#------------------------------------------------------------------------------
#$Date: 2022-07-03 19:12:12 +0300 (Sun, 03 Jul 2022) $
#$Revision: 276506 $
#$URL: file:///home/coder/svn-repositories/cod/cif/3/00/03/3000397.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3000397
loop_
_publ_author_name
'Vinci, Doriana'
'Chateigner, Daniel'
_journal_name_full               'Personal communication to COD'
_journal_year                    2022
_chemical_formula_moiety         'C5 H12 Cl3 N2 Pt1'
_chemical_formula_sum            'C5 H12 Cl3 N2 Pt'
_chemical_formula_weight         401.61
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     direct
_cell_angle_alpha                90
_cell_angle_beta                 105.654(2)
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   37.154(2)
_cell_length_b                   5.9294(3)
_cell_length_c                   21.8080(12)
_cell_measurement_reflns_used    2780
_cell_measurement_temperature    293
_cell_measurement_theta_max      40
_cell_measurement_theta_min      5
_cell_volume                     4626.1(4)
_computing_cell_refinement       'DENZO/SCALEPACK (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Nonius, 2001).'
_computing_data_reduction        'Apex2 (Bruker AXS, 2006)'
_computing_molecular_graphics    'CAMERON (Watkin et al., 1996)'
_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       Area
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       'φ & ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.084
_diffrn_reflns_limit_h_max       40
_diffrn_reflns_limit_h_min       -40
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            22391
_diffrn_reflns_theta_full        23.266
_diffrn_reflns_theta_max         23.266
_diffrn_reflns_theta_min         1.940
_diffrn_standards_interval_count .
_diffrn_standards_interval_time  .
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    12.775
_exptl_absorpt_correction_T_max  0.63
_exptl_absorpt_correction_T_min  0.47
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'DENZO/SCALEPACK (Otwinowski & Minor, 1997)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.306
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       lamellar
_exptl_crystal_F_000             2960
_exptl_crystal_size_max          0.210
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.036
_refine_diff_density_max         1.56
_refine_diff_density_min         -2.07
_refine_ls_extinction_method     None
_refine_ls_goodness_of_fit_ref   1.0570
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     227
_refine_ls_number_reflns         1840
_refine_ls_number_restraints     54
_refine_ls_R_factor_all          0.0907
_refine_ls_R_factor_gt           0.0422
_refine_ls_shift/su_max          0.0022650
_refine_ls_shift/su_mean         0.0001637
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0784
_refine_ls_wR_factor_gt          0.0445
_refine_ls_wR_factor_ref         0.0416
_reflns_limit_h_max              39
_reflns_limit_h_min              -40
_reflns_limit_k_max              6
_reflns_limit_k_min              0
_reflns_limit_l_max              24
_reflns_limit_l_min              0
_reflns_number_gt                2060
_reflns_number_total             3328
_reflns_threshold_expression     I>2.0σ(I)
_cod_data_source_file            pivalonitrili.cif
_cod_data_source_block           platinum_pivnit
_cod_depositor_comments
;Releasing structure 3000397 into public domain as personal
 communication to COD.
