33(7) . .
Sc4 O18 K02 93.51(6) . .
Si16 O18 K23 95.90(8) . .
Sc4 O18 K23 103.81(7) . .
K02 O18 K23 96.31(5) . .
Si16 O18 K31 92.75(7) . .
Sc4 O18 K31 86.14(6) . .
K02 O18 K31 177.77(7) . .
K23 O18 K31 81.65(4) . .
Si16 O18 K10 80.42(7) . .
Sc4 O18 K10 79.44(6) . .
K02 O18 K10 95.28(5) . .
K23 O18 K10 167.74(6) . .
K31 O18 K10 86.83(5) . .
Si16 O19 Si16 173.96(18) 4 .
Si16 O19 K13 92.67(9) 4 .
Si16 O19 K13 92.67(9) . .
Si16 O19 K02 87.03(9) 4 .
Si16 O19 K02 87.03(9) . .
K13 O19 K02 141.71(10) . .
Si16 O19 K10 90.00(9) 4 .
Si16 O19 K10 90.00(9) . .
K13 O19 K10 117.83(8) . .
K02 O19 K10 100.46(8) . .
Si9 O20 Si9 169.05(18) 4_565 .
Si9 O20 K09 93.46(9) 4_565 .
Si9 O20 K09 93.46(9) . .
Si9 O20 K05 91.08(9) 4_565 .
Si9 O20 K05 91.08(9) . .
K09 O20 K05 129.34(10) . .
Si9 O20 K30 84.70(9) 4_565 .
Si9 O20 K30 84.71(9) . .
K09 O20 K30 114.43(8) . .
K05 O20 K30 116.22(9) . .
Si11 O21 Sc5 149.62(10) . .
Si11 O21 K34 113.93(10) . 1_455
Sc5 O21 K34 87.35(6) . 1_455
Si11 O21 K13 100.13(9) . .
Sc5 O21 K13 100.55(7) . .
K34 O21 K13 91.88(5) 1_455 .
Si13 O22 Si13 146.89(16) 2_556 .
Si13 O22 K15 92.41(5) 2_556 3_566
Si13 O22 K15 111.77(6) . 3_566
Si13 O22 K15 111.77(6) 2_556 .
Si13 O22 K15 92.40(5) . .
K15 O22 K15 87.15(6) 3_566 .
Si18 O23 Sc7 155.02(11) . .
Si18 O23 K11 90.56(9) . .
Sc7 O23 K11 114.01(7) . .
Si18 O23 K08 89.41(8) . .
Sc7 O23 K08 89.03(6) . .
K11 O23 K08 103.55(6) . .
Si18 O23 K16 88.40(8) . .
Sc7 O23 K16 93.37(6) . .
K11 O23 K16 75.49(4) . .
K08 O23 K16 177.60(8) . .
Si18 O23 K29 77.87(7) . .
Sc7 O23 K29 77.40(5) . .
K11 O23 K29 158.65(7) . .
K08 O23 K29 94.32(5) . .
K16 O23 K29 86.19(5) . .
Si11 O24 Sc6 168.35(11) 1_655 .
Si11 O24 K11 99.30(8) 1_655 .
Sc6 O24 K11 82.98(6) . .
Si11 O24 K28 79.60(7) 1_655 .
Sc6 O24 K28 88.75(6) . .
K11 O24 K28 103.30(5) . .
Si11 O24 K13 88.73(7) 1_655 1_655
Sc6 O24 K13 89.94(6) . 1_655
K11 O24 K13 171.06(6) . 1_655
K28 O24 K13 81.90(4) . 1_655
Si17 O25 Sc1 164.53(10) . .
Si17 O25 K09 92.12(7) . .
Sc1 O25 K09 91.09(6) . .
Si17 O25 K03 85.14(7) . .
Sc1 O25 K03 93.17(6) . .
K09 O25 K03 173.27(6) . .
Si7 O26 Si12 136.56(12) . .
Si7 O26 K02 121.81(9) . .
Si12 O26 K02 97.73(7) . .
Si7 O26 K25 105.07(8) . .
Si12 O26 K25 91.02(7) . .
K02 O26 K25 89.98(6) . .
Si7 O26 K23 80.90(7) . .
Si12 O26 K23 80.22(7) . .
K02 O26 K23 92.33(5) . .
K25 O26 K23 171.17(6) . .
Si2 O27 Si3 131.95(11) . .
Si2 O27 K21 122.24(9) . .
Si3 O27 K21 98.40(8) . .
Si2 O27 K20 106.70(8) . .
Si3 O27 K20 92.02(7) . .
K21 O27 K20 95.83(5) . .
Si10 O28 Si10 161.95(18) 4_565 .
Si10 O28 K09 98.74(9) 4_565 .
Si10 O28 K09 98.75(9) . .
Si10 O28 K16 81.87(9) 4_565 .
Si10 O28 K16 81.86(9) . .
K09 O28 K16 140.18(9) . .
Si10 O28 K05 89.29(9) 4_565 .
Si10 O28 K05 89.29(9) . .
K09 O28 K05 108.78(8) . .
K16 O28 K05 111.03(7) . .
Si1 O29 Si1 163.61(17) 4_565 .
Si1 O29 K36 85.03(8) 4_565 .
Si1 O29 K36 85.03(8) . .
Si1 O29 K36 98.18(9) 4_565 3_665
Si1 O29 K36 98.18(9) . 3_665
K36 O29 K36 124.43(8) . 3_665
Si1 O29 K24 85.01(9) 4_565 .
Si1 O29 K24 85.01(9) . .
K36 O29 K24 104.94(7) . .
K36 O29 K24 130.63(8) 3_665 .
Si6 O30 Si6 169.68(18) . 4
Si6 O30 K13 95.15(9) . .
Si6 O30 K13 95.15(9) 4 .
Si6 O30 K20 87.45(9) . 3
Si6 O30 K20 87.45(9) 4 3
K13 O30 K20 115.71(9) . 3
Si6 O30 K10 88.02(9) . .
Si6 O30 K10 88.02(9) 4 .
K13 O30 K10 116.49(8) . .
K20 O30 K10 127.81(9) 3 .
Si3 O31 Sc2 154.05(10) . .
Si3 O31 K21 97.53(8) . .
Sc2 O31 K21 91.52(6) . .
Si3 O31 K12 101.20(8) . .
Sc2 O31 K12 102.15(7) . .
K21 O31 K12 95.14(5) . .
Si3 O31 K17 74.86(6) . 3_665
Sc2 O31 K17 93.57(6) . 3_665
K21 O31 K17 171.12(7) . 3_665
K12 O31 K17 90.90(5) . 3_665
Si9 O32 Sc1 152.95(10) . .
Si9 O32 K09 82.88(7) . .
Sc1 O32 K09 95.57(6) . .
Si9 O32 K35 100.32(8) . .
Sc1 O32 K35 106.57(6) . .
K09 O32 K35 86.91(5) . .
Si9 O32 K06 80.19(7) . .
Sc1 O32 K06 99.45(6) . .
K09 O32 K06 163.08(7) . .
K35 O32 K06 96.18(4) . .
Si9 O32 K30 69.64(6) . .
Sc1 O32 K30 83.61(5) . .
K09 O32 K30 94.21(4) . .
K35 O32 K30 169.62(6) . .
K06 O32 K30 79.84(4) . .