;
_cod_original_cell_volume        4626.2(4)
_cod_original_sg_symbol_H-M      'C 1 2/c 1 '
_cod_original_formula_sum        'C5 H12 Cl3 N2 Pt1'
_cod_database_code               3000397
_cod_database_fobs_code          3000397
_iucr_refine_instructions_details_constraints
;
#LIST     12                                                                    
BLOCK SCALE X'S, U'S 
EQUIV PART(1001, OCC) PART(1002, OCC) 
WEIGHT -1 PART(1002, OCC) 
RIDE N   (   3,X'S) H   (  36,X'S) H   (  34,X'S) H   (  35,X'S) 
RIDE N   (   1,X'S) H   (  13,X'S) H   (  12,X'S) H   (  11,X'S) 
RIDE C   (   3,X'S) H   (  33,X'S) H   (  31,X'S) H   (  32,X'S) 
RIDE C   (   4,X'S) H   (  41,X'S) H   (  42,X'S) H   (  43,X'S) 
RIDE C   (   5,X'S) H   (  51,X'S) H   (  53,X'S) H   (  52,X'S) 
RIDE C   (  81,X'S) H   ( 812,X'S) H   ( 811,X'S) H   ( 813,X'S) 
RIDE C   (  91,X'S) H   ( 911,X'S) H   ( 913,X'S) H   ( 912,X'S) 
RIDE C   (  80,X'S) H   ( 802,X'S) H   ( 801,X'S) H   ( 803,X'S) 
RIDE C   (  90,X'S) H   ( 901,X'S) H   ( 903,X'S) H   ( 902,X'S) 
RIDE C   ( 100,X'S) H   (1002,X'S) H   (1001,X'S) H   (1003,X'S) 
RIDE C   ( 101,X'S) H   (1011,X'S) H   (1013,X'S) H   (1012,X'S) 
END                                                                             
;
_iucr_refine_instructions_details_restraints
;
#LIST     16                                                                    
SAME  C(7)  C(80)  C(90)  C(101) AND 
CONT C(7)  C(81)  C(91)  C(100) 
SIMU  C(7)  C(80)  C(90)  C(101) AND 
CONT C(7)  C(81)  C(91)  C(100) 
DELU  C(7)  C(80)  C(90)  C(101) AND 
CONT C(7)  C(81)  C(91)  C(100) 
REM   HREST   START (DO NOT REMOVE THIS LINE) 
REM   HREST   END (DO NOT REMOVE THIS LINE) 
END                                                                             
;
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z
x+1/2,y+1/2,z
-x+1/2,-y+1/2,-z
-x,y,-z+1/2
x,-y,z+1/2
-x+1/2,y+1/2,-z+1/2
x+1/2,-y+1/2,z+1/2
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_attached_hydrogens
N3 N 0.3644(4) 0.547(3) -0.1881(7) 0.0617 1.0000 Uani . . . . . .
H31 H 0.3167 1.2162 -0.0242 0.1128 1.0000 Uiso R . . . . .
H32 H 0.2887 1.2578 0.0162 0.1128 1.0000 Uiso R . . . . .
H33 H 0.2844 1.0470 -0.0273 0.1128 1.0000 Uiso R . . . . .
H36 H 0.3533 0.5207 -0.2337 0.0851 1.0000 Uiso R . . . . .
H34 H 0.3469 0.4917 -0.1668 0.0851 1.0000 Uiso R . . . . .
H35 H 0.3717 0.6943 -0.1776 0.0821 1.0000 Uiso R . . . . .
N1 N 0.2173(4) 0.491(2) 0.1967(6) 0.0495 1.0000 Uani . . . . . .
N2 N 0.2851(4) 0.814(3) 0.1175(7) 0.0459 1.0000 Uani . . . . . .
N4 N 0.4530(5) 0.127(3) -0.1421(9) 0.0698 1.0000 Uani . . . . . .
C1 C 0.3035(6) 0.906(3) 0.0908(9) 0.0530 1.0000 Uani . . . . . .
C2 C 0.3275(6) 1.008(4) 0.0551(9) 0.0561 1.0000 Uani . . . . . .
C3 C 0.3016(7) 1.151(4) 0.0008(10) 0.0931 1.0000 Uani . . . . . .
C4 C 0.3573(6) 1.151(4) 0.0958(11) 0.0822 1.0000 Uani . . . . . .
C5 C 0.3465(8) 0.819(4) 0.0284(11) 0.1054 1.0000 Uani . . . . . .
C6 C 0.4817(7) 0.056(4) -0.1312(13) 0.0863 1.0000 Uani . . . . . .
Pt2 Pt 0.40727(2) 0.32619(13) -0.16505(3) 0.0448 1.0000 Uani . . . . . .
Cl1 Cl 0.20930(15) 0.9456(8) 0.1331(2) 0.0565 1.0000 Uani . . . . . .
Cl2 Cl 0.29378(14) 0.3684(8) 0.1856(2) 0.0536 1.0000 Uani . . . . . .
Cl3 Cl 0.37836(19) 0.1322(11) -0.0997(3) 0.0923 1.0000 Uani . . . . . .
Cl4 Cl 0.4336(2) 0.5225(12) -0.2323(4) 0.1074 1.0000 Uani . . . . . .
Cl5 Cl 0.4351(2) 0.5603(11) -0.0818(4) 0.1181 1.0000 Uani . . . . . .
Cl6 Cl 0.3760(2) 0.0965(10) -0.2474(3) 0.0971 1.0000 Uani . . . . . .