Si13 O33 Si13 173.91(18) . 4
Si13 O33 K34 90.66(9) . 3_656
Si13 O33 K34 90.66(9) 4 3_656
Si13 O33 K26 91.71(9) . .
Si13 O33 K26 91.71(9) 4 .
K34 O33 K26 133.29(9) 3_656 .
Si18 O34 Sc6 153.39(11) . .
Si18 O34 K11 84.89(7) . .
Sc6 O34 K11 94.70(6) . .
Si18 O34 K12 83.95(7) . 3_655
Sc6 O34 K12 99.47(7) . 3_655
K11 O34 K12 165.43(7) . 3_655
Si18 O34 K17 107.85(8) . .
Sc6 O34 K17 98.70(6) . .
K11 O34 K17 87.54(5) . .
K12 O34 K17 87.00(5) 3_655 .
Si13 O35 Sc9 153.71(10) . .
Si13 O35 K27 109.78(9) . 3_666
Sc9 O35 K27 87.07(6) . 3_666
Si13 O35 K15 97.41(8) . .
Sc9 O35 K15 103.12(7) . .
K27 O35 K15 88.88(5) 3_666 .
Si13 O35 K26 80.87(7) . .
Sc9 O35 K26 82.14(6) . .
K27 O35 K26 169.10(7) 3_666 .
K15 O35 K26 92.04(5) . .
Si5 O36 Sc2 168.54(10) . .
Si5 O36 K01 89.11(8) . .
Sc2 O36 K01 100.57(6) . .
Si5 O36 K21 83.05(7) . .
Sc2 O36 K21 89.24(6) . .
K01 O36 K21 99.65(6) . .
Si5 O36 K24 85.72(7) . .
Sc2 O36 K24 102.65(6) . .
K01 O36 K24 74.67(4) . .
K21 O36 K24 167.52(7) . .
Si1 O37 Sc2 151.24(9) . .
Si1 O37 K18 89.03(7) . .
Sc2 O37 K18 110.42(7) . .
Si1 O37 K07 94.90(8) . .
Sc2 O37 K07 103.14(6) . .
K18 O37 K07 97.02(5) . .
Si7 O38 Sc9 147.49(9) . .
Si7 O38 K26 105.95(9) . .
Sc9 O38 K26 96.34(7) . .
Si7 O38 K25 98.33(8) . .
Sc9 O38 K25 103.07(6) . .
K26 O38 K25 94.96(5) . .
Si7 O38 K33 79.95(7) . .
Sc9 O38 K33 79.19(5) . .
K26 O38 K33 173.70(7) . .
K25 O38 K33 81.86(4) . .
Si7 O38 K15 73.79(6) . .
Sc9 O38 K15 82.10(5) . .
K26 O38 K15 92.29(6) . .
K25 O38 K15 170.55(6) . .
K33 O38 K15 91.48(4) . .
Si15 O39 Sc7 161.69(11) . .
Si15 O39 K05 89.36(8) . .
Sc7 O39 K05 108.95(7) . .
Si15 O39 K04 88.02(8) . .
Sc7 O39 K04 92.90(6) . .
K05 O39 K04 87.32(5) . .
Si2 O40 Sc4 154.10(10) . .
Si2 O40 K10 104.90(9) . .
Sc4 O40 K10 100.82(7) . .
Si2 O40 K31 85.70(7) . .
Sc4 O40 K31 86.59(6) . .
K10 O40 K31 100.58(6) . .
Si5 O41 Sc4 147.54(9) . .
Si5 O41 K14 104.55(8) . .
Sc4 O41 K14 97.05(7) . .
Si5 O41 K01 92.66(8) . .
Sc4 O41 K01 113.34(7) . .
K14 O41 K01 85.08(5) . .
Si5 O41 K03 76.40(6) . .
Sc4 O41 K03 80.52(5) . .
K14 O41 K03 87.95(5) . .
K01 O41 K03 165.14(7) . .
Si12 O42 Sc4 151.25(10) . .
Si12 O42 K03 106.30(9) . .
Sc4 O42 K03 102.45(7) . .
Si12 O42 K02 96.46(8) . .
Sc4 O42 K02 86.76(6) . .
K03 O42 K02 84.35(5) . .
Si12 O42 K14 88.41(7) . .
Sc4 O42 K14 85.11(6) . .
K03 O42 K14 102.11(6) . .
K02 O42 K14 170.54(7) . .
Si14 O43 Si14 158.08(17) . 4
Si14 O43 K25 81.17(9) . .
Si14 O43 K25 81.17(9) 4 .
Si14 O43 K06 100.25(9) . .
Si14 O43 K06 100.25(9) 4 .
K25 O43 K06 123.22(9) . .
Si14 O43 K32 87.40(9) . 3_656
Si14 O43 K32 87.40(9) 4 3_656
K25 O43 K32 112.36(7) . 3_656
K06 O43 K32 124.43(8) . 3_656
Si12 O44 Si12 171.26(19) 4_565 .
Si12 O44 K23 90.23(9) 4_565 .
Si12 O44 K23 90.23(9) . .
Si12 O44 K14 85.74(9) 4_565 .
Si12 O44 K14 85.74(9) . .
K23 O44 K14 105.61(8) . .
Si12 O44 K33 93.83(9) 4_565 .
Si12 O44 K33 93.82(9) . .
K23 O44 K33 115.94(8) . .
K14 O44 K33 138.45(8) . .
Si10 O45 Sc7 154.42(10) . .
Si10 O45 K29 103.55(8) . .
Sc7 O45 K29 102.00(7) . .
Si10 O45 K04 86.97(7) . .
Sc7 O45 K04 96.61(6) . .
K29 O45 K04 84.62(5) . .
Si10 O45 K16 86.56(7) . .
Sc7 O45 K16 89.98(6) . .
K29 O45 K16 95.22(6) . .
K04 O45 K16 173.30(7) . .
Si12 O46 Sc1 141.28(9) . .
Si12 O46 K25 109.76(8) . .
Sc1 O46 K25 108.29(7) . .
Si12 O46 K03 83.67(7) . .
Sc1 O46 K03 100.89(7) . .
K25 O46 K03 93.64(5) . .
Si12 O46 K33 82.14(6) . .
Sc1 O46 K33 91.21(6) . .
K25 O46 K33 89.66(5) . .
K03 O46 K33 165.73(6) . .
Si8 O47 Sc7 154.24(10) . .
Si8 O47 K32 90.63(8) . .
Sc7 O47 K32 112.94(7) . .
Si8 O47 K08 99.80(8) . .
Sc7 O47 K08 93.59(6) . .
K32 O47 K08 82.83(5) . .
Si1 O48 Sc8 168.62(10) . .
Si1 O48 K18 94.04(8) . .
Sc8 O48 K18 95.11(7) . .
Si1 O48 K36 87.75(7) . .
Sc8 O48 K36 84.28(6) . .
K18 O48 K36 170.91(7) . .
Si1 O48 K07 93.34(8) . 3_655
Sc8 O48 K07 94.59(6) . 3_655
K18 O48 K07 82.16(4) . 3_655
K36 O48 K07 88.84(5) . 3_655
Si2 O49 Sc10 153.64(10) . .
Si2 O49 K10 82.84(7) . .
Sc10 O49 K10 105.72(7) . .
Si2 O49 K20 101.27(8) . .
Sc10 O49 K20 102.20(6) . .