Pt1 Pt 0.25204(2) 0.65811(12) 0.15893(3) 0.0360 1.0000 Uani . . . . . .
C7 C 0.5205(4) -0.019(4) -0.1106(10) 0.0924 1.0000 Uani D . . . . .
C81 C 0.5324(14) -0.058(11) -0.1716(16) 0.1175 0.45(3) Uani D . P 1 2 .
C91 C 0.5466(11) 0.142(7) -0.069(2) 0.1066 0.45(3) Uani D . P 1 2 .
C80 C 0.5422(11) 0.181(6) -0.127(3) 0.1216 0.55(3) Uani D . P 1 1 .
C90 C 0.5354(12) -0.076(9) -0.0422(12) 0.1218 0.55(3) Uani D . P 1 1 .
C100 C 0.5197(14) -0.256(6) -0.084(3) 0.1239 0.45(3) Uani D . P 1 2 .
C101 C 0.5248(12) -0.201(6) -0.1575(18) 0.0992 0.55(3) Uani D . P 1 1 .
H51 H 0.3622 0.8805 0.0047 0.1183 1.0000 Uiso R . . . . .
H53 H 0.3610 0.7293 0.0622 0.1183 1.0000 Uiso R . . . . .
H52 H 0.3278 0.7279 0.0012 0.1183 1.0000 Uiso R . . . . .
H812 H 0.5576 -0.1091 -0.1594 0.1428 0.45(3) Uiso R . P 1 2 .
H811 H 0.5300 0.0623 -0.2011 0.1428 0.45(3) Uiso R . P 1 2 .
H813 H 0.5165 -0.1789 -0.1909 0.1428 0.45(3) Uiso R . P 1 2 .
H911 H 0.5714 0.0839 -0.0574 0.1422 0.45(3) Uiso R . P 1 2 .
H913 H 0.5452 0.2675 -0.0965 0.1422 0.45(3) Uiso R . P 1 2 .
H912 H 0.5401 0.1887 -0.0315 0.1422 0.45(3) Uiso R . P 1 2 .
H802 H 0.5682 0.1485 -0.1175 0.1430 0.55(3) Uiso R . P 1 1 .
H801 H 0.5325 0.1963 -0.1722 0.1430 0.55(3) Uiso R . P 1 1 .
H803 H 0.5384 0.3169 -0.1071 0.1430 0.55(3) Uiso R . P 1 1 .
H901 H 0.5604 -0.1259 -0.0355 0.1516 0.55(3) Uiso R . P 1 1 .
H903 H 0.5352 0.0613 -0.0198 0.1516 0.55(3) Uiso R . P 1 1 .
H902 H 0.5215 -0.1870 -0.0270 0.1516 0.55(3) Uiso R . P 1 1 .
H1002 H 0.5443 -0.3166 -0.0700 0.1576 0.45(3) Uiso R . P 1 2 .
H1001 H 0.5038 -0.3620 -0.1108 0.1576 0.45(3) Uiso R . P 1 2 .
H1003 H 0.5106 -0.2247 -0.0482 0.1576 0.45(3) Uiso R . P 1 2 .
H1011 H 0.5497 -0.2569 -0.1467 0.1302 0.55(3) Uiso R . P 1 1 .
H1013 H 0.5182 -0.1484 -0.2002 0.1302 0.55(3) Uiso R . P 1 1 .
H1012 H 0.5082 -0.3185 -0.1533 0.1302 0.55(3) Uiso R . P 1 1 .
H13 H 0.1947 0.4600 0.1875 0.0500 1.0000 Uiso R . . . . .
H12 H 0.2259 0.4010 0.2182 0.0500 1.0000 Uiso R . . . . .
H11 H 0.2105 0.5400 0.2293 0.0500 1.0000 Uiso R . . . . .
H41 H 0.3722 1.2149 0.0709 0.1011 1.0000 Uiso R . . . . .
H42 H 0.3726 1.0597 0.1283 0.1011 1.0000 Uiso R . . . . .
H43 H 0.3466 1.2690 0.1146 0.1011 1.0000 Uiso R . . . . .