K10 O49 K20 97.47(5) . .
Si5 O50 Si17 137.42(12) . .
Si5 O50 K24 103.92(8) . .
Si17 O50 K24 110.32(8) . .
Si5 O50 K14 93.74(7) . .
Si17 O50 K14 113.69(8) . .
K24 O50 K14 84.49(6) . .
Si18 O51 Si18 169.21(18) . 4
Si18 O51 K12 92.02(9) . 3_655
Si18 O51 K12 92.02(9) 4 3_655
Si18 O51 K29 93.06(9) . .
Si18 O51 K29 93.06(9) 4 .
K12 O51 K29 123.38(9) 3_655 .
Si18 O51 K08 84.96(9) . .
Si18 O51 K08 84.96(9) 4 .
K12 O51 K08 132.81(9) 3_655 .
K29 O51 K08 103.81(8) . .
Si6 O52 Sc6 150.79(9) . 1_455
Si6 O52 K28 104.94(8) . 1_455
Sc6 O52 K28 102.60(7) 1_455 1_455
Si6 O52 K22 87.25(7) . 1_455
Sc6 O52 K22 104.34(7) 1_455 1_455
K28 O52 K22 85.88(5) 1_455 1_455
Si6 O52 K13 77.71(6) . .
Sc6 O52 K13 91.24(6) 1_455 .
K28 O52 K13 93.30(5) 1_455 .
K22 O52 K13 164.20(7) 1_455 .
Si14 O53 Sc9 170.76(11) . .
Si14 O53 K33 96.33(9) . .
Sc9 O53 K33 92.58(6) . .
Si14 O53 K19 99.92(9) . .
Sc9 O53 K19 84.69(6) . .
K33 O53 K19 75.13(4) . .
Si14 O53 K25 75.90(7) . .
Sc9 O53 K25 101.73(6) . .
K33 O53 K25 90.09(5) . .
K19 O53 K25 164.23(6) . .
Si14 O53 K32 92.72(8) . 3_656
Sc9 O53 K32 79.44(5) . 3_656
K33 O53 K32 161.31(6) . 3_656
K19 O53 K32 87.23(5) . 3_656
K25 O53 K32 108.00(4) . 3_656
Si15 O54 Sc3 157.20(10) . .
Si15 O54 K05 96.46(8) . .
Sc3 O54 K05 96.84(7) . .
Si15 O54 K30 95.42(7) . 3_666
Sc3 O54 K30 101.93(6) . 3_666
K05 O54 K30 94.38(5) . 3_666
Si15 O54 K06 85.22(7) . 3_656
Sc3 O54 K06 82.26(6) . 3_656
K05 O54 K06 177.30(7) . 3_656
K30 O54 K06 83.34(4) 3_666 3_656
Si2 O55 Si2 161.69(18) 4_565 .
Si2 O55 K31 81.63(9) 4_565 .
Si2 O55 K31 81.63(9) . .
Si2 O55 K22 98.39(9) 4_565 3_665
Si2 O55 K22 98.39(9) . 3_665
K31 O55 K22 132.63(8) . 3_665
Si2 O55 K01 88.14(9) 4_565 .
Si2 O55 K01 88.14(9) . .
K31 O55 K01 102.03(7) . .
K22 O55 K01 125.34(8) 3_665 .
Si14 O57 Sc1 143.73(10) . .
Si14 O57 K30 108.54(9) . .
Sc1 O57 K30 107.50(7) . .
Si14 O57 K33 82.26(7) . .
Sc1 O57 K33 100.95(6) . .
K30 O57 K33 91.13(5) . .
Si14 O57 K06 85.09(7) . .
Sc1 O57 K06 92.80(6) . .
K30 O57 K06 87.21(5) . .
K33 O57 K06 165.99(7) . .
Si7 O58 Sc5 169.71(11) . .
Si7 O58 K26 82.46(7) . .
Sc5 O58 K26 107.38(6) . .
Si7 O58 K15 79.07(6) . .
Sc5 O58 K15 104.33(6) . .
K26 O58 K15 85.02(5) . .
Si7 O58 K23 74.71(7) . .
Sc5 O58 K23 95.01(6) . .
K26 O58 K23 151.99(6) . .
K15 O58 K23 105.91(4) . .
Si16 O59 Sc5 150.69(10) . .
Si16 O59 K23 91.63(8) . .
Sc5 O59 K23 104.53(7) . .
Si16 O59 K28 96.50(8) . 1_455
Sc5 O59 K28 104.16(6) . 1_455
K23 O59 K28 100.55(5) . 1_455
Si16 O59 K13 73.78(6) . .
Sc5 O59 K13 90.27(6) . .
K23 O59 K13 164.95(7) . .
K28 O59 K13 77.97(4) 1_455 .
Si4 O60 Sc2 148.43(10) . 2_655
Si4 O60 K36 89.60(8) . .
Sc2 O60 K36 114.85(7) 2_655 .
Si4 O60 K17 105.39(8) . .
Sc2 O60 K17 90.11(6) 2_655 .
K36 O60 K17 100.54(5) . .
Si4 O60 K12 70.43(6) . 3_655
Sc2 O60 K12 85.81(6) 2_655 3_655
K36 O60 K12 159.26(7) . 3_655
K17 O60 K12 80.25(4) . 3_655
Si10 O61 Sc8 147.88(10) . .
Si10 O61 K35 106.96(9) . .
Sc8 O61 K35 98.01(6) . .
Si10 O61 K29 89.41(8) . .
Sc8 O61 K29 109.61(7) . .
K35 O61 K29 92.66(5) . .
Si10 O61 K09 72.36(6) . .
Sc8 O61 K09 89.33(6) . .
K35 O61 K09 87.28(5) . .
K29 O61 K09 160.84(7) . .
Si6 O62 Sc10 153.72(10) . .
Si6 O62 K22 93.33(8) . 1_455
Sc10 O62 K22 110.55(7) . 1_455
Si6 O62 K20 74.36(6) . 3
Sc10 O62 K20 93.95(6) . 3
K22 O62 K20 90.59(5) 1_455 3
Si8 O63 Sc9 172.73(11) . 2_656
Si8 O63 K27 86.01(7) . .
Sc9 O63 K27 86.79(6) 2_656 .
Si8 O63 K32 86.84(7) . .
Sc9 O63 K32 100.41(7) 2_656 .
K27 O63 K32 165.90(7) . .
Si8 O63 K19 90.41(7) . 3_666
Sc9 O63 K19 88.77(6) 2_656 3_666
K27 O63 K19 91.90(5) . 3_666
K32 O63 K19 100.29(6) . 3_666
Si15 O64 Si15 165.59(18) . 4
Si15 O64 K06 97.15(9) . 3_656
Si15 O64 K06 97.15(9) 4 3_656
Si15 O64 K04 85.81(9) . .
Si15 O64 K04 85.81(9) 4 .
K06 O64 K04 118.32(8) 3_656 .
Si17 O65 Sc8 148.06(10) . .
Si17 O65 K09 99.34(8) . .
Sc8 O65 K09 105.01(7) . .
Si17 O65 K24 89.58(7) . .
Sc8 O65 K24 106.38(7) . .
K09 O65 K24 99.08(5) . .
Si17 O65 K35 76.67(6) . .
Sc8 O65 K35 85.36(6) . .
K09 O65 K35 84.44(5) . .
K24 O65 K35 166.21(7) . .
Si17 O65 K18 77.68(6) . .
Sc8 O65 K18 77.15(5) . .
K09 O65 K18 176.52(6) . .
K24 O65 K18 82.78(4) . .
K35 O65 K18 93.07(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sc1 F13 2.0075(7) . y
Sc1 F19 2.1233(7) . y
Sc1 O25 2.0436(18) . y
Sc1 O32 2.1317(18) . y
Sc1 O46 2.0005(17) . y
Sc1 O57 2.0715(19) . y
Sc1 K25 3.6447(9) . ?
Sc1 K09 3.8051(9) . ?
Sc1 K30 3.8201(8) . ?
Sc1 K03 3.8950(9) . ?
Sc1 K33 3.9991(9) . ?
Sc1 K06 4.0745(9) . ?
Sc2 F6 2.1138(7) . y
Sc2 F8 2.0358(6) . y
Sc2 O31 1.9852(18) . y
Sc2 O36 2.1360(19) . y
Sc2 O37 2.0884(18) . y
Sc2 O60 2.0347(18) 2_655 y
Sc2 K21 3.5046(9) . ?
Sc2 K17 3.6302(9) 3_665 ?
Sc2 K01 3.7384(9) . ?
Sc2 K12 3.8259(9) . ?
Sc2 K18 4.0519(9) . ?
Sc2 K24 4.0649(9) . ?
Sc3 F4 2.0863(8) . y
Sc3 F15 2.0362(8) . y
Sc3 O9 2.0756(18) 2_656 y
Sc3 O9 2.0756(18) . y
Sc3 O54 2.0177(18) . y
Sc3 O54 2.0177(18) 2_656 y
Sc3 K05 3.5153(8) 3_666 ?
Sc3 K05 3.5154(8) . ?
Sc3 K06 3.5254(8) . ?
Sc3 K06 3.5254(8) 3_656 ?
Sc3 K30 4.0861(8) . ?
Sc3 K30 4.0862(8) 3_666 ?
Sc4 F2 2.0366(7) . y
Sc4 F3 2.1093(7) . y
Sc4 O18 2.0227(18) . y
Sc4 O40 1.9450(18) . y
Sc4 O41 2.0668(18) . y
Sc4 O42 2.2253(18) . y
Sc4 K31 3.4008(8) . ?
Sc4 K10 3.4575(9) . ?
Sc4 K14 3.5002(8) . ?
Sc4 K02 3.5307(8) . ?
Sc4 K03 3.6841(9) . ?
Sc4 K23 3.8457(9) . ?
Sc5 F5 2.1057(7) . y
Sc5 F16 2.0436(7) . y
Sc5 O6 2.0703(18) . y
Sc5 O21 2.1010(18) . y
Sc5 O58 2.0721(18) . y
Sc5 O59 2.0758(18) . y
Sc5 K34 3.2030(8) 1_455 ?
Sc5 K13 3.9419(9) . ?
Sc5 K23 4.0293(9) . ?
Sc5 K26 4.1681(9) . ?
Sc5 K15 4.1986(9) . ?
Sc5 K28 4.2539(9) 1_455 ?
Sc6 F14 2.0935(7) . y
Sc6 F17 2.0440(7) . y
Sc6 O15 2.0942(18) . y
Sc6 O24 2.0919(18) . y
Sc6 O34 1.9846(18) . y
Sc6 O52 2.1748(18) 1_655 y
Sc6 K11 3.5178(9) . ?
Sc6 K28 3.7043(9) . ?
Sc6 K12 3.7682(9) 3_655 ?
Sc6 K22 3.8046(9) . ?
Sc6 K20 3.8285(9) 3_655 ?
Sc6 K13 3.8333(9) 1_655 ?
Sc7 F1 2.0710(7) . y
Sc7 F7 2.0802(7) . y
Sc7 O23 2.1622(19) . y
Sc7 O39 1.9770(19) . y
Sc7 O45 1.9573(18) . y
Sc7 O47 2.1765(18) . y
Sc7 K29 3.5164(8) . ?
Sc7 K08 3.5563(8) . ?
Sc7 K16 3.7255(8) . ?
Sc7 K04 3.8532(9) . ?
Sc7 K32 3.9875(9) . ?
Sc7 K11 4.0544(9) . ?
Sc8 F10 2.0470(6) . y
Sc8 F11 2.0936(7) . y
Sc8 O4 2.1538(18) . y
Sc8 O48 1.9990(18) . y
Sc8 O61 2.1368(18) . y
Sc8 O65 1.9454(18) . y
Sc8 K36 3.4131(8) . ?
Sc8 K18 3.5085(9) . ?
Sc8 K35 3.6315(9) . ?
Sc8 K07 3.7353(9) 3_655 ?
Sc8 K09 3.9419(9) . ?
Sc8 K24 4.0931(9) . ?
Sc9 F12 2.0683(7) . y
Sc9 F20 2.0747(7) . y
Sc9 O35 1.9787(18) . y
Sc9 O53 2.1764(18) . y
Sc9 O38 2.1777(18) . y
Sc9 O63 1.9564(18) 2_656 y
Sc9 K27 3.2447(8) 3_666 ?
Sc9 K19 3.4079(8) . ?
Sc9 K26 3.4402(8) . ?
Sc9 K33 3.5987(9) . ?
Sc9 K32 3.6258(8) 3_656 ?
Sc9 K15 3.7251(9) . ?
Sc10 F9 2.0234(8) . y
Sc10 F18 2.0991(8) . y
Sc10 O49 2.0837(18) 2 y
Sc10 O49 2.0838(18) . y
Sc10 O62 2.0591(18) . y
Sc10 O62 2.0591(18) 2 y
Sc10 K22 3.7916(8) 1_455 ?
Sc10 K22 3.7916(8) 3_665 ?
Sc10 K20 4.0951(8) 3 ?
Sc10 K20 4.0951(8) . ?
Sc10 K10 4.1533(8) 3 ?
Sc10 K10 4.1534(8) . ?
K01 O41 2.5866(17) 4_565 ?
K01 O41 2.5866(17) . ?
K01 O36 2.7012(17) 4_565 ?
K01 O36 2.7012(17) . ?
K01 F6 2.934(2) . ?
K01 Si5 3.1057(9) . ?
K01 Si5 3.1057(9) 4_565 ?
K01 O14 3.411(2) 3_665 ?
K01 O55 3.417(2) . ?
K01 K24 3.4804(11) . ?
K01 K14 3.4950(11) . ?
K01 Si3 3.6280(10) 4_565 ?
K02 O26 2.6868(18) . ?
K02 O26 2.6868(18) 4 ?
K02 O18 2.7727(17) 4 ?
K02 O18 2.7728(17) . ?
K02 F2 2.7996(19) . ?
K02 O19 2.824(2) . ?
K02 O42 2.8700(17) 4 ?
K02 O42 2.8700(17) . ?
K02 Si16 3.1753(10) 4 ?
K02 Si16 3.1754(10) . ?
K02 Si12 3.3950(9) 4 ?
K02 Si12 3.3950(9) . ?
K03 O42 2.4953(17) 4 ?
K03 O42 2.4953(17) . ?
K03 O5 2.747(3) . ?
K03 F2 2.856(2) . ?
K03 O46 2.9854(17) 4 ?