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Pt -1.7033 8.3905 27.0059 1.5129 17.7639 8.8117 15.7131 0.4246 5.7837 38.6103
11.6883 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Cl 0.1484 0.1585 11.4604 0.0104 7.1964 1.1662 6.2556 18.5194 1.6455 47.7784
-9.5574 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
N 0.0061 0.0033 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826
-11.5290 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
C 0.0033 0.0016 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512
0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998
0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_site_symmetry_1
_geom_angle_atom_site_label_2
_geom_angle_site_symmetry_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
H36 . N3 . H34 . 106.5 no
H36 . N3 . H35 . 114.7 no
H34 . N3 . H35 . 113.5 no
H36 . N3 . Pt2 . 103.6 no
H34 . N3 . Pt2 . 104.5 no
H35 . N3 . Pt2 . 113.0 no
Pt1 . N1 . H13 . 138.0 no
Pt1 . N1 . H12 . 114.5 no
H13 . N1 . H12 . 103.6 no
Pt1 . N1 . H11 . 122.7 no
H13 . N1 . H11 . 77.1 no
H12 . N1 . H11 . 83.7 no
C1 . N2 . Pt1 . 177.3(16) yes
C6 . N4 . Pt2 . 166(2) yes
N2 . C1 . C2 . 176(2) yes
C1 . C2 . C3 . 106.9(17) yes
C1 . C2 . C4 . 112.5(17) yes
C3 . C2 . C4 . 110.6(19) yes
C1 . C2 . C5 . 108.0(18) yes
C3 . C2 . C5 . 111.3(18) yes
C4 . C2 . C5 . 107.5(20) yes
C2 . C3 . H33 . 107.6 no
C2 . C3 . H31 . 108.4 no
H33 . C3 . H31 . 106.4 no
C2 . C3 . H32 . 112.0 no
H33 . C3 . H32 . 110.6 no
H31 . C3 . H32 . 111.7 no
C2 . C4 . H41 . 109.9 no
C2 . C4 . H42 . 108.4 no
H41 . C4 . H42 . 109.5 no
C2 . C4 . H43 . 110.0 no
H41 . C4 . H43 . 109.5 no
H42 . C4 . H43 . 109.5 no
C2 . C5 . H51 . 109.9 no
C2 . C5 . H53 . 109.9 no
H51 . C5 . H53 . 109.5 no
C2 . C5 . H52 . 108.6 no
H51 . C5 . H52 . 109.5 no
H53 . C5 . H52 . 109.5 no
N4 . C6 . C7 . 173(3) yes
N3 . Pt2 . N4 . 175.3(7) yes
N3 . Pt2 . Cl3 . 90.6(5) yes
N4 . Pt2 . Cl3 . 93.2(5) yes
N3 . Pt2 . Cl4 . 87.4(5) yes
N4 . Pt2 . Cl4 . 88.9(5) yes
Cl3 . Pt2 . Cl4 . 177.7(2) yes
N3 . Pt2 . Cl5 . 87.8(5) yes
N4 . Pt2 . Cl5 . 89.4(6) yes
Cl3 . Pt2 . Cl5 . 89.9(3) yes
Cl4 . Pt2 . Cl5 . 91.1(3) yes
N3 . Pt2 . Cl6 . 89.5(5) yes
N4 . Pt2 . Cl6 . 93.5(6) yes
Cl3 . Pt2 . Cl6 . 88.0(3) yes
Cl4 . Pt2 . Cl6 . 90.8(3) yes
Cl5 . Pt2 . Cl6 . 176.6(3) yes
Cl1 . Pt1 . N1 . 89.3(4) yes
Cl1 . Pt1 . Cl2 . 178.82(17) yes
N1 . Pt1 . Cl2 . 89.5(4) yes
Cl1 . Pt1 . N2 . 90.9(5) yes
N1 . Pt1 . N2 . 176.9(6) yes
Cl2 . Pt1 . N2 . 90.3(5) yes
C6 . C7 . C80 . 103(2) yes
C6 . C7 . C90 . 117(2) yes
C80 . C7 . C90 . 109.80(10) yes
C6 . C7 . C101 . 106(2) yes
C80 . C7 . C101 . 103.27(10) yes