K03 O46 2.9854(17) . ?
K03 O1 3.075(3) . ?
K03 O25 3.2049(17) . ?
K03 O25 3.2049(17) 4 ?
K03 Si12 3.2654(9) 4 ?
K03 Si12 3.2654(9) . ?
K03 Si5 3.4090(11) . ?
K04 O17 2.3941(18) . ?
K04 O17 2.3941(18) 4 ?
K04 F1 3.057(2) . ?
K04 O45 3.1015(18) 4 ?
K04 O45 3.1016(18) . ?
K04 O64 3.194(3) . ?
K04 O9 3.2081(18) 4 ?
K04 O9 3.2081(18) . ?
K04 O39 3.2090(17) 4 ?
K04 O39 3.2090(17) . ?
K04 Si9 3.4015(10) . ?
K04 Si9 3.4016(10) 4 ?
K05 O54 2.6485(17) . ?
K05 O54 2.6486(17) 4_565 ?
K05 O20 2.741(2) . ?
K05 F15 2.8656(8) . ?
K05 O39 2.9587(18) 4_565 ?
K05 O39 2.9588(18) . ?
K05 O17 3.1682(17) . ?
K05 O17 3.1682(17) 4_565 ?
K05 O9 3.1934(18) 4_565 ?
K05 O9 3.1934(18) . ?
K05 Si9 3.2225(10) . ?
K05 Si9 3.2225(10) 4_565 ?
K06 O9 2.5391(17) . ?
K06 O9 2.5391(17) 4 ?
K06 F4 2.8417(8) . ?
K06 O64 2.846(3) 3_656 ?
K06 O43 2.979(2) . ?
K06 O32 3.1399(18) 4 ?
K06 O32 3.1399(18) . ?
K06 O54 3.1755(18) 2_656 ?
K06 O54 3.1755(18) 3_656 ?
K06 Si9 3.2719(10) . ?
K06 Si9 3.2719(10) 4 ?
K06 O57 3.4088(17) . ?
K07 O7 2.7755(16) 3_655 ?
K07 O7 2.7755(16) . ?
K07 O8 2.936(2) 3_655 ?
K07 O48 2.9993(18) 2_655 ?
K07 O48 2.9993(18) 3_655 ?
K07 O4 3.0667(17) 3_655 ?
K07 O4 3.0667(17) 2_655 ?
K07 O37 3.1459(18) . ?
K07 O37 3.1459(18) 4 ?
K07 F10 3.147(2) 3_655 ?
K07 Si4 3.2299(10) 3_655 ?
K07 Si4 3.2299(10) 2_655 ?
K08 O47 2.6795(17) 4 ?
K08 O47 2.6795(17) . ?
K08 O10 2.8588(17) . ?
K08 O10 2.8589(17) 4 ?
K08 O23 2.8604(17) 4 ?
K08 O23 2.8604(17) . ?
K08 O51 2.923(2) . ?
K08 F1 3.129(2) . ?
K08 Si18 3.2031(10) . ?
K08 Si18 3.2031(10) 4 ?
K08 Si8 3.3370(10) 4 ?
K08 Si8 3.3370(10) . ?
K09 O28 2.589(2) . ?
K09 O20 2.623(2) . ?
K09 O32 2.9519(17) . ?
K09 O32 2.9519(17) 4_565 ?
K09 O65 2.9613(17) 4_565 ?
K09 O65 2.9613(17) . ?
K09 F19 3.0250(19) . ?
K09 O25 3.1710(17) 4_565 ?
K09 O25 3.1710(17) . ?
K09 Si9 3.1782(10) 4_565 ?
K09 Si9 3.1782(10) . ?
K09 Si10 3.2253(10) 4_565 ?
K10 O40 2.5167(17) 4 ?
K10 O40 2.5168(17) . ?
K10 O19 2.929(3) . ?
K10 F2 3.023(2) . ?
K10 O49 3.0723(18) . ?
K10 O49 3.0724(18) 4 ?
K10 O30 3.129(3) . ?
K10 O13 3.1438(18) . ?
K10 O13 3.1438(18) 4 ?
K10 O18 3.1992(18) . ?
K10 O18 3.1992(18) 4 ?
K10 Si2 3.2884(9) 4 ?
K11 O23 2.6610(17) 4_565 ?
K11 O23 2.6610(17) . ?
K11 O34 2.7463(17) . ?
K11 O34 2.7463(17) 4_565 ?
K11 F17 2.9802(19) . ?
K11 Si18 3.0532(9) . ?
K11 Si18 3.0532(9) 4_565 ?
K11 O24 3.0956(17) . ?
K11 O24 3.0956(17) 4_565 ?
K11 O16 3.270(2) 3_666 ?
K11 O2 3.356(2) 1_655 ?
K11 K16 3.4155(11) . ?
K12 O8 2.579(2) 3_655 ?
K12 O51 2.669(3) 3_655 ?
K12 O31 2.8794(17) . ?
K12 O31 2.8794(17) 4 ?
K12 O34 2.8932(17) 3_655 ?
K12 O34 2.8932(17) 2_655 ?
K12 F8 3.127(2) . ?
K12 Si18 3.1556(10) 3_655 ?
K12 Si18 3.1556(10) 2_655 ?
K12 O15 3.1724(18) 3_655 ?
K12 O15 3.1724(18) 2_655 ?
K12 Si4 3.2224(10) 2_655 ?
K13 O30 2.609(3) . ?
K13 O19 2.777(2) . ?
K13 O21 2.9726(18) . ?
K13 O21 2.9727(18) 4 ?
K13 F14 2.999(2) 1_455 ?
K13 O52 3.1100(17) 4 ?
K13 O52 3.1100(17) . ?
K13 O13 3.1893(18) 4 ?
K13 O13 3.1894(18) . ?
K13 Si6 3.2133(10) 4 ?
K13 Si6 3.2134(10) . ?
K13 O24 3.2145(17) 4_455 ?
K14 O41 2.5825(17) . ?
K14 O41 2.5825(17) 4_565 ?
K14 F3 2.7476(19) . ?
K14 O50 2.8405(18) . ?
K14 O50 2.8405(18) 4_565 ?
K14 O42 2.8983(17) . ?
K14 O42 2.8983(17) 4_565 ?
K14 O44 2.929(3) . ?
K14 Si12 3.2348(10) 4_565 ?
K14 Si12 3.2348(10) . ?
K14 Si5 3.3645(10) 4_565 ?
K14 Si5 3.3645(10) . ?
K15 O35 2.7388(17) 4_565 ?
K15 O35 2.7389(17) . ?
K15 O11 2.894(2) . ?
K15 O22 2.9071(17) 3_566 ?
K15 O22 2.9071(17) . ?
K15 F12 3.114(2) . ?
K15 O58 3.1745(17) . ?
K15 O58 3.1746(17) 4_565 ?
K15 Si7 3.2699(10) 4_565 ?
K15 Si7 3.2699(10) . ?
K15 O38 3.3363(17) . ?
K15 O38 3.3364(17) 4_565 ?
K16 O3 2.4288(18) . ?
K16 O3 2.4289(18) 4_565 ?
K16 O23 2.9094(17) . ?
K16 O23 2.9094(17) 4_565 ?
K16 O45 3.1706(18) . ?
K16 O45 3.1706(18) 4_565 ?
K16 F7 3.1990(18) . ?
K16 Si18 3.2232(9) 4_565 ?
K16 Si18 3.2233(9) . ?
K16 O28 3.339(2) . ?
K16 Si10 3.4833(10) . ?
K17 O14 2.549(3) . ?
K17 O31 2.9183(17) 2_655 ?
K17 O31 2.9183(17) 3_665 ?
K17 Si3 2.9466(10) 2_655 ?
K17 Si3 2.9466(10) 3_665 ?
K17 O60 3.0024(17) 4_565 ?
K17 O60 3.0024(17) . ?
K17 O34 3.1049(17) 4_565 ?
K17 O34 3.1050(17) . ?
K17 O3 3.2466(18) 4_565 ?
K17 O3 3.2466(18) . ?
K17 F6 3.264(2) 3_665 ?
K18 O48 2.7109(17) . ?
K18 O48 2.7110(17) 4 ?
K18 F10 2.781(2) . ?
K18 O37 2.8192(18) . ?
K18 O37 2.8192(18) 4 ?
K18 O1 3.012(3) . ?
K18 Si1 3.2290(9) 4 ?
K18 Si1 3.2290(9) . ?
K18 O65 3.3844(18) . ?
K18 O65 3.3844(18) 4 ?
K18 Si17 3.4280(11) 4 ?
K18 Si17 3.4280(11) . ?
K19 F12 2.725(2) . ?
K19 O12 2.7474(18) . ?
K19 O12 2.7474(18) 4_565 ?
K19 O53 2.8316(16) 4_565 ?
K19 O53 2.8316(16) . ?
K19 O63 2.8326(17) 2_656 ?
K19 O63 2.8326(17) 3_666 ?
K19 O16 2.961(3) . ?
K19 Si8 3.2423(10) 3_666 ?
K19 Si8 3.2423(10) 2_656 ?
K19 Si14 3.3727(10) . ?
K19 Si14 3.3728(10) 4_565 ?
K20 O15 2.6962(17) 2_655 ?
K20 O15 2.6962(17) 3_655 ?
K20 O27 2.8952(18) . ?
K20 O27 2.8952(18) 4 ?
K20 O30 2.974(2) 3 ?
K20 O49 3.1124(18) . ?
K20 O49 3.1124(18) 4 ?
K20 F14 3.244(2) 3_655 ?
K20 Si6 3.3394(10) 3 ?
K20 Si6 3.3394(10) 2 ?
K20 O62 3.4007(17) 3 ?
K20 O62 3.4007(17) 2 ?
K21 O27 2.7263(18) 4 ?
K21 O27 2.7264(18) . ?
K21 O5 2.738(2) . ?
K21 O36 2.8069(17) . ?
K21 O36 2.8070(17) 4 ?
K21 O31 2.8359(17) . ?
K21 O31 2.8359(17) 4 ?
K21 F8 2.847(2) . ?
K21 Si5 3.0479(10) . ?
K21 Si5 3.0479(10) 4 ?
K21 Si3 3.4491(10) 4 ?
K21 Si3 3.4491(10) . ?
K22 O62 2.5421(17) 4_665 ?
K22 O62 2.5421(17) 1_655 ?
K22 O52 2.6291(17) 4_665 ?
K22 O52 2.6291(17) 1_655 ?
K22 Si6 3.0650(9) 4_665 ?
K22 Si6 3.0650(9) 1_655 ?
K22 F17 3.0979(19) . ?
K22 F18 3.1575(8) 1_655 ?
K22 O14 3.184(2) . ?
K22 O15 3.3345(18) . ?
K22 O15 3.3345(18) 4_565 ?
K22 O55 3.345(3) 3_665 ?
K23 O18 2.8234(17) 4_565 ?
K23 O18 2.8234(17) . ?
K23 O44 2.843(2) . ?
K23 O59 2.9716(18) . ?
K23 O59 2.9716(18) 4_565 ?
K23 F3 3.034(2) . ?
K23 O11 3.041(2) . ?
K23 O26 3.0803(18) . ?
K23 O26 3.0803(18) 4_565 ?
K23 Si7 3.2454(10) 4_565 ?
K23 Si7 3.2454(10) . ?
K23 Si12 3.2724(10) 4_565 ?
K24 O50 2.5083(18) 4_565 ?
K24 O50 2.5083(18) . ?
K24 O36 3.0220(17) 4_565 ?
K24 O36 3.0220(17) . ?
K24 O65 3.0943(18) . ?
K24 O65 3.0944(18) 4_565 ?
K24 F6 3.173(2) . ?
K24 Si5 3.3021(9) 4_565 ?
K24 Si5 3.3021(9) . ?
K24 O29 3.306(3) . ?
K24 Si17 3.4852(9) 4_565 ?
K25 O46 2.4829(16) . ?
K25 O46 2.4830(16) 4 ?
K25 O26 2.9396(18) 4 ?
K25 O26 2.9396(18) . ?
K25 O43 2.952(2) . ?
K25 F13 3.0582(19) . ?
K25 O38 3.1281(18) 4 ?
K25 O38 3.1282(18) . ?
K25 Si14 3.1419(10) 4 ?
K25 Si14 3.1420(10) . ?
K25 O53 3.1727(17) . ?
K25 O53 3.1727(17) 4 ?
K26 O38 2.4335(17) . ?
K26 O38 2.4336(17) 4 ?
K26 O33 2.808(3) . ?
K26 F20 2.879(2) . ?
K26 O58 3.0503(17) . ?
K26 O58 3.0503(17) 4 ?
K26 O35 3.0977(17) 4 ?
K26 O35 3.0977(17) . ?
K26 Si7 3.2496(9) . ?
K26 Si7 3.2496(9) 4 ?
K26 Si13 3.2597(10) . ?
K26 Si13 3.2597(10) 4 ?
K27 O35 2.6746(17) 3_666 ?
K27 O35 2.6746(17) 2_656 ?
K27 O63 2.7004(17) . ?
K27 O63 2.7004(17) 4_565 ?
K27 F12 2.768(2) 3_666 ?
K27 O16 2.786(2) 3_666 ?
K27 Si8 3.0219(10) . ?
K27 Si8 3.0219(10) 4_565 ?
K27 O2 3.119(3) 1_655 ?
K27 O6 3.1641(18) 4_665 ?
K27 O6 3.1641(18) 1_655 ?
K27 Sc9 3.2448(8) 3_666 ?
K28 O52 2.5614(17) 1_655 ?
K28 O52 2.5614(17) 4_665 ?
K28 O2 2.974(3) 1_655 ?
K28 O13 3.0490(18) 4_665 ?
K28 O13 3.0490(18) 1_655 ?
K28 F17 3.0818(18) . ?
K28 O24 3.1031(18) 4_565 ?
K28 O24 3.1031(18) . ?
K28 Si11 3.2133(10) 4_665 ?
K28 Si11 3.2133(10) 1_655 ?
K28 O59 3.2398(17) 4_665 ?
K28 O59 3.2398(17) 1_655 ?
K29 O45 2.5425(17) . ?
K29 O45 2.5425(17) 4 ?
K29 F1 2.605(2) . ?
K29 O51 2.813(3) . ?
K29 O61 2.9716(18) . ?
K29 O61 2.9716(18) 4 ?
K29 O3 3.2090(18) . ?
K29 O3 3.2090(18) 4 ?
K29 O8 3.232(3) . ?