C90 . C7 . C101 . 115.79(10) yes
C6 . C7 . C81 . 106(3) yes
C6 . C7 . C91 . 115(2) yes
C81 . C7 . C91 . 109.79(10) yes
C6 . C7 . C100 . 106(2) yes
C81 . C7 . C100 . 103.27(10) yes
C91 . C7 . C100 . 115.79(10) yes
C7 . C81 . H812 . 107.3 no
C7 . C81 . H811 . 118.5 no
H812 . C81 . H811 . 109.5 no
C7 . C81 . H813 . 102.1 no
H812 . C81 . H813 . 109.5 no
H811 . C81 . H813 . 109.5 no
C7 . C91 . H911 . 110.7 no
C7 . C91 . H913 . 101.4 no
H911 . C91 . H913 . 109.5 no
C7 . C91 . H912 . 115.9 no
H911 . C91 . H912 . 109.5 no
H913 . C91 . H912 . 109.5 no
C7 . C80 . H802 . 111.1 no
C7 . C80 . H801 . 104.1 no
H802 . C80 . H801 . 109.5 no
C7 . C80 . H803 . 113.1 no
H802 . C80 . H803 . 109.5 no
H801 . C80 . H803 . 109.5 no
C7 . C90 . H901 . 108.0 no
C7 . C90 . H903 . 105.6 no
H901 . C90 . H903 . 109.5 no
C7 . C90 . H902 . 114.6 no
H901 . C90 . H902 . 109.5 no
H903 . C90 . H902 . 109.5 no
C7 . C100 . H1002 . 110.9 no
C7 . C100 . H1001 . 116.7 no
H1002 . C100 . H1001 . 109.5 no
C7 . C100 . H1003 . 100.4 no
H1002 . C100 . H1003 . 109.5 no
H1001 . C100 . H1003 . 109.5 no
C7 . C101 . H1011 . 110.6 no
C7 . C101 . H1013 . 112.3 no
H1011 . C101 . H1013 . 109.5 no
C7 . C101 . H1012 . 105.5 no
H1011 . C101 . H1012 . 109.5 no
H1013 . C101 . H1012 . 109.5 no
loop_
_geom_bond_atom_site_label_1
_geom_bond_site_symmetry_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
N3 . H36 . 0.981 no
N3 . H34 . 0.956 no
N3 . H35 . 0.923 no
N3 . Pt2 . 2.020(14) yes
H31 . C3 . 0.963 no
H32 . C3 . 0.912 no
H33 . C3 . 0.975 no
N1 . Pt1 . 1.977(13) yes
N1 . H13 . 0.827 no
N1 . H12 . 0.725 no
N1 . H11 . 0.866 no
N2 . C1 . 1.15(2) yes
N2 . Pt1 . 1.943(16) yes
N4 . C6 . 1.11(3) yes
N4 . Pt2 . 2.018(19) yes
C1 . C2 . 1.46(3) yes
C2 . C3 . 1.56(3) yes
C2 . C4 . 1.49(3) yes
C2 . C5 . 1.52(3) yes
C4 . H41 . 0.950 no
C4 . H42 . 0.950 no
C4 . H43 . 0.950 no
C5 . H51 . 0.950 no
C5 . H53 . 0.950 no
C5 . H52 . 0.950 no
C6 . C7 . 1.46(3) yes
Pt2 . Cl3 . 2.309(5) yes
Pt2 . Cl4 . 2.289(6) yes
Pt2 . Cl5 . 2.298(6) yes
Pt2 . Cl6 . 2.304(6) yes
Cl1 . Pt1 . 2.294(5) yes
Cl2 . Pt1 . 2.282(5) yes
C7 . C80 . 1.531(10) yes
C7 . C90 . 1.484(10) yes
C7 . C101 . 1.525(10) yes
C7 . C81 . 1.528(10) yes
C7 . C91 . 1.486(10) yes
C7 . C100 . 1.524(10) yes
C81 . H812 . 0.950 no
C81 . H811 . 0.950 no
C81 . H813 . 0.950 no
C91 . H911 . 0.950 no
C91 . H913 . 0.950 no
C91 . H912 . 0.950 no
C80 . H802 . 0.950 no
C80 . H801 . 0.950 no
C80 . H803 . 0.950 no
C90 . H901 . 0.950 no
C90 . H903 . 0.950 no
C90 . H902 . 0.950 no
C100 . H1002 . 0.950 no
C100 . H1001 . 0.950 no
C100 . H1003 . 0.950 no
C101 . H1011 . 0.950 no
C101 . H1013 . 0.950 no
C101 . H1012 . 0.950 no