K29 O23 3.2846(18) . ?
K29 O23 3.2847(18) 4 ?
K29 Si18 3.3048(10) 4 ?
K30 O57 2.6465(17) . ?
K30 O57 2.6466(17) 4_565 ?
K30 O12 2.8855(18) . ?
K30 O12 2.8855(18) 4_565 ?
K30 O20 2.935(3) . ?
K30 F19 3.1287(19) . ?
K30 O54 3.1606(17) 3_666 ?
K30 O54 3.1606(17) 2_656 ?
K30 Si9 3.2291(10) 4_565 ?
K30 Si9 3.2291(10) . ?
K30 O9 3.2623(18) . ?
K30 O9 3.2623(18) 4_565 ?
K31 F3 2.7342(19) . ?
K31 O13 2.8490(18) . ?
K31 O13 2.8491(18) 4_565 ?
K31 O18 2.8734(17) . ?
K31 O18 2.8734(17) 4_565 ?
K31 O40 2.9076(17) 4_565 ?
K31 O40 2.9076(17) . ?
K31 O55 3.002(3) . ?
K31 Si2 3.1976(10) 4_565 ?
K31 Si2 3.1977(10) . ?
K31 Si16 3.3711(9) 4_565 ?
K31 Si16 3.3711(9) . ?
K32 O47 2.5986(17) . ?
K32 O47 2.5986(17) 4 ?
K32 O63 2.7195(16) 4 ?
K32 O63 2.7196(16) . ?
K32 F20 2.849(2) 3_656 ?
K32 Si8 3.0585(9) . ?
K32 Si8 3.0585(9) 4 ?
K32 O53 3.3263(18) 2_656 ?
K32 O53 3.3263(18) 3_656 ?
K32 O43 3.371(3) 3_656 ?
K32 Sc9 3.6259(9) 2_656 ?
K33 O11 2.703(2) . ?
K33 F12 2.708(2) . ?
K33 O53 2.7697(17) . ?
K33 O53 2.7698(17) 4_565 ?
K33 O57 3.0497(17) 4_565 ?
K33 O57 3.0498(17) . ?
K33 O44 3.119(3) . ?
K33 Si14 3.2426(9) 4_565 ?
K33 Si14 3.2426(9) . ?
K33 O38 3.3024(17) 4_565 ?
K33 O38 3.3024(17) . ?
K33 Si7 3.4050(10) 4_565 ?
K34 O21 2.5166(17) 4_655 ?
K34 O21 2.5166(17) 1_655 ?
K34 F16 2.6534(19) 1_655 ?
K34 O33 2.783(2) 3_656 ?
K34 O6 2.8102(17) 1_655 ?
K34 O6 2.8102(17) 4_655 ?
K34 O10 2.9866(18) 4 ?
K34 O10 2.9867(18) . ?
K34 Sc5 3.2030(8) 1_655 ?
K34 Sc5 3.2030(8) 4_655 ?
K34 Si13 3.2135(10) 2_656 ?
K34 Si13 3.2135(10) 3_656 ?
K35 O61 2.6534(17) 4 ?
K35 O61 2.6534(17) . ?
K35 O1 2.905(2) . ?
K35 F10 2.991(2) . ?
K35 O17 3.0103(17) 4 ?
K35 O17 3.0103(17) . ?
K35 O32 3.1003(18) 4 ?
K35 O32 3.1003(18) . ?
K35 O65 3.2280(17) 4 ?
K35 O65 3.2281(17) . ?
K35 Si17 3.2628(10) . ?
K35 Si17 3.2629(10) 4 ?
K36 F11 2.663(2) . ?
K36 O4 2.6948(17) . ?
K36 O4 2.6948(17) 4_565 ?
K36 O48 2.9730(18) 4_565 ?
K36 O48 2.9731(18) . ?
K36 O60 2.9932(17) . ?
K36 O60 2.9933(17) 4_565 ?
K36 O29 3.013(2) . ?
K36 O29 3.111(2) 3_665 ?
K36 Si1 3.3086(10) . ?
K36 Si1 3.3086(10) 4_565 ?
K36 Si4 3.3588(9) . ?
Si1 O7 1.6589(11) . y
Si1 O29 1.6533(8) . y
Si1 O37 1.6229(18) . y
Si1 O48 1.5734(18) . y
Si1 K07 3.4673(10) 3_655 ?
Si1 K36 3.7248(10) 3_665 ?
Si2 O27 1.7327(18) . y
Si2 O40 1.5662(18) . y
Si2 O49 1.6166(18) . y
Si2 O55 1.6229(9) . y
Si2 K22 3.9255(11) 3_665 ?
Si3 O14 1.6512(8) 3_665 y
Si3 O15 1.6080(18) 2_655 y
Si3 O31 1.6264(18) . y
Si3 O27 1.7516(18) . y
Si3 K17 2.9466(10) 3_665 ?
Si3 K22 3.7852(10) 3_665 ?
Si4 O3 1.6304(17) . y
Si4 O4 1.6216(19) . y
Si4 O8 1.6234(8) . y
Si4 O60 1.5451(19) . y
Si4 K12 3.2223(10) 3_655 ?
Si4 K07 3.2298(10) 3_655 ?
Si5 O5 1.6106(9) . y
Si5 O36 1.5752(19) . y
Si5 O41 1.6032(19) . y
Si5 O50 1.6275(17) . y
Si6 O13 1.5912(18) . y
Si6 O30 1.6563(8) . y
Si6 O52 1.7070(18) . y
Si6 O62 1.5711(19) . y
Si6 K22 3.0650(9) 1_455 ?
Si6 K20 3.3394(10) 3 ?
Si6 K28 3.4248(10) 1_455 ?
Si7 O11 1.6362(9) . y
Si7 O26 1.6194(17) . y
Si7 O38 1.5862(18) . y
Si7 O58 1.5901(18) . y
Si8 O10 1.6319(17) . y
Si8 O16 1.6568(9) 3_666 y
Si8 O47 1.5846(19) . y
Si8 O63 1.5571(18) . y
Si8 K19 3.2423(10) 3_666 ?
Si9 O9 1.5304(19) . y
Si9 O17 1.7371(19) . y
Si9 O20 1.6435(8) . y
Si9 O32 1.5990(18) . y
Si10 O17 1.7079(18) . y
Si10 O28 1.5701(8) . y
Si10 O45 1.6452(18) . y
Si10 O61 1.5478(18) . y
Si11 O2 1.5885(8) . y
Si11 O10 1.7457(18) 1_455 y
Si11 O21 1.4760(19) . y
Si11 O24 1.5650(18) 1_455 y
Si11 K28 3.2134(10) 1_455 ?
Si11 K34 3.3949(10) 1_455 ?
Si11 K27 3.6538(10) 1_455 ?
Si11 K11 3.6876(11) 1_455 ?
Si11 K08 3.9121(10) 1_455 ?
Si12 O26 1.7453(17) . y
Si12 O42 1.5194(18) . y
Si12 O44 1.6085(8) . y
Si12 O46 1.6923(18) . y
Si13 O6 1.6555(19) 2_556 y
Si13 O22 1.5603(9) . y
Si13 O33 1.5741(7) . y
Si13 O35 1.6189(19) . y
Si13 K34 3.2135(10) 3_656 ?
Si13 K27 3.5644(9) 3_666 ?
Si13 K15 3.7750(10) 3_566 ?
Si13 K26 3.8687(11) 3_556 ?
Si14 O12 1.8011(18) . y
Si14 O43 1.6195(9) . y
Si14 O53 1.4081(19) . y
Si14 O57 1.5868(19) . y
Si14 K32 3.6731(11) 3_656 ?
Si15 O12 1.6487(18) 2_656 y
Si15 O39 1.4904(19) . y
Si15 O54 1.6898(18) . y
Si15 O64 1.6629(8) . y
Si15 K06 3.4707(10) 3_656 ?
Si15 K30 3.7223(10) 3_666 ?
Si15 K19 3.8568(10) 3_666 ?
Si16 O13 1.6535(18) . y
Si16 O18 1.6303(19) . y
Si16 O19 1.6060(8) . y
Si16 O59 1.5746(19) . y
Si16 K28 3.7590(10) 1_455 ?
Si17 O1 1.5672(8) . y
Si17 O25 1.5965(19) . y
Si17 O50 1.7005(17) . y
Si17 O65 1.6267(19) . y
Si18 O3 1.7650(17) . y
Si18 O23 1.4711(19) . y
Si18 O34 1.6011(19) . y
Si18 O51 1.5912(8) . y
Si18 K12 3.1556(10) 3_655 ?
F1 Sc7 2.0710(7) 4 ?
F2 Sc4 2.0366(7) 4 ?
F3 Sc4 2.1093(7) 4_565 ?
F4 Sc3 2.0863(8) 3_656 ?
F4 K06 2.8418(8) 3_656 ?
F5 Sc5 2.1057(7) 4_565 ?
F6 Sc2 2.1139(7) 4_565 ?
F6 K17 3.265(2) 3_665 ?
F7 Sc7 2.0802(7) 4_565 ?
F8 Sc2 2.0358(7) 4 ?
F9 Sc10 2.0234(8) 3 ?
F10 Sc8 2.0470(6) 4 ?
F10 K07 3.147(2) 3_655 ?
F11 Sc8 2.0936(7) 4_565 ?
F12 Sc9 2.0683(7) 4_565 ?
F12 K27 2.768(2) 3_666 ?
F13 Sc1 2.0075(7) 4 ?
F14 Sc6 2.0935(7) 4 ?
F14 K13 2.999(2) 1_655 ?
F14 K20 3.244(2) 3_655 ?
F14 K12 3.361(2) 3_655 ?
F15 Sc3 2.0362(8) 3_666 ?
F15 K05 2.8656(8) 3_666 ?
F16 Sc5 2.0436(7) 4 ?
F16 K34 2.6535(19) 1_455 ?
F17 Sc6 2.0440(7) 4_565 ?
F18 Sc10 2.0991(8) 3_565 ?
F18 K22 3.1576(8) 3_665 ?
F18 K22 3.1576(8) 1_455 ?
F19 Sc1 2.1232(7) 4_565 ?
F20 Sc9 2.0747(7) 4 ?
F20 K32 2.849(2) 3_656 ?
O1 Si17 1.5672(8) 4 ?
O2 Si11 1.5884(8) 4_565 ?
O2 K28 2.974(3) 1_455 ?
O2 K27 3.119(3) 1_455 ?
O2 K11 3.356(2) 1_455 ?
O3 K12 3.2916(19) 3_655 ?
O4 K07 3.0666(17) 3_655 ?
O5 Si5 1.6106(9) 4 ?
O6 Si13 1.6553(19) 2_556 ?
O6 K34 2.8102(17) 1_455 ?
O6 K27 3.1641(18) 1_455 ?
O7 Si1 1.6589(11) 2_655 ?
O7 K07 2.7755(16) 3_655 ?
O8 Si4 1.6234(8) 4 ?
O8 K12 2.579(2) 3_655 ?
O8 K07 2.936(2) 3_655 ?
O10 Si11 1.7457(18) 1_655 ?
O11 Si7 1.6362(9) 4_565 ?
O12 Si15 1.6487(18) 2_656 ?
O13 K28 3.0491(18) 1_455 ?
O14 Si3 1.6512(8) 2_655 ?
O14 Si3 1.6512(8) 3_665 ?
O14 K01 3.411(2) 3_665 ?
O15 Si3 1.6080(18) 2_655 ?
O15 K20 2.6961(17) 3_655 ?
O15 K12 3.1724(18) 3_655 ?
O16 Si8 1.6568(9) 2_656 ?
O16 Si8 1.6568(9) 3_666 ?
O16 K27 2.786(2) 3_666 ?
O16 K11 3.270(2) 3_666 ?
O19 Si16 1.6060(8) 4 ?
O20 Si9 1.6434(8) 4_565 ?
O21 K34 2.5167(17) 1_455 ?
O22 Si13 1.5603(9) 2_556 ?
O22 K15 2.9071(17) 3_566 ?
O24 Si11 1.5650(18) 1_655 ?
O24 K13 3.2144(17) 1_655 ?
O28 Si10 1.5701(8) 4_565 ?
O29 Si1 1.6532(8) 4_565 ?
O29 K36 3.111(2) 3_665 ?
O30 Si6 1.6564(8) 4 ?
O30 K20 2.974(2) 3 ?
O31 K17 2.9183(17) 3_665 ?
O33 Si13 1.5741(8) 4 ?
O33 K34 2.783(2) 3_656 ?
O34 K12 2.8932(17) 3_655 ?
O35 K27 2.6746(17) 3_666 ?
O43 Si14 1.6195(9) 4 ?
O43 K32 3.371(3) 3_656 ?
O44 Si12 1.6084(8) 4_565 ?
O48 K07 2.9994(18) 3_655 ?
O51 Si18 1.5912(8) 4 ?
O51 K12 2.669(3) 3_655 ?
O52 Sc6 2.1749(18) 1_455 ?
O52 K28 2.5614(17) 1_455 ?
O52 K22 2.6290(17) 1_455 ?
O53 K32 3.3263(18) 3_656 ?
O54 K30 3.1607(17) 3_666 ?
O54 K06 3.1755(17) 3_656 ?
O55 Si2 1.6229(9) 4_565 ?
O55 K22 3.345(3) 3_665 ?
O59 K28 3.2398(17) 1_455 ?
O60 Sc2 2.0347(18) 2_655 ?
O60 K12 3.3922(17) 3_655 ?
O62 K22 2.5421(17) 1_455 ?
O62 K20 3.4006(17) 3 ?
O63 Sc9 1.9565(18) 2_656 ?
O63 K19 2.8327(17) 3_666 ?
O64 Si15 1.6629(8) 4 ?
O64 K06 2.847(3) 3_656 ?
loop_
_publcif_info_datablock.id
_publcif_info_datablock.publ_exptl
_publcif_info_datablock.publ_geom
_publcif_info_datablock.structure
{9c7527d8-f9a1-4280-9998-e33738fbf57e} y y y
loop_
_publcif_info_exptl_table_extra_item
sin_theta_over_lambda_max
loop_
_publcif_info_tables.block_id
_publcif_info_tables.reference_item
{9c7527d8-f9a1-4280-9998-e33738fbf57e} '_publcif_info_datablock.publ_exptl'
{9c7527d8-f9a1-4280-9998-e33738fbf57e} '_geom_bond_atom_site_label_1'
loop_
_publcif_info_cif.paper_type
CB
